#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:11:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180828 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/59/2015964.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015964_Fobs loop_ _publ_author_name 'Seijas, Luis E.' 'Delgado, Gerzon E.' 'Mora, Asilo\'e J.' 'Bahsas, Ali' 'Brice\~no, Alexander' _publ_section_title ; (2S)-1-Carbamoylpyrrolidine-2-carboxylic acid ; _journal_coeditor_code SK3108 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o303 _journal_page_last o305 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.4711 _cell_length_b 9.7815 _cell_length_c 12.5242 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.7606 _cod_data_source_file sk3108Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AHPRO in p212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 92.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 120.75 131.74 1.68 o 4 0 0 351.29 391.25 8.04 o 6 0 0 3.34 3.24 0.80 o 1 1 0 3445.29 3070.69 13.38 o 2 1 0 34.49 32.60 0.93 o 3 1 0 747.97 816.97 6.43 o 4 1 0 7.37 8.74 0.79 o 5 1 0 29.47 28.62 1.74 o 6 1 0 58.83 60.33 4.84 o 7 1 0 15.85 16.22 1.28 o 0 2 0 79.79 76.25 1.49 o 1 2 0 8521.57 7681.60 32.25 o 2 2 0 1742.02 1750.51 9.11 o 3 2 0 370.97 392.65 4.18 o 4 2 0 99.39 112.05 4.26 o 5 2 0 57.67 62.79 4.29 o 6 2 0 1.57 1.96 0.53 o 7 2 0 15.51 18.35 1.60 o 1 3 0 361.49 297.54 4.55 o 2 3 0 1466.72 1461.63 12.83 o 3 3 0 466.52 507.92 6.33 o 4 3 0 182.15 197.59 4.42 o 5 3 0 27.37 25.73 1.77 o 6 3 0 2.47 0.71 0.48 o 7 3 0 1.90 0.91 0.72 o 0 4 0 315.02 337.46 3.83 o 1 4 0 497.76 525.96 3.96 o 2 4 0 599.81 638.24 6.55 o 3 4 0 19.12 18.95 0.92 o 4 4 0 49.25 52.87 2.92 o 5 4 0 66.12 60.92 2.62 o 6 4 0 49.20 56.13 3.33 o 1 5 0 262.15 232.86 2.70 o 2 5 0 419.33 426.05 5.55 o 3 5 0 180.52 192.27 4.60 o 4 5 0 51.31 65.64 4.68 o 5 5 0 16.33 16.34 1.38 o 6 5 0 0.02 -0.01 0.54 o 0 6 0 220.53 211.98 8.52 o 1 6 0 36.84 35.82 1.35 o 2 6 0 0.98 -0.29 0.46 o 3 6 0 27.15 31.90 1.97 o 4 6 0 1.95 0.96 0.91 o 5 6 0 47.34 44.48 2.82 o 6 6 0 0.53 0.46 0.69 o 1 7 0 124.48 129.79 5.35 o 2 7 0 78.19 75.05 4.93 o 3 7 0 24.35 24.58 1.52 o 4 7 0 27.21 24.89 2.05 o 5 7 0 3.42 3.82 0.85 o 0 8 0 2.27 3.41 0.86 o 1 8 0 0.96 1.88 0.46 o 2 8 0 5.33 4.86 0.61 o 3 8 0 2.11 1.93 0.76 o 4 8 0 7.36 6.31 0.97 o 5 8 0 5.18 7.08 1.55 o 1 9 0 0.00 0.88 0.44 o 2 9 0 37.76 41.87 2.46 o 3 9 0 4.72 3.28 0.81 o 4 9 0 1.85 2.71 0.60 o 0 10 0 3.18 5.50 1.46 o 1 10 0 0.27 0.97 0.74 o 2 10 0 2.60 2.57 0.77 o 3 10 0 0.32 -0.41 0.64 o 1 11 0 3.91 3.20 0.74 o 1 0 1 57.31 45.24 0.40 o 2 0 1 1091.43 1015.62 3.32 o 3 0 1 74.12 76.50 1.26 o 4 0 1 12.95 14.84 0.57 o 5 0 1 21.36 23.11 1.74 o 6 0 1 1.04 0.85 0.52 o 7 0 1 2.84 1.28 0.75 o 0 1 1 3.20 8.69 0.52 o 1 1 1 1715.91 1588.02 4.90 o 2 1 1 192.68 191.83 1.21 o 3 1 1 652.01 644.13 3.58 o 4 1 1 79.48 69.84 1.59 o 5 1 1 5.69 4.30 0.28 o 6 1 1 17.06 17.51 1.04 o 7 1 1 9.24 7.73 0.69 o 0 2 1 321.97 270.84 1.37 o 1 2 1 1060.76 959.66 10.63 o 2 2 1 874.78 829.28 3.30 o 3 2 1 119.30 119.59 1.13 o 4 2 1 18.28 16.63 0.59 o 5 2 1 0.96 1.46 0.19 o 6 2 1 10.78 9.25 0.73 o 7 2 1 10.43 10.33 0.72 o 0 3 1 20.58 22.05 0.78 o 1 3 1 3090.55 2949.60 7.28 o 2 3 1 135.54 136.82 1.11 o 3 3 1 5.16 6.65 0.35 o 4 3 1 17.51 17.96 0.56 o 5 3 1 26.01 30.99 1.46 o 6 3 1 38.60 35.99 1.72 o 7 3 1 2.74 2.60 0.51 o 0 4 1 844.12 844.59 5.65 o 1 4 1 87.04 85.92 1.41 o 2 4 1 406.91 419.85 3.19 o 3 4 1 7.85 5.29 0.22 o 4 4 1 67.86 76.22 2.88 o 5 4 1 21.90 23.57 1.06 o 6 4 1 3.17 2.78 0.40 o 7 4 1 1.37 0.70 1.26 o 0 5 1 1.00 1.57 0.24 o 1 5 1 251.44 254.15 2.15 o 2 5 1 341.06 333.32 3.11 o 3 5 1 1.90 1.88 0.21 o 4 5 1 91.91 93.61 3.91 o 5 5 1 6.40 6.87 0.49 o 6 5 1 4.84 4.04 0.57 o 0 6 1 0.11 0.51 0.28 o 1 6 1 119.30 116.12 2.49 o 2 6 1 92.58 92.92 2.21 o 3 6 1 231.21 275.30 8.73 o 4 6 1 58.99 66.94 3.10 o 5 6 1 5.16 4.70 0.45 o 6 6 1 2.06 2.82 0.48 o 0 7 1 9.87 11.32 0.59 o 1 7 1 29.96 33.08 1.36 o 2 7 1 13.78 13.14 0.73 o 3 7 1 36.25 35.30 1.47 o 4 7 1 2.04 1.44 0.50 o 5 7 1 1.92 1.06 0.79 o 0 8 1 4.92 5.12 0.57 o 1 8 1 30.58 28.03 1.19 o 2 8 1 1.82 1.22 0.34 o 3 8 1 5.73 7.48 0.58 o 4 8 1 7.49 7.05 0.70 o 5 8 1 5.38 5.32 0.49 o 0 9 1 19.12 20.89 1.68 o 1 9 1 0.45 0.36 0.36 o 2 9 1 32.41 38.97 1.74 o 3 9 1 7.71 4.62 0.67 o 4 9 1 3.87 4.20 0.43 o 0 10 1 10.15 10.21 1.13 o 1 10 1 17.04 17.93 1.00 o 2 10 1 10.99 14.33 0.85 o 3 10 1 12.92 13.67 0.85 o 0 11 1 1.53 0.41 0.95 o 1 11 1 5.38 6.03 0.63 o 0 0 2 3562.63 3291.67 16.09 o 1 0 2 121.89 91.68 0.72 o 2 0 2 803.14 676.82 2.90 o 3 0 2 230.55 228.35 2.25 o 4 0 2 34.32 32.11 1.18 o 5 0 2 26.26 31.47 2.25 o 6 0 2 0.21 0.13 0.69 o 7 0 2 24.55 24.25 2.08 o 0 1 2 6560.83 5734.82 11.35 o 1 1 2 715.21 690.23 1.86 o 2 1 2 16.05 12.63 0.38 o 3 1 2 200.77 191.93 1.47 o 4 1 2 199.07 206.16 2.17 o 5 1 2 138.83 151.66 5.41 o 6 1 2 21.64 21.91 1.23 o 7 1 2 3.78 4.08 0.57 o 0 2 2 358.81 330.32 1.17 o 1 2 2 1585.83 1484.07 4.27 o 2 2 2 463.73 444.40 2.32 o 3 2 2 58.99 50.90 1.08 o 4 2 2 33.00 34.15 1.01 o 5 2 2 0.56 0.61 0.23 o 6 2 2 18.50 21.98 0.92 o 7 2 2 7.47 6.68 0.55 o 0 3 2 135.75 150.66 0.82 o 1 3 2 1181.09 1075.18 3.19 o 2 3 2 751.28 797.20 4.07 o 3 3 2 505.04 547.45 4.98 o 4 3 2 44.09 41.11 1.18 o 5 3 2 24.88 27.42 1.13 o 6 3 2 18.07 18.06 1.12 o 7 3 2 0.92 2.00 0.65 o 0 4 2 269.47 236.87 3.46 o 1 4 2 384.93 359.95 1.98 o 2 4 2 381.36 402.20 3.06 o 3 4 2 56.40 52.48 1.55 o 4 4 2 4.91 3.46 0.26 o 5 4 2 127.44 137.39 6.59 o 6 4 2 5.09 3.08 0.51 o 7 4 2 1.29 0.30 0.82 o 0 5 2 124.26 115.83 1.57 o 1 5 2 48.68 41.71 0.86 o 2 5 2 51.66 51.36 1.31 o 3 5 2 137.75 137.79 2.68 o 4 5 2 52.82 55.26 2.49 o 5 5 2 3.68 3.60 0.46 o 6 5 2 8.09 8.10 0.61 o 0 6 2 377.71 397.16 5.70 o 1 6 2 66.27 66.92 1.78 o 2 6 2 50.86 45.64 1.28 o 3 6 2 25.55 24.95 1.25 o 4 6 2 17.20 19.00 1.05 o 5 6 2 1.98 1.96 0.60 o 6 6 2 9.85 9.56 0.79 o 0 7 2 147.75 146.36 7.10 o 1 7 2 88.01 97.43 3.22 o 2 7 2 38.20 41.64 1.91 o 3 7 2 83.63 87.46 3.29 o 4 7 2 19.95 16.45 1.17 o 5 7 2 10.53 8.46 0.54 o 0 8 2 73.75 85.89 4.74 o 1 8 2 26.86 30.78 1.18 o 2 8 2 11.35 14.65 0.81 o 3 8 2 1.88 1.63 0.42 o 4 8 2 5.03 7.80 0.67 o 5 8 2 0.50 1.25 0.48 o 0 9 2 6.78 9.44 0.88 o 1 9 2 6.09 6.64 0.47 o 2 9 2 66.86 71.54 3.18 o 3 9 2 5.56 8.33 0.71 o 4 9 2 1.33 0.41 0.48 o 0 10 2 0.05 0.18 0.53 o 1 10 2 24.61 25.47 1.28 o 2 10 2 3.33 3.96 0.56 o 3 10 2 0.95 1.45 0.57 o 0 11 2 0.90 -0.13 0.73 o 1 11 2 4.56 3.56 0.50 o 1 0 3 217.38 226.95 0.82 o 2 0 3 916.08 838.76 5.01 o 3 0 3 50.50 44.31 1.04 o 4 0 3 192.78 187.33 3.73 o 5 0 3 0.54 1.00 0.33 o 6 0 3 3.74 4.38 0.64 o 7 0 3 0.77 1.13 0.65 o 0 1 3 11.82 10.72 0.37 o 1 1 3 522.39 421.27 0.97 o 2 1 3 60.44 68.52 0.49 o 3 1 3 86.88 84.48 0.82 o 4 1 3 76.12 74.40 1.77 o 5 1 3 1.92 2.10 0.20 o 6 1 3 2.56 2.16 0.26 o 7 1 3 2.20 2.71 0.51 o 0 2 3 63.78 52.92 0.49 o 1 2 3 447.60 404.31 1.55 o 2 2 3 361.09 375.09 1.93 o 3 2 3 21.16 15.93 0.48 o 4 2 3 286.25 303.17 3.59 o 5 2 3 19.30 19.53 0.84 o 6 2 3 3.64 3.14 0.64 o 7 2 3 1.42 1.57 0.69 o 0 3 3 9.44 11.20 0.49 o 1 3 3 104.74 93.15 0.75 o 2 3 3 527.93 519.59 3.59 o 3 3 3 32.26 37.05 1.06 o 4 3 3 36.96 36.96 1.04 o 5 3 3 18.24 20.68 0.84 o 6 3 3 20.26 20.50 1.03 o 7 3 3 0.57 0.44 0.66 o 0 4 3 99.59 121.17 1.12 o 1 4 3 309.82 337.94 2.49 o 2 4 3 70.30 66.67 1.34 o 3 4 3 68.23 66.79 2.02 o 4 4 3 0.23 -0.20 0.23 o 5 4 3 10.47 10.29 0.54 o 6 4 3 27.23 30.08 1.45 o 7 4 3 1.99 2.01 0.97 o 0 5 3 106.60 104.30 1.65 o 1 5 3 72.97 73.91 1.35 o 2 5 3 31.95 33.03 0.84 o 3 5 3 97.03 99.37 2.22 o 4 5 3 16.58 15.21 0.74 o 5 5 3 23.25 25.95 1.07 o 6 5 3 0.26 1.48 0.68 o 0 6 3 83.07 90.63 3.52 o 1 6 3 115.95 117.50 2.03 o 2 6 3 133.74 137.62 3.26 o 3 6 3 15.25 16.83 0.80 o 4 6 3 100.41 113.60 5.20 o 5 6 3 11.77 17.35 0.86 o 6 6 3 2.01 1.75 0.56 o 0 7 3 83.97 80.32 2.97 o 1 7 3 29.75 27.91 0.97 o 2 7 3 2.21 2.51 0.47 o 3 7 3 119.54 127.08 5.75 o 4 7 3 26.07 25.69 1.22 o 5 7 3 4.07 4.05 0.59 o 0 8 3 6.91 8.65 0.97 o 1 8 3 9.66 11.38 0.58 o 2 8 3 14.03 13.11 0.73 o 3 8 3 65.86 59.13 2.45 o 4 8 3 0.79 0.55 0.61 o 5 8 3 11.94 11.04 1.00 o 0 9 3 12.13 12.14 0.83 o 1 9 3 9.59 10.15 0.51 o 2 9 3 15.69 20.22 0.94 o 3 9 3 9.88 11.01 0.62 o 4 9 3 12.57 10.44 0.98 o 0 10 3 5.80 3.84 0.86 o 1 10 3 5.28 5.75 0.51 o 2 10 3 25.26 22.79 1.26 o 3 10 3 0.38 0.42 0.57 o 0 11 3 0.06 -0.78 0.82 o 1 11 3 2.03 2.52 0.58 o 0 0 4 273.52 232.87 2.19 o 1 0 4 76.55 80.79 0.66 o 2 0 4 963.50 978.35 5.54 o 3 0 4 0.59 0.14 0.20 o 4 0 4 6.11 6.47 0.29 o 5 0 4 27.71 33.05 1.98 o 6 0 4 84.24 95.22 5.88 o 7 0 4 2.93 2.64 0.64 o 0 1 4 21.22 21.73 0.35 o 1 1 4 462.48 417.68 0.90 o 2 1 4 131.22 119.48 0.70 o 3 1 4 428.03 459.47 3.49 o 4 1 4 103.59 113.37 1.86 o 5 1 4 147.34 169.49 4.42 o 6 1 4 7.30 7.66 0.73 o 7 1 4 12.30 9.28 0.71 o 0 2 4 134.58 154.30 1.03 o 1 2 4 233.15 263.95 1.21 o 2 2 4 266.47 304.11 1.95 o 3 2 4 25.55 22.43 0.63 o 4 2 4 13.47 11.70 0.35 o 5 2 4 9.44 9.14 0.41 o 6 2 4 56.76 60.77 2.50 o 7 2 4 18.31 18.33 1.88 o 0 3 4 373.72 314.34 2.19 o 1 3 4 167.15 159.35 1.01 o 2 3 4 308.41 300.26 2.14 o 3 3 4 303.79 318.36 3.15 o 4 3 4 80.89 76.02 1.85 o 5 3 4 68.17 71.22 3.29 o 6 3 4 5.35 8.23 0.59 o 7 3 4 1.78 1.43 0.52 o 0 4 4 185.58 238.50 2.25 o 1 4 4 311.10 328.53 2.33 o 2 4 4 178.55 177.48 1.62 o 3 4 4 54.42 60.41 1.61 o 4 4 4 9.04 12.93 0.57 o 5 4 4 79.73 89.66 3.81 o 6 4 4 3.47 3.18 0.63 o 7 4 4 6.79 7.02 1.84 o 0 5 4 96.13 92.45 1.53 o 1 5 4 87.80 90.90 1.52 o 2 5 4 10.16 10.09 0.32 o 3 5 4 40.73 39.26 1.16 o 4 5 4 165.08 184.93 3.99 o 5 5 4 16.61 20.52 0.99 o 6 5 4 0.51 1.43 0.65 o 0 6 4 72.08 65.58 2.35 o 1 6 4 97.32 101.22 2.03 o 2 6 4 52.57 55.35 1.62 o 3 6 4 20.01 16.96 0.72 o 4 6 4 23.66 21.27 1.14 o 5 6 4 5.20 5.30 0.63 o 6 6 4 3.77 3.48 0.50 o 0 7 4 13.44 12.96 0.63 o 1 7 4 9.27 8.32 0.38 o 2 7 4 41.72 43.90 1.72 o 3 7 4 50.35 49.64 2.32 o 4 7 4 4.56 3.77 0.44 o 5 7 4 3.67 4.87 0.62 o 0 8 4 86.82 90.39 3.84 o 1 8 4 4.09 4.45 0.45 o 2 8 4 4.41 3.11 0.23 o 3 8 4 17.18 16.62 1.56 o 4 8 4 1.84 0.57 0.50 o 5 8 4 2.81 2.60 0.56 o 0 9 4 14.31 10.47 0.96 o 1 9 4 34.65 35.99 1.53 o 2 9 4 13.86 16.76 0.81 o 3 9 4 0.87 0.37 0.38 o 4 9 4 0.67 1.38 0.49 o 0 10 4 0.45 0.17 0.64 o 1 10 4 8.37 9.35 0.53 o 2 10 4 9.87 10.60 1.14 o 3 10 4 1.88 0.84 0.53 o 0 11 4 1.69 2.52 1.18 o 1 11 4 3.93 1.18 0.70 o 1 0 5 63.16 74.29 0.58 o 2 0 5 126.38 116.55 1.15 o 3 0 5 37.85 37.22 1.33 o 4 0 5 213.48 246.10 5.10 o 5 0 5 6.30 7.51 0.87 o 6 0 5 0.05 0.23 0.35 o 7 0 5 0.76 1.22 0.59 o 0 1 5 1060.20 1062.37 5.29 o 1 1 5 227.26 235.42 0.99 o 2 1 5 115.04 133.74 0.93 o 3 1 5 18.54 15.13 0.41 o 4 1 5 23.60 21.17 0.64 o 5 1 5 20.30 19.82 0.87 o 6 1 5 1.79 1.90 0.29 o 7 1 5 0.70 0.71 0.51 o 0 2 5 23.31 25.69 0.68 o 1 2 5 10.43 10.58 0.28 o 2 2 5 136.72 135.99 1.08 o 3 2 5 47.27 49.92 1.24 o 4 2 5 8.49 8.67 0.28 o 5 2 5 7.62 7.21 0.39 o 6 2 5 4.39 3.94 0.55 o 7 2 5 0.24 0.20 0.59 o 0 3 5 62.21 58.15 0.86 o 1 3 5 107.89 116.01 0.88 o 2 3 5 85.47 99.17 0.98 o 3 3 5 81.10 82.22 1.81 o 4 3 5 52.90 51.19 1.71 o 5 3 5 11.52 12.98 0.65 o 6 3 5 11.81 12.91 0.75 o 7 3 5 3.97 3.29 0.78 o 0 4 5 4.40 5.39 0.31 o 1 4 5 16.65 18.39 0.47 o 2 4 5 102.67 96.52 1.41 o 3 4 5 66.45 67.23 1.80 o 4 4 5 14.17 11.93 0.42 o 5 4 5 9.74 9.06 0.52 o 6 4 5 5.92 6.97 0.77 o 7 4 5 0.10 3.35 2.45 o 0 5 5 53.45 39.87 1.38 o 1 5 5 34.60 36.45 0.99 o 2 5 5 35.10 35.18 0.91 o 3 5 5 18.47 18.16 0.59 o 4 5 5 31.68 35.78 1.75 o 5 5 5 0.07 1.24 0.33 o 6 5 5 2.45 3.25 0.47 o 0 6 5 7.97 8.84 0.43 o 1 6 5 3.39 3.34 0.18 o 2 6 5 3.96 3.21 0.20 o 3 6 5 26.17 24.53 0.94 o 4 6 5 1.56 1.31 0.32 o 5 6 5 1.65 2.24 0.54 o 6 6 5 0.93 1.62 0.73 o 0 7 5 77.19 80.57 3.21 o 1 7 5 36.45 32.15 1.18 o 2 7 5 22.76 23.36 0.84 o 3 7 5 1.85 2.26 0.50 o 4 7 5 8.77 8.13 0.70 o 5 7 5 1.42 1.54 0.41 o 0 8 5 2.29 3.65 1.04 o 1 8 5 6.27 4.65 0.59 o 2 8 5 8.14 9.13 0.46 o 3 8 5 38.65 41.87 1.85 o 4 8 5 6.56 5.78 0.52 o 5 8 5 6.92 6.18 1.02 o 0 9 5 13.64 14.94 0.93 o 1 9 5 14.41 15.75 0.65 o 2 9 5 15.28 14.97 0.75 o 3 9 5 1.68 1.39 0.44 o 4 9 5 14.51 12.82 1.41 o 0 10 5 9.57 9.49 0.83 o 1 10 5 0.32 1.27 0.67 o 2 10 5 7.30 7.92 0.71 o 3 10 5 1.54 2.50 0.69 o 0 11 5 2.77 2.32 1.16 o 1 11 5 0.10 0.67 0.86 o 0 0 6 9.20 11.85 0.89 o 1 0 6 49.78 45.94 0.64 o 2 0 6 422.29 448.63 4.33 o 3 0 6 32.87 37.54 1.33 o 4 0 6 4.56 6.04 0.35 o 5 0 6 81.32 91.76 5.25 o 6 0 6 69.95 74.35 4.35 o 7 0 6 0.22 1.68 0.78 o 0 1 6 159.70 161.65 1.43 o 1 1 6 85.72 76.99 0.57 o 2 1 6 429.24 480.46 3.33 o 3 1 6 136.28 144.40 1.92 o 4 1 6 9.59 8.79 0.32 o 5 1 6 52.44 55.30 2.70 o 6 1 6 40.39 41.67 1.90 o 7 1 6 5.32 5.39 0.73 o 0 2 6 34.62 33.60 0.58 o 1 2 6 730.86 791.69 4.81 o 2 2 6 7.15 7.79 0.21 o 3 2 6 143.91 146.35 1.68 o 4 2 6 49.93 51.53 1.50 o 5 2 6 96.35 102.69 4.25 o 6 2 6 9.76 10.65 0.59 o 7 2 6 17.50 16.10 2.06 o 0 3 6 126.98 137.33 1.47 o 1 3 6 320.35 382.58 2.74 o 2 3 6 55.82 57.28 1.13 o 3 3 6 2.45 2.88 0.16 o 4 3 6 131.30 141.28 3.94 o 5 3 6 13.90 16.00 0.67 o 6 3 6 4.64 4.64 0.58 o 7 3 6 4.11 2.59 0.76 o 0 4 6 330.95 350.86 4.01 o 1 4 6 83.45 79.21 1.17 o 2 4 6 6.20 6.37 0.19 o 3 4 6 37.56 35.15 1.07 o 4 4 6 69.13 61.40 2.76 o 5 4 6 15.12 14.26 0.61 o 6 4 6 4.51 4.54 0.43 o 0 5 6 111.14 127.15 2.22 o 1 5 6 9.59 9.54 0.28 o 2 5 6 1.72 1.77 0.14 o 3 5 6 107.47 99.11 2.82 o 4 5 6 25.06 28.04 1.37 o 5 5 6 1.82 1.26 0.45 o 6 5 6 0.82 0.96 0.43 o 0 6 6 1.50 1.41 0.20 o 1 6 6 119.32 138.30 3.43 o 2 6 6 50.28 46.46 1.26 o 3 6 6 1.99 1.52 0.26 o 4 6 6 7.35 8.28 0.63 o 5 6 6 0.18 0.53 0.46 o 6 6 6 7.00 6.87 1.11 o 0 7 6 8.29 7.05 0.51 o 1 7 6 0.68 0.93 0.20 o 2 7 6 4.28 6.41 0.37 o 3 7 6 7.69 8.30 0.44 o 4 7 6 1.20 1.23 0.40 o 5 7 6 7.17 8.59 0.83 o 0 8 6 43.15 46.77 2.47 o 1 8 6 6.54 7.99 0.49 o 2 8 6 4.84 5.44 0.30 o 3 8 6 5.70 7.48 0.63 o 4 8 6 1.65 1.64 0.42 o 5 8 6 1.45 0.11 0.68 o 0 9 6 0.04 0.50 0.50 o 1 9 6 0.82 0.88 0.29 o 2 9 6 0.64 -0.16 0.54 o 3 9 6 1.74 1.96 0.50 o 4 9 6 0.76 0.85 0.74 o 0 10 6 3.24 1.83 0.74 o 1 10 6 9.11 7.81 0.73 o 2 10 6 4.09 4.13 0.52 o 3 10 6 0.58 2.18 0.86 o 0 11 6 2.53 1.78 1.17 o 1 0 7 110.59 115.43 1.53 o 2 0 7 157.24 167.06 1.91 o 3 0 7 111.88 120.34 1.90 o 4 0 7 1.80 2.42 0.28 o 5 0 7 82.16 85.39 4.54 o 6 0 7 0.05 0.61 0.52 o 7 0 7 0.13 0.82 0.83 o 0 1 7 279.61 284.72 3.26 o 1 1 7 26.55 23.77 0.38 o 2 1 7 101.18 106.21 1.01 o 3 1 7 3.35 3.52 0.14 o 4 1 7 59.25 54.49 1.52 o 5 1 7 1.95 2.69 0.30 o 6 1 7 5.44 3.26 0.54 o 7 1 7 0.88 1.65 0.73 o 0 2 7 48.26 45.19 0.70 o 1 2 7 111.21 112.55 1.10 o 2 2 7 45.41 49.77 0.95 o 3 2 7 21.14 20.42 0.56 o 4 2 7 24.45 22.28 0.66 o 5 2 7 3.99 4.66 0.35 o 6 2 7 2.40 2.53 0.51 o 7 2 7 5.05 2.67 1.07 o 0 3 7 84.73 85.02 1.30 o 1 3 7 28.57 27.86 0.74 o 2 3 7 74.65 78.16 1.31 o 3 3 7 18.26 15.83 0.50 o 4 3 7 20.00 18.89 0.76 o 5 3 7 22.34 21.32 0.88 o 6 3 7 1.61 1.58 0.52 o 7 3 7 1.31 1.42 0.73 o 0 4 7 80.72 82.82 2.00 o 1 4 7 19.99 18.87 0.48 o 2 4 7 5.48 5.87 0.18 o 3 4 7 78.59 69.58 1.86 o 4 4 7 15.61 14.82 0.75 o 5 4 7 2.13 2.23 0.39 o 6 4 7 5.07 5.58 0.55 o 0 5 7 172.30 184.97 3.13 o 1 5 7 65.08 68.80 2.06 o 2 5 7 28.02 28.77 0.82 o 3 5 7 53.44 51.26 1.92 o 4 5 7 10.07 10.06 0.53 o 5 5 7 1.16 0.91 0.39 o 6 5 7 2.66 2.46 0.95 o 0 6 7 1.98 2.52 0.32 o 1 6 7 10.85 10.34 0.39 o 2 6 7 94.31 88.45 3.22 o 3 6 7 3.68 5.32 0.42 o 4 6 7 1.71 2.00 0.37 o 5 6 7 0.66 0.98 0.41 o 6 6 7 1.27 2.02 0.68 o 0 7 7 38.42 34.58 1.93 o 1 7 7 32.72 29.60 1.36 o 2 7 7 15.54 15.51 0.63 o 3 7 7 43.40 41.42 1.78 o 4 7 7 2.15 1.51 0.41 o 5 7 7 4.65 4.85 0.61 o 0 8 7 16.02 17.88 1.01 o 1 8 7 8.50 10.67 0.51 o 2 8 7 29.95 28.31 1.12 o 3 8 7 3.42 4.99 0.55 o 4 8 7 1.52 0.54 0.61 o 5 8 7 0.42 -0.16 0.98 o 0 9 7 0.30 0.88 1.22 o 1 9 7 6.93 7.42 0.72 o 2 9 7 7.42 6.50 0.53 o 3 9 7 2.59 2.65 0.50 o 4 9 7 3.03 1.60 0.78 o 0 10 7 0.49 1.15 0.70 o 1 10 7 3.77 3.62 0.44 o 2 10 7 1.02 0.88 0.50 o 3 10 7 3.54 3.38 2.03 o 0 0 8 28.97 35.30 2.45 o 1 0 8 4.34 5.06 0.27 o 2 0 8 50.53 60.75 1.24 o 3 0 8 18.46 20.82 0.99 o 4 0 8 5.62 5.47 0.36 o 5 0 8 6.57 7.34 0.60 o 6 0 8 1.00 1.23 0.49 o 7 0 8 2.50 2.29 1.18 o 0 1 8 60.90 64.67 2.99 o 1 1 8 222.59 251.59 3.40 o 2 1 8 233.45 253.03 2.48 o 3 1 8 23.29 23.26 0.75 o 4 1 8 53.25 49.22 1.74 o 5 1 8 8.18 7.60 0.39 o 6 1 8 13.33 12.97 0.81 o 7 1 8 0.55 1.00 0.70 o 0 2 8 185.88 167.16 2.96 o 1 2 8 110.19 119.65 1.76 o 2 2 8 16.50 14.58 0.39 o 3 2 8 3.37 3.73 0.15 o 4 2 8 86.55 81.13 2.89 o 5 2 8 15.05 13.97 0.62 o 6 2 8 2.40 2.15 0.39 o 7 2 8 4.29 2.22 0.87 o 0 3 8 31.68 32.05 1.10 o 1 3 8 5.17 5.98 0.17 o 2 3 8 3.09 2.11 0.15 o 3 3 8 33.05 28.79 0.86 o 4 3 8 44.89 42.41 1.85 o 5 3 8 6.66 5.82 0.54 o 6 3 8 12.18 11.80 0.97 o 7 3 8 3.48 3.75 1.23 o 0 4 8 86.81 83.31 2.18 o 1 4 8 41.53 36.26 1.15 o 2 4 8 2.26 2.21 0.19 o 3 4 8 32.75 30.28 1.20 o 4 4 8 13.18 10.58 0.56 o 5 4 8 20.59 21.11 1.06 o 6 4 8 1.78 0.84 0.74 o 0 5 8 43.80 42.07 1.67 o 1 5 8 41.81 40.61 1.10 o 2 5 8 70.74 57.74 1.79 o 3 5 8 29.70 29.91 1.40 o 4 5 8 1.84 2.73 0.40 o 5 5 8 1.04 0.65 0.35 o 6 5 8 2.10 0.91 0.72 o 0 6 8 0.48 1.05 0.23 o 1 6 8 70.97 66.58 2.36 o 2 6 8 33.85 33.28 1.38 o 3 6 8 16.51 11.53 0.66 o 4 6 8 0.44 0.65 0.29 o 5 6 8 3.72 4.07 0.61 o 6 6 8 9.22 8.93 1.33 o 0 7 8 7.28 6.64 0.90 o 1 7 8 15.39 14.63 0.76 o 2 7 8 7.91 8.58 0.44 o 3 7 8 0.74 0.84 0.39 o 4 7 8 2.90 2.83 0.52 o 5 7 8 7.89 6.33 0.76 o 0 8 8 49.75 51.94 2.95 o 1 8 8 9.22 10.07 0.81 o 2 8 8 3.32 5.25 0.44 o 3 8 8 4.71 5.53 0.52 o 4 8 8 2.29 1.28 0.61 o 5 8 8 2.56 1.78 1.66 o 0 9 8 0.03 -0.55 0.73 o 1 9 8 5.55 4.30 0.41 o 2 9 8 1.66 2.57 0.45 o 3 9 8 8.22 7.21 0.79 o 4 9 8 3.06 1.41 1.13 o 0 10 8 6.65 8.74 1.28 o 1 10 8 5.78 4.80 0.65 o 2 10 8 3.33 3.30 0.60 o 3 10 8 0.01 -0.69 1.96 o 1 0 9 45.44 50.15 1.28 o 2 0 9 63.64 68.86 2.16 o 3 0 9 67.00 64.42 2.03 o 4 0 9 4.23 4.49 0.58 o 5 0 9 36.34 36.80 2.46 o 6 0 9 3.54 1.90 0.59 o 7 0 9 3.44 4.35 1.63 o 0 1 9 5.84 5.20 0.39 o 1 1 9 12.46 10.61 0.36 o 2 1 9 18.53 14.99 0.45 o 3 1 9 10.16 9.94 0.30 o 4 1 9 3.91 3.59 0.21 o 5 1 9 5.41 3.93 0.49 o 6 1 9 0.72 0.77 0.54 o 7 1 9 0.79 2.48 1.54 o 0 2 9 0.20 0.56 0.16 o 1 2 9 35.10 36.98 0.77 o 2 2 9 8.22 8.48 0.27 o 3 2 9 100.08 110.91 1.90 o 4 2 9 23.86 22.22 0.74 o 5 2 9 10.09 9.17 0.47 o 6 2 9 1.09 1.23 0.55 o 7 2 9 1.75 0.85 1.46 o 0 3 9 17.53 16.06 0.70 o 1 3 9 9.54 8.62 0.29 o 2 3 9 6.29 5.36 0.18 o 3 3 9 20.83 20.37 0.77 o 4 3 9 0.95 1.57 0.27 o 5 3 9 2.67 2.33 0.42 o 6 3 9 0.22 0.94 0.44 o 0 4 9 137.16 163.75 3.06 o 1 4 9 64.25 73.08 1.43 o 2 4 9 45.41 41.74 1.56 o 3 4 9 80.88 76.38 3.13 o 4 4 9 13.92 15.53 0.77 o 5 4 9 10.19 9.73 0.55 o 6 4 9 0.04 0.57 0.50 o 0 5 9 5.04 4.77 0.38 o 1 5 9 41.33 41.31 1.41 o 2 5 9 45.42 41.17 1.48 o 3 5 9 14.91 15.33 0.77 o 4 5 9 8.92 8.57 0.48 o 5 5 9 4.69 5.89 0.51 o 6 5 9 1.27 0.60 0.89 o 0 6 9 5.83 7.20 0.61 o 1 6 9 23.43 21.73 0.90 o 2 6 9 20.83 18.78 0.84 o 3 6 9 4.52 4.69 0.63 o 4 6 9 4.65 5.04 0.44 o 5 6 9 5.56 6.62 0.85 o 0 7 9 14.31 13.11 0.66 o 1 7 9 7.70 8.88 0.49 o 2 7 9 35.15 35.38 1.62 o 3 7 9 0.42 0.19 0.34 o 4 7 9 1.92 1.80 0.51 o 5 7 9 0.88 0.33 0.64 o 0 8 9 0.09 0.09 0.47 o 1 8 9 23.72 19.01 1.26 o 2 8 9 8.67 8.01 0.49 o 3 8 9 11.42 9.91 1.02 o 4 8 9 2.15 1.91 0.54 o 0 9 9 0.56 0.99 0.61 o 1 9 9 0.97 0.51 0.48 o 2 9 9 14.14 11.84 1.17 o 3 9 9 6.77 5.63 0.80 o 0 10 9 13.10 9.73 1.42 o 1 10 9 0.81 0.71 0.48 o 2 10 9 0.10 0.31 0.69 o 0 0 10 299.11 373.90 13.22 o 1 0 10 3.28 1.75 0.54 o 2 0 10 2.60 2.05 0.21 o 3 0 10 98.61 101.96 4.03 o 4 0 10 1.39 1.13 0.35 o 5 0 10 0.43 0.22 0.73 o 6 0 10 1.12 0.83 1.68 o 0 1 10 24.40 24.68 1.25 o 1 1 10 87.15 90.66 2.45 o 2 1 10 96.82 102.47 1.57 o 3 1 10 21.97 17.99 0.67 o 4 1 10 28.30 28.89 0.95 o 5 1 10 1.29 1.96 0.36 o 6 1 10 4.50 3.71 0.71 o 0 2 10 92.00 98.97 4.94 o 1 2 10 211.33 234.19 3.45 o 2 2 10 11.46 10.63 0.40 o 3 2 10 3.43 3.02 0.24 o 4 2 10 25.79 24.23 0.92 o 5 2 10 2.96 3.08 0.41 o 6 2 10 4.58 4.21 0.75 o 0 3 10 233.10 247.89 4.97 o 1 3 10 10.46 9.90 0.29 o 2 3 10 2.06 1.48 0.13 o 3 3 10 19.25 18.61 0.78 o 4 3 10 30.24 30.20 1.45 o 5 3 10 1.04 0.54 0.42 o 6 3 10 1.45 1.94 0.67 o 0 4 10 1.33 1.34 0.22 o 1 4 10 28.78 25.59 0.90 o 2 4 10 28.77 27.73 0.89 o 3 4 10 6.70 4.59 0.42 o 4 4 10 2.76 1.84 0.36 o 5 4 10 2.28 2.11 0.64 o 6 4 10 4.56 4.22 0.83 o 0 5 10 1.82 1.81 0.27 o 1 5 10 59.42 65.16 2.00 o 2 5 10 67.45 60.96 2.05 o 3 5 10 11.82 12.36 0.60 o 4 5 10 6.46 6.33 0.44 o 5 5 10 5.44 4.41 0.76 o 0 6 10 0.00 0.00 0.30 o 1 6 10 8.27 7.46 0.32 o 2 6 10 4.02 2.13 0.34 o 3 6 10 6.17 6.34 0.38 o 4 6 10 11.73 11.51 1.21 o 5 6 10 3.74 4.14 0.98 o 0 7 10 0.18 -0.36 0.49 o 1 7 10 16.79 16.30 0.66 o 2 7 10 18.24 18.38 1.18 o 3 7 10 0.37 1.03 0.34 o 4 7 10 4.51 3.75 0.73 o 0 8 10 11.42 9.10 1.16 o 1 8 10 0.78 1.11 0.35 o 2 8 10 2.13 2.05 0.55 o 3 8 10 5.43 5.26 1.02 o 4 8 10 1.34 0.02 1.04 o 0 9 10 0.75 1.30 0.70 o 1 9 10 0.63 1.25 0.48 o 2 9 10 0.18 1.22 0.90 o 3 9 10 2.15 3.07 1.06 o 0 10 10 0.40 -1.28 1.90 o 1 10 10 0.18 -0.15 1.10 o 1 0 11 32.64 34.98 2.04 o 2 0 11 3.00 1.97 0.42 o 3 0 11 13.54 16.84 1.07 o 4 0 11 1.39 0.40 0.39 o 5 0 11 8.39 7.69 1.38 o 6 0 11 3.17 2.36 1.42 o 0 1 11 100.89 104.44 5.76 o 1 1 11 25.94 27.10 1.19 o 2 1 11 128.65 150.47 2.29 o 3 1 11 20.98 22.76 0.86 o 4 1 11 13.17 11.99 0.56 o 5 1 11 0.24 0.47 0.68 o 6 1 11 1.13 2.17 1.01 o 0 2 11 31.19 34.25 2.40 o 1 2 11 55.40 60.57 2.23 o 2 2 11 13.92 15.51 0.55 o 3 2 11 21.49 21.31 0.92 o 4 2 11 4.93 4.05 0.54 o 5 2 11 1.27 0.45 0.59 o 6 2 11 4.50 0.82 1.20 o 0 3 11 48.05 44.73 2.32 o 1 3 11 14.91 15.44 0.64 o 2 3 11 16.47 17.36 0.83 o 3 3 11 33.55 34.80 1.75 o 4 3 11 3.89 3.91 0.50 o 5 3 11 7.88 5.89 0.90 o 6 3 11 1.67 2.38 1.64 o 0 4 11 70.02 78.61 2.88 o 1 4 11 12.70 12.98 0.62 o 2 4 11 1.94 1.78 0.52 o 3 4 11 9.21 7.93 0.57 o 4 4 11 1.22 0.91 0.52 o 5 4 11 3.39 4.07 1.37 o 0 5 11 17.40 18.15 0.99 o 1 5 11 11.05 12.89 0.61 o 2 5 11 12.45 11.67 0.70 o 3 5 11 0.07 0.67 0.35 o 4 5 11 0.09 1.45 0.63 o 5 5 11 0.77 2.37 1.47 o 0 6 11 0.72 1.92 0.56 o 1 6 11 14.82 15.42 0.82 o 2 6 11 3.30 2.32 0.56 o 3 6 11 2.40 1.56 0.59 o 4 6 11 2.10 1.00 0.62 o 0 7 11 0.91 2.17 0.80 o 1 7 11 4.80 4.39 0.54 o 2 7 11 0.50 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