#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:10:25 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180826 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/57/2015781.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015781_Fobs loop_ _publ_author_name 'Suresh, J.' 'Suresh Kumar, R.' 'Perumal, S.' 'Mostad, A.' 'Natarajan, S.' _publ_section_title ; Ethyl 4-hydroxy-2,6-diphenyl-5-(phenylsulfanyl)pyridine-3-carboxylate and ethyl 2,6-bis(4-fluorophenyl)-4-hydroxy-5-(4-methylphenylsulfanyl)pyridine-3-carboxylate: supramolecular aggregation through C---H···O, C---H···F and C---H···\p interactions ; _journal_coeditor_code DN3034 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o141 _journal_page_last o144 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.041 _cell_angle_gamma 90.000 _cell_length_a 10.3728 _cell_length_b 17.1008 _cell_length_c 12.9444 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7495 _cod_data_source_file dn3034Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' snadq in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 203.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 494.20 557.43 23.39 o 2 0 0 8939.37 8817.20 171.89 o 3 0 0 195.59 121.73 2.55 o 4 0 0 2278.32 1906.92 61.24 o 5 0 0 2602.84 2690.32 19.41 o 6 0 0 801.41 970.06 17.92 o 7 0 0 12.70 7.47 1.05 o 8 0 0 248.56 236.02 6.04 o 9 0 0 70.52 66.09 3.15 o 10 0 0 1679.18 1614.19 84.34 o 11 0 0 110.20 120.74 6.04 o 12 0 0 1172.02 1116.49 36.43 o 1 1 0 423.61 445.22 6.80 o 2 1 0 1477.40 1290.59 20.84 o 3 1 0 4236.78 4274.25 23.62 o 4 1 0 92.29 135.13 1.49 o 5 1 0 317.54 330.76 2.51 o 6 1 0 432.17 354.37 6.05 o 7 1 0 466.10 382.95 2.90 o 8 1 0 236.04 248.93 2.84 o 9 1 0 234.47 220.36 3.93 o 10 1 0 98.28 89.09 4.74 o 11 1 0 56.41 56.22 2.89 o 12 1 0 47.14 48.89 6.72 o 0 2 0 8457.33 8275.57 213.48 o 1 2 0 818.40 874.09 24.58 o 2 2 0 8029.51 7679.10 158.78 o 3 2 0 224.59 213.74 2.61 o 4 2 0 448.42 398.51 4.06 o 5 2 0 1643.24 1919.40 17.25 o 6 2 0 51.51 44.51 1.85 o 7 2 0 744.92 701.96 9.46 o 8 2 0 324.26 305.86 3.72 o 9 2 0 119.35 97.53 3.28 o 10 2 0 188.42 199.22 6.56 o 11 2 0 0.08 0.47 2.18 o 12 2 0 2.83 -1.62 1.62 o 1 3 0 5119.44 4872.55 100.51 o 2 3 0 326.12 413.25 8.44 o 3 3 0 1224.55 1154.58 6.91 o 4 3 0 284.72 316.95 3.79 o 5 3 0 2606.65 2582.02 25.59 o 6 3 0 101.70 77.63 1.50 o 7 3 0 4029.59 4030.68 49.32 o 8 3 0 792.71 773.58 7.24 o 9 3 0 1204.61 1068.94 13.65 o 10 3 0 4.71 7.35 1.44 o 11 3 0 441.25 438.99 13.49 o 12 3 0 23.81 20.98 2.31 o 0 4 0 4155.88 4532.57 145.45 o 1 4 0 3552.04 3701.45 58.81 o 2 4 0 859.28 820.63 17.60 o 3 4 0 2736.70 2479.70 43.92 o 4 4 0 42.63 16.29 0.75 o 5 4 0 77.66 133.93 1.73 o 6 4 0 66.28 51.20 1.37 o 7 4 0 19.06 5.43 0.78 o 8 4 0 1594.05 1572.60 23.22 o 9 4 0 2171.48 2014.05 38.74 o 10 4 0 193.62 197.67 4.26 o 11 4 0 0.10 -1.39 1.39 o 12 4 0 279.52 309.86 14.71 o 1 5 0 0.39 13.00 1.14 o 2 5 0 75.05 60.97 1.75 o 3 5 0 2186.32 2206.70 35.21 o 4 5 0 13.71 40.38 1.28 o 5 5 0 339.96 436.67 7.04 o 6 5 0 2455.10 2329.51 23.59 o 7 5 0 133.01 128.33 2.55 o 8 5 0 2558.86 2416.22 47.17 o 9 5 0 84.89 123.32 3.37 o 10 5 0 9.83 9.79 2.16 o 11 5 0 147.82 124.07 4.87 o 12 5 0 1.87 -0.93 1.77 o 0 6 0 264.62 301.88 11.40 o 1 6 0 631.80 610.34 13.87 o 2 6 0 980.43 1070.91 24.40 o 3 6 0 982.59 1175.89 28.81 o 4 6 0 26.87 32.02 0.97 o 5 6 0 492.41 425.94 7.32 o 6 6 0 269.98 264.59 3.18 o 7 6 0 742.14 774.27 15.41 o 8 6 0 987.02 1028.15 16.25 o 9 6 0 9.36 4.20 1.06 o 10 6 0 19.28 23.61 2.31 o 11 6 0 10.68 11.10 1.76 o 12 6 0 36.11 37.03 3.66 o 1 7 0 31.15 96.46 1.53 o 2 7 0 1271.56 1400.05 19.49 o 3 7 0 301.75 246.91 4.67 o 4 7 0 29.21 48.46 1.37 o 5 7 0 427.92 420.15 4.48 o 6 7 0 268.93 270.29 6.68 o 7 7 0 5.42 4.73 0.99 o 8 7 0 0.26 -0.70 0.85 o 9 7 0 3.40 1.82 0.98 o 10 7 0 809.72 813.21 7.97 o 11 7 0 178.97 178.71 8.80 o 12 7 0 60.64 44.71 6.25 o 0 8 0 3488.09 3280.39 130.01 o 1 8 0 805.64 944.50 25.05 o 2 8 0 38.62 71.99 1.61 o 3 8 0 263.19 245.77 3.12 o 4 8 0 232.50 194.91 3.11 o 5 8 0 338.93 357.74 5.60 o 6 8 0 577.54 577.88 8.23 o 7 8 0 873.18 901.01 12.64 o 8 8 0 83.24 93.56 2.29 o 9 8 0 2.77 6.58 1.10 o 10 8 0 10.64 14.03 1.45 o 11 8 0 6.65 6.94 1.56 o 12 8 0 158.57 168.15 5.47 o 1 9 0 3192.94 3175.54 77.48 o 2 9 0 768.79 895.37 19.46 o 3 9 0 147.50 127.67 4.35 o 4 9 0 204.27 204.90 5.07 o 5 9 0 205.20 210.37 2.43 o 6 9 0 1032.56 1005.30 18.93 o 7 9 0 220.86 217.56 4.87 o 8 9 0 41.53 47.96 1.75 o 9 9 0 32.91 29.67 2.03 o 10 9 0 134.65 138.80 3.83 o 11 9 0 5.22 0.78 1.59 o 0 10 0 231.27 210.54 6.77 o 1 10 0 372.28 395.11 9.87 o 2 10 0 352.93 314.99 7.06 o 3 10 0 614.07 693.93 11.26 o 4 10 0 41.87 46.53 1.39 o 5 10 0 424.36 399.83 7.39 o 6 10 0 1229.43 1203.54 13.60 o 7 10 0 5.15 5.74 0.98 o 8 10 0 509.70 493.58 9.23 o 9 10 0 176.98 176.33 4.25 o 10 10 0 740.98 716.54 12.38 o 11 10 0 339.38 352.94 8.21 o 1 11 0 485.08 474.48 6.72 o 2 11 0 782.37 817.25 17.24 o 3 11 0 94.01 110.23 2.10 o 4 11 0 3701.42 3757.85 67.70 o 5 11 0 375.90 358.03 4.68 o 6 11 0 3732.87 3806.50 65.04 o 7 11 0 97.40 116.28 2.28 o 8 11 0 614.14 596.48 9.36 o 9 11 0 1.77 1.00 1.14 o 10 11 0 463.91 488.41 6.77 o 11 11 0 0.14 -0.26 2.07 o 0 12 0 24.17 37.84 2.02 o 1 12 0 1098.82 1179.52 31.61 o 2 12 0 21.26 11.82 1.29 o 3 12 0 533.96 562.16 10.65 o 4 12 0 56.32 48.80 1.38 o 5 12 0 37.16 49.76 1.60 o 6 12 0 357.68 369.35 7.77 o 7 12 0 278.61 245.22 3.17 o 8 12 0 1.54 3.37 1.14 o 9 12 0 99.80 107.97 2.58 o 10 12 0 12.10 17.56 1.69 o 1 13 0 637.23 568.88 14.17 o 2 13 0 1021.28 1036.63 20.75 o 3 13 0 47.84 48.53 1.29 o 4 13 0 370.81 423.81 9.34 o 5 13 0 243.39 206.13 3.23 o 6 13 0 179.19 182.95 5.87 o 7 13 0 36.16 28.59 1.88 o 8 13 0 263.43 281.09 5.86 o 9 13 0 34.93 29.58 1.89 o 10 13 0 211.77 200.05 4.23 o 0 14 0 516.78 532.81 21.71 o 1 14 0 5445.81 5361.52 103.00 o 2 14 0 1747.22 1729.04 31.55 o 3 14 0 1008.10 1010.09 15.00 o 4 14 0 61.49 54.55 1.62 o 5 14 0 360.59 326.35 4.92 o 6 14 0 8.35 10.44 1.12 o 7 14 0 64.33 63.69 2.06 o 8 14 0 29.73 31.37 1.73 o 9 14 0 18.44 14.62 1.59 o 10 14 0 107.35 122.33 6.30 o 1 15 0 26.22 32.68 1.20 o 2 15 0 116.98 107.40 1.73 o 3 15 0 240.88 241.07 4.71 o 4 15 0 1.87 4.54 0.98 o 5 15 0 275.94 269.14 8.28 o 6 15 0 223.07 235.64 5.10 o 7 15 0 538.44 549.59 11.62 o 8 15 0 64.50 60.81 2.35 o 9 15 0 79.51 68.15 2.60 o 0 16 0 2223.69 2258.02 49.78 o 1 16 0 476.56 492.05 8.83 o 2 16 0 24.64 23.11 1.30 o 3 16 0 181.13 171.62 4.51 o 4 16 0 2.28 0.90 1.11 o 5 16 0 29.41 22.01 1.65 o 6 16 0 2.92 0.90 1.25 o 7 16 0 264.74 279.20 6.93 o 8 16 0 0.18 -0.10 1.47 o 9 16 0 2.68 3.33 1.98 o 1 17 0 293.42 293.41 8.04 o 2 17 0 3.88 2.09 1.07 o 3 17 0 574.17 581.39 19.95 o 4 17 0 49.28 65.94 2.37 o 5 17 0 335.78 351.41 7.98 o 6 17 0 329.69 332.46 9.96 o 7 17 0 201.21 198.91 4.29 o 8 17 0 274.63 296.16 5.93 o 0 18 0 107.33 101.93 3.12 o 1 18 0 1.17 0.57 1.22 o 2 18 0 317.87 312.53 12.20 o 3 18 0 47.64 52.50 2.41 o 4 18 0 289.34 275.65 6.66 o 5 18 0 26.86 30.58 2.39 o 6 18 0 12.87 19.65 1.75 o 7 18 0 13.60 23.62 1.94 o 1 19 0 71.78 72.40 2.39 o 2 19 0 6.71 5.25 1.41 o 3 19 0 43.98 39.30 2.64 o 4 19 0 904.57 943.78 18.44 o 5 19 0 325.26 352.68 10.35 o 6 19 0 129.94 148.79 4.56 o 7 19 0 3.68 3.76 1.99 o 0 20 0 4.10 0.69 2.18 o 1 20 0 187.48 185.13 6.23 o 2 20 0 22.35 30.53 2.12 o 3 20 0 8.22 8.02 1.60 o 4 20 0 274.41 307.57 10.60 o 5 20 0 47.26 48.32 3.39 o 6 20 0 36.04 25.32 2.54 o 1 21 0 13.17 17.62 2.15 o 2 21 0 24.48 25.20 2.05 o 3 21 0 65.56 57.24 2.64 o 4 21 0 6.05 6.66 1.78 o 5 21 0 511.78 549.65 12.91 o 0 22 0 12.31 8.97 2.79 o 1 22 0 77.22 80.52 5.75 o 2 22 0 110.07 111.01 3.95 o 3 22 0 0.05 -1.92 1.92 o -13 1 1 53.34 47.22 4.27 o -12 1 1 32.36 33.60 3.70 o -11 1 1 159.43 173.32 7.20 o -10 1 1 209.51 228.60 7.55 o -9 1 1 114.08 125.94 3.24 o -8 1 1 317.00 309.48 3.70 o -7 1 1 984.58 910.54 11.99 o -6 1 1 36.40 72.29 1.42 o -5 1 1 405.33 478.10 5.72 o -4 1 1 2238.31 2249.44 33.94 o -3 1 1 347.16 441.30 3.29 o -2 1 1 1480.93 1455.36 15.97 o -1 1 1 8979.24 8789.03 171.31 o 0 1 1 114.40 122.84 1.80 o 1 1 1 591.26 613.50 13.58 o 2 1 1 34.43 76.56 1.07 o 3 1 1 4869.89 4790.30 59.89 o 4 1 1 4860.75 4834.92 64.42 o 5 1 1 1562.08 1517.72 7.71 o 6 1 1 251.09 213.03 3.59 o 7 1 1 1519.47 1470.91 14.63 o 8 1 1 60.78 60.20 1.92 o 9 1 1 91.97 66.45 2.13 o 10 1 1 328.48 333.38 7.46 o 11 1 1 309.88 318.38 10.02 o 12 1 1 76.83 76.06 6.61 o -13 2 1 263.58 292.63 11.96 o -12 2 1 2.93 -1.62 1.62 o -11 2 1 794.55 739.44 22.47 o -10 2 1 57.90 46.80 3.81 o -9 2 1 53.48 70.57 2.05 o -8 2 1 160.12 182.97 2.22 o -7 2 1 614.32 640.05 4.33 o -6 2 1 17.16 2.49 0.61 o -5 2 1 361.87 444.64 4.10 o -4 2 1 6162.90 5705.28 66.22 o -3 2 1 10.61 23.28 0.76 o -2 2 1 4764.38 5309.22 88.25 o -1 2 1 790.48 862.12 17.88 o 0 2 1 0.30 2.76 0.19 o 1 2 1 8207.42 8285.60 129.34 o 2 2 1 5071.36 4881.61 70.87 o 3 2 1 9715.51 8926.79 115.81 o 4 2 1 6181.07 6392.44 57.92 o 5 2 1 219.73 292.17 3.26 o 6 2 1 566.16 582.30 6.30 o 7 2 1 1.12 0.96 0.78 o 8 2 1 381.52 372.16 8.84 o 9 2 1 1.92 1.03 1.86 o 10 2 1 217.12 214.37 4.81 o 11 2 1 73.54 51.86 5.85 o 12 2 1 91.58 83.12 9.23 o -13 3 1 11.51 5.50 4.49 o -12 3 1 51.87 37.72 2.99 o -11 3 1 13.01 14.40 2.14 o -10 3 1 351.87 333.65 6.02 o -9 3 1 62.50 74.91 2.16 o -8 3 1 386.16 397.32 5.15 o -7 3 1 83.21 56.63 1.33 o -6 3 1 665.37 635.52 4.32 o -5 3 1 136.87 221.94 2.08 o -4 3 1 683.22 769.75 4.89 o -3 3 1 97.67 179.95 2.61 o -2 3 1 3135.44 3103.40 46.01 o -1 3 1 89.64 65.15 1.50 o 0 3 1 155.46 165.89 3.27 o 1 3 1 2153.59 2099.76 47.38 o 2 3 1 3273.10 3022.01 44.94 o 3 3 1 1635.52 1622.35 24.64 o 4 3 1 4749.60 5338.10 99.00 o 5 3 1 440.57 485.70 3.89 o 6 3 1 1148.20 1057.59 8.60 o 7 3 1 59.62 60.53 1.69 o 8 3 1 1237.52 1284.37 20.45 o 9 3 1 20.95 13.83 1.51 o 10 3 1 142.94 156.57 3.51 o 11 3 1 108.50 122.70 4.81 o 12 3 1 170.57 205.81 7.90 o -12 4 1 13.05 8.05 1.88 o -11 4 1 0.01 -0.17 2.09 o -10 4 1 11.80 6.37 1.58 o -9 4 1 295.09 247.53 5.06 o -8 4 1 190.97 212.53 4.21 o -7 4 1 573.39 583.55 7.20 o -6 4 1 582.89 518.42 5.26 o -5 4 1 4.65 3.83 0.65 o -4 4 1 5.25 2.33 0.49 o -3 4 1 33.42 27.80 0.84 o -2 4 1 5120.21 5275.50 109.46 o -1 4 1 2419.05 2729.47 73.91 o 0 4 1 707.72 662.21 10.14 o 1 4 1 4081.74 3975.61 62.87 o 2 4 1 3160.26 3082.12 60.04 o 3 4 1 163.82 180.17 3.90 o 4 4 1 137.66 125.59 1.99 o 5 4 1 318.46 410.91 3.62 o 6 4 1 6.67 10.26 0.94 o 7 4 1 235.83 216.50 4.00 o 8 4 1 266.89 276.36 6.92 o 9 4 1 158.35 137.54 3.85 o 10 4 1 24.75 20.25 1.80 o 11 4 1 20.51 18.45 2.34 o 12 4 1 203.96 231.32 7.96 o -12 5 1 0.98 -1.75 1.75 o -11 5 1 38.68 36.38 3.23 o -10 5 1 218.43 211.13 3.49 o -9 5 1 494.60 457.99 9.41 o -8 5 1 3.65 1.49 0.91 o -7 5 1 806.30 718.05 10.98 o -6 5 1 2489.56 2500.25 33.08 o -5 5 1 80.46 109.89 2.84 o -4 5 1 7107.48 7498.12 83.95 o -3 5 1 4890.60 4948.62 49.75 o -2 5 1 382.50 471.07 10.45 o -1 5 1 8.97 1.99 0.87 o 0 5 1 154.50 218.24 5.90 o 1 5 1 504.76 378.31 4.78 o 2 5 1 415.81 344.46 6.52 o 3 5 1 215.24 179.51 2.45 o 4 5 1 208.69 203.87 3.52 o 5 5 1 0.14 6.25 0.63 o 6 5 1 804.05 809.00 8.30 o 7 5 1 1420.06 1342.79 19.21 o 8 5 1 321.59 330.62 6.06 o 9 5 1 493.31 482.47 9.79 o 10 5 1 72.15 86.39 2.90 o 11 5 1 29.24 20.11 1.91 o 12 5 1 9.12 11.87 6.82 o -12 6 1 39.03 29.78 4.51 o -11 6 1 51.11 41.07 3.80 o -10 6 1 214.81 228.51 3.35 o -9 6 1 182.07 160.87 2.76 o -8 6 1 77.48 77.61 2.07 o -7 6 1 95.08 104.20 1.93 o -6 6 1 552.57 480.04 7.29 o -5 6 1 300.32 272.43 4.19 o -4 6 1 1939.96 1918.83 22.16 o -3 6 1 2422.56 2669.15 50.54 o -2 6 1 84.64 166.33 3.38 o -1 6 1 3664.94 3612.49 106.52 o 0 6 1 3.72 27.84 0.75 o 1 6 1 3263.84 3382.04 61.65 o 2 6 1 49.44 42.36 1.37 o 3 6 1 1072.67 897.54 18.17 o 4 6 1 0.31 5.89 0.81 o 5 6 1 416.87 478.30 8.72 o 6 6 1 2.89 5.37 0.95 o 7 6 1 70.57 63.08 2.23 o 8 6 1 121.00 132.78 2.33 o 9 6 1 21.13 19.83 1.69 o 10 6 1 138.34 137.56 3.96 o 11 6 1 0.24 -0.76 1.61 o 12 6 1 83.89 106.14 4.53 o -12 7 1 7.52 5.59 3.31 o -11 7 1 0.88 -1.61 1.61 o -10 7 1 36.42 39.06 1.99 o -9 7 1 21.80 27.60 1.47 o -8 7 1 782.73 824.38 11.64 o -7 7 1 1.03 1.75 0.82 o -6 7 1 298.76 294.81 4.71 o -5 7 1 0.32 9.44 1.60 o -4 7 1 150.81 176.25 3.53 o -3 7 1 19.14 4.21 0.82 o -2 7 1 1391.65 1593.12 27.84 o -1 7 1 886.46 1020.97 28.64 o 0 7 1 111.91 127.29 2.08 o 1 7 1 247.37 258.06 5.88 o 2 7 1 1323.79 1296.78 18.95 o 3 7 1 1306.68 1591.80 29.80 o 4 7 1 10.37 1.72 0.78 o 5 7 1 76.13 65.34 1.58 o 6 7 1 150.41 164.47 2.86 o 7 7 1 142.66 151.13 3.18 o 8 7 1 0.01 0.43 0.90 o 9 7 1 0.04 -1.00 1.00 o 10 7 1 30.75 29.51 1.89 o 11 7 1 22.13 19.09 2.91 o -12 8 1 184.70 192.02 7.53 o -11 8 1 75.78 76.11 4.14 o -10 8 1 5.98 8.53 1.30 o -9 8 1 445.97 439.41 5.73 o -8 8 1 13.28 13.14 1.13 o -7 8 1 162.48 175.39 2.48 o -6 8 1 517.85 629.30 7.93 o -5 8 1 214.17 211.67 3.86 o -4 8 1 1604.56 1707.98 24.65 o -3 8 1 227.53 243.27 4.53 o -2 8 1 1936.88 1990.64 34.97 o -1 8 1 289.96 284.56 9.41 o 0 8 1 524.23 492.85 7.90 o 1 8 1 107.42 105.77 2.11 o 2 8 1 1590.25 1706.83 36.31 o 3 8 1 290.48 366.71 10.01 o 4 8 1 225.73 262.50 2.87 o 5 8 1 561.62 503.10 11.12 o 6 8 1 246.74 252.05 3.76 o 7 8 1 603.69 569.30 13.02 o 8 8 1 14.68 14.15 1.19 o 9 8 1 0.95 1.50 1.07 o 10 8 1 163.87 184.87 5.45 o 11 8 1 4.31 2.37 1.53 o -12 9 1 77.23 70.22 7.24 o -11 9 1 25.27 24.00 1.75 o -10 9 1 170.77 181.61 3.93 o -9 9 1 734.70 723.93 11.76 o -8 9 1 361.32 354.69 7.31 o -7 9 1 961.67 992.97 19.88 o -6 9 1 8.75 10.25 1.10 o -5 9 1 934.99 941.79 18.19 o -4 9 1 0.39 3.36 0.65 o -3 9 1 2973.54 2850.18 56.49 o -2 9 1 358.43 425.39 5.43 o -1 9 1 1571.56 1924.48 36.76 o 0 9 1 55.69 74.26 1.55 o 1 9 1 649.60 813.60 22.36 o 2 9 1 190.85 173.46 2.46 o 3 9 1 0.10 6.38 0.70 o 4 9 1 2.08 0.23 0.58 o 5 9 1 1860.14 1910.32 29.21 o 6 9 1 673.09 654.79 11.21 o 7 9 1 281.76 267.26 4.88 o 8 9 1 617.57 578.90 13.02 o 9 9 1 106.74 108.46 2.45 o 10 9 1 101.72 95.76 3.67 o 11 9 1 21.07 15.76 1.94 o -11 10 1 21.42 26.94 2.54 o -10 10 1 39.12 46.65 2.08 o -9 10 1 33.33 21.16 1.47 o 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