#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015990.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2015990_Fobs
loop_
_publ_author_name
'Angle, Christina S.'
'Woolard, Kathryn J.'
'Kahn, Michael I.'
'Golen, James A.'
'Rheingold, Arnold L.'
'Doerrer, Linda H.'
_publ_section_title
;
 Metallophilic interactions in
 iodido(2,2':6',2''-terpyridine)platinum(II) diiodidoaurate(I)
;
_journal_coeditor_code           GG3082
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m231
_journal_page_last               m234
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                84.085
_cell_angle_beta                 82.476
_cell_angle_gamma                87.554
_cell_length_a                   8.7124
_cell_length_b                   9.0668
_cell_length_c                   11.9860
_exptl_crystal_F_000             876.00
_reflns_d_resolution_high        0.7511
_[local]_cod_data_source_file    gg3082Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' lhda38 in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            654.42
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 59618.68 55317.26 1430.87 o
2 0 0 6974.81 7467.55 153.48 o
3 0 0 1958.33 2055.94 59.46 o
4 0 0 51816.39 53541.26 1239.23 o
5 0 0 38564.64 39585.95 638.08 o
6 0 0 350.66 391.78 24.48 o
7 0 0 10758.86 11201.91 247.95 o
8 0 0 7930.81 7818.90 309.60 o
9 0 0 5383.75 5439.40 401.61 o
10 0 0 4028.79 4002.04 307.42 o
-10 1 0 123.84 225.24 56.26 o
-9 1 0 23778.90 25567.36 1165.08 o
-8 1 0 52780.69 55015.36 1183.64 o
-7 1 0 6983.09 7210.16 328.14 o
-6 1 0 1576.43 1613.36 63.82 o
-5 1 0 1268.68 1299.63 57.68 o
-4 1 0 62460.88 62757.73 1892.98 o
-3 1 0 8162.60 8679.66 306.26 o
-2 1 0 553.84 653.95 31.80 o
-1 1 0 43517.76 44882.22 599.64 o
0 1 0 148.18 187.56 10.49 o
1 1 0 21460.98 21714.35 332.70 o
2 1 0 363.94 466.20 20.01 o
3 1 0 39312.59 39404.75 613.76 o
4 1 0 31292.39 31643.34 688.32 o
5 1 0 25640.66 25826.84 446.46 o
6 1 0 4588.00 4602.43 127.14 o
7 1 0 2712.69 2840.17 124.34 o
8 1 0 731.88 736.02 52.73 o
9 1 0 2949.92 2914.51 175.16 o
10 1 0 2888.84 2922.78 177.62 o
-10 2 0 3334.03 3076.80 180.40 o
-9 2 0 2374.29 2318.09 147.88 o
-8 2 0 435.94 495.51 42.11 o
-7 2 0 2645.88 2731.82 132.43 o
-6 2 0 6383.67 6050.95 180.22 o
-5 2 0 25293.60 25909.99 575.28 o
-4 2 0 63.94 98.31 14.28 o
-3 2 0 26722.25 27656.35 437.37 o
-2 2 0 1924.32 1884.04 42.85 o
-1 2 0 8438.75 9497.72 163.96 o
0 2 0 22.35 87.35 10.36 o
1 2 0 46903.96 45372.37 1812.63 o
2 2 0 1087.73 1130.45 37.32 o
3 2 0 55084.97 53928.64 824.67 o
4 2 0 1682.48 1770.09 59.06 o
5 2 0 2311.08 2313.49 76.94 o
6 2 0 30303.13 29345.56 1397.43 o
7 2 0 291.34 288.05 27.83 o
8 2 0 5.71 48.31 13.47 o
9 2 0 795.31 855.55 61.45 o
10 2 0 21289.37 22414.49 1344.56 o
-10 3 0 556.66 542.74 49.18 o
-9 3 0 2657.95 2515.79 120.63 o
-8 3 0 6811.69 6611.85 216.15 o
-7 3 0 2422.18 2358.36 104.59 o
-6 3 0 2471.02 2465.52 102.02 o
-5 3 0 8551.75 8491.90 226.22 o
-4 3 0 1167.87 1037.92 40.74 o
-3 3 0 16000.81 15967.85 244.63 o
-2 3 0 15374.12 16441.85 246.66 o
-1 3 0 59.03 94.53 9.73 o
0 3 0 8741.85 8642.07 320.51 o
1 3 0 8499.62 8171.16 227.88 o
2 3 0 171056.22 152116.47 2321.95 o
3 3 0 59681.25 61319.09 936.29 o
4 3 0 7399.38 7451.54 163.27 o
5 3 0 2381.32 2203.76 74.62 o
6 3 0 37494.28 38906.41 794.87 o
7 3 0 32241.61 34167.89 736.94 o
8 3 0 583.42 781.27 56.65 o
9 3 0 8609.73 8699.54 291.54 o
10 3 0 2960.77 3195.26 156.56 o
-10 4 0 4937.66 4768.49 227.64 o
-9 4 0 4011.37 3744.53 155.90 o
-8 4 0 259.55 311.57 42.65 o
-7 4 0 9793.96 9653.52 267.54 o
-6 4 0 39648.54 39808.44 774.95 o
-5 4 0 51408.50 50012.25 925.77 o
-4 4 0 11320.13 11190.65 526.11 o
-3 4 0 6928.88 7159.18 179.24 o
-2 4 0 46506.16 49211.84 760.52 o
-1 4 0 26319.12 28639.30 529.13 o
0 4 0 11377.43 11159.06 208.52 o
1 4 0 31710.88 30414.25 755.38 o
2 4 0 941.17 924.58 39.55 o
3 4 0 5276.61 5448.00 129.92 o
4 4 0 2515.89 2590.95 81.22 o
5 4 0 40163.70 39656.52 926.03 o
6 4 0 24569.78 25010.61 614.11 o
7 4 0 4137.58 4263.27 178.75 o
8 4 0 2124.12 2262.05 124.16 o
9 4 0 493.46 532.01 41.92 o
10 4 0 5746.01 6082.14 240.36 o
-10 5 0 2177.80 2286.61 189.10 o
-9 5 0 15638.79 15114.06 602.77 o
-8 5 0 5604.38 5267.54 189.95 o
-7 5 0 872.63 872.41 55.95 o
-6 5 0 3881.59 3558.69 135.32 o
-5 5 0 3006.81 2998.00 115.14 o
-4 5 0 24283.67 24365.56 498.35 o
-3 5 0 22995.00 23067.10 456.90 o
-2 5 0 14274.76 15380.77 324.52 o
-1 5 0 41.91 63.38 7.38 o
0 5 0 9839.61 10039.51 344.29 o
1 5 0 8492.68 8227.68 233.91 o
2 5 0 867.51 905.22 50.19 o
3 5 0 5041.57 4946.51 128.63 o
4 5 0 447.74 577.21 71.72 o
5 5 0 6231.53 6194.54 209.20 o
6 5 0 235.86 258.79 23.80 o
7 5 0 616.81 679.45 50.48 o
8 5 0 2917.04 3214.83 158.97 o
9 5 0 562.86 583.96 42.29 o
10 5 0 391.75 336.77 30.11 o
-9 6 0 620.18 622.00 55.29 o
-8 6 0 8063.63 7431.13 245.34 o
-7 6 0 333.74 353.55 28.48 o
-6 6 0 1438.85 1398.14 77.29 o
-5 6 0 0.16 35.80 10.08 o
-4 6 0 1231.64 1235.15 87.32 o
-3 6 0 1527.47 1694.90 102.87 o
-2 6 0 10809.37 11033.28 260.16 o
-1 6 0 1111.26 1240.44 103.40 o
0 6 0 1440.11 1695.05 119.01 o
1 6 0 2812.21 2823.23 100.21 o
2 6 0 1794.14 1597.04 71.02 o
3 6 0 622.46 680.96 40.03 o
4 6 0 18007.05 17992.86 422.76 o
5 6 0 16045.06 16912.21 445.62 o
6 6 0 9960.65 10016.88 365.46 o
7 6 0 2013.34 2151.79 120.69 o
8 6 0 6625.65 7190.73 272.88 o
9 6 0 9759.22 10982.04 773.82 o
-8 7 0 4549.48 4501.55 231.39 o
-7 7 0 3746.66 3797.16 203.68 o
-6 7 0 1830.69 1611.96 113.84 o
-5 7 0 118.58 565.48 73.68 o
-4 7 0 10977.37 10706.21 363.16 o
-3 7 0 55238.19 57373.68 2297.50 o
-2 7 0 5854.57 6138.58 240.36 o
-1 7 0 3122.76 3263.49 115.99 o
0 7 0 7718.49 7635.37 204.75 o
1 7 0 33737.53 33313.86 648.00 o
2 7 0 24277.19 23703.75 489.37 o
3 7 0 2608.02 2646.09 129.73 o
4 7 0 2443.42 2389.23 131.46 o
5 7 0 113.81 178.42 21.55 o
6 7 0 5901.28 5870.03 397.07 o
7 7 0 14703.65 15659.62 530.96 o
8 7 0 12587.91 13109.21 489.09 o
9 7 0 856.23 1160.73 115.42 o
-8 8 0 2621.85 1843.08 172.77 o
-7 8 0 24324.71 23322.42 712.16 o
-6 8 0 5032.01 4739.21 233.85 o
-5 8 0 925.54 890.84 77.76 o
-4 8 0 11355.66 11324.34 538.26 o
-3 8 0 854.74 909.44 74.85 o
-2 8 0 18545.32 19559.21 562.61 o
-1 8 0 7288.87 7529.19 279.30 o
0 8 0 25872.62 26205.23 544.11 o
1 8 0 8208.02 8392.73 229.63 o
2 8 0 11513.04 11327.21 330.52 o
3 8 0 8853.16 8679.04 291.99 o
4 8 0 2474.70 2328.92 130.89 o
5 8 0 1274.47 1498.32 178.39 o
6 8 0 84.73 110.63 18.59 o
7 8 0 233.27 181.11 40.65 o
-7 9 0 163.69 137.92 35.21 o
-6 9 0 8714.52 8207.56 344.56 o
-5 9 0 459.72 614.40 71.68 o
-4 9 0 2175.79 2511.76 214.14 o
-3 9 0 3382.99 3516.10 205.25 o
-2 9 0 3764.55 3913.03 194.02 o
-1 9 0 42.59 74.71 13.89 o
0 9 0 5184.38 5433.20 230.33 o
1 9 0 903.26 1053.46 77.29 o
2 9 0 40.68 77.21 12.82 o
3 9 0 1762.02 1798.07 116.87 o
4 9 0 276.78 283.83 27.95 o
5 9 0 257.29 286.73 38.47 o
6 9 0 315.69 505.96 64.97 o
-4 10 0 602.76 679.81 93.28 o
-3 10 0 2026.47 2294.59 247.90 o
-2 10 0 681.20 775.63 96.55 o
-1 10 0 23927.41 26688.70 1200.65 o
0 10 0 2149.72 2309.11 222.49 o
2 10 0 10.86 76.58 21.78 o
3 10 0 17023.98 16145.26 689.25 o
4 10 0 12972.13 12707.00 598.51 o
5 10 0 477.53 472.20 60.98 o
-3 11 0 1164.09 961.46 116.51 o
-2 11 0 6669.52 7760.31 539.71 o
-1 11 0 489.83 783.62 92.19 o
3 11 0 10119.12 9269.47 470.02 o
4 11 0 2632.53 2509.82 198.17 o
-4 -11 1 3818.37 3750.04 259.15 o
-3 -11 1 4573.29 4420.05 286.73 o
0 -11 1 3869.68 4415.33 344.44 o
1 -11 1 11620.67 12205.04 717.20 o
2 -11 1 1671.99 1673.94 179.66 o
3 -11 1 84.82 -1.81 42.10 o
-5 -10 1 237.50 181.84 33.39 o
-4 -10 1 2736.67 2640.12 207.25 o
-3 -10 1 485.81 508.13 55.89 o
-2 -10 1 74.58 117.23 22.87 o
-1 -10 1 98.30 105.62 31.21 o
1 -10 1 338.85 341.54 49.00 o
2 -10 1 234.95 560.76 86.38 o
3 -10 1 723.46 950.21 126.67 o
4 -10 1 42.46 98.36 35.93 o
-6 -9 1 208.19 289.27 42.83 o
-5 -9 1 72.72 117.60 25.77 o
-4 -9 1 3793.69 3504.68 247.17 o
-3 -9 1 5307.82 5073.73 304.16 o
-2 -9 1 2172.65 2071.74 160.79 o
-1 -9 1 67.21 110.84 14.77 o
0 -9 1 11376.11 11280.92 384.68 o
1 -9 1 25701.04 28412.00 1236.58 o
2 -9 1 13542.49 14758.42 801.76 o
3 -9 1 1347.32 1688.46 195.99 o
4 -9 1 3823.56 4459.61 382.55 o
5 -9 1 6414.85 7342.55 533.18 o
6 -9 1 6105.51 6137.54 478.74 o
-7 -8 1 15466.90 15435.32 752.40 o
-6 -8 1 1352.19 1374.87 148.09 o
-5 -8 1 2923.07 2775.87 221.04 o
-4 -8 1 3598.20 3433.18 238.82 o
-3 -8 1 29250.09 28577.24 716.82 o
-2 -8 1 4847.10 4973.47 162.38 o
-1 -8 1 5890.87 6140.21 185.00 o
0 -8 1 14435.59 14638.97 346.29 o
1 -8 1 147.43 160.22 20.95 o
2 -8 1 8027.84 8515.22 308.19 o
3 -8 1 18327.32 18833.08 558.73 o
4 -8 1 19071.36 19776.16 596.70 o
5 -8 1 5390.22 5396.16 337.55 o
6 -8 1 338.79 390.13 36.85 o
7 -8 1 5594.43 5906.94 278.59 o
8 -8 1 3245.57 2734.13 214.14 o
-8 -7 1 5375.54 5387.68 385.46 o
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-5 -7 1 13474.46 13888.49 710.66 o
-4 -7 1 34610.50 35973.02 877.33 o
-3 -7 1 61.15 102.45 17.73 o
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-1 -7 1 363.64 434.01 34.36 o
0 -7 1 7598.30 7490.52 267.49 o
1 -7 1 3926.86 3999.26 200.53 o
2 -7 1 1282.57 1272.73 87.15 o
3 -7 1 2391.90 2574.49 140.38 o
4 -7 1 2858.79 2717.14 148.05 o
5 -7 1 568.23 657.89 60.26 o
6 -7 1 361.74 496.03 46.46 o
7 -7 1 9.69 22.64 15.30 o
8 -7 1 147.25 257.00 52.99 o
-9 -6 1 232.36 288.74 44.46 o
-8 -6 1 5692.20 6212.85 294.24 o
-7 -6 1 337.56 409.13 44.80 o
-6 -6 1 2563.39 2505.91 151.64 o
-5 -6 1 16084.67 15958.70 557.13 o
-4 -6 1 1215.97 1154.18 81.49 o
-3 -6 1 4961.88 4733.62 147.19 o
-2 -6 1 5644.21 5493.73 158.02 o
-1 -6 1 418.02 466.70 36.31 o
0 -6 1 425.93 357.00 25.13 o
1 -6 1 20393.66 21382.67 439.33 o
2 -6 1 4105.14 4297.71 134.94 o
3 -6 1 46860.72 47534.87 3162.78 o
4 -6 1 8765.90 8848.49 305.99 o
5 -6 1 4140.78 3955.97 189.53 o
6 -6 1 96.13 165.68 18.67 o
7 -6 1 13770.57 13282.71 347.44 o
8 -6 1 9032.76 9094.26 274.24 o
9 -6 1 2678.53 2666.76 118.78 o
-10 -5 1 1740.40 1800.28 155.11 o
-9 -5 1 354.84 415.19 33.48 o
-8 -5 1 3147.21 3102.32 155.60 o
-7 -5 1 7762.39 7966.47 274.73 o
-6 -5 1 18710.20 19533.96 572.98 o
-5 -5 1 19482.25 20072.38 471.48 o
-4 -5 1 4314.50 4380.51 124.91 o
-3 -5 1 25117.65 24820.29 459.49 o
-2 -5 1 4786.67 4694.93 122.55 o
-1 -5 1 75226.20 72166.16 2281.96 o
0 -5 1 7117.02 7586.03 186.56 o
1 -5 1 11556.97 12199.79 271.29 o
2 -5 1 34207.28 36357.47 679.92 o
3 -5 1 1070.46 1139.21 54.04 o
4 -5 1 2460.05 2201.19 254.97 o
5 -5 1 4225.98 4268.72 142.18 o
6 -5 1 54496.21 53206.63 1004.95 o
7 -5 1 23639.99 23521.30 522.22 o
8 -5 1 94.98 95.33 15.17 o
9 -5 1 2429.11 2447.18 115.64 o
-10 -4 1 4451.94 5103.82 212.48 o
-9 -4 1 8838.14 9404.67 316.63 o
-8 -4 1 3165.76 3239.90 154.74 o
-7 -4 1 18494.98 19699.98 496.13 o
-6 -4 1 12773.35 13224.30 599.76 o
-5 -4 1 1326.50 1500.60 84.42 o
-4 -4 1 148.71 195.24 15.77 o
-3 -4 1 23673.73 23272.85 404.79 o
-2 -4 1 173857.66 159683.11 2433.05 o
-1 -4 1 12417.25 11885.16 249.96 o
0 -4 1 4828.22 4755.09 156.80 o
1 -4 1 71.01 138.58 13.02 o
2 -4 1 56110.80 58909.20 900.80 o
3 -4 1 29437.00 30403.04 499.47 o
4 -4 1 4095.07 3935.24 90.21 o
5 -4 1 5843.35 5732.30 166.11 o
6 -4 1 5263.61 4918.55 157.11 o
7 -4 1 8487.15 8226.83 236.62 o
8 -4 1 382.42 384.40 31.82 o
9 -4 1 21.67 51.83 13.13 o
10 -4 1 3161.52 3123.99 163.25 o
-10 -3 1 14684.60 15610.41 554.39 o
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-5 -3 1 837.62 927.63 44.30 o
-4 -3 1 1310.05 1483.26 57.14 o
-3 -3 1 18126.45 17386.35 310.85 o
-2 -3 1 199.47 251.62 24.28 o
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0 -3 1 4575.41 4446.44 121.42 o
1 -3 1 25131.67 26321.42 523.41 o
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3 -3 1 34279.49 34984.30 491.08 o
4 -3 1 8.48 53.44 7.33 o
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6 -3 1 114.66 180.72 15.96 o
7 -3 1 11311.46 11148.16 290.37 o
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10 -3 1 4940.97 4775.17 226.63 o
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-8 -2 1 686.55 757.53 55.83 o
-7 -2 1 4080.41 4120.61 162.07 o
-6 -2 1 429.71 432.47 27.91 o
-5 -2 1 7187.59 6994.76 166.11 o
-4 -2 1 5547.60 5465.84 130.98 o
-3 -2 1 11132.87 11311.88 214.13 o
-2 -2 1 6895.12 6914.99 138.20 o
-1 -2 1 65260.83 62974.33 1402.55 o
0 -2 1 2762.96 2748.68 70.83 o
1 -2 1 120456.98 112145.92 3854.96 o
2 -2 1 7223.28 7926.47 127.02 o
3 -2 1 20316.09 21293.35 344.06 o
4 -2 1 44425.82 45520.92 746.37 o
5 -2 1 1920.91 1784.23 62.81 o
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7 -2 1 215.62 281.64 22.43 o
8 -2 1 40418.60 43334.34 861.71 o
9 -2 1 22301.09 21330.78 829.71 o
10 -2 1 124.71 127.21 38.29 o
-10 -1 1 8238.65 8602.81 489.99 o
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-1 -1 1 26271.25 24741.22 398.88 o
0 -1 1 149168.31 116446.83 4892.48 o
1 -1 1 64585.12 63026.33 1490.48 o
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-5 0 1 12183.05 11801.36 234.26 o
-4 0 1 33407.71 33472.43 536.93 o
-3 0 1 33881.18 34581.72 628.83 o
-2 0 1 5854.13 5809.44 110.56 o
-1 0 1 7158.38 7491.33 125.00 o
0 0 1 732.88 677.85 21.98 o
1 0 1 7045.65 6823.34 196.97 o
2 0 1 413.67 519.20 22.47 o
3 0 1 52527.12 53597.98 1546.86 o
4 0 1 25938.95 27316.33 1243.05 o
5 0 1 9385.53 10035.20 209.17 o
6 0 1 1035.29 1051.14 48.88 o
7 0 1 173.05 208.65 21.37 o
8 0 1 8182.63 8024.31 478.55 o
9 0 1 2924.09 2948.55 173.13 o
10 0 1 6120.93 6112.23 627.91 o
-10 1 1 901.15 892.03 75.19 o
-9 1 1 676.46 908.81 80.11 o
-8 1 1 1483.92 1567.38 83.83 o
-7 1 1 1664.13 1852.55 122.77 o
-6 1 1 13873.60 13859.78 275.49 o
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-3 1 1 137.67 142.25 11.93 o
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0 1 1 5943.00 6089.28 166.57 o
1 1 1 10001.78 10336.47 206.79 o
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2 2 15 3544.56 3543.15 280.93 o
3 2 15 724.09 733.17 79.85 o
-1 3 15 78.04 -2.54 32.67 o
0 3 15 229.62 185.47 41.38 o
2 3 15 7024.50 7391.19 461.68 o
3 3 15 6566.52 6291.80 415.22 o
3 4 15 4177.12 5016.43 257.20 o