#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/57/2015771.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015771_Fobs loop_ _publ_author_name 'Lavy, T.' 'Meirovich, N.' 'Sparkes, H. A.' 'Howard, J. A. K.' 'Kaftory, M.' _publ_section_title ; Cocrystals composed of 4,4'-(fluorene-9,9-diyl)diphenol and 6-methyl-2H-pyridone ; _journal_coeditor_code AV3045 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o89 _journal_page_last o92 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.133 _cell_angle_gamma 90.000 _cell_length_a 14.4319 _cell_length_b 14.6645 _cell_length_c 35.6748 _exptl_crystal_F_000 3104.00 _reflns_d_resolution_high 0.8377 _[local]_cod_data_source_file av3045IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' H3br0 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 604.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33051.58 31879.05 508.11 o 4 0 0 47530.13 46825.91 585.04 o 6 0 0 7794.46 7799.33 226.42 o 8 0 0 14430.74 13943.61 412.64 o 10 0 0 5752.57 4938.07 227.22 o 12 0 0 1362.21 1245.12 249.48 o 14 0 0 36.04 45.67 89.65 o 16 0 0 1972.43 1675.60 313.42 o 3 1 0 71688.16 71741.65 928.11 o 5 1 0 11644.20 11254.40 165.78 o 7 1 0 651.18 765.59 76.03 o 9 1 0 8292.61 8167.94 155.02 o 11 1 0 3882.04 3569.48 127.59 o 13 1 0 9.82 0.00 55.75 o 15 1 0 1194.47 1117.10 186.14 o 17 1 0 489.26 462.89 132.23 o 0 2 0 2984.06 2801.68 88.44 o 2 2 0 19981.37 18867.47 202.58 o 4 2 0 5005.74 4828.01 97.81 o 6 2 0 334.06 367.09 42.96 o 8 2 0 210.03 341.74 46.94 o 10 2 0 56.73 134.48 35.74 o 12 2 0 418.07 370.22 63.43 o 14 2 0 102.20 153.62 86.10 o 16 2 0 1804.74 1451.47 212.15 o 1 3 0 19886.02 18899.38 327.39 o 3 3 0 10552.98 10430.18 148.17 o 5 3 0 1930.17 1942.93 70.18 o 7 3 0 4004.74 3944.39 124.06 o 9 3 0 3369.18 3362.75 112.45 o 11 3 0 9.36 69.65 43.31 o 13 3 0 2097.89 2136.00 123.94 o 15 3 0 70.61 70.32 77.06 o 0 4 0 7308.85 6832.89 192.98 o 2 4 0 78545.73 75657.82 1405.86 o 4 4 0 29841.21 29275.84 362.49 o 6 4 0 3928.36 3713.71 103.89 o 8 4 0 1759.32 2010.95 96.58 o 10 4 0 1200.45 1242.48 88.52 o 12 4 0 4060.58 4184.88 171.12 o 14 4 0 4378.83 3880.40 181.78 o 16 4 0 73.46 0.00 103.87 o 1 5 0 21199.02 19094.08 213.70 o 3 5 0 47469.57 48744.32 700.76 o 5 5 0 3886.85 3880.17 192.99 o 7 5 0 7643.58 7565.85 161.73 o 9 5 0 2674.19 2851.90 113.67 o 11 5 0 88.35 41.76 53.71 o 13 5 0 1271.61 1114.77 136.54 o 15 5 0 1.97 151.44 79.62 o 0 6 0 11009.07 10552.26 191.33 o 2 6 0 657.32 740.52 39.92 o 4 6 0 10117.39 10663.49 176.32 o 6 6 0 569.60 660.05 58.18 o 8 6 0 2021.98 2213.21 106.38 o 10 6 0 247.15 309.39 69.01 o 12 6 0 2386.87 2235.91 144.53 o 14 6 0 10.75 10.02 109.50 o 16 6 0 42.71 190.84 112.27 o 1 7 0 8325.17 8769.68 172.56 o 3 7 0 24986.41 25020.73 285.51 o 5 7 0 1363.87 1378.51 76.30 o 7 7 0 7618.75 7469.68 170.81 o 9 7 0 47.81 81.32 46.62 o 11 7 0 906.19 983.55 105.91 o 13 7 0 0.89 0.00 71.02 o 15 7 0 419.40 499.24 115.48 o 0 8 0 18406.47 18422.20 533.68 o 2 8 0 246.95 363.33 43.42 o 4 8 0 5195.82 4912.54 112.06 o 6 8 0 3534.25 3586.64 112.46 o 8 8 0 2490.58 2675.19 132.99 o 10 8 0 4440.34 4045.66 168.16 o 12 8 0 75.32 267.15 95.52 o 14 8 0 145.20 102.59 84.58 o 1 9 0 5868.38 5230.96 170.27 o 3 9 0 1.45 26.79 46.24 o 5 9 0 2814.22 2979.28 117.59 o 7 9 0 79.83 83.15 42.86 o 9 9 0 4079.79 4018.73 139.35 o 11 9 0 322.78 320.80 73.94 o 13 9 0 14.03 112.45 145.70 o 0 10 0 4568.18 4640.34 240.23 o 2 10 0 1249.34 1219.13 118.63 o 4 10 0 4370.91 3618.95 158.69 o 6 10 0 1798.51 1910.10 137.68 o 8 10 0 5929.65 5692.50 329.78 o 10 10 0 4521.75 4348.29 272.11 o 12 10 0 309.15 380.58 171.51 o 14 10 0 277.91 354.78 179.10 o 1 11 0 3.68 40.04 54.28 o 3 11 0 7.02 56.07 66.76 o 5 11 0 23087.24 21871.16 423.52 o 7 11 0 356.88 511.44 90.69 o 9 11 0 28.96 142.52 89.67 o 11 11 0 515.75 496.53 140.18 o 13 11 0 13.25 0.00 143.81 o 0 12 0 10623.31 9375.12 371.85 o 2 12 0 98.02 204.75 64.72 o 4 12 0 161.43 267.70 79.74 o 6 12 0 28434.88 27127.39 507.63 o 8 12 0 2444.82 2440.41 227.07 o 10 12 0 1314.48 1051.23 145.02 o 12 12 0 651.74 995.83 299.38 o 1 13 0 1.15 168.77 66.71 o 3 13 0 4425.58 4317.42 206.98 o 5 13 0 1889.28 1832.36 155.34 o 7 13 0 2353.29 2576.29 182.66 o 9 13 0 1317.34 1510.98 171.12 o 11 13 0 1513.20 1313.93 203.70 o 0 14 0 98.08 0.00 90.62 o 2 14 0 523.48 633.88 104.43 o 4 14 0 894.84 1096.76 124.68 o 6 14 0 1676.09 2032.88 171.70 o 8 14 0 1771.00 1787.65 166.33 o 10 14 0 1088.36 899.96 182.02 o 1 15 0 37.12 85.91 67.50 o 3 15 0 3713.38 4023.08 225.96 o 5 15 0 143.61 169.09 86.15 o 7 15 0 432.29 503.08 125.80 o 0 16 0 49.57 273.69 121.02 o 2 16 0 9.38 231.08 83.78 o 4 16 0 30.76 144.40 78.04 o 6 16 0 1968.17 1847.22 176.56 o 1 17 0 2632.49 2612.43 235.23 o 3 17 0 839.36 869.95 129.44 o -17 1 1 245.32 424.47 136.26 o -15 1 1 1005.59 835.31 165.99 o -13 1 1 466.49 457.98 84.12 o -11 1 1 3099.37 2913.86 122.79 o -9 1 1 4662.72 5240.44 137.03 o -7 1 1 0.12 15.11 24.82 o -5 1 1 1095.32 1156.70 56.89 o -3 1 1 3823.51 3680.35 72.69 o -1 1 1 24271.39 21090.72 451.15 o 1 1 1 4615.61 3727.78 87.78 o 3 1 1 3818.71 3522.27 71.57 o 5 1 1 5751.35 5914.74 112.78 o 7 1 1 11500.66 12451.41 199.41 o 9 1 1 4020.65 4502.07 112.19 o 11 1 1 333.55 417.68 59.65 o 13 1 1 36.74 146.17 64.82 o 15 1 1 7.79 0.00 81.50 o 17 1 1 130.39 0.00 167.90 o -16 2 1 913.64 746.64 184.03 o -14 2 1 459.73 551.95 88.37 o -12 2 1 542.47 570.75 73.41 o -10 2 1 845.23 1086.55 73.32 o -8 2 1 86.93 7.68 32.74 o -6 2 1 12934.13 13920.62 203.87 o -4 2 1 7232.32 7246.48 122.45 o -2 2 1 4010.29 3712.16 68.74 o 0 2 1 20117.80 19217.65 258.31 o 2 2 1 2675.59 2457.58 55.95 o 4 2 1 1122.40 1276.39 57.55 o 6 2 1 38.85 13.85 27.86 o 8 2 1 8459.00 8338.44 167.41 o 10 2 1 50.90 64.26 36.45 o 12 2 1 1704.12 1597.60 103.32 o 14 2 1 224.57 231.34 90.85 o 16 2 1 192.25 208.47 119.98 o -15 3 1 2744.65 2461.82 269.11 o -13 3 1 0.81 86.47 49.55 o -11 3 1 250.84 274.41 56.74 o -9 3 1 25.12 48.67 38.04 o -7 3 1 163.57 235.96 44.81 o -5 3 1 2089.44 2337.78 76.22 o -3 3 1 203684.63 200184.97 1715.26 o -1 3 1 7613.26 6967.42 121.82 o 1 3 1 13708.15 12946.78 173.46 o 3 3 1 35108.81 33963.64 350.38 o 5 3 1 7258.74 7323.67 155.89 o 7 3 1 3442.93 3673.77 121.23 o 9 3 1 608.88 711.10 66.53 o 11 3 1 3101.72 3165.66 126.01 o 13 3 1 7220.12 6999.38 243.95 o 15 3 1 15.40 88.07 97.80 o -16 4 1 178.77 192.22 228.42 o -14 4 1 42.53 127.84 59.89 o -12 4 1 4043.01 3974.34 143.62 o -10 4 1 3.31 23.78 53.87 o -8 4 1 4710.74 3896.96 117.94 o -6 4 1 9069.84 8461.49 159.74 o -4 4 1 2459.21 2334.67 74.56 o -2 4 1 128021.23 128500.12 1846.30 o 0 4 1 34844.17 33028.91 626.12 o 2 4 1 14912.42 14326.55 180.14 o 4 4 1 307.27 469.89 44.20 o 6 4 1 5008.21 4914.19 118.74 o 8 4 1 1695.36 1825.79 94.37 o 10 4 1 2521.38 2366.56 188.92 o 12 4 1 351.81 426.42 76.80 o 14 4 1 1975.76 1979.87 141.61 o 16 4 1 676.73 611.50 145.96 o -15 5 1 1.89 26.72 67.26 o -13 5 1 0.29 0.00 46.33 o -11 5 1 3929.25 3979.81 161.57 o -9 5 1 3667.46 3884.92 126.45 o -7 5 1 1285.12 1195.66 77.93 o -5 5 1 50886.63 50989.12 535.78 o -3 5 1 18697.83 19260.60 242.13 o -1 5 1 23612.59 23413.57 239.64 o 1 5 1 26.69 1.42 26.03 o 3 5 1 3137.54 3175.20 82.24 o 5 5 1 2470.90 2635.43 85.67 o 7 5 1 428.18 622.28 60.69 o 9 5 1 1802.97 2201.48 109.76 o 11 5 1 2449.37 2263.39 130.58 o 13 5 1 29.09 100.22 73.18 o 15 5 1 362.88 317.67 82.39 o -16 6 1 4097.44 4275.52 252.04 o -14 6 1 166.57 74.16 118.19 o -12 6 1 571.91 634.57 87.14 o -10 6 1 11476.79 9676.41 344.38 o -8 6 1 0.68 22.87 36.02 o -6 6 1 1707.12 2002.71 91.74 o -4 6 1 10570.06 11120.43 181.86 o -2 6 1 35814.39 35945.17 604.04 o 0 6 1 2545.03 2728.18 112.32 o 2 6 1 737.13 908.05 49.79 o 4 6 1 10022.03 10242.65 171.12 o 6 6 1 52.42 76.58 35.47 o 8 6 1 1816.81 2009.08 103.39 o 10 6 1 1099.47 1115.43 91.03 o 12 6 1 0.00 60.28 110.08 o 14 6 1 54.25 92.90 76.40 o 16 6 1 549.51 940.02 167.52 o -15 7 1 139.46 131.79 73.31 o -13 7 1 30.95 114.26 77.35 o -11 7 1 592.58 493.31 89.99 o -9 7 1 594.55 664.84 72.11 o -7 7 1 4006.80 4077.32 124.53 o -5 7 1 3148.62 3315.42 118.88 o -3 7 1 6571.06 6529.51 120.32 o -1 7 1 807.97 970.85 53.40 o 1 7 1 2821.16 3350.25 145.23 o 3 7 1 6802.98 6245.32 123.97 o 5 7 1 415.83 424.07 49.68 o 7 7 1 370.98 513.39 66.46 o 9 7 1 556.85 598.48 68.05 o 11 7 1 1820.98 1723.15 132.85 o 13 7 1 1519.60 1470.97 190.47 o 15 7 1 183.84 255.52 120.51 o -14 8 1 1781.51 1929.15 205.50 o -12 8 1 1845.46 1952.58 148.49 o -10 8 1 3602.88 3508.87 157.10 o -8 8 1 3752.90 3489.64 128.98 o -6 8 1 7.10 68.63 35.38 o -4 8 1 2249.25 2208.17 79.19 o -2 8 1 78.07 117.83 31.14 o 0 8 1 172.83 199.80 47.68 o 2 8 1 1624.49 1875.30 59.80 o 4 8 1 345.27 377.29 43.14 o 6 8 1 6120.22 5642.38 142.19 o 8 8 1 4515.98 3971.14 134.20 o 10 8 1 226.14 324.20 68.50 o 12 8 1 1095.96 1029.18 159.98 o 14 8 1 4.59 161.68 164.87 o -13 9 1 3.27 107.53 96.42 o -11 9 1 10.26 124.25 73.72 o -9 9 1 25503.49 23768.97 373.23 o -7 9 1 176.88 272.76 57.23 o -5 9 1 11706.66 11305.92 222.31 o -3 9 1 25.61 55.63 45.26 o -1 9 1 4215.49 4060.26 149.34 o 1 9 1 11.53 18.72 42.75 o 3 9 1 2853.23 3155.22 151.47 o 5 9 1 2829.39 2715.77 122.18 o 7 9 1 3741.13 3621.87 121.06 o 9 9 1 59.82 55.86 45.90 o 11 9 1 140.29 140.56 61.65 o 13 9 1 240.60 437.68 104.31 o -14 10 1 70.61 277.37 160.12 o -12 10 1 569.79 656.43 195.03 o -10 10 1 1997.83 2264.03 224.62 o -8 10 1 6352.74 5919.55 207.84 o -6 10 1 3150.18 3166.97 168.61 o -4 10 1 972.40 1181.72 109.68 o -2 10 1 119.98 154.92 55.81 o 0 10 1 6.02 30.75 49.18 o 2 10 1 638.58 788.98 91.26 o 4 10 1 8900.87 8428.80 325.69 o 6 10 1 581.15 644.18 90.07 o 8 10 1 2254.59 2403.08 176.25 o 10 10 1 261.27 325.02 230.32 o 12 10 1 0.90 61.85 136.60 o 14 10 1 2.50 270.16 164.68 o -13 11 1 11.58 54.26 140.01 o -11 11 1 134.93 156.70 102.85 o -9 11 1 87.75 170.13 86.73 o -7 11 1 236.72 380.23 85.59 o -5 11 1 5231.90 4885.53 188.65 o -3 11 1 402.01 374.15 74.29 o -1 11 1 294.06 342.54 69.46 o 1 11 1 784.09 830.77 97.03 o 3 11 1 93.22 97.08 58.67 o 5 11 1 297.13 429.62 83.63 o 7 11 1 1672.56 1615.67 139.47 o 9 11 1 105.10 179.99 81.39 o 11 11 1 593.16 675.02 210.59 o 13 11 1 1101.19 1244.94 265.23 o -12 12 1 86.63 167.23 153.86 o -10 12 1 218.42 365.64 101.21 o -8 12 1 456.71 603.36 92.72 o -6 12 1 4862.06 5358.23 209.79 o -4 12 1 1098.63 1223.46 123.07 o -2 12 1 47.34 94.17 75.74 o 0 12 1 7802.85 7570.90 235.76 o 2 12 1 7780.62 7324.56 244.28 o 4 12 1 7686.91 7410.15 242.00 o 6 12 1 11318.33 11125.49 572.59 o 8 12 1 144.87 142.85 114.52 o 10 12 1 3019.67 3357.64 298.42 o 12 12 1 301.17 442.83 119.79 o -11 13 1 1067.52 935.62 170.37 o -9 13 1 37.16 126.42 89.11 o -7 13 1 215.70 119.14 79.90 o -5 13 1 2188.16 2285.33 170.52 o -3 13 1 397.77 453.64 86.03 o -1 13 1 136.80 141.94 88.78 o 1 13 1 1509.23 1425.62 131.81 o 3 13 1 17161.24 15670.68 370.74 o 5 13 1 1282.58 1650.99 148.65 o 7 13 1 149.50 123.76 93.63 o 9 13 1 961.68 994.50 143.87 o 11 13 1 77.23 228.32 118.75 o -10 14 1 60.27 97.48 83.68 o -8 14 1 3552.28 3525.53 219.52 o -6 14 1 2327.70 2505.52 186.70 o -4 14 1 720.55 790.34 108.19 o -2 14 1 1978.81 2222.62 170.14 o 0 14 1 186.37 82.52 68.84 o 2 14 1 328.61 447.62 90.78 o 4 14 1 172.77 85.60 72.13 o 6 14 1 108.17 329.30 83.47 o 8 14 1 3244.62 3457.07 216.89 o 10 14 1 807.02 843.10 171.81 o -7 15 1 287.41 290.37 93.13 o -5 15 1 496.11 449.46 110.24 o -3 15 1 392.53 278.19 89.84 o -1 15 1 1358.34 1477.74 143.29 o 1 15 1 20.60 45.23 69.99 o 3 15 1 1362.73 1481.45 147.00 o 5 15 1 796.74 850.20 113.53 o 7 15 1 561.04 785.23 123.12 o -6 16 1 135.32 107.71 107.62 o -4 16 1 1244.01 1272.85 139.55 o -2 16 1 364.35 631.28 158.61 o 0 16 1 234.83 525.84 93.51 o 2 16 1 214.33 161.88 77.65 o 4 16 1 414.11 508.32 101.11 o 6 16 1 238.83 294.65 82.41 o -3 17 1 802.48 807.15 123.21 o -1 17 1 214.76 239.23 83.17 o 1 17 1 70.08 208.95 81.64 o 3 17 1 44.89 309.61 86.90 o -16 0 2 287.67 431.42 182.51 o -14 0 2 1604.52 1634.64 193.70 o -12 0 2 17441.17 16729.83 636.32 o -10 0 2 8220.34 7850.12 296.87 o -8 0 2 95.56 215.58 76.76 o -6 0 2 3290.79 3376.42 116.97 o -4 0 2 2590.45 2512.74 84.63 o -2 0 2 34175.11 32193.47 486.40 o 2 0 2 100233.02 101667.33 1396.09 o 4 0 2 45315.11 45972.68 487.34 o 6 0 2 2397.57 2547.13 82.62 o 8 0 2 14096.19 12467.43 333.83 o 10 0 2 1059.88 1420.27 250.81 o 12 0 2 310.09 514.68 112.96 o 14 0 2 371.86 109.66 141.91 o 16 0 2 2731.35 2170.77 361.98 o -17 1 2 475.82 666.02 240.18 o -15 1 2 5512.15 4977.86 374.51 o -13 1 2 2263.24 2398.39 225.70 o -11 1 2 912.28 1028.30 100.66 o -9 1 2 3383.26 3458.15 111.82 o -7 1 2 838.55 858.36 54.50 o -5 1 2 5220.76 5000.40 102.83 o -3 1 2 10.02 0.00 20.92 o -1 1 2 52930.06 49888.69 444.17 o 1 1 2 1344.90 1270.13 41.89 o 3 1 2 104887.04 102101.00 1006.47 o 5 1 2 14807.84 15094.61 201.14 o 7 1 2 54.39 66.88 29.61 o 9 1 2 1866.50 2157.49 95.77 o 11 1 2 3969.72 3783.20 149.70 o 13 1 2 3.34 76.61 71.12 o 15 1 2 261.48 203.38 110.28 o 17 1 2 53.54 164.66 111.98 o -16 2 2 143.71 72.11 116.28 o -14 2 2 1.13 0.00 58.35 o -12 2 2 816.14 950.11 90.29 o -10 2 2 1250.35 1277.12 78.72 o -8 2 2 2293.95 2671.40 95.91 o -6 2 2 3437.27 3417.43 121.59 o -4 2 2 127.07 59.10 28.55 o -2 2 2 80384.14 77325.20 686.27 o 0 2 2 24889.68 23511.76 260.12 o 2 2 2 12828.93 11881.46 143.45 o 4 2 2 43091.24 43695.28 438.03 o 6 2 2 13116.42 13337.72 199.34 o 8 2 2 6045.96 6917.77 203.55 o 10 2 2 8.59 52.40 34.32 o 12 2 2 18.68 85.71 46.60 o 14 2 2 2.85 212.39 156.33 o 16 2 2 248.27 217.22 195.60 o -15 3 2 57.82 85.01 78.60 o -13 3 2 979.58 850.56 89.20 o -11 3 2 8621.42 7668.82 188.35 o -9 3 2 0.88 75.42 36.89 o -7 3 2 2536.92 2550.06 89.49 o -5 3 2 518.61 504.80 46.51 o -3 3 2 365281.94 367127.91 4561.46 o -1 3 2 12800.28 12311.90 156.53 o 1 3 2 110091.26 110152.00 1161.01 o 3 3 2 16.09 45.24 26.93 o 5 3 2 441.59 525.59 48.09 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681.26 620.96 80.50 o 6 6 22 1904.75 1823.86 157.65 o 8 6 22 44.47 152.45 79.80 o 10 6 22 453.20 567.15 112.76 o 12 6 22 1981.18 1981.78 198.45 o -13 7 22 2023.33 1800.86 174.88 o -11 7 22 1025.91 1045.33 124.49 o -9 7 22 5.98 9.93 56.82 o -7 7 22 5146.76 4716.78 222.96 o -5 7 22 109.86 180.06 56.82 o -3 7 22 3169.78 3105.19 151.97 o -1 7 22 69.12 153.27 56.09 o 1 7 22 11276.41 10812.96 331.07 o 3 7 22 160.89 215.42 73.58 o 5 7 22 1765.16 1861.82 129.02 o 7 7 22 558.43 538.81 100.25 o 9 7 22 81.66 286.83 91.17 o 11 7 22 0.01 42.92 110.23 o 13 7 22 32.16 337.08 146.27 o -12 8 22 416.59 400.39 75.01 o -10 8 22 175.28 265.81 64.98 o -8 8 22 78.27 73.47 104.78 o -6 8 22 3126.59 2934.69 199.24 o -4 8 22 37.90 16.85 68.20 o -2 8 22 1662.62 1691.13 128.21 o 0 8 22 666.19 807.45 93.47 o 2 8 22 2061.40 2103.29 168.01 o 4 8 22 2940.30 2916.65 190.07 o 6 8 22 2067.20 1735.05 268.07 o 8 8 22 130.97 145.52 103.68 o 10 8 22 1963.32 1878.16 237.46 o 12 8 22 35.65 79.43 110.25 o -11 9 22 29.42 259.53 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