#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:11:47 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180829 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/60/2016090.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016090_Fobs loop_ _publ_author_name 'Mague, Joel T.' 'Balakrishna, Maravanji S.' 'Punji, Banudhar' 'Suresh, Devarajan' _publ_section_title ; Two crystalline modifications of 1,1'-thiobis(2-naphthol) ; _journal_coeditor_code FA3098 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o487 _journal_page_last o488 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.181 _cell_angle_gamma 90.000 _cell_length_a 4.8053 _cell_length_b 11.4200 _cell_length_c 26.7318 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file fa3098Iasup2.hkl _cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' msb278 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 251.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 223.42 217.10 11.66 o 4 0 0 183.75 159.50 20.37 o 6 0 0 272.49 278.16 47.19 o 1 1 0 115.92 131.67 5.88 o 2 1 0 1049.39 998.98 15.74 o 3 1 0 2641.26 2664.70 36.13 o 4 1 0 11.41 14.00 8.36 o 5 1 0 133.36 180.22 34.01 o 6 1 0 116.93 103.18 25.67 o 0 2 0 10072.64 10721.70 121.69 o 1 2 0 61.02 64.99 8.03 o 2 2 0 0.69 -1.17 4.97 o 3 2 0 130.23 136.62 8.99 o 4 2 0 486.89 468.02 17.15 o 5 2 0 249.34 279.60 29.65 o 6 2 0 0.83 4.22 22.05 o 1 3 0 30.08 34.47 4.77 o 2 3 0 2218.33 2093.94 25.25 o 3 3 0 15.37 14.16 6.41 o 4 3 0 22.97 12.57 9.13 o 5 3 0 438.84 518.09 35.31 o 6 3 0 120.44 143.84 29.08 o 0 4 0 1808.07 1694.86 27.16 o 1 4 0 3339.76 3522.33 34.75 o 2 4 0 34.29 24.89 5.67 o 3 4 0 129.87 134.18 9.00 o 4 4 0 193.11 218.01 14.05 o 5 4 0 528.39 521.49 45.41 o 1 5 0 97.35 142.74 7.23 o 2 5 0 266.10 244.18 10.66 o 3 5 0 243.91 243.43 13.36 o 4 5 0 75.86 97.77 12.12 o 5 5 0 512.93 445.29 53.19 o 0 6 0 4.98 9.13 6.48 o 1 6 0 188.71 150.89 9.31 o 2 6 0 147.72 169.26 9.45 o 3 6 0 828.10 839.06 24.63 o 4 6 0 16.24 31.10 11.84 o 5 6 0 367.52 386.57 51.57 o 1 7 0 19.50 22.55 6.82 o 2 7 0 399.50 368.26 14.88 o 3 7 0 1.59 -7.97 9.62 o 4 7 0 0.66 -11.41 11.41 o 5 7 0 59.56 56.65 34.15 o 0 8 0 681.61 600.32 30.34 o 1 8 0 680.16 669.41 21.20 o 2 8 0 809.16 727.39 19.94 o 3 8 0 271.29 266.23 18.01 o 4 8 0 167.45 152.90 17.71 o 5 8 0 378.44 461.96 40.45 o 1 9 0 42.15 47.25 10.66 o 2 9 0 6.31 2.72 9.71 o 3 9 0 773.64 718.63 26.15 o 4 9 0 1.80 10.61 14.07 o 0 10 0 543.52 539.85 64.69 o 1 10 0 373.39 331.88 18.62 o 2 10 0 55.98 40.56 11.94 o 3 10 0 5.27 13.50 15.51 o 4 10 0 95.37 95.75 20.98 o 1 11 0 38.20 75.80 37.00 o 2 11 0 433.43 452.14 26.70 o 3 11 0 103.59 123.68 20.47 o 4 11 0 2.23 29.76 23.05 o 0 12 0 7.57 17.45 28.85 o 1 12 0 249.36 300.81 20.22 o 2 12 0 62.68 53.84 17.19 o 3 12 0 149.93 136.06 29.97 o 1 13 0 16.02 9.48 16.07 o 2 13 0 137.34 157.39 22.96 o 3 13 0 104.11 122.86 27.05 o 0 14 0 177.59 142.45 38.46 o 1 14 0 7.12 -3.30 14.19 o 2 14 0 27.11 28.72 31.62 o -5 0 1 495.53 493.64 32.66 o -3 0 1 111.53 118.89 11.30 o -1 0 1 9.89 12.01 4.66 o 1 0 1 3671.84 3863.44 48.11 o 3 0 1 4764.28 5044.03 72.32 o 5 0 1 246.87 226.79 40.45 o -6 1 1 26.48 16.92 24.67 o -5 1 1 17.51 14.67 14.32 o -4 1 1 15.29 8.86 10.78 o -3 1 1 205.56 198.11 10.20 o -2 1 1 220.57 238.65 8.45 o -1 1 1 2142.35 2115.20 20.80 o 0 1 1 4775.06 5213.97 52.08 o 1 1 1 1873.78 1986.36 20.08 o 2 1 1 905.27 861.32 15.50 o 3 1 1 449.70 504.47 16.17 o 4 1 1 479.47 470.37 17.13 o 5 1 1 12.58 31.05 20.66 o 6 1 1 12.07 17.17 23.94 o -6 2 1 45.97 25.74 25.15 o -5 2 1 134.44 123.14 24.96 o -4 2 1 4.23 -4.20 7.46 o -3 2 1 262.25 270.95 10.66 o -2 2 1 4428.48 4485.62 47.35 o -1 2 1 639.31 582.42 9.87 o 0 2 1 243.21 238.10 6.30 o 1 2 1 1372.75 1391.88 16.38 o 2 2 1 346.67 315.43 9.86 o 3 2 1 1112.73 1124.21 19.49 o 4 2 1 1097.71 1002.58 32.52 o 5 2 1 5.96 26.28 18.31 o 6 2 1 72.46 122.53 28.56 o -6 3 1 24.93 24.19 26.29 o -5 3 1 58.99 95.33 41.03 o -4 3 1 339.12 304.16 17.70 o -3 3 1 713.15 662.66 15.11 o -2 3 1 344.45 313.28 9.92 o -1 3 1 10.28 15.45 4.50 o 0 3 1 1388.49 1328.28 15.05 o 1 3 1 989.83 937.58 13.65 o 2 3 1 358.79 367.21 10.74 o 3 3 1 89.87 91.18 9.89 o 4 3 1 463.43 456.26 19.54 o 5 3 1 0.97 -9.47 16.58 o 6 3 1 13.96 10.55 22.74 o -5 4 1 53.51 31.19 15.79 o -4 4 1 239.40 275.18 15.08 o -3 4 1 26.60 30.14 7.96 o -2 4 1 3317.64 3496.63 37.02 o -1 4 1 2233.53 2342.52 25.36 o 0 4 1 1185.89 1169.05 17.37 o 1 4 1 287.66 277.41 8.66 o 2 4 1 1638.32 1604.18 21.95 o 3 4 1 23.88 28.63 6.85 o 4 4 1 1796.65 1798.00 32.79 o 5 4 1 111.63 119.58 65.83 o -5 5 1 106.65 139.05 25.03 o -4 5 1 1019.39 1057.36 27.82 o -3 5 1 1362.95 1269.76 31.56 o -2 5 1 384.12 407.16 11.61 o -1 5 1 9.49 7.85 5.94 o 0 5 1 514.76 428.64 9.17 o 1 5 1 124.44 134.86 7.35 o 2 5 1 2057.87 2165.53 32.83 o 3 5 1 276.47 278.36 12.25 o 4 5 1 1560.71 1618.39 33.79 o 5 5 1 169.17 194.16 40.85 o -5 6 1 8.19 35.46 19.84 o -4 6 1 0.55 25.54 11.81 o -3 6 1 107.74 122.82 15.03 o -2 6 1 5.07 5.80 6.41 o -1 6 1 530.75 505.55 13.92 o 0 6 1 7.32 8.89 5.43 o 1 6 1 195.19 236.78 8.70 o 2 6 1 9.78 15.36 6.14 o 3 6 1 78.49 66.14 11.52 o 4 6 1 6.29 18.41 15.22 o 5 6 1 0.06 35.93 21.78 o -5 7 1 226.40 215.26 28.98 o -4 7 1 91.30 109.28 15.38 o -3 7 1 2.99 12.01 14.58 o -2 7 1 1408.46 1296.84 45.22 o -1 7 1 257.19 254.18 11.76 o 0 7 1 15.55 22.56 6.14 o 1 7 1 1153.88 1186.92 21.96 o 2 7 1 780.99 769.07 19.55 o 3 7 1 865.33 866.92 25.92 o 4 7 1 179.86 194.79 19.83 o 5 7 1 233.49 321.62 58.21 o -5 8 1 521.33 659.09 35.07 o -4 8 1 1.19 -0.37 11.97 o -3 8 1 271.12 292.87 19.61 o -2 8 1 521.40 478.14 22.23 o -1 8 1 2004.29 1920.90 30.50 o 0 8 1 0.99 -7.13 7.13 o 1 8 1 56.51 111.98 33.27 o 2 8 1 133.30 142.09 11.53 o 3 8 1 0.29 -3.50 9.90 o 4 8 1 31.17 15.50 13.14 o 5 8 1 83.95 92.90 47.19 o -4 9 1 265.04 259.86 21.71 o -3 9 1 576.04 522.70 23.29 o -2 9 1 1759.40 1620.71 35.52 o -1 9 1 0.97 -1.56 8.58 o 0 9 1 66.30 77.14 11.76 o 1 9 1 23.12 45.39 11.40 o 2 9 1 0.07 -7.60 9.41 o 3 9 1 209.30 191.02 30.07 o 4 9 1 390.67 344.52 26.84 o -4 10 1 24.04 28.85 17.56 o -3 10 1 607.61 512.16 29.07 o -2 10 1 41.97 28.68 14.80 o -1 10 1 77.64 94.71 17.27 o 0 10 1 36.28 28.04 10.63 o 1 10 1 0.22 -6.85 11.73 o 2 10 1 48.26 46.66 12.25 o 3 10 1 464.56 504.89 29.57 o 4 10 1 89.32 86.64 39.67 o -4 11 1 92.71 79.94 27.03 o -3 11 1 163.50 166.23 25.05 o -2 11 1 5.44 -0.13 13.57 o -1 11 1 128.45 132.08 15.32 o 0 11 1 981.35 1042.53 37.30 o 1 11 1 552.89 560.36 23.59 o 2 11 1 48.71 33.98 15.45 o 3 11 1 0.01 -2.68 15.06 o 4 11 1 68.64 93.78 29.16 o -3 12 1 0.90 -3.63 15.74 o -2 12 1 241.52 285.57 24.31 o -1 12 1 20.09 29.80 12.31 o 0 12 1 194.28 216.65 18.96 o 1 12 1 26.51 36.07 13.64 o 2 12 1 395.27 417.36 37.15 o 3 12 1 1.34 7.10 21.17 o -3 13 1 228.56 250.79 48.68 o -2 13 1 6.54 -13.47 15.39 o -1 13 1 189.55 196.33 19.63 o 0 13 1 28.88 32.80 16.51 o 1 13 1 764.46 828.13 47.57 o 2 13 1 22.02 16.24 16.54 o -2 14 1 23.40 91.96 39.64 o -1 14 1 384.37 455.06 31.15 o 0 14 1 50.51 67.67 16.78 o 1 14 1 161.29 205.33 21.84 o 2 14 1 117.72 140.63 41.66 o -6 0 2 23.99 -27.17 27.17 o -4 0 2 13.39 21.86 14.28 o -2 0 2 2402.11 2482.03 48.67 o 0 0 2 4108.98 4457.84 63.26 o 2 0 2 3148.08 3256.22 47.10 o 4 0 2 337.46 327.02 19.53 o 6 0 2 1204.44 1406.66 86.16 o -6 1 2 236.38 267.80 34.30 o -5 1 2 387.08 398.41 24.12 o -4 1 2 1.44 -8.96 8.96 o -3 1 2 360.90 360.80 11.39 o -2 1 2 1682.75 1709.89 20.78 o -1 1 2 1139.78 1142.31 15.13 o 0 1 2 3439.11 3691.81 33.89 o 1 1 2 9716.10 10531.32 85.38 o 2 1 2 1099.32 1140.58 16.68 o 3 1 2 32.64 58.33 6.77 o 4 1 2 998.72 980.21 22.95 o 5 1 2 20.18 -13.54 42.07 o 6 1 2 15.95 10.93 21.40 o -6 2 2 0.78 -17.44 22.04 o -5 2 2 30.06 27.03 13.25 o -4 2 2 333.11 320.32 15.01 o -3 2 2 4.27 16.74 5.85 o -2 2 2 0.13 3.24 4.62 o -1 2 2 2.54 0.95 3.82 o 0 2 2 2705.51 2871.72 28.35 o 1 2 2 19767.48 20975.89 165.79 o 2 2 2 1207.28 1163.37 17.38 o 3 2 2 0.34 2.79 5.23 o 4 2 2 211.78 196.76 13.42 o 5 2 2 23.78 8.20 18.65 o 6 2 2 73.65 100.02 26.16 o -6 3 2 96.27 71.42 24.48 o -5 3 2 180.81 154.09 17.52 o -4 3 2 27.07 33.83 9.59 o -3 3 2 96.33 92.95 9.25 o -2 3 2 215.10 178.35 9.43 o -1 3 2 547.44 511.56 9.80 o 0 3 2 175.02 162.22 7.33 o 1 3 2 62.61 73.03 5.48 o 2 3 2 1190.36 1174.31 17.98 o 3 3 2 15.14 16.97 6.79 o 4 3 2 591.02 581.26 21.96 o 5 3 2 59.98 62.75 21.75 o 6 3 2 4.14 19.89 37.48 o -5 4 2 529.19 551.41 29.27 o -4 4 2 6.25 -7.69 8.83 o -3 4 2 1163.21 1126.02 22.89 o -2 4 2 105.17 82.83 6.62 o -1 4 2 127.47 128.47 8.08 o 0 4 2 650.54 613.36 13.22 o 1 4 2 425.02 378.59 11.66 o 2 4 2 71.47 78.08 6.99 o 3 4 2 351.84 333.75 12.40 o 4 4 2 105.68 105.89 12.13 o 5 4 2 529.11 617.96 40.09 o -5 5 2 1464.63 1458.42 55.46 o -4 5 2 398.20 385.61 19.72 o -3 5 2 267.27 261.80 13.29 o -2 5 2 45.64 53.18 6.32 o -1 5 2 120.08 129.09 8.57 o 0 5 2 1881.12 1865.49 25.31 o 1 5 2 3951.61 4674.96 45.29 o 2 5 2 282.03 270.81 10.92 o 3 5 2 13.57 1.22 6.76 o 4 5 2 74.07 87.10 11.79 o 5 5 2 4.79 -4.86 17.82 o -5 6 2 269.37 270.41 29.07 o -4 6 2 0.13 3.67 11.11 o -3 6 2 641.64 620.53 21.71 o -2 6 2 277.30 247.24 12.00 o -1 6 2 786.81 803.90 17.31 o 0 6 2 122.77 111.94 8.33 o 1 6 2 352.85 310.58 9.88 o 2 6 2 1285.25 1238.25 20.61 o 3 6 2 0.02 -7.29 7.29 o 4 6 2 103.27 94.06 13.85 o 5 6 2 38.73 0.39 20.20 o -5 7 2 830.53 895.38 88.99 o -4 7 2 0.68 -10.90 10.90 o -3 7 2 10.87 20.75 14.59 o -2 7 2 348.65 363.82 14.21 o -1 7 2 2001.96 2095.23 31.12 o 0 7 2 39.64 28.35 6.52 o 1 7 2 568.99 556.84 15.40 o 2 7 2 767.11 757.89 22.94 o 3 7 2 4.37 -2.19 9.47 o 4 7 2 65.27 60.20 16.06 o 5 7 2 319.54 301.29 34.28 o -5 8 2 22.23 10.70 19.89 o -4 8 2 7.73 12.11 12.57 o -3 8 2 123.21 102.92 14.11 o -2 8 2 1241.29 1117.64 24.45 o -1 8 2 266.26 226.31 12.23 o 0 8 2 323.95 320.02 19.53 o 1 8 2 784.02 767.05 22.57 o 2 8 2 1983.29 1893.50 37.48 o 3 8 2 11.71 9.78 10.41 o 4 8 2 60.28 77.20 20.18 o 5 8 2 0.02 -10.34 21.59 o -4 9 2 577.49 619.29 41.11 o -3 9 2 47.82 42.59 13.29 o -2 9 2 5.63 12.63 11.93 o -1 9 2 5006.08 4923.68 105.57 o 0 9 2 2580.28 2488.39 54.77 o 1 9 2 359.38 374.41 18.07 o 2 9 2 22.07 4.34 10.07 o 3 9 2 671.35 684.73 30.56 o 4 9 2 18.41 29.72 19.15 o -4 10 2 282.94 250.57 26.02 o -3 10 2 74.45 83.21 18.59 o -2 10 2 333.56 342.58 23.45 o -1 10 2 40.22 22.39 10.43 o 0 10 2 244.71 239.11 17.03 o 1 10 2 331.59 314.87 18.17 o 2 10 2 443.23 445.90 21.19 o 3 10 2 26.60 32.87 15.70 o 4 10 2 99.20 100.69 25.17 o -4 11 2 286.81 303.57 29.34 o -3 11 2 183.03 178.71 29.95 o -2 11 2 116.11 112.22 18.95 o -1 11 2 897.10 929.28 29.16 o 0 11 2 14.61 15.74 11.04 o 1 11 2 8.52 -13.12 13.12 o 2 11 2 130.05 150.84 18.40 o 3 11 2 379.25 314.16 25.67 o 4 11 2 217.33 157.25 29.35 o -3 12 2 210.65 185.47 26.06 o -2 12 2 13.67 11.74 15.42 o -1 12 2 0.25 -10.96 10.96 o 0 12 2 0.01 -5.67 11.40 o 1 12 2 326.23 338.68 21.21 o 2 12 2 41.71 63.57 17.61 o 3 12 2 95.39 88.61 31.17 o -3 13 2 8.06 35.66 35.46 o -2 13 2 109.70 107.80 20.55 o -1 13 2 191.21 183.18 19.98 o 0 13 2 643.29 709.15 46.39 o 1 13 2 58.36 89.70 16.34 o 2 13 2 10.71 -10.85 22.74 o -2 14 2 0.29 -29.39 29.39 o -1 14 2 268.70 296.23 28.18 o 0 14 2 3.87 7.15 14.47 o 1 14 2 151.33 199.12 21.73 o 2 14 2 3.49 33.91 36.41 o -5 0 3 265.45 326.81 30.19 o -3 0 3 7099.52 7396.49 97.20 o -1 0 3 6026.80 6117.32 72.57 o 1 0 3 423.26 432.78 15.44 o 3 0 3 571.41 597.74 39.11 o 5 0 3 887.04 956.51 63.71 o -6 1 3 14.12 22.91 51.03 o -5 1 3 23.17 6.20 12.23 o -4 1 3 222.24 210.05 15.61 o -3 1 3 326.25 356.44 11.20 o -2 1 3 779.63 701.52 12.38 o -1 1 3 7115.05 7435.60 68.30 o 0 1 3 1104.86 1185.71 12.20 o 1 1 3 16.33 14.76 4.00 o 2 1 3 365.34 327.45 9.69 o 3 1 3 494.77 505.61 13.29 o 4 1 3 0.10 -0.04 7.32 o 5 1 3 0.01 -5.69 47.09 o 6 1 3 344.52 409.42 53.12 o -6 2 3 28.87 9.96 22.95 o -5 2 3 81.03 104.54 20.62 o -4 2 3 117.24 116.45 13.50 o -3 2 3 892.11 895.46 16.81 o -2 2 3 4.99 -1.41 6.03 o -1 2 3 475.88 459.28 8.56 o 0 2 3 6410.81 6856.17 56.84 o 1 2 3 768.65 746.96 11.74 o 2 2 3 1247.08 1301.09 18.52 o 3 2 3 11.18 12.51 5.81 o 4 2 3 1385.98 1320.59 38.38 o 5 2 3 15.17 40.44 19.20 o 6 2 3 15.19 39.66 23.71 o -6 3 3 14.58 7.28 23.90 o -5 3 3 27.08 42.11 13.88 o -4 3 3 31.36 43.25 9.80 o -3 3 3 76.13 66.73 10.10 o -2 3 3 1513.19 1487.06 20.25 o -1 3 3 132.82 126.00 7.86 o 0 3 3 560.29 545.36 11.21 o 1 3 3 196.54 187.14 7.77 o 2 3 3 179.64 187.71 9.16 o 3 3 3 364.25 379.54 12.56 o 4 3 3 21.21 15.52 9.68 o 5 3 3 172.64 138.12 25.18 o 6 3 3 21.28 -32.90 32.90 o -5 4 3 194.02 198.85 19.00 o -4 4 3 1011.78 989.86 24.54 o -3 4 3 364.44 364.28 14.50 o -2 4 3 1251.19 1307.19 19.00 o -1 4 3 495.01 502.33 14.41 o 0 4 3 3123.93 3177.61 35.30 o 1 4 3 485.49 509.47 11.21 o 2 4 3 171.28 178.90 9.17 o 3 4 3 36.05 35.99 7.89 o 4 4 3 2645.61 2570.21 41.05 o 5 4 3 41.42 40.01 16.51 o -5 5 3 1.05 -2.50 15.52 o -4 5 3 87.74 99.42 13.76 o -3 5 3 483.50 471.73 16.00 o -2 5 3 1151.89 1252.47 19.26 o -1 5 3 1642.02 1627.28 24.25 o 0 5 3 462.55 484.15 12.58 o 1 5 3 105.45 101.29 6.82 o 2 5 3 395.28 381.82 11.94 o 3 5 3 1875.24 1814.05 27.63 o 4 5 3 892.32 911.69 46.41 o 5 5 3 42.90 43.90 21.19 o -5 6 3 28.06 29.65 28.65 o -4 6 3 424.23 421.27 21.19 o -3 6 3 975.83 925.41 25.95 o -2 6 3 168.49 157.75 10.55 o -1 6 3 13.22 15.65 6.29 o 0 6 3 3861.52 4042.81 42.37 o 1 6 3 159.72 136.31 8.08 o 2 6 3 1050.58 1084.84 21.06 o 3 6 3 615.59 569.62 16.18 o 4 6 3 808.48 816.68 31.68 o 5 6 3 64.41 76.95 22.81 o -5 7 3 222.72 236.69 29.70 o -4 7 3 141.25 156.28 17.27 o -3 7 3 18.55 10.90 11.90 o -2 7 3 726.61 649.98 17.75 o -1 7 3 87.36 92.34 8.99 o 0 7 3 83.60 92.61 8.36 o 1 7 3 199.96 178.74 9.15 o 2 7 3 538.19 487.11 16.06 o 3 7 3 160.99 159.35 16.78 o 4 7 3 775.89 708.22 40.82 o 5 7 3 0.01 36.10 22.31 o -5 8 3 93.03 126.63 25.45 o -4 8 3 44.28 46.09 13.85 o -3 8 3 363.27 356.64 22.85 o -2 8 3 279.78 284.72 14.14 o -1 8 3 1108.47 1083.40 22.73 o 0 8 3 217.01 207.65 13.60 o 1 8 3 309.77 273.31 18.57 o 2 8 3 8.22 18.43 7.98 o 3 8 3 470.29 464.33 21.34 o 4 8 3 19.09 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