#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/57/2015778.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015778_Fobs loop_ _publ_author_name 'Sakai, Ken' 'Yokokawa, Kazuo' 'Yokoyama, Yoshimi' _publ_section_title ; Pt~2~^II^ and Pt~2~^III^ dimers containing a Pt~2~(2,2'-bipyridine)~2~(\m-N,N-dimethylguanidinato)~2~ unit ; _journal_coeditor_code BM3021 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m36 _journal_page_last m41 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.712 _cell_angle_gamma 90.000 _cell_length_a 12.6189 _cell_length_b 28.9553 _cell_length_c 14.4197 _exptl_crystal_F_000 2600.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file bm3021IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' kazuo8 in P2(1)/n 2006/02/20 11:17:14 067 KENX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 768.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8699.63 14802.99 509.09 o 4 0 0 460.38 1029.07 150.42 o 6 0 0 114393.00 116977.41 2366.42 o 8 0 0 2107.90 1893.69 306.65 o 10 0 0 89.52 97.33 470.22 o 12 0 0 6195.07 5760.44 1141.62 o 14 0 0 5282.56 5364.94 1228.61 o 2 1 0 18315.22 16907.31 741.81 o 3 1 0 96.08 471.76 72.81 o 4 1 0 1184.89 1177.72 124.62 o 5 1 0 56556.11 56866.49 1089.22 o 6 1 0 32223.30 30869.99 569.66 o 7 1 0 8357.51 7452.73 441.34 o 8 1 0 46276.77 45738.10 704.30 o 9 1 0 33.38 27.76 281.41 o 10 1 0 54.03 43.39 324.97 o 11 1 0 2356.32 1895.74 530.01 o 12 1 0 14663.47 14026.77 1035.04 o 13 1 0 46.37 886.15 593.89 o 14 1 0 5455.41 5651.55 907.42 o 15 1 0 1115.87 1154.44 691.83 o 2 2 0 996.91 246.20 58.30 o 3 2 0 205.01 473.35 98.93 o 4 2 0 1484.04 1296.46 113.92 o 5 2 0 3241.92 3008.90 203.82 o 6 2 0 14312.17 13744.60 367.87 o 7 2 0 99260.51 93496.34 1860.73 o 8 2 0 545.97 407.10 163.35 o 9 2 0 832.43 1064.64 373.09 o 10 2 0 285.40 484.72 385.58 o 11 2 0 1904.91 1966.75 555.35 o 12 2 0 1062.04 1255.84 570.96 o 13 2 0 23049.52 21167.88 1294.03 o 14 2 0 372.05 481.02 589.44 o 15 2 0 439.59 654.87 644.56 o 1 3 0 208523.08 211118.06 5403.23 o 2 3 0 6644.90 5478.02 174.74 o 3 3 0 711.57 2570.08 424.73 o 4 3 0 87.08 229.22 70.45 o 5 3 0 54646.62 53688.29 1151.31 o 6 3 0 7402.00 6453.87 550.95 o 7 3 0 26174.68 25847.06 1098.92 o 8 3 0 502.98 649.21 226.36 o 9 3 0 2443.29 2388.60 326.48 o 10 3 0 50.20 -82.92 337.93 o 11 3 0 12457.90 12779.42 920.29 o 12 3 0 707.60 621.16 529.81 o 13 3 0 119.42 539.25 572.68 o 14 3 0 1196.52 1763.74 672.71 o 15 3 0 3308.59 3154.73 812.98 o 0 4 0 289691.47 339785.22 13348.50 o 1 4 0 18827.67 21845.75 707.19 o 2 4 0 6672.24 5206.13 201.82 o 3 4 0 22264.58 22203.88 1107.26 o 4 4 0 4673.80 4152.27 489.23 o 5 4 0 101.23 80.40 68.84 o 6 4 0 82114.93 81685.02 2108.42 o 7 4 0 38587.82 36162.69 1082.90 o 8 4 0 417.29 385.00 223.60 o 9 4 0 4440.96 4328.94 399.21 o 10 4 0 2057.43 1686.61 483.48 o 11 4 0 2483.92 2312.03 572.81 o 12 4 0 3376.36 3607.79 707.80 o 13 4 0 4737.74 5239.88 844.58 o 14 4 0 4470.72 4923.31 885.09 o 1 5 0 10428.38 6692.68 206.31 o 2 5 0 91092.16 96825.34 810.18 o 3 5 0 691.78 353.84 105.53 o 4 5 0 3699.93 4099.18 313.13 o 5 5 0 764.06 836.11 127.46 o 6 5 0 30686.44 28940.80 1941.75 o 7 5 0 344.87 462.45 154.32 o 8 5 0 62395.00 58331.36 2345.28 o 9 5 0 3367.78 3710.33 388.13 o 10 5 0 259.27 -299.21 332.93 o 11 5 0 2574.24 2147.21 564.40 o 12 5 0 14084.97 14623.28 1058.18 o 13 5 0 1.03 216.21 548.95 o 14 5 0 10342.60 10055.67 1404.34 o 0 6 0 14119.26 14284.34 1114.74 o 1 6 0 39728.53 38744.91 528.60 o 2 6 0 5960.70 5736.40 321.46 o 3 6 0 19993.70 21435.59 430.58 o 4 6 0 178.92 430.51 117.43 o 5 6 0 356.40 312.66 131.54 o 6 6 0 61516.26 54554.51 3328.59 o 7 6 0 56640.22 54369.50 968.24 o 8 6 0 763.44 843.70 256.67 o 9 6 0 248.03 425.54 253.66 o 10 6 0 3196.18 2809.13 533.75 o 11 6 0 623.72 793.39 458.40 o 12 6 0 4397.39 4835.51 781.88 o 13 6 0 14282.08 12637.77 1105.12 o 14 6 0 3340.57 3536.58 784.77 o 1 7 0 102645.19 123706.70 1955.63 o 2 7 0 1902.48 1777.34 154.76 o 3 7 0 328.27 504.27 139.18 o 4 7 0 367.76 278.20 124.52 o 5 7 0 99768.63 99522.88 5254.20 o 6 7 0 1158.81 1368.59 167.54 o 7 7 0 22252.89 21896.49 666.30 o 8 7 0 3659.38 3862.47 372.61 o 9 7 0 5150.78 4800.31 437.43 o 10 7 0 6.14 -21.53 338.50 o 11 7 0 11886.01 10751.27 870.75 o 12 7 0 706.21 289.39 490.70 o 13 7 0 103.76 79.09 500.18 o 14 7 0 632.40 971.98 708.96 o 0 8 0 74633.83 76577.92 6118.92 o 1 8 0 67143.05 74667.76 998.03 o 2 8 0 3323.34 3752.22 214.56 o 3 8 0 5880.28 6990.24 381.02 o 4 8 0 4792.94 4134.48 268.02 o 5 8 0 49.32 23.35 126.41 o 6 8 0 12550.48 12105.83 889.23 o 7 8 0 63379.37 62614.11 1073.07 o 8 8 0 7.72 17.97 213.60 o 9 8 0 7244.23 6682.68 498.89 o 10 8 0 803.96 667.29 325.35 o 11 8 0 2462.24 2585.53 583.34 o 12 8 0 1303.13 1602.99 560.35 o 13 8 0 20127.62 19735.85 1236.46 o 14 8 0 680.83 1005.19 627.27 o 1 9 0 30797.98 32510.22 586.50 o 2 9 0 39337.68 40444.02 721.12 o 3 9 0 3254.58 3241.90 226.58 o 4 9 0 19230.64 19334.42 451.94 o 5 9 0 24543.90 24937.74 1063.51 o 6 9 0 22298.03 19500.43 1841.45 o 7 9 0 3215.13 3914.11 368.86 o 8 9 0 51301.22 50892.63 1701.65 o 9 9 0 3536.75 3332.14 413.70 o 10 9 0 199.59 471.16 319.01 o 11 9 0 7529.14 7317.84 805.05 o 12 9 0 22676.06 21498.34 1234.67 o 13 9 0 25.22 585.84 691.39 o 14 9 0 6610.62 6749.66 985.58 o 0 10 0 116764.20 102722.51 7817.28 o 1 10 0 1785.25 2002.60 142.08 o 2 10 0 9385.08 8867.72 304.86 o 3 10 0 6666.83 9129.50 352.23 o 4 10 0 27958.82 29233.18 804.59 o 5 10 0 2211.23 2456.48 248.63 o 6 10 0 104611.10 108415.90 1687.65 o 7 10 0 2706.81 2311.36 326.30 o 8 10 0 1803.60 2024.16 337.28 o 9 10 0 102.53 39.78 258.82 o 10 10 0 3185.82 2470.74 428.74 o 11 10 0 90.24 24.27 428.61 o 12 10 0 8402.18 8611.74 930.15 o 13 10 0 238.58 136.64 525.50 o 14 10 0 5588.97 5945.06 939.11 o 1 11 0 49887.28 50399.51 1427.68 o 2 11 0 13551.21 13451.51 363.12 o 3 11 0 137.59 11.63 126.32 o 4 11 0 10232.24 11651.88 467.08 o 5 11 0 19187.73 20633.59 518.80 o 6 11 0 25169.15 22889.71 821.86 o 7 11 0 8962.03 10019.67 543.29 o 8 11 0 21778.40 21321.62 830.66 o 9 11 0 2619.57 2472.79 398.69 o 10 11 0 290.16 349.80 326.54 o 11 11 0 8889.35 9433.35 870.47 o 12 11 0 13617.51 12979.62 1034.23 o 13 11 0 11.92 367.42 558.17 o 14 11 0 3817.64 3594.40 821.63 o 0 12 0 3696.22 4466.39 372.08 o 1 12 0 63113.02 64493.97 1869.71 o 2 12 0 1284.23 1154.47 162.36 o 3 12 0 674.66 545.63 160.66 o 4 12 0 2742.24 3227.52 269.74 o 5 12 0 1875.17 2145.78 244.20 o 6 12 0 9288.23 9112.37 536.73 o 7 12 0 69252.34 68701.02 1840.46 o 8 12 0 84.58 285.81 273.16 o 9 12 0 6296.44 5497.55 612.42 o 10 12 0 585.02 235.57 329.59 o 11 12 0 4201.20 3831.35 684.66 o 12 12 0 87.54 649.41 544.82 o 13 12 0 20790.46 19401.76 1381.13 o 14 12 0 393.21 567.78 614.01 o 1 13 0 90427.66 94643.31 2765.31 o 2 13 0 24312.47 22763.16 536.40 o 3 13 0 1154.44 898.06 179.51 o 4 13 0 25.56 7.32 158.11 o 5 13 0 68728.91 71145.44 2612.82 o 6 13 0 3968.88 3221.04 312.45 o 7 13 0 15036.89 14373.00 575.75 o 8 13 0 15082.73 15328.33 699.07 o 9 13 0 2714.00 2911.21 426.66 o 10 13 0 123.82 117.31 328.37 o 11 13 0 10576.03 10479.91 1200.01 o 12 13 0 2166.46 2382.95 652.56 o 13 13 0 166.71 372.93 577.38 o 14 13 0 1386.23 1326.55 864.49 o 0 14 0 93805.77 96522.89 1479.49 o 1 14 0 14556.49 14367.26 886.24 o 2 14 0 16278.96 16617.01 443.99 o 3 14 0 2570.68 2149.03 228.92 o 4 14 0 4614.28 4709.88 323.30 o 5 14 0 947.39 688.93 225.26 o 6 14 0 58660.82 55643.76 2039.69 o 7 14 0 13208.19 12579.69 594.15 o 8 14 0 396.24 319.26 257.88 o 9 14 0 10.96 68.81 251.95 o 10 14 0 941.33 886.33 397.16 o 11 14 0 196.59 153.57 371.94 o 12 14 0 3659.34 3541.76 739.07 o 13 14 0 4896.36 5037.39 1162.12 o 14 14 0 2526.08 2882.02 960.00 o 1 15 0 405.42 381.08 127.08 o 2 15 0 82348.48 89185.77 2516.29 o 3 15 0 570.17 493.58 168.94 o 4 15 0 7248.04 6618.67 382.21 o 5 15 0 1116.81 1395.13 256.51 o 6 15 0 22323.98 23193.46 1226.65 o 7 15 0 824.65 1383.43 377.83 o 8 15 0 25116.12 23665.56 754.59 o 9 15 0 0.41 200.63 272.34 o 10 15 0 201.63 60.17 299.79 o 11 15 0 1519.51 1464.80 402.47 o 12 15 0 10688.25 11014.09 997.35 o 13 15 0 14.63 148.08 543.17 o 0 16 0 157421.38 160946.23 2046.58 o 1 16 0 17231.01 16842.21 933.10 o 2 16 0 1137.79 1526.54 199.64 o 3 16 0 222.96 209.53 163.38 o 4 16 0 3285.06 3440.38 308.17 o 5 16 0 153.43 -10.55 202.54 o 6 16 0 32280.46 31636.63 937.29 o 7 16 0 28906.46 29771.43 1020.74 o 8 16 0 213.99 41.39 258.54 o 9 16 0 1593.39 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2825.93 765.93 o 0 24 0 83198.82 82870.18 1908.79 o 1 24 0 8057.98 8498.59 537.42 o 2 24 0 155.23 204.59 317.21 o 3 24 0 362.85 416.90 323.83 o 4 24 0 565.13 486.03 411.33 o 5 24 0 341.83 528.70 484.71 o 6 24 0 39266.71 36147.88 2614.38 o 7 24 0 4050.92 3497.42 501.75 o 8 24 0 41.95 133.16 331.52 o 9 24 0 98.54 398.84 374.84 o 10 24 0 913.50 1002.36 449.08 o 11 24 0 82.62 -102.74 426.01 o 1 25 0 3810.35 3895.00 432.36 o 2 25 0 8059.94 8283.90 641.44 o 3 25 0 795.15 661.50 371.66 o 4 25 0 1619.47 1393.57 417.50 o 5 25 0 1179.64 1529.50 589.37 o 6 25 0 8739.14 9154.91 886.65 o 7 25 0 1146.31 1388.75 566.60 o 8 25 0 18027.55 18085.95 1195.22 o 9 25 0 399.47 476.55 391.25 o 10 25 0 7.55 11.67 393.40 o 11 25 0 27.60 -242.38 416.94 o 0 26 0 13763.16 12712.00 922.66 o 1 26 0 11832.41 11452.37 630.73 o 2 26 0 204.22 83.21 370.59 o 3 26 0 4208.63 4479.34 559.53 o 4 26 0 3176.44 3325.35 536.46 o 5 26 0 28.87 27.31 454.49 o 6 26 0 7272.10 6298.19 812.99 o 7 26 0 22132.08 21728.47 1266.47 o 8 26 0 1352.03 1295.70 579.92 o 9 26 0 828.10 754.82 604.64 o 10 26 0 377.16 422.54 622.16 o 11 26 0 874.31 731.92 974.90 o 1 27 0 24918.34 25202.44 864.80 o 2 27 0 176.30 37.83 339.30 o 3 27 0 72.43 -105.36 330.60 o 4 27 0 1377.60 879.50 422.83 o 5 27 0 27707.94 27272.92 1344.76 o 6 27 0 141.88 0.75 479.75 o 7 27 0 6300.08 5484.71 832.17 o 8 27 0 54.28 100.20 516.96 o 9 27 0 1072.06 1289.87 639.09 o 10 27 0 356.21 339.48 638.08 o 0 28 0 30863.12 30370.85 1350.51 o 1 28 0 10721.95 10821.77 651.38 o 2 28 0 1796.42 1884.38 463.01 o 3 28 0 788.93 281.41 387.24 o 4 28 0 1784.42 1580.93 587.11 o 5 28 0 724.15 1041.22 569.73 o 6 28 0 10427.56 9943.08 989.30 o 7 28 0 14401.36 14906.00 1158.91 o 8 28 0 44.49 -67.61 548.89 o 9 28 0 518.99 589.22 620.59 o 10 28 0 184.02 104.95 643.31 o 1 29 0 1831.45 1976.70 418.96 o 2 29 0 21464.62 20320.69 1062.95 o 3 29 0 1007.34 793.05 429.20 o 4 29 0 2047.90 2633.28 667.23 o 5 29 0 4109.53 3201.68 735.50 o 6 29 0 6517.89 8627.94 1131.78 o 7 29 0 130.88 319.75 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