#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015876.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015876_Fobs loop_ _publ_author_name 'D\'iaz de Vivar, M. Enriqueta' 'Baggio, Sergio' 'Garland, Mar\'ia Teresa' 'Baggio, Ricardo' _publ_section_title ; An unusual P3~1~2 framework for the Ni(4,4'-bipyridine)(H~2~O)~4~ chain ; _journal_coeditor_code AV3057 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m153 _journal_page_last m156 _journal_volume 63 _journal_year 2007 _space_group_IT_number 152 _symmetry_space_group_name_Hall 'P 31 2"' _symmetry_space_group_name_H-M 'P 31 2 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 11.2916 _cell_length_b 11.2916 _cell_length_c 23.6604 _exptl_crystal_F_000 1356.00 _reflns_d_resolution_high 0.7470 _[local]_cod_data_source_file av3057IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' en16p in P3(1)21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 330.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z+1/3' '-x+y, -x, z+2/3' 'y, x, -z' 'x-y, -y, -z+2/3' '-x, -x+y, -z+1/3' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 3088.71 3516.19 411.81 o 1 1 0 11407.37 11084.70 1486.25 o -1 2 0 10075.43 5870.64 4772.93 o 0 2 0 37002.51 41799.96 2541.17 o 1 2 0 5282.96 5472.72 410.09 o 2 2 0 686.54 570.29 89.59 o -1 3 0 5342.03 4377.02 873.16 o 0 3 0 328.72 381.59 31.82 o 1 3 0 4454.98 4683.84 206.48 o 2 3 0 4895.42 4932.88 408.18 o 3 3 0 814.53 806.32 59.34 o -2 4 0 924.64 450.76 226.74 o -1 4 0 4209.85 3389.10 664.77 o 0 4 0 60.85 78.74 15.84 o 1 4 0 1508.91 1507.53 74.43 o 2 4 0 5696.98 5438.60 446.33 o 3 4 0 949.23 900.94 93.80 o 4 4 0 1876.47 2135.09 99.94 o -2 5 0 4690.72 3304.29 956.33 o -1 5 0 1464.03 1109.16 163.27 o 0 5 0 2406.99 2463.23 177.23 o 1 5 0 3704.19 3972.90 206.26 o 2 5 0 138.11 160.66 23.28 o 3 5 0 2418.79 2421.90 170.05 o 4 5 0 148.44 262.81 49.60 o 5 5 0 79.56 121.14 60.08 o -3 6 0 824.47 428.30 204.69 o -2 6 0 5842.00 3481.40 1168.24 o -1 6 0 3778.44 3518.38 387.71 o 0 6 0 3983.60 3924.16 278.61 o 1 6 0 1036.86 981.57 96.81 o 2 6 0 726.28 787.18 84.91 o 3 6 0 601.33 737.58 63.10 o 4 6 0 888.42 1057.60 101.83 o 5 6 0 1196.03 1368.10 119.47 o -3 7 0 1031.36 601.42 227.04 o -2 7 0 162.54 134.32 37.47 o -1 7 0 1203.61 1022.45 135.81 o 0 7 0 545.76 575.18 90.94 o 1 7 0 323.56 361.98 50.68 o 2 7 0 1069.87 1195.97 86.37 o 3 7 0 828.35 1032.82 102.97 o 4 7 0 540.36 622.80 120.29 o 5 7 0 693.38 884.57 162.62 o -4 8 0 1920.73 1003.93 555.57 o -3 8 0 2283.85 1255.28 451.81 o -2 8 0 647.73 481.50 107.34 o -1 8 0 320.37 362.45 53.51 o 0 8 0 90.89 85.65 35.91 o 1 8 0 1595.32 1479.91 210.09 o 2 8 0 713.79 729.62 93.61 o 3 8 0 547.37 763.25 136.48 o 4 8 0 8.10 58.66 68.09 o -4 9 0 131.05 88.76 40.37 o -3 9 0 647.99 426.14 94.92 o -2 9 0 956.77 612.52 184.16 o -1 9 0 1616.93 1473.48 199.24 o 0 9 0 455.31 337.04 80.44 o 1 9 0 1839.57 2438.25 161.71 o 2 9 0 251.07 340.62 99.12 o 3 9 0 1896.82 2320.86 222.83 o 4 9 0 104.71 178.44 90.81 o -5 10 0 105.60 54.10 56.55 o -4 10 0 863.96 566.67 114.93 o -3 10 0 678.02 530.64 107.84 o -2 10 0 901.46 558.28 159.77 o -1 10 0 1631.58 1416.58 280.42 o 0 10 0 739.21 993.35 119.14 o 1 10 0 715.60 1185.43 131.23 o 2 10 0 92.88 91.52 78.43 o 3 10 0 105.67 190.00 92.67 o -5 11 0 1194.60 611.90 197.52 o -4 11 0 549.10 463.65 76.11 o -3 11 0 517.20 378.53 76.66 o -2 11 0 209.44 223.62 61.09 o -1 11 0 674.28 901.48 119.41 o 0 11 0 1885.00 2241.91 177.81 o 1 11 0 1221.56 1432.11 200.84 o 2 11 0 195.88 227.15 106.02 o 3 11 0 354.68 338.10 256.76 o -6 12 0 213.61 129.92 83.94 o -5 12 0 670.49 566.83 103.54 o -4 12 0 6.69 7.59 44.52 o -3 12 0 1885.54 1652.79 297.61 o -2 12 0 100.67 107.94 54.10 o -1 12 0 1167.64 1378.81 153.68 o 0 12 0 17.52 71.36 74.98 o 1 12 0 60.77 138.56 102.82 o -6 13 0 27.96 7.15 51.86 o -5 13 0 614.72 523.19 111.29 o -4 13 0 98.91 78.74 58.08 o -3 13 0 83.78 106.10 58.08 o -2 13 0 229.89 309.75 90.37 o -1 13 0 37.65 51.32 68.23 o -7 14 0 110.61 170.75 85.15 o -6 14 0 18.08 34.26 57.37 o -5 14 0 215.01 256.36 69.22 o -4 14 0 252.06 24.08 161.93 o -1 1 1 6063.33 6126.09 785.93 o 0 1 1 439.35 521.03 17.64 o 1 1 1 6746.52 7746.54 343.70 o -3 2 1 1521.89 1446.34 120.28 o -2 2 1 771.33 789.24 52.63 o -1 2 1 6357.97 5302.23 1225.95 o 0 2 1 16287.27 16913.71 1572.30 o 1 2 1 8969.63 9407.98 434.56 o 2 2 1 1027.71 1011.48 56.26 o -5 3 1 14561.02 14891.32 769.82 o -4 3 1 4578.74 4345.73 222.17 o -3 3 1 9647.72 9769.90 525.63 o -2 3 1 1381.12 1176.75 196.01 o -1 3 1 9443.57 7610.49 1744.16 o 0 3 1 9015.28 9679.83 646.50 o 1 3 1 8367.86 8491.16 413.34 o 2 3 1 21138.73 21853.03 1868.73 o 3 3 1 4521.17 3956.10 364.71 o -7 4 1 4970.09 5012.45 249.90 o -6 4 1 4556.60 4423.55 372.51 o -5 4 1 5272.03 5397.58 260.52 o -4 4 1 563.90 526.10 40.63 o -3 4 1 3944.37 3174.93 351.24 o -2 4 1 1118.19 697.62 203.42 o -1 4 1 8624.13 7590.32 1120.97 o 0 4 1 3434.69 3506.88 255.19 o 1 4 1 1997.35 2080.18 93.59 o 2 4 1 1132.34 1000.01 98.91 o 3 4 1 75.88 98.86 20.01 o 4 4 1 1577.59 1716.67 65.44 o -9 5 1 3780.36 4017.85 132.13 o -8 5 1 1212.25 1327.07 98.47 o -7 5 1 1644.50 1516.19 191.97 o -6 5 1 4125.25 3899.52 226.83 o -5 5 1 1222.89 1324.78 91.59 o -4 5 1 5383.64 4661.97 523.19 o -3 5 1 15257.37 10250.63 2757.26 o -2 5 1 19842.49 14165.74 4053.17 o -1 5 1 2296.17 1918.13 330.31 o 0 5 1 8870.36 8589.49 633.25 o 1 5 1 989.05 1024.80 70.66 o 2 5 1 11200.38 10703.48 993.96 o 3 5 1 2352.88 2486.03 86.67 o 4 5 1 3009.17 3333.79 211.34 o 5 5 1 42.13 42.32 37.55 o -11 6 1 941.50 1228.51 154.76 o -10 6 1 965.97 1106.60 102.18 o -9 6 1 2515.67 2670.17 107.16 o -8 6 1 3653.41 3404.24 280.92 o -7 6 1 2367.02 2185.48 174.82 o -6 6 1 1978.72 1916.06 137.73 o -5 6 1 3680.11 2924.67 381.59 o -4 6 1 4527.50 3766.70 580.19 o -3 6 1 4443.42 2884.76 799.55 o -2 6 1 1242.37 731.10 234.32 o -1 6 1 1031.69 925.57 123.06 o 0 6 1 1968.04 1861.12 144.37 o 1 6 1 948.06 931.39 111.33 o 2 6 1 1313.72 1355.60 116.95 o 3 6 1 1952.54 2134.31 92.85 o 4 6 1 240.98 265.07 53.09 o 5 6 1 944.91 1090.44 118.48 o 6 6 1 566.87 736.72 146.26 o -12 7 1 664.35 841.97 138.32 o -11 7 1 53.52 101.58 70.51 o -10 7 1 678.87 892.77 110.46 o -9 7 1 1306.80 1450.79 92.89 o -8 7 1 3208.26 3019.70 316.45 o -7 7 1 5205.87 4796.12 552.11 o -6 7 1 2207.56 1812.33 195.90 o -5 7 1 1725.22 1320.98 240.06 o -4 7 1 4529.62 2638.07 766.77 o -3 7 1 54.66 46.78 28.97 o -2 7 1 11471.66 8821.60 1882.57 o -1 7 1 1032.37 814.47 137.71 o 0 7 1 1065.05 1012.97 105.25 o 1 7 1 1400.98 1289.49 211.70 o 2 7 1 665.19 763.64 72.73 o 3 7 1 426.30 563.55 81.51 o 4 7 1 1438.17 1676.97 131.07 o -13 8 1 199.69 165.78 90.46 o -12 8 1 1017.53 1361.08 176.11 o -11 8 1 117.43 120.11 65.11 o -10 8 1 123.77 134.00 53.76 o -9 8 1 1063.36 886.42 165.64 o -8 8 1 280.28 300.42 50.99 o -7 8 1 3088.71 2682.56 292.87 o -6 8 1 3496.22 2809.46 517.36 o -5 8 1 1370.94 819.44 203.60 o -4 8 1 1617.24 909.34 299.68 o -3 8 1 2399.65 1303.16 453.03 o -2 8 1 1233.79 927.68 142.20 o -1 8 1 1722.47 1454.21 203.06 o 0 8 1 550.03 566.55 99.05 o 1 8 1 20.62 63.52 37.30 o 2 8 1 170.52 252.26 49.95 o 3 8 1 317.54 486.98 114.02 o 4 8 1 143.85 170.34 72.50 o -13 9 1 5.04 -26.50 63.12 o -12 9 1 227.29 342.17 106.51 o -11 9 1 95.81 144.50 81.99 o -10 9 1 17.16 -11.12 41.74 o -9 9 1 2140.79 2060.12 409.01 o -8 9 1 949.72 837.20 171.15 o -7 9 1 1374.70 1088.82 228.11 o -6 9 1 2431.65 1622.88 350.73 o -5 9 1 3736.78 2243.74 531.07 o -4 9 1 3156.52 2160.88 681.72 o -3 9 1 1975.12 1334.09 342.03 o -2 9 1 571.92 450.51 123.05 o -1 9 1 36.20 66.08 35.31 o 0 9 1 149.29 195.28 45.53 o 1 9 1 445.48 659.87 96.63 o 2 9 1 444.15 559.20 118.96 o 3 9 1 246.01 352.04 109.01 o -13 10 1 3.16 61.84 84.90 o -12 10 1 91.26 165.00 92.65 o -11 10 1 316.88 429.35 85.66 o -10 10 1 0.13 52.04 50.10 o -9 10 1 8.59 41.83 40.61 o -8 10 1 165.76 141.06 48.38 o -7 10 1 831.98 657.93 114.03 o -6 10 1 1052.85 809.70 150.96 o -5 10 1 30.35 -5.69 37.29 o -4 10 1 257.12 177.18 53.33 o -3 10 1 450.29 361.37 71.47 o -2 10 1 122.12 172.41 51.58 o -1 10 1 390.67 397.56 87.13 o 0 10 1 126.88 135.01 56.82 o 1 10 1 57.72 82.35 51.35 o 2 10 1 35.70 112.11 78.76 o 3 10 1 23.35 155.77 123.86 o -14 11 1 11.99 33.75 83.91 o -13 11 1 33.74 30.30 79.82 o -12 11 1 35.55 114.38 89.92 o -11 11 1 54.52 135.61 62.31 o -10 11 1 324.83 348.45 74.33 o -9 11 1 119.59 119.72 52.12 o -8 11 1 117.25 103.65 50.93 o -7 11 1 38.98 27.07 44.88 o -6 11 1 1101.53 709.16 155.60 o -5 11 1 1001.26 443.68 178.89 o -4 11 1 1257.83 965.76 238.35 o -3 11 1 258.86 274.43 63.78 o -2 11 1 461.00 317.27 67.85 o -1 11 1 59.48 122.29 59.25 o 0 11 1 6.85 9.86 51.48 o 1 11 1 112.36 219.88 100.25 o 2 11 1 336.65 580.55 145.95 o 3 11 1 185.58 448.58 265.08 o -13 12 1 98.89 92.82 99.17 o -12 12 1 5.46 57.94 58.10 o -11 12 1 52.41 126.29 67.40 o -10 12 1 121.12 125.04 62.09 o -9 12 1 300.36 240.04 63.31 o -8 12 1 1065.00 855.23 166.82 o -7 12 1 637.29 425.52 118.48 o -6 12 1 603.68 407.69 149.75 o -5 12 1 1005.68 587.49 172.16 o -4 12 1 119.00 107.32 54.21 o -3 12 1 194.65 215.31 63.46 o -2 12 1 43.73 43.52 60.58 o -1 12 1 101.23 137.74 67.42 o 0 12 1 37.03 79.23 86.74 o 1 12 1 73.72 101.74 101.39 o -12 13 1 74.06 159.16 82.60 o -11 13 1 21.75 88.01 66.41 o -10 13 1 10.23 61.59 55.98 o -9 13 1 8.73 21.13 49.41 o -8 13 1 238.17 182.36 65.01 o -7 13 1 238.94 271.67 68.24 o -6 13 1 641.37 622.60 103.29 o -5 13 1 487.65 380.72 79.23 o -4 13 1 354.98 242.90 62.99 o -3 13 1 22.14 -13.20 52.73 o -2 13 1 410.15 457.65 98.51 o -1 13 1 74.68 116.65 67.09 o -10 14 1 408.27 -9.94 153.47 o -9 14 1 171.27 157.54 68.25 o -8 14 1 687.69 519.03 96.24 o -7 14 1 4.89 8.78 51.72 o -6 14 1 86.61 150.37 65.72 o -5 14 1 121.81 145.98 64.75 o -4 14 1 7.86 85.31 102.23 o -1 1 2 17515.13 18313.21 1782.39 o 0 1 2 8465.11 9095.20 456.51 o 1 1 2 1296.93 1255.77 92.98 o -3 2 2 3524.00 3748.43 164.23 o -2 2 2 20078.00 22382.18 1699.58 o -1 2 2 1151.88 1082.83 87.64 o 0 2 2 31616.46 33428.94 2421.68 o 1 2 2 11307.58 10548.12 1343.93 o 2 2 2 9253.75 9140.91 673.01 o -5 3 2 919.73 890.99 90.16 o -4 3 2 2172.31 2366.70 113.74 o -3 3 2 3197.38 3300.69 220.56 o -2 3 2 3425.75 3297.38 397.27 o -1 3 2 12007.77 10819.51 1593.52 o 0 3 2 1263.46 1319.29 106.82 o 1 3 2 3248.93 3202.20 233.23 o 2 3 2 4020.46 3858.38 319.43 o 3 3 2 2263.45 1922.77 163.88 o -7 4 2 575.89 661.71 42.36 o -6 4 2 1498.16 1472.62 122.38 o -5 4 2 1662.01 1618.89 87.29 o -4 4 2 88.45 105.57 20.42 o -3 4 2 2039.38 1834.98 218.98 o -2 4 2 9434.74 8212.90 1397.61 o -1 4 2 3238.74 2892.89 379.36 o 0 4 2 1391.81 1097.50 100.13 o 1 4 2 1912.96 1926.64 161.93 o 2 4 2 4824.91 4539.03 423.76 o 3 4 2 332.04 301.21 46.28 o 4 4 2 2497.19 2755.48 90.42 o -9 5 2 944.72 1160.92 73.96 o -8 5 2 1824.75 1877.56 138.70 o -7 5 2 3392.40 3325.56 215.44 o -6 5 2 987.80 1067.70 65.95 o -5 5 2 2510.53 2570.75 115.24 o -4 5 2 1843.90 1496.11 172.12 o -3 5 2 1224.24 1002.02 198.94 o -2 5 2 4492.60 3239.21 781.99 o -1 5 2 1972.09 1786.96 230.75 o 0 5 2 1470.96 1492.26 154.88 o 1 5 2 4247.00 4051.12 336.78 o 2 5 2 241.59 207.28 36.09 o 3 5 2 782.78 901.37 69.02 o 4 5 2 2045.70 2278.10 113.40 o 5 5 2 727.44 1040.72 91.99 o -11 6 2 3127.35 3643.35 276.77 o -10 6 2 1103.30 1399.34 159.40 o -9 6 2 555.62 567.46 61.12 o -8 6 2 893.10 836.21 94.83 o -7 6 2 208.78 214.00 43.48 o -6 6 2 498.61 596.54 69.80 o -5 6 2 840.93 728.37 104.80 o -4 6 2 1479.71 1163.19 197.62 o -3 6 2 2239.99 1333.07 391.06 o -2 6 2 4914.75 3563.43 807.99 o -1 6 2 4249.04 3792.43 468.26 o 0 6 2 1708.50 1749.89 142.77 o 1 6 2 339.32 305.74 30.49 o 2 6 2 706.59 954.03 74.28 o 3 6 2 1604.81 1803.21 153.37 o 4 6 2 876.34 1135.18 113.66 o 5 6 2 1319.58 1758.96 176.10 o 6 6 2 542.56 721.83 161.07 o -13 7 2 425.25 518.94 131.97 o -12 7 2 989.76 1218.46 165.88 o -11 7 2 742.42 791.86 135.08 o -10 7 2 772.89 875.42 98.11 o -9 7 2 2218.52 1874.09 306.64 o -8 7 2 60.39 79.32 31.23 o -7 7 2 4113.70 3911.70 402.74 o -6 7 2 192.69 208.83 39.01 o -5 7 2 3485.91 2879.98 427.20 o -4 7 2 580.87 436.08 78.72 o -3 7 2 345.16 199.87 76.80 o -2 7 2 247.99 166.93 43.59 o -1 7 2 406.80 391.26 46.51 o 0 7 2 5030.18 4735.65 421.85 o 1 7 2 0.74 49.17 27.78 o 2 7 2 1480.57 1600.02 106.20 o 3 7 2 296.29 374.04 68.02 o 4 7 2 858.12 924.17 103.58 o 5 7 2 313.77 384.25 115.17 o -13 8 2 39.51 75.32 81.55 o -12 8 2 348.44 556.50 124.50 o -11 8 2 177.98 176.93 83.61 o -10 8 2 887.07 1083.29 112.18 o -9 8 2 289.03 302.56 59.13 o -8 8 2 2714.55 2410.66 363.05 o -7 8 2 54.30 67.64 32.56 o -6 8 2 871.12 650.48 140.79 o -5 8 2 1736.69 1031.23 212.72 o -4 8 2 2461.42 1608.60 370.21 o -3 8 2 821.04 411.89 142.42 o -2 8 2 647.01 316.59 112.40 o -1 8 2 6.10 33.52 29.85 o 0 8 2 3527.07 2994.97 357.08 o 1 8 2 1734.72 1981.83 121.64 o 2 8 2 1213.59 1410.68 120.89 o 3 8 2 554.40 624.25 89.77 o 4 8 2 23.11 143.79 171.78 o -13 9 2 1.46 -14.80 67.23 o -12 9 2 261.45 317.64 104.52 o -11 9 2 792.87 1009.80 120.62 o -10 9 2 94.41 133.54 55.04 o -9 9 2 10258.09 9025.56 1473.65 o -8 9 2 276.72 245.80 60.96 o -7 9 2 2488.94 2197.60 350.88 o -6 9 2 476.83 354.53 60.79 o -5 9 2 962.98 751.59 111.26 o -4 9 2 2051.45 1322.53 391.31 o -3 9 2 1593.74 953.00 347.86 o -2 9 2 1429.26 1017.52 157.02 o -1 9 2 2042.99 1886.76 233.95 o 0 9 2 625.68 758.65 87.58 o 1 9 2 1109.97 1412.79 115.86 o 2 9 2 596.08 845.32 143.17 o 3 9 2 199.63 337.52 102.12 o -14 10 2 20.76 -21.75 73.93 o -13 10 2 114.90 219.70 104.16 o -12 10 2 279.81 329.80 110.93 o -11 10 2 855.29 1137.73 130.59 o -10 10 2 1131.01 1024.07 231.86 o -9 10 2 87.52 131.09 51.33 o -8 10 2 1043.74 861.08 203.28 o -7 10 2 691.31 545.82 124.99 o -6 10 2 1183.41 922.44 145.01 o -5 10 2 763.35 553.09 131.02 o -4 10 2 834.37 521.45 194.38 o -3 10 2 386.37 362.84 63.42 o -2 10 2 1144.33 835.55 180.78 o -1 10 2 1186.87 1159.99 161.83 o 0 10 2 5944.86 6564.01 238.81 o 1 10 2 1097.27 1442.59 188.35 o 2 10 2 588.25 829.65 153.29 o 3 10 2 92.44 227.50 239.57 o -14 11 2 267.10 466.99 140.69 o -13 11 2 490.51 671.21 151.57 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27 292.28 508.06 247.60 o -5 5 27 494.62 514.29 108.85 o -4 5 27 109.59 139.42 81.57 o -3 5 27 300.63 319.47 93.23 o -2 5 27 207.59 231.39 71.70 o -1 5 27 93.76 -6.58 76.49 o 0 5 27 534.13 411.75 136.85 o 1 5 27 106.26 257.82 173.62 o 2 5 27 2.62 -9.76 94.27 o -5 6 27 330.55 525.15 247.47 o -4 6 27 196.29 160.52 99.13 o -3 6 27 151.06 91.48 96.11 o -2 6 27 184.76 324.69 139.19 o -1 6 27 120.33 171.54 152.90 o 0 6 27 70.81 196.84 163.19 o -3 7 27 137.38 185.28 95.15 o -1 1 28 428.27 479.31 106.42 o 0 1 28 1081.11 1400.96 231.50 o 1 1 28 231.43 209.65 181.98 o -3 2 28 88.37 107.79 106.10 o -2 2 28 647.58 428.45 196.52 o -1 2 28 204.62 232.52 101.45 o 0 2 28 85.40 146.75 78.00 o 1 2 28 26.71 98.58 100.97 o 2 2 28 18.23 -15.47 90.89 o -5 3 28 72.20 187.05 172.91 o -4 3 28 38.90 49.78 79.14 o -3 3 28 61.52 45.13 73.36 o -2 3 28 91.20 135.18 66.98 o -1 3 28 15.40 13.52 62.04 o 0 3 28 523.74 230.27 309.96 o 1 3 28 157.94 135.19 123.27 o -5 4 28 26.96 2.12 167.41 o -4 4 28 50.28 112.91 67.64 o 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403.79 142.89 o 0 2 30 118.62 122.66 166.71 o -2 3 30 1.26 -14.26 83.28 o -1 3 30 8.82 74.40 177.70 o -2 4 30 310.85 548.37 183.27 o -1 2 31 21.91 309.92 187.85 o