#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:10:51 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180827 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/58/2015884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015884_Fobs loop_ _publ_author_name 'Forsyth, Craig M.' 'Dean, Pamela M.' 'MacFarlane, Douglas R.' _publ_section_title ; Sodium pyridine-3-carboxylate ; _journal_coeditor_code DN2134 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m169 _journal_page_last m170 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.935 _cell_angle_gamma 90.000 _cell_length_a 20.1983 _cell_length_b 14.1880 _cell_length_c 6.3000 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file dn2134Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Nico_0m in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 295.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 517.09 538.77 9.45 o 4 0 0 53.58 23.71 1.25 o 6 0 0 36065.25 35260.66 273.63 o 8 0 0 17954.82 18033.65 144.44 o 10 0 0 8330.44 8479.53 70.07 o 12 0 0 221.38 208.68 4.89 o 14 0 0 939.61 1001.91 13.24 o 16 0 0 1517.48 1593.41 20.15 o 18 0 0 477.61 476.46 12.52 o 20 0 0 3103.88 2946.16 55.24 o 22 0 0 235.76 255.55 15.36 o 24 0 0 597.73 568.66 32.65 o 1 1 0 10593.84 9855.91 156.03 o 3 1 0 1440.87 1486.24 13.13 o 5 1 0 59.78 56.10 1.13 o 7 1 0 19398.67 18671.33 112.08 o 9 1 0 872.54 884.44 7.30 o 11 1 0 1213.92 1291.55 9.75 o 13 1 0 1348.05 1306.03 10.30 o 15 1 0 169.30 162.21 3.31 o 17 1 0 18.78 19.08 2.09 o 19 1 0 510.50 543.38 10.43 o 21 1 0 214.99 211.96 10.67 o 23 1 0 27.33 34.02 4.47 o 25 1 0 58.56 53.14 6.73 o 0 2 0 5.94 -0.89 0.89 o 2 2 0 650.95 640.43 4.93 o 4 2 0 524.54 530.53 4.28 o 6 2 0 7008.36 6717.93 43.76 o 8 2 0 108.87 97.92 1.89 o 10 2 0 38.97 53.15 1.68 o 12 2 0 257.82 234.49 3.62 o 14 2 0 886.26 825.44 8.16 o 16 2 0 24.08 23.19 1.89 o 18 2 0 302.42 307.76 7.89 o 20 2 0 898.38 883.70 17.45 o 22 2 0 34.51 28.27 4.37 o 24 2 0 235.12 250.70 10.09 o 1 3 0 446.59 443.98 3.79 o 3 3 0 169.38 129.60 1.95 o 5 3 0 257.33 291.20 3.10 o 7 3 0 230.51 210.42 2.80 o 9 3 0 398.38 411.67 4.64 o 11 3 0 2827.25 3057.27 21.26 o 13 3 0 7.05 5.02 0.78 o 15 3 0 13.99 22.77 1.54 o 17 3 0 10.99 11.55 2.41 o 19 3 0 533.06 554.18 11.99 o 21 3 0 38.17 47.56 5.43 o 23 3 0 166.53 164.99 8.67 o 25 3 0 135.56 130.73 8.43 o 0 4 0 27592.50 27793.01 223.89 o 2 4 0 875.36 829.61 6.24 o 4 4 0 1605.51 1556.03 11.02 o 6 4 0 116.56 77.24 1.66 o 8 4 0 2951.28 3007.15 20.59 o 10 4 0 1319.90 1352.45 11.42 o 12 4 0 65.62 87.05 2.39 o 14 4 0 1078.68 1010.03 10.34 o 16 4 0 5.83 8.16 1.35 o 18 4 0 615.05 606.52 11.71 o 20 4 0 1160.02 1132.59 24.46 o 22 4 0 72.15 69.81 7.49 o 24 4 0 132.70 134.27 9.30 o 1 5 0 15536.39 15641.01 95.62 o 3 5 0 1233.84 1223.95 9.28 o 5 5 0 96.87 115.78 2.09 o 7 5 0 3277.16 2965.43 20.88 o 9 5 0 61.43 84.77 2.13 o 11 5 0 273.59 357.05 4.85 o 13 5 0 151.81 173.49 3.48 o 15 5 0 624.77 639.63 9.05 o 17 5 0 32.77 41.43 3.49 o 19 5 0 1.36 2.60 2.05 o 21 5 0 19.28 14.03 4.98 o 23 5 0 187.49 197.50 10.41 o 0 6 0 56451.41 57159.15 505.24 o 2 6 0 612.01 618.98 5.66 o 4 6 0 104.99 110.63 2.13 o 6 6 0 20988.62 21466.89 136.37 o 8 6 0 197.63 291.08 3.98 o 10 6 0 541.39 425.10 5.26 o 12 6 0 587.61 598.49 7.00 o 14 6 0 962.14 896.50 10.44 o 16 6 0 2566.49 2511.86 30.29 o 18 6 0 805.16 786.00 15.97 o 20 6 0 444.62 451.63 14.38 o 22 6 0 0.60 6.32 2.98 o 24 6 0 127.09 127.92 10.92 o 1 7 0 745.18 657.60 6.12 o 3 7 0 0.63 3.04 0.68 o 5 7 0 1538.73 1430.63 11.70 o 7 7 0 4542.11 4530.51 31.58 o 9 7 0 2471.19 2434.33 18.47 o 11 7 0 57.79 58.27 2.15 o 13 7 0 1601.01 1572.29 15.40 o 15 7 0 369.55 362.51 8.05 o 17 7 0 159.43 153.45 6.92 o 19 7 0 201.66 216.71 9.90 o 21 7 0 138.47 133.95 12.73 o 23 7 0 27.75 38.98 7.37 o 0 8 0 400.85 234.66 4.86 o 2 8 0 55.23 66.42 1.86 o 4 8 0 674.27 783.96 7.69 o 6 8 0 5741.86 5518.69 39.03 o 8 8 0 113.94 109.48 2.66 o 10 8 0 20.16 16.62 1.36 o 12 8 0 17.55 15.87 1.67 o 14 8 0 2884.27 2830.38 32.99 o 16 8 0 82.73 80.46 5.33 o 18 8 0 566.45 554.40 15.90 o 20 8 0 22.15 27.14 5.78 o 22 8 0 74.38 82.98 7.73 o 1 9 0 968.54 1037.16 9.39 o 3 9 0 0.01 2.30 0.72 o 5 9 0 1060.62 1116.25 9.99 o 7 9 0 459.04 438.97 5.66 o 9 9 0 913.57 874.37 9.63 o 11 9 0 1844.00 1828.93 17.94 o 13 9 0 1344.60 1360.74 18.53 o 15 9 0 5.73 3.96 2.35 o 17 9 0 679.33 687.15 23.03 o 19 9 0 24.59 22.89 4.44 o 21 9 0 626.57 622.33 18.41 o 0 10 0 88.82 63.33 3.22 o 2 10 0 1212.00 1220.64 10.95 o 4 10 0 157.71 153.55 3.55 o 6 10 0 151.93 133.27 3.06 o 8 10 0 1334.06 1315.21 13.40 o 10 10 0 57.73 62.82 3.16 o 12 10 0 2824.09 2706.40 31.01 o 14 10 0 1803.72 1827.02 27.81 o 16 10 0 339.32 361.31 12.59 o 18 10 0 121.09 106.93 7.89 o 20 10 0 614.21 644.84 18.64 o 1 11 0 101.27 101.72 2.98 o 3 11 0 485.73 461.02 6.22 o 5 11 0 638.83 612.86 7.78 o 7 11 0 2620.96 2542.86 24.94 o 9 11 0 693.58 712.41 11.39 o 11 11 0 471.03 473.13 11.40 o 13 11 0 581.12 570.04 13.17 o 15 11 0 2473.88 2445.98 42.07 o 17 11 0 9.22 10.64 3.49 o 19 11 0 537.03 558.20 17.18 o 0 12 0 1601.15 1633.37 26.87 o 2 12 0 652.47 623.04 9.23 o 4 12 0 116.57 91.53 3.44 o 6 12 0 3576.09 3524.25 34.57 o 8 12 0 127.72 162.86 5.89 o 10 12 0 169.72 152.45 7.07 o 12 12 0 520.22 524.48 12.67 o 14 12 0 597.83 586.42 16.50 o 16 12 0 245.96 246.64 10.80 o 18 12 0 0.68 2.47 2.93 o 1 13 0 1606.15 1403.46 19.62 o 3 13 0 75.01 62.74 3.99 o 5 13 0 29.31 14.73 2.60 o 7 13 0 3672.27 3358.93 43.87 o 9 13 0 2274.39 2146.23 29.38 o 11 13 0 74.71 80.80 6.66 o 13 13 0 131.72 132.40 8.31 o 15 13 0 1.27 0.49 2.88 o 17 13 0 65.81 52.63 6.39 o 0 14 0 3691.84 3445.54 63.46 o 2 14 0 136.39 127.96 5.90 o 4 14 0 420.13 347.28 9.86 o 6 14 0 666.17 640.04 15.20 o 8 14 0 432.78 446.35 13.78 o 10 14 0 141.46 164.49 9.02 o 12 14 0 307.92 278.09 11.28 o 14 14 0 929.81 970.16 23.46 o 16 14 0 3.70 8.90 3.66 o 1 15 0 301.30 360.58 12.11 o 3 15 0 709.94 669.70 17.45 o 5 15 0 42.14 47.52 5.45 o 7 15 0 1240.45 1264.14 31.19 o 9 15 0 27.37 26.31 4.64 o 11 15 0 79.38 106.23 7.95 o 13 15 0 1203.35 1280.33 31.58 o 15 15 0 208.50 213.70 11.24 o 0 16 0 932.53 1033.33 44.64 o 2 16 0 66.53 53.03 5.98 o 4 16 0 183.34 176.64 9.43 o 6 16 0 376.02 380.69 13.36 o 8 16 0 803.40 883.07 21.89 o 10 16 0 367.13 394.24 14.16 o 12 16 0 218.56 235.39 11.19 o 1 17 0 26.99 27.52 4.61 o 3 17 0 1.56 2.65 2.80 o 5 17 0 15.60 24.58 4.41 o 7 17 0 359.15 428.64 16.51 o 9 17 0 183.59 168.95 10.09 o 0 18 0 704.42 771.35 29.49 o 2 18 0 329.47 400.43 14.48 o 4 18 0 71.97 101.72 8.25 o -25 1 1 17.45 19.77 4.30 o -23 1 1 416.80 460.34 12.08 o -21 1 1 226.63 236.42 6.80 o -19 1 1 721.11 692.47 12.52 o -17 1 1 3.98 4.64 1.11 o -15 1 1 1256.09 1315.77 11.93 o -13 1 1 492.56 592.49 5.61 o -11 1 1 605.04 482.46 4.97 o -9 1 1 149.70 136.26 2.06 o -7 1 1 2168.67 2269.18 14.34 o -5 1 1 87600.66 86897.31 519.83 o -3 1 1 47.28 45.59 0.73 o -1 1 1 6.31 8.01 0.30 o 1 1 1 30165.98 31123.37 184.08 o 3 1 1 15.87 16.77 0.68 o 5 1 1 133.79 163.01 2.23 o 7 1 1 6524.73 6280.71 40.49 o 9 1 1 1515.47 1497.12 12.21 o 11 1 1 1047.77 1179.81 10.56 o 13 1 1 582.04 547.43 6.49 o 15 1 1 432.86 406.34 5.74 o 17 1 1 100.79 111.19 4.71 o 19 1 1 954.63 875.64 18.39 o 21 1 1 156.84 165.87 8.40 o 23 1 1 282.64 295.23 12.40 o 25 1 1 453.41 470.90 24.74 o -26 2 1 61.08 78.00 6.74 o -24 2 1 16.00 18.68 3.67 o -22 2 1 28.32 34.82 3.59 o -20 2 1 2017.64 2001.09 26.16 o -18 2 1 193.22 187.84 5.92 o -16 2 1 1235.95 1306.90 13.45 o -14 2 1 17.94 17.47 1.46 o -12 2 1 1065.11 963.11 8.38 o -10 2 1 13.37 17.08 0.91 o -8 2 1 628.96 631.66 5.21 o -6 2 1 2960.19 3419.74 21.38 o -4 2 1 14107.90 13722.37 82.29 o -2 2 1 2624.78 2483.35 20.83 o 0 2 1 8658.04 8927.89 54.06 o 2 2 1 73.05 79.30 1.73 o 4 2 1 53.42 46.67 1.19 o 6 2 1 7606.74 8143.89 52.27 o 8 2 1 11471.07 11747.41 74.00 o 10 2 1 2423.42 2450.86 18.52 o 12 2 1 2247.01 2434.49 19.53 o 14 2 1 204.44 180.87 3.70 o 16 2 1 3824.05 3737.69 32.23 o 18 2 1 37.88 29.36 3.99 o 20 2 1 422.93 371.51 11.60 o 22 2 1 23.76 18.98 3.91 o 24 2 1 41.34 49.83 6.35 o -25 3 1 5.28 9.43 3.40 o -23 3 1 47.33 46.09 5.87 o -21 3 1 738.21 732.06 13.65 o -19 3 1 1847.46 1845.26 24.30 o -17 3 1 266.08 271.10 6.24 o -15 3 1 0.03 1.88 0.89 o -13 3 1 1465.42 1351.14 11.94 o -11 3 1 735.29 711.36 6.74 o -9 3 1 35.39 24.34 1.12 o -7 3 1 672.45 739.75 6.38 o -5 3 1 1816.21 2039.07 14.35 o -3 3 1 374.86 358.92 3.24 o -1 3 1 0.29 1.06 0.33 o 1 3 1 63.86 69.29 1.69 o 3 3 1 1387.06 1432.47 10.51 o 5 3 1 890.64 789.49 6.90 o 7 3 1 6911.30 7270.11 46.10 o 9 3 1 15915.09 15917.92 105.38 o 11 3 1 279.42 285.59 4.41 o 13 3 1 930.73 959.61 9.92 o 15 3 1 1700.68 1736.54 15.86 o 17 3 1 154.06 157.99 6.15 o 19 3 1 101.35 85.90 6.99 o 21 3 1 12.22 10.75 3.78 o 23 3 1 2.92 3.51 2.82 o -24 4 1 376.36 398.03 14.09 o -22 4 1 318.85 335.65 10.25 o -20 4 1 2824.95 2883.59 34.66 o -18 4 1 4020.26 4072.13 41.51 o -16 4 1 20.52 11.75 1.61 o -14 4 1 2173.95 2149.69 18.31 o -12 4 1 3786.52 3778.58 26.78 o -10 4 1 1029.59 1097.56 9.75 o -8 4 1 749.38 785.65 7.24 o -6 4 1 698.86 567.52 5.30 o -4 4 1 1383.33 1324.05 9.93 o -2 4 1 1001.04 898.62 7.16 o 0 4 1 570.29 435.70 3.88 o 2 4 1 16479.10 16180.15 107.22 o 4 4 1 126.71 128.21 2.36 o 6 4 1 3218.38 3521.11 25.35 o 8 4 1 19321.88 19880.62 137.45 o 10 4 1 6117.43 6228.88 43.42 o 12 4 1 961.40 846.04 8.99 o 14 4 1 7971.47 7964.08 63.47 o 16 4 1 3417.29 3337.04 34.15 o 18 4 1 2204.01 2182.69 38.00 o 20 4 1 339.12 357.46 12.87 o 22 4 1 1043.78 989.86 24.12 o 24 4 1 131.94 116.79 8.17 o -25 5 1 1153.71 1251.76 28.18 o -23 5 1 1059.23 1102.90 25.08 o -21 5 1 962.59 986.48 18.84 o -19 5 1 379.17 377.40 9.03 o -17 5 1 27.61 27.59 2.62 o -15 5 1 7.88 6.75 1.16 o -13 5 1 3466.24 3518.17 27.42 o -11 5 1 0.02 1.99 0.67 o -9 5 1 2930.02 3084.39 22.68 o -7 5 1 4328.26 4515.08 31.06 o -5 5 1 1225.78 1035.81 9.82 o -3 5 1 249.46 247.16 2.97 o -1 5 1 2122.58 2121.38 14.63 o 1 5 1 466.82 284.42 3.28 o 3 5 1 13111.49 13662.37 88.67 o 5 5 1 3167.67 3382.99 24.35 o 7 5 1 384.79 278.90 3.86 o 9 5 1 3564.45 3669.41 26.40 o 11 5 1 123.81 146.62 3.14 o 13 5 1 18.29 17.52 1.57 o 15 5 1 2317.61 2322.74 26.13 o 17 5 1 227.22 220.94 9.61 o 19 5 1 1572.34 1570.27 30.79 o 21 5 1 1632.04 1640.35 32.91 o 23 5 1 95.64 108.81 8.77 o -24 6 1 34.51 45.36 5.93 o -22 6 1 12.95 15.34 3.56 o -20 6 1 28.08 33.07 3.93 o -18 6 1 383.68 371.20 8.09 o -16 6 1 429.81 444.52 8.54 o -14 6 1 3417.01 3440.01 30.25 o -12 6 1 309.37 296.38 4.61 o -10 6 1 114.58 113.15 2.58 o -8 6 1 55.44 68.30 1.91 o -6 6 1 15674.01 16363.67 107.44 o -4 6 1 2856.20 2677.24 18.50 o -2 6 1 2515.21 2393.23 16.26 o 0 6 1 106.16 61.83 1.60 o 2 6 1 12169.34 12168.88 75.28 o 4 6 1 387.55 408.55 4.80 o 6 6 1 106.36 102.62 2.26 o 8 6 1 8.66 30.36 1.63 o 10 6 1 1693.38 1759.24 14.44 o 12 6 1 279.87 284.68 4.70 o 14 6 1 2336.53 2256.70 22.23 o 16 6 1 19.25 25.38 3.50 o 18 6 1 4.62 -0.93 2.63 o 20 6 1 26.03 25.36 4.72 o 22 6 1 1255.88 1234.89 28.04 o -23 7 1 289.88 290.24 11.86 o -21 7 1 832.95 825.76 18.68 o -19 7 1 2.50 2.51 2.41 o -17 7 1 522.89 523.33 9.80 o -15 7 1 591.36 568.63 10.64 o -13 7 1 53.62 55.51 2.74 o -11 7 1 798.81 882.58 9.07 o -9 7 1 70.81 95.68 2.32 o -7 7 1 1077.18 1057.72 9.20 o -5 7 1 17090.55 18269.97 113.48 o -3 7 1 666.71 703.07 6.33 o -1 7 1 633.64 685.60 6.20 o 1 7 1 6410.11 6842.54 43.67 o 3 7 1 121.61 169.14 3.01 o 5 7 1 0.00 -0.55 0.55 o 7 7 1 24.37 42.93 1.78 o 9 7 1 797.50 852.07 8.66 o 11 7 1 1194.06 1094.03 11.03 o 13 7 1 1442.12 1356.84 14.85 o 15 7 1 168.60 151.63 6.82 o 17 7 1 135.76 117.96 7.80 o 19 7 1 198.44 175.43 9.62 o 21 7 1 789.85 753.02 20.42 o 23 7 1 707.53 725.07 30.32 o -22 8 1 45.57 47.33 5.95 o -20 8 1 270.93 265.47 9.08 o -18 8 1 668.57 646.56 12.79 o -16 8 1 1758.34 1750.84 23.19 o -14 8 1 515.07 544.60 10.41 o -12 8 1 140.20 155.42 3.95 o -10 8 1 16.43 28.12 1.65 o -8 8 1 409.99 442.75 5.44 o -6 8 1 20.93 34.42 1.59 o -4 8 1 273.85 330.04 4.08 o -2 8 1 189.38 165.58 2.74 o 0 8 1 109.13 110.52 2.36 o 2 8 1 1441.62 1519.00 12.98 o 4 8 1 393.82 442.27 5.49 o 6 8 1 342.84 278.64 4.18 o 8 8 1 719.73 716.51 7.91 o 10 8 1 1628.48 1591.40 14.92 o 12 8 1 3570.25 3480.35 32.66 o 14 8 1 2189.46 2148.03 28.88 o 16 8 1 519.16 514.16 15.12 o 18 8 1 123.81 137.73 9.62 o 20 8 1 27.64 30.62 5.50 o 22 8 1 638.31 677.60 22.71 o -21 9 1 399.04 387.69 13.80 o -19 9 1 439.75 452.21 10.86 o -17 9 1 1128.27 1098.51 19.68 o -15 9 1 3.52 0.44 1.88 o -13 9 1 1450.41 1465.00 19.84 o -11 9 1 3.57 9.71 1.91 o -9 9 1 87.39 83.77 2.70 o -7 9 1 0.11 1.61 0.78 o -5 9 1 336.93 322.64 4.51 o -3 9 1 237.87 241.29 3.65 o -1 9 1 409.40 386.43 4.89 o 1 9 1 321.20 294.73 4.40 o 3 9 1 1865.13 1852.87 16.18 o 5 9 1 26.91 30.92 1.69 o 7 9 1 1963.51 1807.53 15.47 o 9 9 1 3829.89 3813.09 31.05 o 11 9 1 358.00 326.52 6.54 o 13 9 1 2850.80 2654.20 34.02 o 15 9 1 1400.72 1375.92 27.54 o 17 9 1 6.26 2.72 3.42 o 19 9 1 316.33 343.84 13.05 o 21 9 1 752.12 760.99 21.04 o -22 10 1 6.96 12.50 4.12 o -20 10 1 1848.76 1871.48 35.78 o -18 10 1 1141.18 1179.77 24.72 o -16 10 1 244.56 242.73 8.28 o -14 10 1 3751.74 3823.92 45.25 o -12 10 1 2296.51 2314.57 27.15 o -10 10 1 26.32 26.35 2.36 o -8 10 1 451.62 457.80 6.78 o -6 10 1 3959.62 3846.39 28.89 o -4 10 1 392.94 367.23 5.36 o -2 10 1 3044.63 2856.94 22.18 o 0 10 1 135.92 142.11 3.28 o 2 10 1 13562.05 13124.57 99.02 o 4 10 1 387.80 367.23 5.74 o 6 10 1 989.79 987.28 10.74 o 8 10 1 5484.15 5352.45 44.95 o 10 10 1 4545.69 4384.80 44.77 o 12 10 1 32.09 52.67 4.25 o 14 10 1 2877.63 2747.30 45.47 o 16 10 1 1267.14 1245.14 26.69 o 18 10 1 1101.17 1084.87 25.22 o 20 10 1 387.46 388.52 14.60 o -21 11 1 37.02 47.54 5.67 o -19 11 1 8.20 16.19 4.00 o -17 11 1 375.94 356.22 13.32 o -15 11 1 29.08 30.70 4.27 o -13 11 1 255.68 276.10 8.12 o -11 11 1 0.22 1.46 1.63 o -9 11 1 529.89 541.87 9.91 o -7 11 1 2889.70 2940.19 26.77 o -5 11 1 2079.43 2097.09 19.57 o -3 11 1 552.98 529.92 6.96 o -1 11 1 32.02 33.26 1.99 o 1 11 1 460.39 501.69 7.25 o 3 11 1 2788.96 2746.50 24.35 o 5 11 1 1367.18 1386.03 15.49 o 7 11 1 242.76 242.89 5.83 o 9 11 1 89.94 108.74 5.38 o 11 11 1 375.89 407.45 10.73 o 13 11 1 4.51 4.86 2.77 o 15 11 1 770.66 819.04 20.50 o 17 11 1 65.91 66.88 9.07 o 19 11 1 58.05 55.57 6.58 o -18 12 1 104.58 135.16 8.83 o -16 12 1 15.93 21.63 3.74 o -14 12 1 144.06 145.16 6.97 o -12 12 1 67.45 88.88 5.11 o -10 12 1 27.49 35.67 3.48 o -8 12 1 740.66 674.05 11.54 o -6 12 1 1.11 2.96 1.86 o -4 12 1 1722.24 1749.27 19.53 o -2 12 1 162.93 158.58 4.52 o 0 12 1 2232.92 2265.62 22.78 o 2 12 1 164.28 118.82 4.61 o 4 12 1 595.77 493.52 9.99 o 6 12 1 0.57 5.72 1.97 o 8 12 1 240.53 245.48 8.08 o 10 12 1 3.01 4.00 2.72 o 12 12 1 1.98 3.90 2.79 o 14 12 1 318.25 338.70 12.50 o 16 12 1 35.82 51.11 6.13 o 18 12 1 70.67 83.65 12.29 o -17 13 1 35.62 48.35 5.85 o -15 13 1 112.82 124.09 7.46 o -13 13 1 132.76 132.37 6.76 o -11 13 1 1661.55 1694.78 26.64 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