#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/61/2016185.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016185_Fobs loop_ _publ_author_name 'Yang, Hexiong' 'Zwick, Justin' 'Downs, Robert T.' 'Costin, Gelu' _publ_section_title ; Isokite, CaMg(PO~4~)F~0.8~(OH)~0.2~, isomorphous with titanite ; _journal_coeditor_code FA3103 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i89 _journal_page_last i90 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.246 _cell_angle_gamma 90.000 _cell_length_a 6.5109 _cell_length_b 8.7301 _cell_length_c 6.9046 _exptl_crystal_F_000 351.20 _reflns_d_resolution_high 0.6181 _[local]_cod_data_source_file fa3103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' isokite in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 152.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 23342.35 22361.67 190.97 o 4 0 0 5872.37 5690.25 82.27 o 6 0 0 6963.54 6753.91 102.17 o 8 0 0 2774.79 2593.70 105.49 o 1 1 0 34.99 26.12 1.66 o 3 1 0 1333.79 1464.36 15.81 o 5 1 0 144.29 139.47 7.68 o 7 1 0 46.75 48.00 8.12 o 9 1 0 29.31 7.02 11.79 o 0 2 0 632.32 660.89 13.70 o 2 2 0 742.58 786.66 9.85 o 4 2 0 90.07 87.48 5.28 o 6 2 0 95.00 74.91 9.56 o 8 2 0 309.92 344.59 29.78 o 1 3 0 12078.58 11428.38 88.22 o 3 3 0 13827.75 13318.89 97.26 o 5 3 0 6802.29 6742.86 72.94 o 7 3 0 2671.82 2708.59 67.66 o 9 3 0 1157.37 1145.79 52.37 o 0 4 0 2.11 1.11 2.44 o 2 4 0 24.29 24.92 3.44 o 4 4 0 451.15 445.78 13.15 o 6 4 0 290.59 273.95 14.94 o 8 4 0 1.31 -6.75 7.44 o 1 5 0 12.49 11.18 2.79 o 3 5 0 2532.64 2595.79 31.98 o 5 5 0 735.33 729.34 18.83 o 7 5 0 168.30 153.25 15.15 o 9 5 0 134.95 115.43 33.44 o 0 6 0 1788.84 1674.35 61.38 o 2 6 0 6514.12 6325.83 61.03 o 4 6 0 5264.11 5263.37 75.46 o 6 6 0 1431.39 1504.08 34.08 o 8 6 0 1275.05 1274.30 105.47 o 1 7 0 241.59 230.60 9.29 o 3 7 0 306.70 311.10 14.89 o 5 7 0 128.39 116.80 11.83 o 7 7 0 11.70 25.50 16.47 o 0 8 0 1222.72 1091.84 31.55 o 2 8 0 159.19 158.89 9.33 o 4 8 0 188.23 167.18 14.81 o 6 8 0 583.61 659.89 50.59 o 8 8 0 61.88 71.78 24.73 o 1 9 0 5563.16 5267.47 64.43 o 3 9 0 1646.50 1617.33 42.00 o 5 9 0 1380.15 1335.74 67.90 o 7 9 0 1274.42 1205.66 73.14 o 0 10 0 61.70 58.65 10.98 o 2 10 0 40.17 43.75 8.48 o 4 10 0 0.75 -6.57 9.55 o 6 10 0 0.98 -5.81 13.84 o 1 11 0 289.07 293.49 18.07 o 3 11 0 1.01 -4.47 11.57 o 5 11 0 4.19 1.77 13.25 o 0 12 0 2002.62 2011.87 70.88 o 2 12 0 1424.16 1437.01 88.79 o 4 12 0 1528.75 1642.18 86.93 o 1 13 0 32.17 15.56 13.51 o 3 13 0 91.40 65.13 24.64 o 0 14 0 43.23 15.54 20.87 o -9 1 1 2.76 11.12 11.52 o -7 1 1 118.87 91.80 8.72 o -5 1 1 590.14 605.86 12.49 o -3 1 1 4293.77 4591.08 35.60 o -1 1 1 36.90 38.81 2.14 o 1 1 1 182.70 190.20 5.64 o 3 1 1 279.86 250.13 6.43 o 5 1 1 241.91 230.50 15.33 o 7 1 1 199.38 215.63 21.56 o 9 1 1 0.24 8.49 11.57 o -8 2 1 0.27 0.00 6.55 o -6 2 1 81.82 88.18 7.25 o -4 2 1 87.99 87.07 4.92 o -2 2 1 799.56 984.80 10.71 o 0 2 1 201.25 247.09 5.72 o 2 2 1 1543.10 1603.70 18.04 o 4 2 1 199.20 193.57 7.46 o 6 2 1 107.29 94.15 11.65 o 8 2 1 71.98 53.94 14.20 o -9 3 1 383.65 352.72 33.37 o -7 3 1 66.23 75.50 8.83 o -5 3 1 325.05 347.02 10.40 o -3 3 1 471.58 485.73 9.07 o -1 3 1 0.41 1.92 1.68 o 1 3 1 8034.84 9077.60 92.26 o 3 3 1 1959.30 2069.93 21.79 o 5 3 1 138.47 130.33 8.46 o 7 3 1 128.81 143.54 17.81 o 9 3 1 210.55 192.49 29.79 o -8 4 1 176.98 178.52 17.51 o -6 4 1 235.92 232.84 16.63 o -4 4 1 564.51 567.50 11.43 o -2 4 1 558.67 576.88 10.93 o 0 4 1 4082.69 4415.02 36.73 o 2 4 1 45.37 34.40 3.36 o 4 4 1 196.25 192.72 8.38 o 6 4 1 9.61 4.38 5.77 o 8 4 1 19.27 17.66 12.30 o -9 5 1 16.49 17.31 18.51 o -7 5 1 324.53 330.64 18.79 o -5 5 1 10.83 10.85 3.87 o -3 5 1 214.78 234.78 7.64 o -1 5 1 1331.06 1257.87 17.43 o 1 5 1 315.18 318.79 8.89 o 3 5 1 15.73 12.85 3.72 o 5 5 1 103.19 108.36 11.04 o 7 5 1 3.73 1.40 6.91 o -8 6 1 3.63 4.76 14.77 o -6 6 1 177.07 150.56 13.58 o -4 6 1 543.08 543.90 15.20 o -2 6 1 1018.13 1010.93 17.24 o 0 6 1 48.16 49.46 4.52 o 2 6 1 40.89 34.13 5.03 o 4 6 1 518.75 527.10 17.36 o 6 6 1 495.26 550.23 23.99 o 8 6 1 20.70 30.83 17.00 o -7 7 1 2.15 12.60 11.31 o -5 7 1 58.50 55.56 8.81 o -3 7 1 121.01 122.66 10.24 o -1 7 1 22.55 14.17 4.02 o 1 7 1 5.66 4.76 2.91 o 3 7 1 23.11 23.20 5.70 o 5 7 1 32.67 33.35 10.91 o 7 7 1 16.67 17.48 12.79 o -8 8 1 38.99 52.13 23.82 o -6 8 1 331.94 368.05 60.19 o -4 8 1 747.34 786.59 21.93 o -2 8 1 1427.09 1378.73 29.62 o 0 8 1 371.88 374.49 13.26 o 2 8 1 27.07 38.17 6.88 o 4 8 1 815.19 756.27 30.71 o 6 8 1 724.50 788.06 51.02 o -7 9 1 233.71 256.80 40.31 o -5 9 1 27.09 23.58 9.41 o -3 9 1 8.61 11.08 6.16 o -1 9 1 532.75 535.09 17.14 o 1 9 1 50.82 51.95 7.80 o 3 9 1 30.13 43.15 10.74 o 5 9 1 250.64 310.93 35.71 o 7 9 1 10.97 13.84 18.76 o -6 10 1 114.49 100.02 26.79 o -4 10 1 178.83 170.26 15.34 o -2 10 1 40.93 41.73 7.28 o 0 10 1 508.20 503.78 17.21 o 2 10 1 16.09 27.02 8.73 o 4 10 1 36.93 35.44 18.19 o 6 10 1 0.19 14.88 18.22 o -5 11 1 316.62 349.07 46.10 o -3 11 1 425.80 481.99 45.69 o -1 11 1 152.77 151.54 11.83 o 1 11 1 959.53 953.71 31.79 o 3 11 1 612.77 660.00 51.09 o 5 11 1 28.06 16.04 16.97 o -4 12 1 217.98 236.16 30.30 o -2 12 1 110.67 123.66 19.81 o 0 12 1 360.96 363.40 27.42 o 2 12 1 799.72 763.70 57.55 o 4 12 1 85.27 80.72 25.73 o -3 13 1 20.40 9.19 13.82 o -1 13 1 45.57 24.97 18.69 o 1 13 1 71.54 56.56 23.07 o 3 13 1 9.48 11.64 15.38 o 0 14 1 240.19 213.57 48.93 o -10 0 2 210.32 175.43 37.95 o -8 0 2 2721.11 2751.79 67.92 o -6 0 2 2695.98 2557.35 47.89 o -4 0 2 938.40 911.15 17.69 o -2 0 2 8302.30 8749.72 88.86 o 0 0 2 6485.30 6776.88 105.62 o 2 0 2 7551.21 7731.00 97.05 o 4 0 2 5913.50 5943.82 160.42 o 6 0 2 435.13 386.09 33.89 o 8 0 2 342.37 282.51 38.11 o -9 1 2 501.39 498.48 25.98 o -7 1 2 1225.53 1225.34 25.07 o -5 1 2 439.27 437.30 11.10 o -3 1 2 5192.14 5175.42 36.46 o -1 1 2 8803.02 9136.22 60.29 o 1 1 2 193.35 96.46 4.15 o 3 1 2 2726.57 2706.49 26.86 o 5 1 2 1778.34 1771.66 38.74 o 7 1 2 261.62 280.29 24.16 o -10 2 2 375.67 419.83 57.37 o -8 2 2 928.73 947.76 31.50 o -6 2 2 3188.23 3168.23 44.38 o -4 2 2 2945.01 2886.65 30.27 o -2 2 2 64.70 15.82 2.15 o 0 2 2 7741.74 7583.93 90.34 o 2 2 2 10105.90 9988.08 128.59 o 4 2 2 1575.10 1621.50 24.88 o 6 2 2 742.34 741.51 33.00 o 8 2 2 418.26 395.08 31.38 o -9 3 2 436.87 456.68 36.67 o -7 3 2 410.85 408.20 16.85 o -5 3 2 1455.85 1430.92 21.06 o -3 3 2 3669.04 3748.77 33.61 o -1 3 2 3941.55 3942.24 30.11 o 1 3 2 2019.53 1929.76 38.80 o 3 3 2 852.63 791.88 15.30 o 5 3 2 1179.74 1155.85 36.17 o 7 3 2 1101.05 1122.95 44.00 o -8 4 2 541.18 550.16 27.43 o -6 4 2 835.70 808.70 19.59 o -4 4 2 3467.35 3543.34 41.23 o -2 4 2 9897.10 10174.21 83.77 o 0 4 2 4392.37 4312.57 38.55 o 2 4 2 1513.02 1433.05 19.38 o 4 4 2 1995.64 1940.74 34.26 o 6 4 2 1298.78 1318.91 31.92 o 8 4 2 567.56 623.89 57.43 o -9 5 2 615.79 659.00 45.14 o -7 5 2 693.17 700.37 24.27 o -5 5 2 4149.10 4098.78 42.92 o -3 5 2 7222.00 7257.75 62.64 o -1 5 2 7243.81 7075.83 61.54 o 1 5 2 6367.39 6219.92 59.13 o 3 5 2 1955.85 1937.60 42.61 o 5 5 2 2024.98 1990.40 39.76 o 7 5 2 2012.04 2063.06 65.27 o -8 6 2 38.20 32.02 14.11 o -6 6 2 404.34 404.48 16.27 o -4 6 2 1247.96 1171.52 31.50 o -2 6 2 162.21 155.96 7.81 o 0 6 2 1072.49 1053.87 20.94 o 2 6 2 659.97 610.84 16.22 o 4 6 2 63.95 53.16 8.04 o 6 6 2 801.25 832.01 28.14 o -9 7 2 284.94 271.48 45.05 o -7 7 2 803.85 774.38 78.95 o -5 7 2 2461.78 2412.57 42.37 o -3 7 2 509.72 533.95 14.94 o -1 7 2 783.68 801.60 18.80 o 1 7 2 5915.06 5622.44 60.38 o 3 7 2 1856.99 1893.06 38.37 o 5 7 2 371.88 391.08 20.46 o 7 7 2 463.50 511.47 35.64 o -8 8 2 1088.07 1017.01 70.42 o -6 8 2 1083.58 1122.25 47.86 o -4 8 2 1533.04 1581.96 32.38 o -2 8 2 4579.50 4611.02 57.62 o 0 8 2 2435.54 2314.62 37.86 o 2 8 2 1711.82 1739.02 50.85 o 4 8 2 2380.53 2493.50 50.62 o 6 8 2 694.45 719.99 50.76 o -7 9 2 924.87 1020.98 90.89 o -5 9 2 358.26 348.43 20.45 o -3 9 2 255.52 251.62 15.91 o -1 9 2 572.37 601.62 18.74 o 1 9 2 809.75 809.61 26.18 o 3 9 2 1327.31 1294.41 40.08 o 5 9 2 440.36 573.61 44.12 o -6 10 2 126.14 107.87 21.55 o -4 10 2 299.81 297.57 17.71 o -2 10 2 575.59 568.58 19.76 o 0 10 2 346.78 397.68 21.24 o 2 10 2 187.15 159.89 22.31 o 4 10 2 253.90 217.99 30.74 o -5 11 2 486.58 509.50 41.46 o -3 11 2 426.82 398.42 18.48 o -1 11 2 644.11 659.69 28.31 o 1 11 2 951.12 926.64 71.95 o 3 11 2 1077.40 842.28 52.90 o 5 11 2 359.25 344.67 41.45 o -4 12 2 427.85 450.88 32.84 o -2 12 2 1247.14 1311.06 55.93 o 0 12 2 414.01 409.99 51.49 o 2 12 2 203.31 148.71 28.72 o 4 12 2 594.29 612.61 53.63 o -3 13 2 257.74 295.75 33.57 o -1 13 2 285.62 283.57 31.57 o 1 13 2 2.26 3.09 15.04 o -9 1 3 4.58 1.68 7.98 o -7 1 3 37.85 27.67 6.24 o -5 1 3 16.79 17.65 3.77 o -3 1 3 214.58 236.04 7.76 o -1 1 3 4035.80 4523.02 32.96 o 1 1 3 551.89 559.63 14.60 o 3 1 3 382.05 345.91 21.73 o 5 1 3 12.92 14.94 7.28 o 7 1 3 183.35 135.87 18.60 o -10 2 3 37.08 4.67 18.44 o -8 2 3 73.21 64.44 8.52 o -6 2 3 183.45 171.50 12.22 o -4 2 3 106.36 132.57 6.67 o -2 2 3 1305.70 1603.38 18.73 o 0 2 3 208.16 202.27 9.61 o 2 2 3 30.22 33.79 5.57 o 4 2 3 20.23 10.53 4.89 o 6 2 3 53.33 43.49 11.55 o 8 2 3 21.95 17.58 11.81 o -9 3 3 11.79 6.39 13.39 o -7 3 3 613.52 607.27 19.13 o -5 3 3 2028.10 1943.42 27.62 o -3 3 3 98.92 111.82 6.04 o -1 3 3 229.63 241.44 7.01 o 1 3 3 1884.07 2026.73 33.79 o 3 3 3 247.14 274.55 11.04 o 5 3 3 490.43 497.83 23.24 o 7 3 3 58.50 54.58 13.85 o -10 4 3 5.12 -10.62 16.81 o -8 4 3 97.09 91.56 14.87 o -6 4 3 0.93 6.05 4.49 o -4 4 3 362.42 337.50 12.26 o -2 4 3 223.19 217.50 7.38 o 0 4 3 437.87 444.95 10.52 o 2 4 3 807.47 760.91 32.81 o 4 4 3 498.94 473.21 21.50 o 6 4 3 60.18 83.92 14.17 o -9 5 3 30.15 20.08 20.00 o -7 5 3 30.60 22.29 6.67 o -5 5 3 9.67 2.83 4.38 o -3 5 3 240.91 235.50 8.84 o -1 5 3 187.16 185.15 9.13 o 1 5 3 11.99 7.65 4.01 o 3 5 3 684.45 684.23 30.63 o 5 5 3 17.70 32.91 7.20 o 7 5 3 5.20 12.50 11.27 o -8 6 3 109.52 106.54 21.67 o -6 6 3 14.26 12.43 5.13 o -4 6 3 164.31 159.52 10.76 o -2 6 3 1482.41 1421.88 24.80 o 0 6 3 390.67 383.84 11.88 o 2 6 3 50.77 54.84 19.43 o 4 6 3 34.70 31.60 8.68 o 6 6 3 69.25 69.96 20.76 o -9 7 3 18.82 21.88 38.10 o -7 7 3 17.64 20.56 13.87 o -5 7 3 19.46 14.66 8.00 o -3 7 3 62.15 58.95 7.19 o -1 7 3 161.53 177.30 10.43 o 1 7 3 52.16 49.17 8.15 o 3 7 3 1.81 4.26 5.36 o 5 7 3 6.28 -3.34 7.03 o -8 8 3 152.27 170.68 48.21 o -6 8 3 1.10 -0.02 6.06 o -4 8 3 315.73 283.06 13.99 o -2 8 3 1535.34 1542.94 28.33 o 0 8 3 556.30 552.68 30.56 o 2 8 3 210.49 229.06 26.45 o 4 8 3 117.54 112.09 12.43 o 6 8 3 137.00 136.94 20.47 o -7 9 3 45.06 58.73 18.52 o -5 9 3 22.50 24.28 7.85 o -3 9 3 355.72 335.34 15.81 o -1 9 3 23.68 37.73 8.28 o 1 9 3 25.34 16.20 9.28 o 3 9 3 371.39 414.45 41.55 o 5 9 3 20.95 8.30 14.59 o -6 10 3 35.40 35.12 30.60 o -4 10 3 157.63 154.22 13.61 o -2 10 3 22.88 19.31 10.27 o 0 10 3 103.29 81.29 29.16 o 2 10 3 251.70 221.44 27.50 o 4 10 3 242.92 276.25 31.83 o -5 11 3 550.04 597.28 51.22 o -3 11 3 39.49 32.91 12.68 o -1 11 3 286.01 290.75 24.08 o 1 11 3 582.53 625.97 44.53 o 3 11 3 154.95 171.30 27.77 o -4 12 3 228.08 250.74 37.06 o -2 12 3 35.76 52.70 25.83 o 0 12 3 316.01 283.51 37.95 o 2 12 3 276.37 301.04 37.36 o -3 13 3 2.96 10.60 15.06 o -1 13 3 14.45 7.53 16.83 o 1 13 3 2.44 -9.14 12.79 o -8 0 4 1982.51 2053.70 57.14 o -6 0 4 5704.62 5698.83 85.74 o -4 0 4 20621.73 20641.71 242.94 o -2 0 4 9576.97 9915.79 102.25 o 0 0 4 4591.80 4573.94 63.73 o 2 0 4 12616.09 12859.53 155.39 o 4 0 4 5749.24 5768.29 141.38 o 6 0 4 2190.17 2099.71 82.40 o -9 1 4 78.53 100.02 28.88 o -7 1 4 160.29 146.86 10.99 o -5 1 4 26.51 20.61 4.06 o -3 1 4 31.22 33.08 3.85 o -1 1 4 998.35 1078.24 13.26 o 1 1 4 10.11 7.31 2.81 o 3 1 4 28.54 34.43 10.61 o 5 1 4 108.51 92.14 24.10 o 7 1 4 48.63 38.37 12.63 o -10 2 4 42.73 72.10 27.56 o -8 2 4 0.42 -2.30 6.34 o -6 2 4 445.44 453.21 17.71 o -4 2 4 46.37 50.86 5.03 o -2 2 4 17.81 21.06 2.94 o 0 2 4 138.63 144.46 9.13 o 2 2 4 66.95 73.49 10.61 o 4 2 4 427.41 440.95 50.35 o 6 2 4 185.44 188.73 19.32 o -9 3 4 1668.69 1714.33 69.14 o -7 3 4 2881.46 2917.09 48.54 o -5 3 4 3507.15 3474.07 44.45 o -3 3 4 6115.09 6068.59 55.59 o -1 3 4 11624.26 11576.03 108.40 o 1 3 4 7602.08 7540.24 92.24 o 3 3 4 3334.57 3155.65 98.98 o 5 3 4 2135.58 2220.72 130.49 o 7 3 4 1286.31 1357.32 49.41 o -10 4 4 125.29 154.29 28.27 o -8 4 4 68.60 58.89 11.46 o -6 4 4 20.50 8.07 6.57 o -4 4 4 2.07 2.45 3.47 o -2 4 4 119.42 137.97 6.41 o 0 4 4 390.82 370.93 12.50 o 2 4 4 139.72 119.21 17.79 o 4 4 4 8.25 5.29 8.80 o 6 4 4 7.72 17.73 10.22 o -9 5 4 228.48 221.04 42.98 o -7 5 4 451.25 444.81 20.20 o -5 5 4 12.03 23.97 5.66 o -3 5 4 87.80 87.40 6.70 o -1 5 4 2557.92 2610.89 34.25 o 1 5 4 660.10 663.70 38.04 o 3 5 4 43.14 34.08 13.67 o 5 5 4 235.80 269.00 25.64 o -8 6 4 1341.52 1386.45 61.15 o -6 6 4 2167.51 2287.38 38.83 o -4 6 4 1073.63 1060.46 27.31 o -2 6 4 4193.10 4201.72 51.78 o 0 6 4 5427.77 5222.17 82.12 o 2 6 4 1454.12 1376.67 47.34 o 4 6 4 1660.20 1734.36 60.63 o 6 6 4 1155.81 1286.53 72.45 o -9 7 4 84.86 80.50 22.35 o -7 7 4 192.90 156.51 16.73 o -5 7 4 184.84 181.70 12.17 o -3 7 4 0.47 2.23 4.26 o -1 7 4 53.63 35.83 6.83 o 1 7 4 50.12 49.19 14.19 o 3 7 4 31.48 31.78 10.53 o 5 7 4 468.90 465.50 75.35 o -8 8 4 115.96 108.05 23.87 o -6 8 4 58.33 68.73 8.61 o -4 8 4 609.26 654.62 22.22 o -2 8 4 181.99 181.21 13.34 o 0 8 4 104.46 104.72 12.62 o 2 8 4 672.54 693.25 34.81 o 4 8 4 110.37 107.55 14.31 o -7 9 4 811.97 885.87 54.69 o -5 9 4 2582.50 2722.34 41.67 o -3 9 4 2895.41 3014.46 53.81 o -1 9 4 978.44 964.58 41.41 o 1 9 4 1564.71 1643.17 51.29 o 3 9 4 2262.66 2338.01 61.79 o 5 9 4 1082.04 1250.50 95.03 o -6 10 4 57.06 34.74 18.26 o -4 10 4 45.55 39.51 10.72 o -2 10 4 15.79 8.26 8.46 o 0 10 4 13.22 15.82 8.60 o 2 10 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