#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016183.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016183_Fobs loop_ _publ_author_name 'Abe, Taichi' 'Shinozaki, Kazuteru' 'Ikeda, Noriaki' 'Suzuki, Takayoshi' _publ_section_title ; [2,6-Bis(5-methyl-2-pyridyl)phenyl-\k^3^N,C^1^,N']chloridoplatinum(II) ; _journal_coeditor_code BM3040 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m456 _journal_page_last m458 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.092 _cell_angle_gamma 90.000 _cell_length_a 9.6574 _cell_length_b 12.9691 _cell_length_c 12.9617 _exptl_crystal_F_000 928.00 _reflns_d_resolution_high 0.7711 _[local]_cod_data_source_file bm3040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' suzuki15' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2034.56 2141.06 17.50 o 4 0 0 10726.83 10498.21 231.09 o 6 0 0 13394.64 12953.43 620.27 o 8 0 0 456.64 484.83 61.66 o 10 0 0 10723.24 10838.25 381.28 o 2 1 0 47700.49 48580.96 1058.98 o 3 1 0 24423.86 24826.67 260.42 o 4 1 0 13378.21 13401.42 119.39 o 5 1 0 553.54 551.96 9.93 o 6 1 0 4515.05 4434.27 52.97 o 7 1 0 9170.31 8237.47 598.78 o 8 1 0 6615.67 6257.10 188.75 o 9 1 0 3231.14 3182.60 100.62 o 10 1 0 27.29 64.11 36.59 o 11 1 0 278.67 307.50 42.68 o 0 2 0 3265.18 3359.17 35.09 o 1 2 0 26021.82 26448.29 327.24 o 2 2 0 9265.73 9666.62 86.69 o 3 2 0 4285.56 4376.71 48.59 o 4 2 0 129.60 141.36 8.51 o 5 2 0 33108.64 32775.30 482.22 o 6 2 0 39.17 63.10 7.84 o 7 2 0 3515.38 3439.38 49.37 o 8 2 0 847.01 749.45 37.74 o 9 2 0 6772.48 6234.62 322.19 o 10 2 0 476.01 518.82 35.17 o 11 2 0 6129.02 6159.05 264.21 o 1 3 0 9133.84 8868.04 81.40 o 2 3 0 7298.52 7452.09 78.14 o 3 3 0 32533.95 32159.61 497.23 o 4 3 0 7523.40 7536.18 76.46 o 5 3 0 1964.51 2132.93 31.08 o 6 3 0 2747.84 2807.86 49.11 o 7 3 0 20060.75 20240.39 289.26 o 8 3 0 3833.65 3629.00 53.77 o 9 3 0 4303.35 3968.06 212.98 o 10 3 0 54.49 59.06 29.19 o 11 3 0 1115.70 1111.96 64.00 o 0 4 0 36368.55 35743.41 758.97 o 1 4 0 5968.80 5809.59 52.97 o 2 4 0 265.71 281.64 16.83 o 3 4 0 12.02 31.60 7.49 o 4 4 0 39000.11 38880.66 696.76 o 5 4 0 3345.77 3248.11 45.64 o 6 4 0 28065.54 28379.62 433.04 o 7 4 0 457.80 451.75 14.36 o 8 4 0 95.09 105.58 11.36 o 9 4 0 1426.29 1321.73 31.13 o 10 4 0 6146.89 6090.56 162.57 o 11 4 0 696.13 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