#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:11:47 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180829 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/60/2016023.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016023_Fobs loop_ _publ_author_name 'Wagner, Pawe\/l' 'Officer, David L.' 'Kubicki, Maciej' _publ_section_title ; Flip-type disorder in 3-substituted 2,2':5',2''-terthiophenes ; _journal_coeditor_code DN3048 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o400 _journal_page_last o404 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.840 _cell_angle_gamma 90.000 _cell_length_a 18.9340 _cell_length_b 27.2700 _cell_length_c 7.5190 _exptl_crystal_F_000 1712.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file dn3048IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' e222 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 785.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2356.06 2487.01 96.90 o 3 0 0 1902.95 1915.32 77.52 o 4 0 0 38713.87 36423.45 1272.58 o 5 0 0 2.65 3.23 19.38 o 6 0 0 4961.22 4399.11 167.95 o 7 0 0 462.52 439.26 35.53 o 8 0 0 50492.28 52130.39 1821.66 o 9 0 0 18.11 38.76 25.84 o 10 0 0 915.88 926.98 58.14 o 11 0 0 350.97 471.56 45.22 o 12 0 0 3954.69 4001.83 164.72 o 13 0 0 9.12 148.57 38.76 o 14 0 0 37873.70 34650.24 1227.36 o 15 0 0 1413.78 1686.00 96.90 o 16 0 0 6872.63 6304.74 251.93 o 17 0 0 36.59 45.22 32.30 o 19 0 0 63.36 0.00 41.99 o 20 0 0 1045.23 1030.33 74.29 o 21 0 0 24.50 0.00 41.99 o 22 0 0 611.18 691.20 77.52 o 1 1 0 0.12 0.72 4.23 o 2 1 0 814.89 817.37 27.41 o 3 1 0 2444.01 2461.75 68.40 o 4 1 0 5660.96 5712.36 148.40 o 5 1 0 5048.22 4993.56 132.41 o 6 1 0 3962.88 3779.87 150.19 o 7 1 0 4.08 17.64 22.61 o 8 1 0 182.60 174.24 56.52 o 9 1 0 1672.51 1634.46 55.92 o 10 1 0 1544.61 1628.55 56.96 o 11 1 0 858.93 1008.56 43.21 o 12 1 0 4006.78 4185.30 138.89 o 13 1 0 80.59 86.24 22.50 o 14 1 0 11.34 7.43 54.91 o 15 1 0 544.89 530.25 53.29 o 16 1 0 301.64 192.52 27.41 o 17 1 0 613.78 583.26 40.37 o 18 1 0 666.65 710.44 95.28 o 19 1 0 2.19 44.50 30.27 o 20 1 0 3585.66 3855.04 124.46 o 21 1 0 15.92 36.77 37.14 o 22 1 0 26.72 89.17 49.02 o 0 2 0 2936.25 538.15 522.72 o 1 2 0 235.17 260.33 7.16 o 2 2 0 10603.91 10294.33 166.84 o 3 2 0 3763.92 3831.50 82.66 o 4 2 0 1131.08 1163.59 53.29 o 5 2 0 13135.63 12071.03 306.01 o 6 2 0 1635.89 1660.26 52.53 o 7 2 0 388.14 342.49 22.84 o 8 2 0 416.14 424.88 27.41 o 9 2 0 2976.98 2878.97 84.41 o 10 2 0 1294.03 1378.19 50.09 o 11 2 0 13566.65 14004.66 359.70 o 12 2 0 795.52 981.16 59.75 o 13 2 0 770.51 720.66 38.62 o 14 2 0 1273.52 1261.74 52.53 o 15 2 0 4312.95 4171.33 124.46 o 16 2 0 952.98 943.88 51.35 o 17 2 0 1560.95 1496.94 63.83 o 18 2 0 94.47 142.85 54.91 o 19 2 0 1908.50 2266.23 84.41 o 20 2 0 1.01 35.54 28.17 o 21 2 0 419.67 336.32 31.82 o 22 2 0 384.09 418.56 37.75 o 1 3 0 12338.73 12062.27 193.65 o 2 3 0 23.31 38.59 5.62 o 3 3 0 4594.51 4738.20 87.53 o 4 3 0 32.62 49.52 11.19 o 5 3 0 14429.10 14508.28 297.09 o 6 3 0 163.03 196.06 18.27 o 7 3 0 1389.97 1243.35 44.49 o 8 3 0 342.84 331.76 23.90 o 9 3 0 33198.98 32159.14 801.48 o 10 3 0 39.37 65.55 19.31 o 11 3 0 2628.76 2693.39 84.41 o 12 3 0 290.97 270.17 29.69 o 13 3 0 359.34 321.58 59.75 o 14 3 0 0.43 0.00 19.38 o 15 3 0 1273.53 1174.12 71.06 o 16 3 0 1.45 4.52 28.48 o 17 3 0 857.00 836.93 37.79 o 18 3 0 3.19 0.00 17.90 o 19 3 0 510.80 513.18 34.57 o 20 3 0 133.88 190.33 34.96 o 21 3 0 596.57 690.37 38.97 o 22 3 0 10.41 0.00 43.60 o 0 4 0 12.63 21.96 6.65 o 1 4 0 4345.25 4224.86 71.03 o 2 4 0 469.31 529.96 12.13 o 3 4 0 17749.66 18157.29 284.23 o 4 4 0 0.07 17.90 11.65 o 5 4 0 2343.76 2247.16 53.37 o 6 4 0 652.43 655.57 27.43 o 7 4 0 18723.46 18649.00 381.01 o 8 4 0 2924.33 2979.88 85.57 o 9 4 0 16823.03 16631.39 342.60 o 10 4 0 798.95 862.85 33.61 o 11 4 0 902.76 961.55 44.69 o 12 4 0 24.67 51.08 15.95 o 13 4 0 42.14 34.01 20.96 o 14 4 0 226.88 271.37 27.42 o 15 4 0 725.25 860.26 78.15 o 16 4 0 0.50 0.00 21.08 o 17 4 0 3971.40 4003.58 100.03 o 18 4 0 104.64 169.69 22.22 o 19 4 0 94.42 117.52 24.65 o 20 4 0 14.34 26.46 35.93 o 21 4 0 1248.25 1283.34 76.38 o 22 4 0 116.58 94.95 44.61 o 1 5 0 1255.02 1311.60 25.64 o 2 5 0 1452.20 1443.06 38.17 o 3 5 0 10664.49 10833.24 171.81 o 4 5 0 19109.62 19231.60 301.38 o 5 5 0 390.13 399.88 15.70 o 6 5 0 4878.39 4746.33 103.73 o 7 5 0 136.03 195.17 32.30 o 8 5 0 3485.51 3903.05 89.23 o 9 5 0 686.69 761.85 29.06 o 10 5 0 267.61 176.48 21.80 o 11 5 0 1527.40 1471.93 43.49 o 12 5 0 8.51 9.09 14.33 o 13 5 0 340.11 337.82 30.76 o 14 5 0 518.86 568.40 31.99 o 15 5 0 220.77 259.98 25.06 o 16 5 0 3211.74 3087.06 80.75 o 17 5 0 247.26 286.11 46.00 o 18 5 0 4928.21 5087.51 123.43 o 19 5 0 169.28 190.76 27.19 o 20 5 0 865.35 930.90 46.54 o 21 5 0 22.08 51.35 26.42 o 22 5 0 209.97 270.30 31.74 o 0 6 0 21626.03 22124.96 463.65 o 1 6 0 71.37 107.63 7.48 o 2 6 0 25805.26 25415.24 368.45 o 3 6 0 0.08 31.26 22.38 o 4 6 0 41.05 67.70 17.43 o 5 6 0 43.12 69.39 8.91 o 6 6 0 1634.13 1763.16 39.63 o 7 6 0 4.31 6.46 10.45 o 8 6 0 1974.80 2268.38 57.04 o 9 6 0 14.49 43.80 14.01 o 10 6 0 1070.42 1234.58 38.88 o 11 6 0 7.73 19.14 16.58 o 12 6 0 7021.51 6943.03 153.50 o 13 6 0 136.86 102.50 22.22 o 14 6 0 1095.56 1034.73 39.07 o 15 6 0 8.86 33.79 27.82 o 16 6 0 1428.36 1383.87 48.94 o 17 6 0 64.72 79.67 23.77 o 18 6 0 4.84 0.00 21.32 o 19 6 0 394.29 383.73 31.35 o 20 6 0 892.15 821.30 38.97 o 21 6 0 88.11 97.11 22.84 o 22 6 0 476.24 445.88 33.70 o 1 7 0 559.00 532.81 15.73 o 2 7 0 852.39 869.07 33.74 o 3 7 0 2150.93 2266.03 40.59 o 4 7 0 7.13 12.80 9.70 o 5 7 0 1306.59 1444.90 29.12 o 6 7 0 1469.17 1656.34 37.47 o 7 7 0 214.48 341.83 19.58 o 8 7 0 7555.97 7895.50 168.26 o 9 7 0 484.84 550.47 25.97 o 10 7 0 68.66 96.22 17.35 o 11 7 0 981.79 906.46 33.57 o 12 7 0 53.16 101.98 39.91 o 13 7 0 386.96 385.54 24.52 o 14 7 0 1834.19 1798.58 53.30 o 15 7 0 0.57 13.17 17.11 o 16 7 0 753.45 769.33 35.92 o 17 7 0 889.36 800.03 48.49 o 18 7 0 630.67 555.16 48.81 o 19 7 0 189.18 142.77 32.13 o 20 7 0 9.77 21.78 38.26 o 21 7 0 3.32 0.00 24.10 o 0 8 0 728.21 812.95 27.94 o 1 8 0 89.45 97.26 6.47 o 2 8 0 1662.94 1701.43 29.69 o 3 8 0 1609.33 1669.72 34.87 o 4 8 0 492.61 513.91 15.09 o 5 8 0 2090.53 2003.09 38.34 o 6 8 0 4064.39 3973.23 72.07 o 7 8 0 3496.15 4228.34 82.31 o 8 8 0 3078.41 3123.16 74.45 o 9 8 0 7471.41 7115.15 153.95 o 10 8 0 658.53 750.76 28.42 o 11 8 0 191.14 229.13 43.35 o 12 8 0 1156.79 1173.02 40.29 o 13 8 0 381.61 418.29 46.05 o 14 8 0 56.98 111.18 46.83 o 15 8 0 3341.35 3173.31 82.58 o 16 8 0 1.45 0.00 20.34 o 17 8 0 3874.90 3913.77 100.03 o 18 8 0 144.07 200.28 23.36 o 19 8 0 114.90 88.11 24.21 o 20 8 0 539.09 585.48 39.07 o 21 8 0 73.76 117.56 37.61 o 1 9 0 24.27 34.10 6.09 o 2 9 0 249.76 262.43 10.11 o 3 9 0 32994.07 32306.48 501.91 o 4 9 0 679.22 656.43 17.29 o 5 9 0 1690.12 2100.78 39.72 o 6 9 0 580.12 620.69 18.20 o 7 9 0 1757.90 1737.30 39.85 o 8 9 0 6.76 28.57 26.89 o 9 9 0 212.80 166.44 23.24 o 10 9 0 108.63 124.75 17.79 o 11 9 0 17511.24 17483.80 362.29 o 12 9 0 48.22 25.73 17.34 o 13 9 0 3187.34 2965.94 76.97 o 14 9 0 235.23 231.76 21.56 o 15 9 0 665.51 693.29 31.59 o 16 9 0 4.80 28.51 17.29 o 17 9 0 263.32 303.46 49.52 o 18 9 0 219.25 171.38 21.75 o 19 9 0 33.69 35.62 29.71 o 21 9 0 1611.32 1721.84 77.25 o 0 10 0 264.90 236.64 13.13 o 1 10 0 2441.83 2374.10 36.80 o 2 10 0 1587.69 1529.06 30.56 o 3 10 0 67.20 63.10 18.68 o 4 10 0 3385.95 3453.58 60.09 o 5 10 0 2269.67 2343.88 43.46 o 6 10 0 2065.86 2052.62 40.08 o 7 10 0 218.66 397.60 16.27 o 8 10 0 4058.58 4518.24 88.29 o 9 10 0 154.14 301.68 21.36 o 10 10 0 694.21 676.53 29.06 o 11 10 0 12.11 50.67 45.44 o 12 10 0 2127.85 2127.35 58.72 o 13 10 0 821.11 808.73 36.05 o 14 10 0 1.35 17.23 30.71 o 15 10 0 1861.46 1874.18 63.75 o 16 10 0 61.68 79.67 24.24 o 17 10 0 457.55 433.06 48.66 o 18 10 0 769.08 697.63 45.51 o 19 10 0 568.42 621.93 45.51 o 20 10 0 49.75 17.76 56.52 o 21 10 0 4.56 77.52 101.74 o 1 11 0 180.21 233.70 13.13 o 2 11 0 21382.10 22155.96 347.00 o 3 11 0 11.94 0.00 9.69 o 4 11 0 403.45 502.39 17.62 o 5 11 0 480.44 580.55 17.09 o 6 11 0 33.27 159.48 11.56 o 7 11 0 36.12 23.75 10.09 o 8 11 0 6285.20 5990.62 113.71 o 9 11 0 1.71 13.76 12.53 o 10 11 0 250.23 322.00 20.34 o 11 11 0 50.30 0.00 15.23 o 12 11 0 375.63 472.42 43.95 o 13 11 0 70.83 62.42 21.07 o 14 11 0 3000.47 2863.46 74.40 o 15 11 0 720.03 637.28 30.94 o 16 11 0 1816.59 1835.29 95.28 o 17 11 0 121.62 144.44 28.65 o 18 11 0 22.52 26.00 46.83 o 19 11 0 32.79 102.40 30.68 o 20 11 0 45.94 31.18 27.45 o 21 11 0 4.27 90.44 58.14 o 0 12 0 1866.88 2117.24 62.78 o 1 12 0 143.31 193.79 19.70 o 2 12 0 10660.93 11505.50 183.97 o 3 12 0 53.07 44.63 11.35 o 4 12 0 19327.83 21007.03 330.06 o 5 12 0 28.98 19.93 16.85 o 6 12 0 4337.70 4803.25 81.84 o 7 12 0 105.99 105.51 11.16 o 8 12 0 3753.93 4063.37 72.42 o 9 12 0 242.70 291.57 18.65 o 10 12 0 669.88 665.78 25.24 o 11 12 0 173.52 187.82 21.36 o 12 12 0 8800.97 8389.57 182.67 o 13 12 0 299.29 379.24 39.92 o 14 12 0 3255.78 3216.46 105.06 o 15 12 0 0.81 63.69 28.48 o 16 12 0 392.19 328.35 37.22 o 18 12 0 606.11 459.94 37.63 o 19 12 0 205.61 211.46 43.60 o 20 12 0 82.91 122.29 62.98 o 1 13 0 7473.52 8140.79 132.34 o 2 13 0 1588.53 1832.06 41.52 o 3 13 0 2545.60 2764.73 75.06 o 4 13 0 884.39 1102.80 28.93 o 5 13 0 32.50 26.89 14.32 o 6 13 0 3444.60 3386.29 60.46 o 7 13 0 99.79 51.30 15.79 o 8 13 0 1867.08 1878.46 39.17 o 9 13 0 97.82 94.03 15.85 o 10 13 0 117.87 157.36 18.48 o 11 13 0 392.27 330.09 35.53 o 12 13 0 2435.84 2403.23 148.57 o 13 13 0 6637.00 6615.00 184.99 o 14 13 0 2679.59 2719.17 90.19 o 15 13 0 237.51 162.70 27.94 o 16 13 0 429.67 469.98 75.90 o 17 13 0 46.23 46.83 31.97 o 18 13 0 96.42 67.71 56.52 o 19 13 0 164.17 195.04 34.04 o 20 13 0 401.85 384.65 51.68 o 0 14 0 3379.78 3525.59 97.89 o 1 14 0 1266.15 1282.61 27.54 o 2 14 0 113.26 94.72 12.77 o 3 14 0 11229.11 11023.18 198.87 o 4 14 0 1190.55 1350.26 34.24 o 5 14 0 33.67 29.77 12.59 o 6 14 0 1061.17 1065.67 30.62 o 7 14 0 6993.79 6864.26 129.44 o 8 14 0 28.22 20.17 13.75 o 9 14 0 646.59 642.51 32.79 o 10 14 0 27.69 15.27 18.16 o 11 14 0 35.39 34.97 26.78 o 12 14 0 333.44 377.27 34.91 o 13 14 0 1263.43 1152.14 54.67 o 14 14 0 159.69 176.03 103.36 o 15 14 0 232.17 214.04 56.52 o 16 14 0 352.33 361.10 38.62 o 17 14 0 0.20 0.00 22.84 o 18 14 0 14.51 56.45 51.68 o 19 14 0 329.59 328.08 71.06 o 20 14 0 2.08 61.13 29.28 o 1 15 0 29029.49 29821.81 466.15 o 2 15 0 13.61 10.38 15.38 o 3 15 0 3388.93 3505.37 70.62 o 4 15 0 498.12 527.08 20.47 o 5 15 0 7592.71 7597.49 141.46 o 6 15 0 468.01 469.96 21.76 o 7 15 0 279.17 355.64 19.19 o 8 15 0 15.67 8.95 11.70 o 9 15 0 5132.61 5102.41 101.66 o 10 15 0 20.47 19.72 21.61 o 11 15 0 131.40 126.49 22.22 o 12 15 0 51.91 40.37 27.41 o 13 15 0 14102.97 13639.53 356.26 o 14 15 0 530.78 492.71 35.34 o 15 15 0 8297.31 8159.81 226.07 o 16 15 0 21.07 29.07 93.67 o 17 15 0 12.92 0.00 45.22 o 18 15 0 267.21 234.07 33.35 o 19 15 0 105.17 185.13 36.33 o 0 16 0 165.41 244.67 16.21 o 1 16 0 891.47 1074.49 54.04 o 2 16 0 212.21 187.10 18.18 o 3 16 0 331.69 313.42 18.01 o 4 16 0 1829.67 1998.61 46.70 o 5 16 0 4979.62 4722.22 92.81 o 6 16 0 632.13 625.81 24.37 o 7 16 0 120.58 126.74 22.38 o 8 16 0 559.60 575.94 23.60 o 9 16 0 756.48 711.87 33.10 o 10 16 0 763.41 761.13 35.61 o 11 16 0 267.28 203.31 24.20 o 12 16 0 1689.76 1528.07 61.66 o 13 16 0 2798.88 2816.01 94.60 o 14 16 0 22.79 152.88 75.90 o 15 16 0 338.78 437.07 41.11 o 16 16 0 19.56 66.50 50.06 o 17 16 0 71.98 0.00 25.84 o 18 16 0 6.09 36.70 58.14 o 19 16 0 1165.87 1316.13 63.83 o 1 17 0 1251.80 1273.32 33.33 o 2 17 0 4123.44 4545.65 89.31 o 3 17 0 7.50 6.03 20.05 o 4 17 0 3696.15 3705.36 75.50 o 5 17 0 312.86 304.12 18.76 o 6 17 0 8612.46 8995.07 166.66 o 7 17 0 1.63 21.17 19.07 o 8 17 0 902.89 850.15 29.38 o 9 17 0 2037.42 2062.82 85.78 o 10 17 0 20751.66 20582.58 426.33 o 11 17 0 59.78 69.38 41.51 o 12 17 0 399.43 392.40 28.32 o 13 17 0 603.27 569.82 37.63 o 14 17 0 7492.34 7305.16 205.51 o 15 17 0 917.82 902.42 58.21 o 16 17 0 56.90 77.29 61.37 o 17 17 0 107.02 77.52 26.87 o 18 17 0 0.09 14.80 27.12 o 19 17 0 97.67 151.11 100.13 o 0 18 0 9940.09 9473.16 247.79 o 1 18 0 63.14 125.39 35.65 o 2 18 0 545.42 579.08 23.45 o 3 18 0 49.25 47.37 14.30 o 4 18 0 4672.36 4736.27 93.52 o 5 18 0 15.62 34.64 14.30 o 6 18 0 4405.18 4390.81 88.66 o 7 18 0 2.33 16.93 32.92 o 8 18 0 1348.96 1308.35 38.23 o 9 18 0 49.60 64.60 38.76 o 10 18 0 9858.66 9620.53 209.95 o 11 18 0 139.30 108.93 42.42 o 12 18 0 1.70 2.07 16.09 o 13 18 0 132.99 147.84 74.29 o 14 18 0 2303.71 2461.19 88.98 o 15 18 0 11.97 47.03 41.99 o 16 18 0 188.52 194.52 66.21 o 17 18 0 67.05 90.98 35.53 o 18 18 0 138.61 188.50 40.37 o 1 19 0 3919.08 4001.95 94.96 o 2 19 0 14.16 4.11 17.30 o 3 19 0 1595.26 1526.39 46.54 o 4 19 0 1118.12 1066.96 32.43 o 5 19 0 14.04 42.93 16.17 o 6 19 0 1265.06 1231.62 36.07 o 7 19 0 67.95 65.24 28.02 o 8 19 0 4915.62 4887.99 124.58 o 9 19 0 1035.37 1045.56 41.24 o 10 19 0 1720.30 1614.57 51.95 o 11 19 0 482.87 409.18 29.76 o 12 19 0 288.79 274.55 24.55 o 13 19 0 404.85 283.65 64.60 o 14 19 0 165.28 139.37 37.14 o 15 19 0 1961.70 2084.80 82.12 o 16 19 0 74.76 39.74 54.91 o 17 19 0 4.39 0.00 35.53 o 18 19 0 28.62 0.00 23.26 o 0 20 0 632.81 586.57 34.91 o 1 20 0 3984.91 4160.35 84.98 o 2 20 0 21.72 26.34 33.38 o 3 20 0 204.58 288.39 25.67 o 4 20 0 8.25 0.00 15.82 o 5 20 0 8495.19 8289.90 155.24 o 6 20 0 407.43 473.78 25.33 o 7 20 0 324.95 297.29 25.31 o 8 20 0 52.19 66.88 26.87 o 9 20 0 2120.18 2077.21 61.12 o 10 20 0 109.07 112.06 28.70 o 11 20 0 5522.59 5478.31 129.25 o 12 20 0 196.54 190.71 25.57 o 13 20 0 24.44 0.00 22.72 o 14 20 0 15.45 0.00 22.50 o 15 20 0 3.82 0.00 29.07 o 16 20 0 57.91 73.40 40.37 o 17 20 0 2.12 52.79 41.99 o 1 21 0 11823.33 11713.77 214.68 o 2 21 0 325.62 305.29 37.67 o 3 21 0 7281.78 7304.98 161.42 o 4 21 0 25.05 0.00 24.81 o 5 21 0 9947.94 9906.31 213.13 o 6 21 0 196.67 217.21 32.30 o 7 21 0 1329.29 1283.23 43.62 o 8 21 0 15.88 18.50 23.05 o 9 21 0 24.94 47.32 20.34 o 10 21 0 478.11 434.15 29.17 o 11 21 0 903.88 865.02 62.29 o 12 21 0 55.45 0.00 30.02 o 13 21 0 114.88 139.94 34.01 o 14 21 0 85.39 92.59 29.07 o 15 21 0 1196.71 1241.69 59.25 o 16 21 0 31.43 0.00 23.90 o 17 21 0 1457.28 1527.56 69.63 o 0 22 0 1347.73 1468.42 58.21 o 1 22 0 962.03 1052.97 35.35 o 2 22 0 791.98 840.94 37.20 o 3 22 0 1611.01 1641.90 82.72 o 4 22 0 190.34 173.11 24.05 o 5 22 0 1778.08 1901.86 138.89 o 6 22 0 964.16 1029.91 50.09 o 7 22 0 2142.00 2067.79 200.25 o 8 22 0 807.34 698.85 48.45 o 9 22 0 519.79 462.28 31.82 o 10 22 0 1311.73 1294.82 47.22 o 11 22 0 172.94 170.45 32.15 o 12 22 0 122.83 115.91 26.73 o 13 22 0 336.11 319.33 27.19 o 14 22 0 359.14 331.30 31.73 o 15 22 0 6.28 36.03 27.39 o 16 22 0 303.57 377.33 43.21 o 1 23 0 111.52 170.47 21.35 o 2 23 0 4038.09 4182.24 86.94 o 3 23 0 2.73 9.69 20.90 o 4 23 0 3538.37 3775.50 119.89 o 5 23 0 43.52 50.45 23.90 o 6 23 0 794.59 654.23 43.60 o 7 23 0 7.26 25.84 38.76 o 8 23 0 59.61 0.00 24.81 o 9 23 0 438.90 400.09 35.34 o 10 23 0 1584.08 1568.30 67.11 o 11 23 0 38.48 4.61 29.07 o 12 23 0 0.14 0.00 28.83 o 13 23 0 0.28 0.00 18.71 o 14 23 0 52.73 0.00 23.90 o 15 23 0 1.21 0.00 38.76 o 0 24 0 195.67 157.82 75.90 o 1 24 0 204.68 156.97 20.24 o 2 24 0 8751.04 8453.71 160.66 o 3 24 0 8.67 0.00 25.60 o 4 24 0 484.88 485.78 69.44 o 5 24 0 78.89 70.93 28.48 o 6 24 0 2412.59 2237.50 81.84 o 7 24 0 90.06 93.39 24.81 o 8 24 0 113.23 121.66 33.35 o 9 24 0 165.63 148.42 33.06 o 10 24 0 219.33 216.36 40.37 o 11 24 0 7.60 0.00 41.99 o 12 24 0 3091.68 3040.15 103.90 o 13 24 0 228.12 182.50 27.41 o 14 24 0 0.71 9.22 24.82 o 15 24 0 133.26 204.69 42.21 o 1 25 0 563.86 602.99 27.67 o 2 25 0 1381.95 1437.80 43.51 o 3 25 0 696.61 709.61 43.21 o 4 25 0 539.58 500.47 39.92 o 5 25 0 164.01 152.76 33.35 o 6 25 0 219.29 183.70 27.41 o 7 25 0 27.10 40.30 51.68 o 8 25 0 273.56 225.24 56.52 o 9 25 0 267.04 263.21 38.76 o 10 25 0 15.00 0.00 25.84 o 11 25 0 260.49 358.66 72.67 o 12 25 0 3.30 0.00 48.45 o 13 25 0 76.10 61.62 29.43 o 14 25 0 97.12 140.54 180.87 o 0 26 0 18.38 12.92 43.60 o 1 26 0 762.88 809.69 31.83 o 2 26 0 1.79 70.25 24.55 o 3 26 0 19.33 129.85 48.88 o 4 26 0 86.47 155.38 45.22 o 5 26 0 579.26 531.74 44.49 o 6 26 0 245.14 318.00 46.83 o 7 26 0 3023.65 3405.78 111.63 o 8 26 0 234.28 211.91 35.34 o 9 26 0 756.92 850.89 46.78 o 10 26 0 4.88 6.33 25.34 o 11 26 0 169.11 206.23 34.03 o 12 26 0 0.78 0.00 35.53 o 13 26 0 290.79 393.93 66.21 o 1 27 0 8.60 45.38 24.82 o 2 27 0 40.38 0.00 33.60 o 3 27 0 1027.63 1182.21 45.90 o 4 27 0 0.52 22.89 24.45 o 5 27 0 2729.53 2670.87 94.76 o 6 27 0 8.37 17.44 26.87 o 7 27 0 314.47 352.95 58.14 o 8 27 0 0.65 2.92 37.14 o 9 27 0 28.88 94.03 30.27 o 10 27 0 6.95 0.00 27.45 o 11 27 0 598.25 497.96 47.31 o 12 27 0 25.59 71.06 48.45 o 0 28 0 725.83 658.90 67.83 o 1 28 0 701.08 684.50 35.49 o 2 28 0 367.98 547.10 34.15 o 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