#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/60/2016025.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016025_Fobs loop_ _publ_author_name 'Ring, Joshua R.' 'Parkin, Sean' 'Crooks, Peter A.' _publ_section_title ; (4-Methoxy-3-nitrobenzylideneamino)guanidinium chloride ; _journal_coeditor_code FA3076 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o392 _journal_page_last o394 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.179 _cell_angle_gamma 90.000 _cell_length_a 16.7260 _cell_length_b 5.1384 _cell_length_c 14.0045 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high .7702 _[local]_cod_data_source_file fa3076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' k05174 - P21/c (transformed from P21/a)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 151.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 192.97 168.36 3.72 o 2 0 0 554.80 565.70 10.95 o 3 0 0 2390.55 2167.36 41.26 o 4 0 0 8787.05 8454.56 168.75 o 5 0 0 9343.48 8744.94 178.14 o 6 0 0 6171.83 6028.69 122.21 o 7 0 0 54.99 47.13 1.96 o 8 0 0 104.43 90.93 3.13 o 9 0 0 123.73 112.63 3.32 o 10 0 0 2236.03 2223.48 53.97 o 11 0 0 2574.86 2714.29 74.11 o 12 0 0 352.30 339.07 11.93 o 13 0 0 1469.87 1486.49 45.56 o 14 0 0 129.09 122.60 4.69 o 15 0 0 318.02 333.98 11.15 o 16 0 0 1639.47 1804.83 52.21 o 17 0 0 36.06 42.04 5.87 o 18 0 0 31.45 30.11 5.87 o 19 0 0 221.80 245.99 10.75 o 20 0 0 7.76 -8.02 8.02 o 21 0 0 123.24 141.96 12.71 o 1 1 0 184.32 160.53 4.40 o 2 1 0 966.91 963.94 13.39 o 3 1 0 4639.90 4148.39 49.42 o 4 1 0 4230.15 4027.84 56.83 o 5 1 0 3831.10 3628.76 46.72 o 6 1 0 20.15 8.82 .83 o 7 1 0 109.17 72.84 1.59 o 8 1 0 37.42 34.52 2.64 o 9 1 0 10.68 10.36 2.74 o 10 1 0 71.90 85.82 2.42 o 11 1 0 30.97 26.26 1.72 o 12 1 0 1.58 1.16 1.50 o 13 1 0 59.01 54.45 2.89 o 14 1 0 8.99 6.22 5.48 o 15 1 0 8.61 9.68 2.91 o 16 1 0 195.88 170.95 5.96 o 17 1 0 147.32 132.76 6.14 o 18 1 0 250.19 260.96 7.60 o 19 1 0 175.87 181.37 6.57 o 20 1 0 13.89 13.57 6.67 o 21 1 0 34.38 7.17 6.63 o 0 2 0 5257.55 5215.81 210.98 o 1 2 0 16.87 12.61 .90 o 2 2 0 259.17 272.20 4.35 o 3 2 0 9.59 4.76 .80 o 4 2 0 2927.18 2956.83 40.24 o 5 2 0 399.14 338.63 4.48 o 6 2 0 41.66 57.92 2.15 o 7 2 0 3647.78 3724.37 47.55 o 8 2 0 681.22 637.71 9.39 o 9 2 0 1122.36 1177.34 20.59 o 10 2 0 905.05 955.97 23.27 o 11 2 0 367.23 383.27 7.68 o 12 2 0 562.78 579.42 13.45 o 13 2 0 280.89 293.31 7.94 o 14 2 0 71.69 71.17 3.70 o 15 2 0 6.95 5.01 3.42 o 16 2 0 959.65 1051.59 30.02 o 17 2 0 42.31 47.50 4.50 o 18 2 0 81.26 74.48 6.22 o 19 2 0 12.59 14.23 5.31 o 20 2 0 243.26 221.51 13.82 o 1 3 0 387.34 400.89 7.59 o 2 3 0 2055.23 1917.47 37.15 o 3 3 0 801.43 731.48 15.15 o 4 3 0 45.03 31.32 1.71 o 5 3 0 18.81 15.47 2.05 o 6 3 0 232.43 224.44 8.99 o 7 3 0 164.30 139.98 5.28 o 8 3 0 484.32 471.72 9.39 o 9 3 0 996.03 1019.07 19.95 o 10 3 0 1200.70 1212.79 20.14 o 11 3 0 451.97 453.74 10.95 o 12 3 0 12.83 11.69 5.48 o 13 3 0 21.73 25.00 2.95 o 14 3 0 159.31 158.37 5.11 o 15 3 0 66.11 51.05 8.11 o 16 3 0 39.63 51.38 9.87 o 17 3 0 1.02 7.49 6.48 o 18 3 0 134.54 118.49 15.74 o 19 3 0 55.13 66.02 9.10 o 0 4 0 1.47 1.50 6.84 o 1 4 0 113.35 108.00 3.34 o 2 4 0 4.05 -.75 2.35 o 3 4 0 30.63 19.39 2.31 o 4 4 0 33.33 32.69 2.89 o 5 4 0 .19 1.59 2.17 o 6 4 0 89.95 73.41 3.59 o 7 4 0 .70 1.61 3.52 o 8 4 0 12.58 8.23 3.43 o 9 4 0 312.44 332.03 12.91 o 10 4 0 16.35 14.55 7.43 o 11 4 0 45.29 63.86 6.13 o 12 4 0 106.27 106.36 8.99 o 13 4 0 82.60 68.64 16.52 o 14 4 0 .95 20.18 6.18 o 15 4 0 793.60 876.45 29.73 o 16 4 0 16.74 6.30 6.70 o 17 4 0 42.28 28.87 6.74 o 1 5 0 85.54 81.09 6.55 o 2 5 0 66.84 81.59 14.18 o 3 5 0 83.69 91.95 6.94 o 4 5 0 47.26 63.98 6.09 o 5 5 0 .34 -2.44 11.44 o 6 5 0 10.20 12.71 5.67 o 7 5 0 253.14 293.31 12.12 o 8 5 0 .98 -1.42 7.33 o 9 5 0 72.39 79.00 9.26 o 10 5 0 15.97 7.43 9.58 o 11 5 0 10.99 5.95 6.87 o 12 5 0 85.67 129.66 25.03 o 13 5 0 6.96 13.30 9.97 o 14 5 0 10.16 -8.17 9.58 o 0 6 0 177.40 204.53 17.01 o 1 6 0 163.13 169.66 9.39 o 2 6 0 22.03 32.07 6.93 o 3 6 0 12.71 31.17 7.23 o 4 6 0 79.48 72.62 8.26 o 5 6 0 402.00 447.91 28.16 o 6 6 0 80.99 75.67 10.95 o 7 6 0 46.97 37.54 13.10 o 8 6 0 69.37 71.96 13.30 o 9 6 0 28.23 4.39 10.49 o -21 1 1 2.11 .98 6.36 o -20 1 1 16.27 18.18 5.32 o -19 1 1 .00 -4.56 4.56 o -18 1 1 271.42 295.39 7.42 o -17 1 1 2.77 -1.17 3.04 o -16 1 1 37.76 35.23 3.28 o -15 1 1 251.16 258.26 6.64 o -14 1 1 267.81 262.96 6.76 o -13 1 1 181.56 173.56 4.65 o -12 1 1 129.60 124.08 3.85 o -11 1 1 305.65 269.13 11.93 o -10 1 1 52.81 45.24 1.86 o -9 1 1 53.19 43.93 4.50 o -8 1 1 1152.44 1212.12 16.01 o -7 1 1 697.66 678.67 8.14 o -6 1 1 208.67 231.14 3.56 o -5 1 1 6.38 14.15 2.25 o -4 1 1 18547.07 18465.11 322.31 o -3 1 1 1573.87 1509.65 17.62 o -2 1 1 4258.84 4072.98 113.12 o -1 1 1 1241.80 1378.04 21.44 o 0 1 1 4301.13 3812.04 56.09 o 1 1 1 212.89 236.51 3.81 o 2 1 1 61.49 65.30 2.44 o 3 1 1 22954.12 22087.31 508.83 o 4 1 1 5034.27 5032.87 69.32 o 5 1 1 643.27 635.09 8.12 o 6 1 1 24.41 29.28 1.03 o 7 1 1 1615.32 1677.60 21.88 o 8 1 1 1023.78 961.30 13.67 o 9 1 1 61.62 30.67 1.55 o 10 1 1 181.04 162.58 5.67 o 11 1 1 35.05 26.67 3.62 o 12 1 1 319.70 309.46 6.39 o 13 1 1 8.53 8.28 2.64 o 14 1 1 1423.14 1443.40 30.14 o 15 1 1 181.95 175.85 5.74 o 16 1 1 183.14 177.54 5.32 o 17 1 1 .47 10.89 4.51 o 18 1 1 83.15 65.86 6.48 o 19 1 1 527.48 560.47 18.89 o 20 1 1 183.83 197.14 9.10 o 21 1 1 .02 13.42 7.89 o -20 2 1 109.24 119.58 15.25 o -19 2 1 96.58 89.73 12.51 o -18 2 1 136.58 114.26 6.29 o -17 2 1 95.42 72.24 5.28 o -16 2 1 441.67 489.01 11.46 o -15 2 1 555.49 577.03 16.33 o -14 2 1 837.46 874.15 18.90 o -13 2 1 66.10 65.13 3.73 o -12 2 1 95.27 80.22 3.03 o -11 2 1 175.52 159.24 9.09 o -10 2 1 892.11 924.12 15.40 o -9 2 1 29.81 42.55 2.25 o -8 2 1 74.58 57.64 3.32 o -7 2 1 5339.56 5433.66 93.47 o -6 2 1 14.71 8.80 .83 o -5 2 1 260.45 261.28 4.40 o -4 2 1 823.29 699.88 16.62 o -3 2 1 544.92 501.21 7.18 o -2 2 1 206.75 184.63 6.16 o -1 2 1 301.89 253.09 4.40 o 0 2 1 3155.62 3016.68 57.54 o 1 2 1 3176.07 2924.53 48.45 o 2 2 1 395.28 371.93 9.48 o 3 2 1 992.40 911.37 15.22 o 4 2 1 4276.73 4572.90 68.95 o 5 2 1 1918.65 1774.40 24.95 o 6 2 1 481.39 476.38 6.76 o 7 2 1 528.37 463.81 6.40 o 8 2 1 5039.56 5383.10 92.20 o 9 2 1 536.95 544.77 8.77 o 10 2 1 10.42 10.53 4.60 o 11 2 1 295.86 281.56 6.10 o 12 2 1 744.56 765.52 17.31 o 13 2 1 31.85 27.30 5.28 o 14 2 1 2.02 -1.41 3.25 o 15 2 1 23.44 15.99 3.39 o 16 2 1 142.03 156.59 9.29 o 17 2 1 10.41 16.05 4.23 o 18 2 1 25.47 17.82 4.56 o 19 2 1 94.71 71.99 12.51 o 20 2 1 1.35 -1.59 6.78 o -19 3 1 62.83 83.73 19.46 o -18 3 1 4.61 -8.00 8.41 o -17 3 1 1.08 -5.89 11.93 o -16 3 1 28.50 32.39 5.37 o -15 3 1 13.69 9.85 5.26 o -14 3 1 77.33 69.26 6.55 o -13 3 1 287.83 279.51 6.77 o -12 3 1 827.17 890.38 17.81 o -11 3 1 74.52 60.06 2.99 o -10 3 1 87.92 83.33 4.11 o -9 3 1 545.89 604.13 11.58 o -8 3 1 163.88 151.17 6.94 o -7 3 1 56.67 53.24 2.05 o -6 3 1 31.04 27.75 1.63 o -5 3 1 282.80 258.79 6.59 o -4 3 1 493.55 503.01 10.75 o -3 3 1 154.74 140.83 3.23 o -2 3 1 .83 1.76 1.08 o -1 3 1 13.44 13.01 1.42 o 0 3 1 251.66 256.39 5.80 o 1 3 1 1127.47 1165.74 24.72 o 2 3 1 129.50 114.21 3.18 o 3 3 1 2.88 1.29 1.45 o 4 3 1 515.82 545.23 11.76 o 5 3 1 85.22 86.03 2.99 o 6 3 1 186.87 153.80 4.09 o 7 3 1 66.40 53.58 2.64 o 8 3 1 440.11 423.44 7.16 o 9 3 1 4.82 5.70 1.56 o 10 3 1 23.97 23.22 2.74 o 11 3 1 942.74 1018.74 20.99 o 12 3 1 1736.61 1858.02 38.87 o 13 3 1 90.37 74.67 4.50 o 14 3 1 108.50 114.89 5.98 o 15 3 1 80.28 77.56 6.45 o 16 3 1 6.96 13.60 5.45 o 17 3 1 6.76 22.15 6.90 o 18 3 1 21.23 18.29 8.02 o 19 3 1 .26 -.81 23.17 o -17 4 1 167.15 156.14 11.18 o -16 4 1 3.31 3.28 8.30 o -15 4 1 424.87 448.18 18.10 o -14 4 1 519.78 531.15 23.76 o -13 4 1 53.73 76.12 7.50 o -12 4 1 246.61 232.93 9.20 o -11 4 1 88.65 94.32 12.51 o -10 4 1 204.78 217.05 10.75 o -9 4 1 1255.89 1347.57 46.05 o -8 4 1 510.49 531.66 15.21 o -7 4 1 775.05 801.82 20.73 o -6 4 1 9.06 8.21 3.72 o -5 4 1 1220.10 1267.49 34.81 o -4 4 1 1121.24 1161.52 25.82 o -3 4 1 1848.01 2012.40 48.41 o -2 4 1 34.59 29.15 2.25 o -1 4 1 346.51 368.36 8.07 o 0 4 1 176.27 148.22 4.50 o 1 4 1 1331.27 1347.43 22.51 o 2 4 1 113.54 105.26 3.33 o 3 4 1 515.18 515.44 12.91 o 4 4 1 10.28 14.01 8.11 o 5 4 1 200.74 192.04 5.87 o 6 4 1 126.73 118.50 5.08 o 7 4 1 289.78 292.69 8.41 o 8 4 1 10.96 12.45 10.56 o 9 4 1 192.72 181.15 6.86 o 10 4 1 126.10 127.78 6.01 o 11 4 1 25.65 19.95 4.50 o 12 4 1 712.49 785.31 20.71 o 13 4 1 254.81 273.65 11.54 o 14 4 1 121.26 101.01 7.37 o 15 4 1 243.34 229.04 18.19 o 16 4 1 45.32 64.77 10.27 o 17 4 1 64.70 48.08 8.64 o -14 5 1 .52 -1.17 10.36 o -13 5 1 1.23 -4.99 9.58 o -12 5 1 128.36 152.92 10.16 o -11 5 1 59.99 53.61 8.17 o -10 5 1 46.30 43.10 8.77 o -9 5 1 12.51 -7.89 8.57 o -8 5 1 106.56 118.75 7.46 o -7 5 1 91.21 96.84 8.02 o -6 5 1 2.69 3.39 6.65 o -5 5 1 119.19 119.55 9.68 o -4 5 1 29.62 20.90 4.65 o -3 5 1 37.06 41.79 8.90 o -2 5 1 132.65 127.44 16.52 o -1 5 1 508.78 567.85 18.58 o 0 5 1 165.36 170.70 6.58 o 1 5 1 50.14 37.54 4.11 o 2 5 1 54.29 49.14 12.71 o 3 5 1 123.02 127.30 7.23 o 4 5 1 167.76 172.07 7.29 o 5 5 1 335.61 352.83 10.82 o 6 5 1 15.56 9.91 4.93 o 7 5 1 5.33 4.50 5.87 o 8 5 1 97.54 98.36 7.82 o 9 5 1 96.98 141.38 14.08 o 10 5 1 68.67 50.46 8.92 o 11 5 1 3.80 4.79 7.63 o 12 5 1 23.53 5.48 8.60 o 13 5 1 13.61 17.26 8.52 o 14 5 1 236.83 257.38 17.70 o -9 6 1 60.52 66.29 14.27 o -8 6 1 169.97 167.38 18.19 o -7 6 1 10.73 -3.08 9.35 o -6 6 1 12.70 -3.32 10.75 o -5 6 1 32.13 22.20 10.10 o -4 6 1 56.74 38.48 7.45 o -3 6 1 19.34 21.51 9.19 o -2 6 1 72.67 77.81 11.83 o -1 6 1 255.31 304.05 11.78 o 0 6 1 40.43 32.66 8.02 o 1 6 1 40.65 36.37 8.41 o 2 6 1 596.88 684.04 41.75 o 3 6 1 157.51 187.33 11.34 o 4 6 1 4.22 5.28 7.04 o 5 6 1 7.32 5.10 7.56 o 6 6 1 .07 16.93 8.07 o 7 6 1 36.67 38.33 9.58 o 8 6 1 24.48 -1.37 10.17 o 9 6 1 27.53 28.11 11.45 o -21 0 2 1152.36 1205.50 41.45 o -20 0 2 488.85 516.81 16.62 o -19 0 2 243.50 241.10 9.58 o -18 0 2 130.43 132.18 6.65 o -17 0 2 900.69 995.30 29.92 o -16 0 2 251.19 272.78 8.80 o -15 0 2 516.31 554.75 16.62 o -14 0 2 137.78 123.19 5.48 o -13 0 2 266.44 289.40 9.78 o -12 0 2 1708.48 1850.79 50.06 o -11 0 2 306.08 349.82 10.17 o -10 0 2 146.95 192.22 5.48 o -9 0 2 966.27 896.16 17.79 o -8 0 2 566.18 516.81 11.15 o -7 0 2 2125.82 2072.53 38.52 o -6 0 2 3872.01 3771.38 62.77 o -5 0 2 1484.96 1427.25 25.22 o -4 0 2 44.28 61.40 1.37 o -3 0 2 433.35 509.19 8.02 o -2 0 2 313.99 400.86 6.45 o -1 0 2 9043.96 8705.05 161.91 o 0 0 2 205.40 221.55 3.52 o 1 0 2 1204.66 1110.47 15.06 o 2 0 2 412.42 373.29 6.65 o 3 0 2 822.63 632.77 10.17 o 4 0 2 5078.87 4888.11 79.98 o 5 0 2 32.57 33.44 .98 o 6 0 2 25.58 27.96 1.17 o 7 0 2 3211.02 3037.91 51.23 o 8 0 2 85.77 66.09 2.15 o 9 0 2 3103.88 3297.59 67.66 o 10 0 2 27.22 33.05 2.54 o 11 0 2 6.95 2.93 2.15 o 12 0 2 1349.09 1578.59 39.30 o 13 0 2 627.38 669.72 20.53 o 14 0 2 81.32 94.45 5.87 o 15 0 2 182.74 189.09 8.60 o 16 0 2 286.60 332.22 16.43 o 17 0 2 139.75 131.21 8.60 o 18 0 2 37.09 46.93 7.82 o 19 0 2 87.58 77.63 11.15 o 20 0 2 9.53 5.87 8.41 o 21 0 2 .24 -2.54 13.69 o -21 1 2 21.40 21.32 9.29 o -20 1 2 23.78 25.36 5.12 o -19 1 2 10.55 10.55 4.42 o -18 1 2 198.52 206.02 6.18 o -17 1 2 110.34 90.70 4.42 o -16 1 2 2.12 .23 2.75 o -15 1 2 345.19 371.97 17.11 o -14 1 2 9.58 5.60 2.25 o -13 1 2 102.85 101.52 4.69 o -12 1 2 149.35 130.58 3.33 o -11 1 2 64.67 55.98 2.16 o -10 1 2 820.69 775.18 13.73 o -9 1 2 310.21 268.88 4.04 o -8 1 2 313.02 328.44 6.26 o -7 1 2 86.02 90.84 1.73 o -6 1 2 1.95 1.80 1.66 o -5 1 2 903.96 1033.02 12.36 o -4 1 2 8363.86 8082.95 180.29 o -3 1 2 2712.35 2699.55 35.00 o -2 1 2 680.82 700.64 31.58 o -1 1 2 487.11 506.56 8.21 o 0 1 2 630.51 661.68 12.51 o 1 1 2 76.99 69.52 1.56 o 2 1 2 4515.94 4429.32 63.75 o 3 1 2 4299.67 4135.51 57.30 o 4 1 2 9278.45 9223.60 133.40 o 5 1 2 607.19 572.17 11.93 o 6 1 2 110.26 92.03 1.72 o 7 1 2 959.09 1011.93 13.24 o 8 1 2 106.79 96.21 2.00 o 9 1 2 2512.92 2691.86 52.89 o 10 1 2 218.03 225.93 4.56 o 11 1 2 279.31 276.93 6.26 o 12 1 2 270.62 258.09 5.68 o 13 1 2 59.82 48.26 2.71 o 14 1 2 77.68 74.62 3.87 o 15 1 2 645.07 640.26 16.50 o 16 1 2 47.24 46.53 4.22 o 17 1 2 6.01 5.06 7.04 o 18 1 2 1.37 2.60 7.52 o 19 1 2 141.25 144.20 23.95 o 20 1 2 4.61 12.61 21.41 o 21 1 2 1.57 13.79 8.59 o -20 2 2 6.59 12.61 6.74 o -19 2 2 7.22 2.84 5.59 o -18 2 2 .11 9.34 5.39 o -17 2 2 128.17 120.46 5.73 o -16 2 2 159.22 167.82 6.46 o -15 2 2 15.53 16.44 2.72 o -14 2 2 887.10 977.66 20.57 o -13 2 2 90.02 84.74 3.17 o -12 2 2 1180.03 1243.16 25.13 o -11 2 2 9.03 4.41 1.69 o -10 2 2 153.02 128.47 9.78 o -9 2 2 24.56 20.90 1.56 o -8 2 2 1284.16 1389.29 32.46 o -7 2 2 2965.52 3159.31 42.93 o -6 2 2 254.91 234.81 3.33 o -5 2 2 388.84 347.17 10.75 o -4 2 2 152.32 172.32 2.77 o -3 2 2 1964.48 1925.18 27.44 o -2 2 2 35.70 32.40 1.03 o -1 2 2 3569.02 3511.12 58.07 o 0 2 2 567.02 524.38 8.35 o 1 2 2 504.23 501.70 8.09 o 2 2 2 228.95 204.24 3.32 o 3 2 2 104.48 85.43 2.08 o 4 2 2 1742.70 1704.43 33.24 o 5 2 2 2034.59 2232.21 30.76 o 6 2 2 262.65 294.00 4.54 o 7 2 2 1234.55 1280.28 18.76 o 8 2 2 289.69 284.80 6.55 o 9 2 2 399.34 378.82 8.90 o 10 2 2 223.84 218.77 4.98 o 11 2 2 9.07 10.44 2.60 o 12 2 2 45.86 35.06 2.96 o 13 2 2 184.69 194.34 6.28 o 14 2 2 12.47 6.65 2.86 o 15 2 2 4.81 3.83 3.58 o 16 2 2 38.37 27.71 4.83 o 17 2 2 41.21 37.95 5.18 o 18 2 2 150.59 140.85 9.97 o 19 2 2 21.68 30.05 12.81 o 20 2 2 1.40 -8.16 8.16 o -19 3 2 89.58 81.30 9.25 o -18 3 2 34.98 20.11 7.65 o -17 3 2 266.47 301.31 19.95 o -16 3 2 157.66 156.63 7.27 o -15 3 2 291.06 354.36 33.83 o -14 3 2 190.33 216.49 7.88 o -13 3 2 44.71 46.90 4.01 o -12 3 2 297.64 288.22 7.93 o -11 3 2 3725.17 4089.26 101.07 o -10 3 2 194.50 190.74 4.04 o -9 3 2 104.91 87.13 8.21 o -8 3 2 110.69 106.28 2.81 o -7 3 2 787.80 745.52 15.87 o -6 3 2 1108.88 988.49 18.51 o -5 3 2 760.58 758.89 14.75 o -4 3 2 53.02 56.02 1.97 o -3 3 2 269.86 261.77 6.65 o -2 3 2 362.26 310.11 13.69 o -1 3 2 2601.73 2572.94 52.67 o 0 3 2 1630.40 1831.91 40.31 o 1 3 2 243.14 213.75 4.08 o 2 3 2 .19 2.31 1.27 o 3 3 2 256.60 191.46 4.02 o 4 3 2 1134.28 1149.91 23.41 o 5 3 2 945.67 959.80 19.54 o 6 3 2 154.88 147.54 4.45 o 7 3 2 422.19 452.41 11.54 o 8 3 2 170.81 150.29 4.11 o 9 3 2 186.18 167.67 5.28 o 10 3 2 88.35 86.79 2.96 o 11 3 2 948.86 1108.77 24.20 o 12 3 2 344.32 325.54 8.43 o 13 3 2 137.16 135.34 5.43 o 14 3 2 291.57 278.13 11.54 o 15 3 2 403.23 434.84 12.53 o 16 3 2 194.64 206.11 12.42 o 17 3 2 59.81 60.62 10.46 o 18 3 2 40.38 48.44 8.26 o 19 3 2 124.16 95.45 13.60 o -17 4 2 59.72 63.99 10.71 o -16 4 2 339.17 378.77 22.49 o -15 4 2 115.73 108.35 10.95 o -14 4 2 5.54 12.01 6.99 o -13 4 2 5.63 3.54 11.54 o -12 4 2 23.86 22.68 7.04 o -11 4 2 74.91 89.41 6.51 o -10 4 2 .83 .98 5.28 o -9 4 2 32.15 32.36 5.49 o -8 4 2 48.86 46.27 4.12 o -7 4 2 212.71 228.89 12.42 o -6 4 2 1390.81 1498.42 46.54 o -5 4 2 622.76 688.62 25.52 o -4 4 2 342.97 370.35 10.18 o -3 4 2 674.03 678.62 14.04 o -2 4 2 241.94 253.03 6.26 o -1 4 2 163.46 147.05 5.67 o 0 4 2 109.56 105.59 3.91 o 1 4 2 .62 1.02 1.16 o 2 4 2 172.00 160.04 15.06 o 3 4 2 44.36 40.14 3.62 o 4 4 2 147.26 149.54 4.94 o 5 4 2 122.72 111.53 4.53 o 6 4 2 303.12 309.77 10.66 o 7 4 2 129.71 119.34 4.59 o 8 4 2 661.80 647.99 24.74 o 9 4 2 27.15 20.17 4.50 o 10 4 2 28.47 34.89 4.38 o 11 4 2 2.78 -1.56 2.99 o 12 4 2 150.01 163.80 7.89 o 13 4 2 19.43 11.13 5.96 o 14 4 2 15.92 4.33 6.54 o 15 4 2 6.56 3.63 6.76 o 16 4 2 124.86 123.88 10.11 o 17 4 2 .14 2.40 6.98 o -14 5 2 81.78 84.02 11.34 o -13 5 2 88.38 89.17 11.34 o -12 5 2 1.86 20.40 7.97 o -11 5 2 81.42 86.11 12.12 o -10 5 2 81.46 75.05 13.10 o -9 5 2 41.52 23.87 16.13 o -8 5 2 81.10 83.50 10.75 o -7 5 2 191.37 191.82 9.97 o -6 5 2 132.32 146.07 8.80 o -5 5 2 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