#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/61/2016177.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016177_Fobs loop_ _publ_author_name 'Gubanov, Alexander I.' 'Kuratieva, Natalia V.' _publ_section_title ; Double complexes [Co(NH~3~)~5~(H~2~O)]~2~[Zr~3~F~18~]·6H~2~O and [Co(NH~3~)~6~]~2~[Zr~3~F~18~]·6H~2~O ; _journal_coeditor_code BC3047 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i83 _journal_page_last i85 _journal_volume 63 _journal_year 2007 _space_group_IT_number 72 _symmetry_space_group_name_Hall '-I 2 2c' _symmetry_space_group_name_H-M 'I b a m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.1440 _cell_length_b 12.7191 _cell_length_c 14.6859 _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.8002 _[local]_cod_data_source_file bc3047Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Co(NH3)5(H2O)]2(Zr3F18)*(H2O)6 iIbam' _shelx_refln_list_code 4 _shelx_f_calc_maximum 707.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'x, -y, -z+1/2' '-x, y, -z+1/2' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z+1' '-x+1/2, y+1/2, -z+1' '-x, -y, -z' 'x, y, -z' '-x, y, z-1/2' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, y+1/2, -z+1/2' '-x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 15593.15 12781.51 173.39 o 4 0 0 23901.70 19732.25 327.76 o 6 0 0 107200.35 105814.09 1714.52 o 8 0 0 319458.59 339909.28 5973.99 o 10 0 0 29185.53 26353.64 553.53 o 12 0 0 125.25 158.57 74.85 o 14 0 0 75.51 184.82 82.98 o 16 0 0 2714.17 3356.83 517.03 o 18 0 0 45730.61 39828.80 1695.56 o 20 0 0 867.53 1106.30 344.00 o 1 1 0 44274.09 41795.03 610.03 o 3 1 0 8897.79 6363.62 94.49 o 5 1 0 77806.63 78732.85 660.20 o 7 1 0 24089.31 25936.31 394.54 o 9 1 0 70871.60 74947.69 894.00 o 11 1 0 19310.77 18407.86 390.72 o 13 1 0 15240.66 13751.17 397.53 o 15 1 0 3608.00 3485.84 205.59 o 17 1 0 11196.23 11177.04 596.34 o 19 1 0 4.24 0.00 88.27 o 0 2 0 63336.90 64025.22 715.01 o 2 2 0 40504.25 44323.36 335.32 o 4 2 0 215156.20 221117.69 1528.24 o 6 2 0 28481.34 31425.42 397.61 o 8 2 0 18744.00 18766.76 297.40 o 10 2 0 15673.38 16060.74 299.30 o 12 2 0 3628.44 3987.78 170.46 o 14 2 0 37541.81 38366.98 688.66 o 16 2 0 45.49 60.18 104.07 o 18 2 0 4312.98 4523.80 451.49 o 20 2 0 2652.72 1924.29 307.96 o 1 3 0 79461.98 87595.98 598.49 o 3 3 0 199.88 346.04 50.88 o 5 3 0 0.10 67.42 39.18 o 7 3 0 1397.61 1641.19 92.83 o 9 3 0 151615.47 156316.81 1597.00 o 11 3 0 1857.00 2122.52 128.15 o 13 3 0 9169.64 8658.28 264.92 o 15 3 0 3498.12 3413.65 261.20 o 17 3 0 25218.89 25600.45 925.81 o 19 3 0 4562.89 4762.51 470.43 o 0 4 0 92540.99 92618.36 927.14 o 2 4 0 5734.67 5142.29 119.72 o 4 4 0 460.66 729.42 69.51 o 6 4 0 105.00 44.41 46.79 o 8 4 0 43680.65 43303.99 560.24 o 10 4 0 29589.77 27902.36 507.92 o 12 4 0 527.68 739.63 84.06 o 14 4 0 8420.60 9790.78 407.30 o 16 4 0 78.02 209.35 84.32 o 18 4 0 31162.75 28489.97 1021.54 o 1 5 0 86346.05 99217.39 918.12 o 3 5 0 9312.51 9897.48 214.69 o 5 5 0 190239.64 188631.80 2223.35 o 7 5 0 13738.38 14993.58 299.90 o 9 5 0 3946.71 4371.78 171.85 o 11 5 0 9106.75 8411.88 252.10 o 13 5 0 79014.66 77228.04 1071.35 o 15 5 0 1942.82 1724.99 208.81 o 17 5 0 6744.97 7220.25 496.48 o 19 5 0 1132.09 1671.71 297.32 o 0 6 0 22652.49 21380.41 389.39 o 2 6 0 29.63 73.55 45.01 o 4 6 0 69356.73 70547.07 766.19 o 6 6 0 4441.86 4769.04 168.09 o 8 6 0 2895.42 3171.48 144.23 o 10 6 0 9085.13 8217.16 260.56 o 12 6 0 10206.62 9451.42 321.26 o 14 6 0 34148.09 33979.24 854.28 o 16 6 0 500.97 642.14 160.97 o 18 6 0 10874.16 9687.18 596.43 o 1 7 0 53189.76 51413.64 579.35 o 3 7 0 5556.71 5356.87 181.81 o 5 7 0 4689.85 5242.48 183.39 o 7 7 0 20916.09 21237.84 399.13 o 9 7 0 109442.87 107916.10 1297.19 o 11 7 0 1950.85 2058.42 161.56 o 13 7 0 15401.67 14588.82 531.39 o 15 7 0 9473.35 8884.41 431.26 o 17 7 0 14409.95 15144.97 750.87 o 0 8 0 31768.23 31560.19 788.59 o 2 8 0 10818.56 10012.30 265.59 o 4 8 0 134963.27 129727.38 1278.27 o 6 8 0 794.96 897.54 95.78 o 8 8 0 3670.18 3659.47 174.06 o 10 8 0 28.51 146.13 53.42 o 12 8 0 1672.51 2166.80 239.33 o 14 8 0 20932.41 20072.26 791.67 o 16 8 0 1753.45 2121.95 353.87 o 1 9 0 391.91 522.63 83.95 o 3 9 0 13670.89 12824.07 320.40 o 5 9 0 105707.83 102260.97 1265.60 o 7 9 0 4563.30 4437.41 193.96 o 9 9 0 4851.19 4913.97 238.06 o 11 9 0 7221.14 6751.62 419.01 o 13 9 0 45216.07 42253.58 1005.35 o 15 9 0 2.35 63.90 74.71 o 0 10 0 91784.63 84533.20 1766.75 o 2 10 0 100.77 115.64 54.79 o 4 10 0 11683.58 11002.69 311.89 o 6 10 0 2656.91 2639.75 191.22 o 8 10 0 20653.48 19465.26 502.56 o 10 10 0 5806.11 6251.44 358.12 o 12 10 0 459.69 688.59 149.83 o 14 10 0 270.15 342.07 140.57 o 1 11 0 9580.11 9528.79 346.05 o 3 11 0 2.31 80.05 52.95 o 5 11 0 5050.68 5327.99 227.94 o 7 11 0 71.57 100.69 59.78 o 9 11 0 23088.13 22484.27 899.18 o 11 11 0 1145.95 1099.00 185.59 o 13 11 0 2581.30 3435.53 326.67 o 0 12 0 5306.86 5171.31 634.99 o 2 12 0 2831.43 3139.64 241.81 o 4 12 0 47280.57 44001.41 833.59 o 6 12 0 3638.72 4355.88 342.71 o 8 12 0 1775.32 2054.82 247.82 o 10 12 0 875.97 640.89 198.09 o 12 12 0 2583.54 2770.57 301.52 o 1 13 0 4020.69 4307.07 265.36 o 3 13 0 13.28 0.00 46.07 o 5 13 0 5999.91 5693.00 355.44 o 7 13 0 1269.06 1467.06 210.26 o 9 13 0 12160.69 12049.35 544.32 o 11 13 0 270.68 385.53 144.16 o 0 14 0 51263.71 48374.72 1339.68 o 2 14 0 636.81 681.89 151.52 o 4 14 0 302.15 587.63 192.03 o 6 14 0 2227.70 2863.38 298.24 o 8 14 0 15545.85 15481.19 638.10 o 1 15 0 1199.30 1479.09 420.90 o 3 15 0 219.03 161.91 85.23 o 5 15 0 10484.02 9380.19 496.07 o 2 1 1 69853.74 55789.04 301.46 o 4 1 1 3471.66 2800.62 53.28 o 6 1 1 42396.35 43005.43 324.28 o 8 1 1 16956.95 18000.71 201.49 o 10 1 1 2963.07 2914.78 90.05 o 12 1 1 7070.51 6738.70 148.17 o 14 1 1 2518.44 2675.35 125.31 o 16 1 1 5421.37 5066.36 238.39 o 18 1 1 1.81 30.69 71.09 o 20 1 1 3527.53 3452.46 287.13 o 1 2 1 3395.66 3825.85 50.68 o 3 2 1 3656.31 3791.58 56.24 o 5 2 1 5022.10 6540.16 103.94 o 7 2 1 1436.02 1396.98 61.75 o 9 2 1 2598.57 2640.07 82.72 o 11 2 1 5244.75 5319.68 127.15 o 13 2 1 72.53 138.69 40.37 o 15 2 1 162.13 138.00 46.58 o 17 2 1 1841.22 1727.83 211.66 o 19 2 1 7.19 26.02 66.25 o 2 3 1 15690.35 17163.55 135.04 o 4 3 1 33.94 0.00 12.26 o 6 3 1 826.56 1026.14 54.14 o 8 3 1 6046.08 5675.10 116.65 o 10 3 1 15183.84 14709.04 220.02 o 12 3 1 1120.22 1440.18 82.53 o 14 3 1 249.23 281.99 50.20 o 16 3 1 6092.26 5394.08 250.50 o 18 3 1 43.05 0.00 54.65 o 1 4 1 10109.23 8507.25 101.87 o 3 4 1 948.99 456.78 37.55 o 5 4 1 220.89 220.11 35.80 o 7 4 1 38084.89 39286.20 358.55 o 9 4 1 0.55 31.96 23.37 o 11 4 1 7368.83 7466.62 162.85 o 13 4 1 1199.15 1354.01 95.05 o 15 4 1 7691.94 7590.81 260.61 o 17 4 1 1236.77 1470.30 183.97 o 19 4 1 1213.40 1411.26 189.47 o 2 5 1 16485.80 16686.64 181.39 o 4 5 1 483.17 508.65 49.07 o 6 5 1 4087.72 3719.12 99.88 o 8 5 1 3098.08 2665.21 94.09 o 10 5 1 7909.52 7633.61 162.88 o 12 5 1 1412.04 1272.64 83.97 o 14 5 1 64.02 189.99 59.73 o 16 5 1 1070.79 1078.08 138.53 o 18 5 1 11.55 107.10 75.92 o 1 6 1 5325.68 5262.52 107.05 o 3 6 1 25774.18 25226.37 275.64 o 5 6 1 9118.00 9327.41 163.54 o 7 6 1 13864.57 13491.97 209.23 o 9 6 1 614.30 621.54 64.69 o 11 6 1 3909.90 3713.51 120.47 o 13 6 1 505.25 651.44 83.68 o 15 6 1 3188.23 3579.80 220.46 o 17 6 1 1016.54 922.03 156.41 o 2 7 1 677.25 689.62 57.44 o 4 7 1 8.20 0.00 21.63 o 6 7 1 69.91 53.57 26.95 o 8 7 1 977.68 778.74 62.44 o 10 7 1 714.50 847.51 66.10 o 12 7 1 2.87 23.28 34.78 o 14 7 1 47.92 77.30 48.41 o 16 7 1 152.08 180.63 64.02 o 18 7 1 24.44 151.35 72.20 o 1 8 1 3333.71 3860.98 117.75 o 3 8 1 25598.25 24324.87 303.40 o 5 8 1 1650.22 1562.65 93.23 o 7 8 1 3903.13 4090.48 132.74 o 9 8 1 0.66 0.00 20.10 o 11 8 1 7114.62 6530.58 217.64 o 13 8 1 664.25 843.37 110.38 o 15 8 1 1978.04 2051.54 168.55 o 17 8 1 1258.90 1076.04 158.96 o 2 9 1 1131.21 1086.47 89.73 o 4 9 1 45.92 26.99 32.37 o 6 9 1 3640.45 3819.24 134.03 o 8 9 1 791.58 795.41 85.41 o 10 9 1 939.10 950.68 99.23 o 12 9 1 1349.56 1816.42 158.69 o 14 9 1 509.56 555.95 111.67 o 16 9 1 928.97 829.18 127.83 o 1 10 1 5462.57 5675.88 169.60 o 3 10 1 1681.59 2059.17 126.43 o 5 10 1 81.49 83.62 43.40 o 7 10 1 7638.83 6748.96 184.58 o 9 10 1 169.15 233.50 59.98 o 11 10 1 4141.40 4285.24 231.63 o 13 10 1 822.21 675.45 107.71 o 15 10 1 1610.31 1728.15 179.70 o 2 11 1 2181.77 2612.06 136.82 o 4 11 1 530.64 488.16 69.39 o 6 11 1 3706.91 3839.98 150.16 o 8 11 1 1499.99 1436.20 147.73 o 10 11 1 197.13 372.98 88.32 o 12 11 1 2604.12 3028.92 213.75 o 14 11 1 131.70 305.50 80.86 o 1 12 1 311.13 347.78 67.00 o 3 12 1 254.37 294.55 52.35 o 5 12 1 695.89 753.18 86.32 o 7 12 1 664.67 1065.08 155.34 o 9 12 1 0.29 49.56 45.29 o 11 12 1 233.97 425.15 97.16 o 13 12 1 28.27 45.11 64.60 o 2 13 1 8662.04 7997.20 245.53 o 4 13 1 1636.05 1854.75 135.69 o 6 13 1 4539.09 4600.73 259.41 o 8 13 1 1062.01 1142.25 130.67 o 10 13 1 1222.77 1408.69 147.22 o 1 14 1 121.24 68.51 44.54 o 3 14 1 121.02 100.86 88.27 o 5 14 1 9.77 3.61 48.38 o 7 14 1 48.50 0.00 46.52 o 9 14 1 36.28 213.91 76.99 o 2 15 1 2717.42 2735.38 234.52 o 4 15 1 798.90 660.61 172.24 o 6 15 1 1481.17 1436.91 152.97 o 0 0 2 86666.55 86337.07 1148.81 o 2 0 2 34918.25 37626.82 308.99 o 4 0 2 181501.50 187327.31 1407.03 o 6 0 2 12.15 28.35 24.48 o 8 0 2 15479.62 15832.80 260.54 o 10 0 2 1142.11 1395.66 102.53 o 12 0 2 1253.63 1573.08 117.16 o 14 0 2 22411.38 23892.32 515.54 o 16 0 2 1442.27 2038.23 220.02 o 18 0 2 6497.21 6217.38 463.78 o 20 0 2 3908.26 3045.90 383.53 o 1 1 2 72731.09 70765.51 378.22 o 3 1 2 42.77 466.72 24.11 o 5 1 2 51005.91 53369.20 328.32 o 7 1 2 3362.59 4148.59 91.21 o 9 1 2 143672.47 147376.03 893.49 o 11 1 2 7499.25 6619.15 145.89 o 13 1 2 14382.51 13583.41 231.62 o 15 1 2 3220.68 3209.58 181.35 o 17 1 2 22304.17 21503.63 588.49 o 19 1 2 619.52 827.21 143.75 o 0 2 2 499967.28 498519.00 3975.32 o 2 2 2 9067.45 6941.68 67.02 o 4 2 2 43415.22 46421.98 287.07 o 6 2 2 7842.49 7571.54 113.80 o 8 2 2 103007.50 104278.47 705.35 o 10 2 2 24829.38 23086.57 276.26 o 12 2 2 102.95 137.38 28.81 o 14 2 2 3408.54 4423.54 169.41 o 16 2 2 116.72 185.82 100.22 o 18 2 2 39358.02 34281.07 784.86 o 1 3 2 2312.73 1399.91 39.31 o 3 3 2 839.38 642.01 33.43 o 5 3 2 43391.00 40519.18 311.27 o 7 3 2 21406.43 22437.33 232.10 o 9 3 2 22658.90 24248.13 280.53 o 11 3 2 4974.92 4805.11 124.59 o 13 3 2 42156.46 39261.41 447.87 o 15 3 2 22.58 46.99 46.17 o 17 3 2 6526.77 7484.77 304.04 o 19 3 2 293.69 348.22 101.87 o 0 4 2 50462.46 51696.24 502.71 o 2 4 2 16.80 0.00 21.56 o 4 4 2 58249.33 55541.64 442.33 o 6 4 2 8763.16 9741.13 146.26 o 8 4 2 7639.15 7295.28 142.80 o 10 4 2 560.86 602.45 55.43 o 12 4 2 10941.84 10190.92 205.03 o 14 4 2 35563.33 34797.23 518.98 o 16 4 2 100.92 201.02 97.34 o 18 4 2 7088.52 6828.95 343.01 o 1 5 2 29521.67 30585.29 284.20 o 3 5 2 14.76 60.54 22.97 o 5 5 2 13377.29 13834.30 211.53 o 7 5 2 3584.35 3494.70 104.56 o 9 5 2 96713.28 94197.58 826.43 o 11 5 2 194.85 259.33 47.11 o 13 5 2 14391.71 13723.65 310.41 o 15 5 2 2784.01 3370.17 223.82 o 17 5 2 18841.18 18593.71 502.59 o 19 5 2 2640.85 3034.10 265.25 o 0 6 2 96480.58 95431.97 932.77 o 2 6 2 24938.07 25695.18 289.37 o 4 6 2 40631.72 38860.40 372.17 o 6 6 2 6.23 10.08 30.38 o 8 6 2 16453.95 16698.98 269.19 o 10 6 2 578.67 548.93 55.61 o 12 6 2 1483.92 1962.58 134.82 o 14 6 2 16273.64 16168.20 393.71 o 16 6 2 2073.21 2296.85 196.75 o 18 6 2 11874.84 11066.90 449.50 o 1 7 2 1630.88 2048.41 86.08 o 3 7 2 14816.21 14145.34 213.91 o 5 7 2 143303.16 139062.70 919.08 o 7 7 2 11654.33 11453.33 209.61 o 9 7 2 12355.40 12928.24 234.02 o 11 7 2 5583.30 5105.76 187.89 o 13 7 2 59452.86 55827.59 787.97 o 15 7 2 64.96 111.02 61.96 o 17 7 2 2574.58 3207.61 266.74 o 0 8 2 84942.89 85643.39 940.76 o 2 8 2 5849.31 5755.50 143.10 o 4 8 2 48720.49 47018.63 505.78 o 6 8 2 657.29 705.48 58.02 o 8 8 2 20447.39 19835.74 303.80 o 10 8 2 856.71 1150.30 107.21 o 12 8 2 1542.06 1989.38 160.62 o 14 8 2 8382.03 8627.36 301.28 o 16 8 2 777.11 776.83 112.01 o 1 9 2 14143.41 14130.43 254.31 o 3 9 2 74.65 76.50 28.87 o 5 9 2 9951.23 9961.10 213.13 o 7 9 2 5028.89 4818.65 138.81 o 9 9 2 40838.86 40910.75 583.01 o 11 9 2 1578.95 1820.74 155.51 o 13 9 2 7090.53 7278.14 278.01 o 15 9 2 3657.78 3662.66 256.61 o 0 10 2 28253.09 25648.88 496.95 o 2 10 2 2361.71 2521.72 136.62 o 4 10 2 53291.51 52056.19 631.25 o 6 10 2 816.93 775.88 80.81 o 8 10 2 3284.67 3765.69 184.29 o 10 10 2 33.02 33.56 50.02 o 12 10 2 3537.28 4269.35 235.78 o 14 10 2 16739.66 16368.95 445.90 o 1 11 2 1575.20 2042.49 120.79 o 3 11 2 3450.18 3403.84 157.55 o 5 11 2 24760.43 23658.03 400.08 o 7 11 2 2006.83 2243.11 177.48 o 9 11 2 9042.82 8661.27 302.76 o 11 11 2 630.34 820.90 117.82 o 13 11 2 17168.88 16584.02 455.21 o 0 12 2 44485.46 42223.74 808.27 o 2 12 2 300.46 181.04 46.35 o 4 12 2 1908.84 2318.21 159.04 o 6 12 2 1624.74 1855.71 145.01 o 8 12 2 13979.06 13873.66 395.61 o 10 12 2 6779.52 6535.36 277.83 o 12 12 2 8.72 82.88 56.93 o 1 13 2 4869.28 5130.43 197.33 o 3 13 2 3.11 0.00 30.45 o 5 13 2 7241.12 6963.94 234.29 o 7 13 2 165.29 222.89 77.09 o 9 13 2 17181.01 16362.18 456.15 o 11 13 2 525.54 450.18 111.47 o 0 14 2 5431.86 5290.74 348.63 o 2 14 2 2136.65 2331.20 202.80 o 4 14 2 24085.42 22770.55 531.77 o 6 14 2 471.04 433.26 99.35 o 8 14 2 2146.30 2372.85 194.61 o 1 15 2 4499.55 5256.67 302.90 o 3 15 2 181.95 222.95 118.89 o 5 15 2 3784.27 4895.99 351.82 o 2 1 3 56130.02 63880.17 378.44 o 4 1 3 5129.24 5526.71 77.02 o 6 1 3 3566.45 3296.03 79.92 o 8 1 3 24409.76 25152.61 255.43 o 10 1 3 12519.55 12484.03 201.14 o 12 1 3 1082.59 1170.53 71.62 o 14 1 3 1699.25 1684.97 117.40 o 16 1 3 5177.04 5279.71 219.21 o 18 1 3 122.72 9.53 80.01 o 1 2 3 5170.26 6983.20 72.51 o 3 2 3 6336.37 7396.58 116.41 o 5 2 3 35426.45 40441.60 322.94 o 7 2 3 42860.28 43017.83 349.60 o 9 2 3 588.20 462.66 60.94 o 11 2 3 167.62 77.21 21.57 o 13 2 3 493.73 488.04 59.00 o 15 2 3 3683.25 4228.73 194.29 o 17 2 3 23.76 54.05 47.66 o 19 2 3 169.19 262.72 90.24 o 2 3 3 11549.68 15523.11 134.85 o 4 3 3 475.11 498.60 36.83 o 6 3 3 60477.50 68015.80 499.06 o 8 3 3 10972.17 11194.08 230.69 o 10 3 3 23.44 8.33 33.72 o 12 3 3 8852.58 8545.44 193.05 o 14 3 3 3178.73 3409.05 162.76 o 16 3 3 1561.46 1722.10 161.99 o 18 3 3 19.17 32.41 76.37 o 1 4 3 6572.45 7295.04 112.64 o 3 4 3 16153.17 15598.23 170.20 o 5 4 3 472.92 495.61 43.17 o 7 4 3 87.75 125.44 33.89 o 9 4 3 4491.53 3996.46 119.33 o 11 4 3 4056.73 3986.81 136.88 o 13 4 3 1604.61 1545.80 104.49 o 15 4 3 292.24 180.67 56.25 o 17 4 3 1787.05 1501.60 159.96 o 19 4 3 122.73 305.45 93.92 o 2 5 3 1824.20 2662.40 78.91 o 4 5 3 1141.56 1000.02 55.30 o 6 5 3 288.68 359.63 40.26 o 8 5 3 260.84 217.76 45.25 o 10 5 3 15.10 113.63 38.38 o 12 5 3 4.66 57.81 54.88 o 14 5 3 6.63 0.00 37.88 o 16 5 3 71.47 54.32 63.15 o 18 5 3 13.83 106.82 76.99 o 1 6 3 44119.14 43419.69 384.13 o 3 6 3 28237.97 26366.72 312.76 o 5 6 3 747.05 995.32 69.74 o 7 6 3 19476.30 17734.12 246.07 o 9 6 3 217.85 231.55 47.47 o 11 6 3 11217.85 11459.71 248.79 o 13 6 3 1846.25 2108.50 140.66 o 15 6 3 1909.47 2176.79 188.79 o 17 6 3 2196.32 2662.68 215.09 o 2 7 3 280.85 344.08 50.31 o 4 7 3 0.04 0.00 24.70 o 6 7 3 7336.56 6683.53 165.73 o 8 7 3 456.32 580.25 69.90 o 10 7 3 4736.03 4687.33 158.79 o 12 7 3 51.43 47.31 37.77 o 14 7 3 344.00 339.54 72.09 o 16 7 3 272.67 346.58 85.99 o 1 8 3 14240.51 13560.17 220.33 o 3 8 3 2285.98 2448.87 102.88 o 5 8 3 528.51 761.95 65.72 o 7 8 3 17103.63 16431.13 265.52 o 9 8 3 73.84 5.50 21.94 o 11 8 3 1370.46 1628.44 128.70 o 13 8 3 459.54 768.71 104.62 o 15 8 3 805.72 826.62 130.59 o 17 8 3 420.23 614.15 108.97 o 2 9 3 591.03 705.22 66.48 o 4 9 3 1781.93 1634.07 100.83 o 6 9 3 2139.47 2473.13 112.41 o 8 9 3 8.03 36.11 59.29 o 10 9 3 82.00 67.38 39.42 o 12 9 3 1904.32 1756.34 151.18 o 14 9 3 50.75 49.98 48.50 o 16 9 3 423.01 481.42 98.85 o 1 10 3 3331.27 3591.24 139.57 o 3 10 3 2988.68 2863.45 137.57 o 5 10 3 1800.93 1770.91 111.97 o 7 10 3 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784.98 1434.17 97.76 o 7 8 7 3877.06 3900.96 138.69 o 9 8 7 201.86 254.10 49.81 o 11 8 7 7562.60 7642.40 256.50 o 13 8 7 310.77 302.77 114.60 o 15 8 7 1509.51 1800.05 180.72 o 2 9 7 11.05 22.60 24.83 o 4 9 7 29.34 94.31 32.13 o 6 9 7 2872.72 3764.80 145.77 o 8 9 7 6.42 62.17 42.84 o 10 9 7 62.85 135.87 51.66 o 12 9 7 1239.39 1429.00 146.25 o 14 9 7 656.27 893.74 127.41 o 1 10 7 758.91 825.05 89.32 o 3 10 7 915.33 1065.32 105.04 o 5 10 7 56.44 128.02 48.18 o 7 10 7 2462.01 2884.91 165.93 o 9 10 7 23.79 112.73 53.34 o 11 10 7 1806.02 2119.59 164.53 o 13 10 7 815.63 869.33 134.14 o 2 11 7 4093.97 4369.15 231.12 o 4 11 7 312.30 512.10 77.62 o 6 11 7 4549.30 4546.10 208.15 o 8 11 7 2878.48 3458.89 190.32 o 10 11 7 1253.29 2002.90 194.89 o 12 11 7 2122.32 2541.06 198.37 o 1 12 7 1412.29 2012.32 216.55 o 3 12 7 513.99 771.26 102.04 o 5 12 7 892.45 1189.44 126.10 o 7 12 7 2380.66 2637.93 193.99 o 9 12 7 1.34 0.00 64.60 o 2 13 7 5285.03 5502.90 234.87 o 4 13 7 1588.67 1820.35 176.87 o 6 13 7 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2 8 545.70 796.04 99.97 o 1 3 8 43723.12 44074.31 344.10 o 3 3 8 600.21 418.13 40.69 o 5 3 8 20230.18 20874.06 239.87 o 7 3 8 1127.32 1151.15 87.27 o 9 3 8 87620.60 84825.42 878.89 o 11 3 8 180.59 284.15 101.07 o 13 3 8 11423.89 11930.50 257.09 o 15 3 8 3507.91 3902.03 267.27 o 17 3 8 14028.28 13242.33 371.35 o 0 4 8 123820.49 115701.71 1210.94 o 2 4 8 9058.25 9273.84 161.40 o 4 4 8 13157.91 15797.72 210.27 o 6 4 8 4163.03 4576.84 155.46 o 8 4 8 31382.46 31563.82 420.35 o 10 4 8 8887.89 8666.71 257.06 o 12 4 8 130.99 234.58 51.47 o 14 4 8 2236.20 2722.19 157.71 o 16 4 8 699.17 813.72 97.84 o 1 5 8 818.40 666.69 48.57 o 3 5 8 6183.97 5404.70 126.88 o 5 5 8 83334.96 82385.20 658.89 o 7 5 8 3801.63 3698.70 95.95 o 9 5 8 8470.01 8037.67 251.65 o 11 5 8 6755.97 7091.72 168.90 o 13 5 8 39431.02 38665.55 508.87 o 15 5 8 339.04 546.61 92.97 o 17 5 8 4633.63 5039.67 318.87 o 0 6 8 27641.85 26358.67 427.64 o 2 6 8 126.18 185.30 38.85 o 4 6 8 15627.52 16268.08 261.97 o 6 6 8 385.60 389.58 56.74 o 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9 578.92 855.89 118.87 o 1 12 9 3.62 335.32 79.12 o 3 12 9 1208.09 1483.03 148.30 o 5 12 9 471.75 502.87 85.74 o 7 12 9 1.74 0.00 47.80 o 2 13 9 4323.01 4247.68 255.66 o 4 13 9 198.66 267.85 71.01 o 6 13 9 1313.72 1444.16 182.69 o 0 0 10 11389.61 11811.47 331.22 o 2 0 10 3134.16 2724.49 118.29 o 4 0 10 105383.02 105556.15 1741.26 o 6 0 10 602.57 550.96 72.23 o 8 0 10 34.65 164.63 46.44 o 10 0 10 879.54 1063.10 170.41 o 12 0 10 4773.32 4847.39 208.49 o 14 0 10 13645.99 12390.43 458.29 o 16 0 10 2218.57 2505.31 240.60 o 1 1 10 9648.11 10149.08 158.58 o 3 1 10 6820.63 6098.06 147.06 o 5 1 10 37283.60 36902.68 401.91 o 7 1 10 256.39 169.84 43.83 o 9 1 10 21709.66 20376.69 266.89 o 11 1 10 1086.60 1384.04 77.07 o 13 1 10 11441.94 11468.53 315.58 o 15 1 10 277.56 312.08 84.12 o 0 2 10 79890.14 73412.28 725.78 o 2 2 10 1715.47 1899.64 78.32 o 4 2 10 34756.29 36288.46 364.10 o 6 2 10 402.19 642.42 55.29 o 8 2 10 21978.50 22078.94 252.56 o 10 2 10 6220.26 6998.46 150.06 o 12 2 10 247.66 430.06 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12935.28 12572.22 344.18 o 10 6 10 3747.35 4585.54 264.00 o 12 6 10 244.41 196.99 68.20 o 14 6 10 5727.22 5855.26 301.38 o 1 7 10 1217.52 1372.23 92.95 o 3 7 10 1521.69 1557.38 97.53 o 5 7 10 30262.08 30035.34 365.12 o 7 7 10 756.76 904.87 70.16 o 9 7 10 12932.22 12521.12 363.10 o 11 7 10 1013.51 1075.25 141.53 o 13 7 10 19270.01 19885.79 561.29 o 0 8 10 41484.70 36856.55 828.21 o 2 8 10 206.32 249.63 65.52 o 4 8 10 8074.79 8701.39 196.22 o 6 8 10 451.68 482.11 58.14 o 8 8 10 15388.13 15480.53 281.80 o 10 8 10 2534.47 3040.57 128.58 o 12 8 10 0.76 0.00 62.34 o 1 9 10 15550.86 15389.33 376.77 o 3 9 10 9.88 0.00 59.34 o 5 9 10 2511.01 2759.23 170.38 o 7 9 10 425.80 516.11 85.49 o 9 9 10 25793.46 24847.39 518.97 o 11 9 10 692.71 1048.77 107.50 o 0 10 10 24972.71 23528.49 695.18 o 2 10 10 443.64 534.14 92.56 o 4 10 10 24781.90 24022.32 496.83 o 6 10 10 31.60 10.00 46.90 o 8 10 10 3504.01 4427.43 224.13 o 10 10 10 36.95 105.92 49.34 o 1 11 10 1954.55 2673.39 208.26 o 3 11 10 2468.64 2280.02 176.20 o 5 11 10 13620.87 12818.82 346.53 o 7 11 10 462.99 575.72 103.04 o 9 11 10 4695.12 4676.04 272.56 o 0 12 10 19971.32 19450.82 681.95 o 2 12 10 96.23 64.72 61.35 o 4 12 10 3133.73 4037.52 218.96 o 6 12 10 565.98 685.76 128.14 o 1 13 10 1545.91 2053.53 184.36 o 3 13 10 310.15 422.41 79.06 o 2 1 11 12262.99 11703.41 184.17 o 4 1 11 2067.11 2334.10 98.67 o 6 1 11 4523.65 4154.34 123.96 o 8 1 11 4992.90 4729.34 130.64 o 10 1 11 1553.19 2043.78 91.01 o 12 1 11 2339.35 2434.20 112.94 o 14 1 11 102.97 144.53 57.90 o 16 1 11 2375.61 2675.56 159.29 o 1 2 11 4657.16 4318.88 110.67 o 3 2 11 884.05 1501.46 72.51 o 5 2 11 16.93 50.03 42.97 o 7 2 11 3593.37 3249.44 104.11 o 9 2 11 559.84 609.19 48.21 o 11 2 11 12.53 163.35 66.59 o 13 2 11 311.38 314.55 42.82 o 15 2 11 166.65 189.90 47.58 o 2 3 11 1010.91 1037.58 74.77 o 4 3 11 6.05 97.87 30.98 o 6 3 11 1381.07 1776.73 72.89 o 8 3 11 1286.24 1682.51 154.73 o 10 3 11 84.23 109.10 54.18 o 12 3 11 677.07 867.25 125.04 o 14 3 11 8.58 75.02 46.57 o 1 4 11 1517.28 1901.13 88.81 o 3 4 11 8191.06 8065.94 166.15 o 5 4 11 327.17 331.65 85.12 o 7 4 11 3984.66 3656.89 228.13 o 9 4 11 317.27 139.50 62.23 o 11 4 11 6616.56 6155.34 276.45 o 13 4 11 309.77 480.12 124.51 o 15 4 11 1395.58 1653.89 177.76 o 2 5 11 3299.11 3154.98 116.02 o 4 5 11 97.51 104.47 30.80 o 6 5 11 43.23 118.77 39.43 o 8 5 11 1233.63 1898.76 166.43 o 10 5 11 5302.04 5320.44 257.54 o 12 5 11 30.87 218.25 70.26 o 14 5 11 14.10 24.79 66.04 o 1 6 11 372.43 457.43 62.16 o 3 6 11 7328.37 6684.74 176.74 o 5 6 11 1178.85 1156.88 77.27 o 7 6 11 2183.15 2316.79 95.21 o 9 6 11 577.79 551.54 105.98 o 11 6 11 1291.55 1285.94 153.64 o 13 6 11 453.65 520.85 101.47 o 2 7 11 508.09 393.35 72.98 o 4 7 11 6.62 90.82 55.07 o 6 7 11 544.01 816.82 86.60 o 8 7 11 388.44 616.53 100.52 o 10 7 11 38.35 124.99 105.98 o 12 7 11 2.77 69.82 59.64 o 1 8 11 4054.50 4626.59 203.48 o 3 8 11 1457.51 1715.06 140.44 o 5 8 11 223.76 411.20 86.01 o 7 8 11 5860.42 5818.29 186.35 o 9 8 11 3.86 0.00 39.43 o 11 8 11 509.81 283.34 100.58 o 2 9 11 1385.70 1679.36 144.34 o 4 9 11 350.80 380.78 111.08 o 6 9 11 466.49 624.91 99.07 o 8 9 11 83.91 153.92 62.06 o 10 9 11 632.05 979.65 102.77 o 1 10 11 45.03 223.52 61.92 o 3 10 11 1913.68 2295.17 173.43 o 5 10 11 54.82 124.22 70.30 o 7 10 11 361.47 480.18 108.56 o 9 10 11 35.04 155.15 55.90 o 2 11 11 703.40 570.08 151.01 o 4 11 11 105.35 80.73 51.15 o 6 11 11 428.05 509.36 92.81 o 8 11 11 935.37 1490.28 150.97 o 1 12 11 298.88 546.31 92.21 o 3 12 11 211.94 78.55 63.18 o 5 12 11 9.82 129.94 56.21 o 0 0 12 104556.08 97439.77 2574.82 o 2 0 12 56.05 86.60 33.62 o 4 0 12 12135.12 13001.05 358.92 o 6 0 12 12.81 102.30 48.68 o 8 0 12 17030.95 17021.92 387.11 o 10 0 12 7946.08 8680.96 273.19 o 12 0 12 278.73 533.24 105.65 o 14 0 12 5257.45 5118.95 444.24 o 1 1 12 3368.65 3819.53 103.58 o 3 1 12 1569.99 1426.38 97.52 o 5 1 12 24313.12 23738.76 331.78 o 7 1 12 2868.63 2727.67 111.88 o 9 1 12 12017.29 11576.30 211.62 o 11 1 12 1383.28 1865.31 97.01 o 13 1 12 15737.73 16188.76 359.81 o 15 1 12 378.81 418.50 92.62 o 0 2 12 6348.90 5445.55 177.38 o 2 2 12 818.60 1010.42 69.09 o 4 2 12 30993.06 33182.27 374.75 o 6 2 12 3924.83 3505.98 130.75 o 8 2 12 1780.12 2162.22 112.52 o 10 2 12 7.13 81.30 94.44 o 12 2 12 2788.54 3151.12 213.69 o 14 2 12 13142.71 12006.62 293.88 o 1 3 12 8891.81 9696.21 194.10 o 3 3 12 240.58 201.79 42.59 o 5 3 12 7517.58 7415.61 204.54 o 7 3 12 1.16 191.95 50.53 o 9 3 12 28016.85 25323.67 552.38 o 11 3 12 7.76 138.43 54.18 o 13 3 12 7153.30 7626.25 330.19 o 0 4 12 29265.42 26626.51 624.65 o 2 4 12 1304.85 1273.85 85.60 o 4 4 12 6441.42 7416.54 205.44 o 6 4 12 196.14 368.67 43.84 o 8 4 12 14546.49 13797.31 398.43 o 10 4 12 4799.44 5329.56 225.64 o 12 4 12 453.73 501.95 100.78 o 14 4 12 2011.39 2506.52 216.38 o 1 5 12 45.25 214.22 47.41 o 3 5 12 1128.28 1198.32 90.41 o 5 5 12 19952.21 18678.39 314.17 o 7 5 12 405.67 207.90 105.01 o 9 5 12 6237.14 5718.40 253.17 o 11 5 12 750.28 990.07 144.15 o 13 5 12 13678.42 13561.66 453.00 o 0 6 12 25402.82 23126.97 615.46 o 2 6 12 31.89 97.13 45.41 o 4 6 12 19787.21 19449.86 428.17 o 6 6 12 7.16 67.43 48.96 o 8 6 12 7853.84 7631.03 351.99 o 10 6 12 2176.93 3098.71 263.51 o 12 6 12 1989.69 2669.11 248.52 o 1 7 12 17866.29 17751.83 390.17 o 3 7 12 244.96 395.79 75.38 o 5 7 12 1184.41 1480.52 106.61 o 7 7 12 307.84 269.07 78.66 o 9 7 12 26830.06 25064.42 601.58 o 11 7 12 398.72 279.66 126.53 o 0 8 12 25035.11 22580.04 654.04 o 2 8 12 846.70 882.96 128.96 o 4 8 12 21736.04 21527.05 488.71 o 6 8 12 98.70 122.07 60.76 o 8 8 12 5383.19 5639.76 159.55 o 10 8 12 679.89 966.46 157.88 o 1 9 12 2307.95 2645.37 182.15 o 3 9 12 2070.33 2479.63 192.00 o 5 9 12 17868.72 17675.37 454.48 o 7 9 12 62.99 121.29 78.50 o 9 9 12 4943.08 4997.53 257.96 o 0 10 12 17849.85 15155.11 568.47 o 2 10 12 9.34 7.08 45.03 o 4 10 12 4623.11 5283.59 259.70 o 6 10 12 24.65 116.51 58.11 o 8 10 12 6329.06 6338.22 248.04 o 1 11 12 2741.52 3049.59 358.46 o 3 11 12 14.34 136.82 61.37 o 5 11 12 2739.81 3175.43 220.22 o 0 12 12 1307.66 1085.82 180.84 o 2 1 13 4154.53 3818.85 142.03 o 4 1 13 205.31 329.23 53.33 o 6 1 13 3829.01 3800.29 142.64 o 8 1 13 2749.96 2786.23 190.08 o 10 1 13 563.01 952.20 81.48 o 12 1 13 987.11 1407.06 104.92 o 14 1 13 264.76 546.39 71.24 o 1 2 13 1908.26 2386.11 135.55 o 3 2 13 2518.84 2794.03 130.24 o 5 2 13 834.22 929.29 79.92 o 7 2 13 517.12 666.59 104.42 o 9 2 13 1071.64 1362.69 63.90 o 11 2 13 2414.44 2839.25 199.01 o 13 2 13 10.28 147.49 56.91 o 2 3 13 8532.50 7861.98 226.36 o 4 3 13 295.14 474.01 58.39 o 6 3 13 1105.80 1287.15 80.82 o 8 3 13 1842.44 2223.24 112.34 o 10 3 13 5674.81 5458.89 226.44 o 12 3 13 1374.52 1948.65 179.21 o 1 4 13 77.32 333.42 60.40 o 3 4 13 229.95 568.70 74.20 o 5 4 13 247.86 476.64 61.64 o 7 4 13 1074.58 1390.74 74.38 o 9 4 13 445.34 352.52 88.79 o 11 4 13 862.80 846.66 122.93 o 13 4 13 133.16 158.35 71.92 o 2 5 13 83.43 58.28 75.49 o 4 5 13 1.65 6.16 50.59 o 6 5 13 99.39 292.42 62.42 o 8 5 13 3.22 208.90 84.40 o 10 5 13 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