#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016225.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016225_Fobs loop_ _publ_author_name 'Meng, Xiang-Gao' 'Zhou, Chun-Shan' 'Wang, Li' 'Liu, Chang-Lin' _publ_section_title ; Two salts of 5-sulfosalicylic acid and 3-aminopyridine ; _journal_coeditor_code AV3101 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o667 _journal_page_last o670 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.957 _cell_angle_gamma 90.000 _cell_length_a 13.9642 _cell_length_b 12.8331 _cell_length_c 15.7831 _exptl_crystal_F_000 1296.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file av3101IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 061216bm in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 504.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14741.67 16449.20 460.90 o 4 0 0 254302.41 263555.88 7190.47 o 6 0 0 234.80 341.48 18.96 o 8 0 0 2750.88 2680.77 84.90 o 10 0 0 1446.46 1694.14 53.12 o 12 0 0 147.55 174.21 25.88 o 14 0 0 34.53 9.42 38.28 o 16 0 0 0.71 0.00 47.98 o 1 1 0 1407.71 1477.48 27.60 o 2 1 0 2423.75 2685.08 49.81 o 3 1 0 3018.19 2960.91 55.47 o 4 1 0 14662.43 15620.81 281.19 o 5 1 0 384.95 418.66 11.77 o 6 1 0 44.96 49.38 6.27 o 7 1 0 1704.89 1671.26 34.10 o 8 1 0 1384.83 1384.13 30.19 o 9 1 0 149.04 186.46 11.06 o 10 1 0 428.82 434.32 16.93 o 11 1 0 0.03 0.00 7.90 o 12 1 0 297.52 367.63 31.63 o 13 1 0 8.22 8.20 13.87 o 14 1 0 29.28 8.34 21.65 o 15 1 0 0.84 18.29 24.95 o 16 1 0 0.80 0.00 43.13 o 0 2 0 137.92 139.74 9.72 o 1 2 0 1332.89 1605.84 28.83 o 2 2 0 1580.98 1492.36 27.29 o 3 2 0 58519.37 65324.47 1086.68 o 4 2 0 355.87 353.72 10.56 o 5 2 0 337.39 385.55 19.70 o 6 2 0 685.08 654.55 17.60 o 7 2 0 11867.47 12775.54 233.88 o 8 2 0 70.05 70.40 8.35 o 9 2 0 287.70 306.79 13.63 o 10 2 0 1.18 0.97 7.46 o 11 2 0 0.11 0.00 10.00 o 12 2 0 31.73 41.67 12.43 o 13 2 0 23.59 44.32 18.27 o 14 2 0 3.39 3.62 21.91 o 15 2 0 2.02 0.00 30.88 o 16 2 0 1.69 0.00 33.61 o 1 3 0 923.14 922.34 21.17 o 2 3 0 1484.37 1456.40 27.45 o 3 3 0 1.95 7.93 3.60 o 4 3 0 248.97 244.91 9.39 o 5 3 0 24.94 37.88 5.52 o 6 3 0 273.55 247.07 10.07 o 7 3 0 1938.85 2046.45 40.75 o 8 3 0 245.33 270.77 12.30 o 9 3 0 105.75 101.62 10.88 o 10 3 0 127.74 143.33 19.84 o 11 3 0 65.15 59.67 13.50 o 12 3 0 50.92 59.39 14.57 o 13 3 0 43.25 32.41 16.47 o 14 3 0 2.99 21.06 21.73 o 15 3 0 20.20 12.86 29.93 o 16 3 0 0.00 0.00 31.92 o 0 4 0 7981.08 9116.88 254.12 o 1 4 0 1013.46 999.36 23.77 o 2 4 0 3774.99 3967.00 74.60 o 3 4 0 610.84 584.58 14.93 o 4 4 0 1035.39 925.53 20.27 o 5 4 0 3.61 4.86 4.35 o 6 4 0 0.19 7.01 5.00 o 7 4 0 665.85 669.70 18.52 o 8 4 0 908.75 914.46 23.30 o 9 4 0 256.78 286.26 15.10 o 10 4 0 358.91 382.95 32.63 o 11 4 0 0.16 0.00 11.23 o 12 4 0 8.41 9.09 17.00 o 13 4 0 21.37 0.00 16.84 o 14 4 0 12.54 44.68 25.14 o 15 4 0 5.02 42.60 29.31 o 16 4 0 4.01 5.61 35.76 o 1 5 0 7.49 11.07 3.68 o 2 5 0 51.09 62.82 5.64 o 3 5 0 123.41 121.31 7.08 o 4 5 0 2100.53 2191.76 41.86 o 5 5 0 508.39 480.77 14.39 o 6 5 0 1098.17 1065.17 24.34 o 7 5 0 11.89 12.79 5.98 o 8 5 0 5.31 3.89 6.80 o 9 5 0 414.19 431.69 23.03 o 10 5 0 44.35 47.58 12.67 o 11 5 0 142.34 151.35 20.01 o 12 5 0 39.33 36.80 18.01 o 13 5 0 28.05 11.73 19.17 o 14 5 0 0.00 0.00 19.97 o 15 5 0 0.56 20.88 40.69 o 0 6 0 194.66 169.23 11.96 o 1 6 0 334.23 266.97 10.25 o 2 6 0 4.35 0.62 4.39 o 3 6 0 393.59 406.05 12.99 o 4 6 0 152.06 149.54 8.60 o 5 6 0 1012.50 982.09 22.96 o 6 6 0 403.37 388.95 18.25 o 7 6 0 112.74 128.60 9.66 o 8 6 0 136.43 144.87 14.28 o 9 6 0 111.29 142.41 15.39 o 10 6 0 849.57 850.83 40.68 o 11 6 0 146.04 125.79 20.28 o 12 6 0 110.57 75.56 20.19 o 13 6 0 70.78 87.35 23.56 o 14 6 0 63.58 75.81 24.60 o 15 6 0 14.21 0.00 29.40 o 1 7 0 2104.48 2239.80 46.63 o 2 7 0 36.74 29.88 5.75 o 3 7 0 1854.92 1811.34 36.78 o 4 7 0 91.71 103.15 8.11 o 5 7 0 18.43 33.07 7.53 o 6 7 0 86.86 90.25 8.63 o 7 7 0 233.82 271.21 16.05 o 8 7 0 133.64 110.01 16.09 o 9 7 0 760.41 837.78 43.62 o 10 7 0 300.78 288.73 25.24 o 11 7 0 100.01 131.05 38.26 o 12 7 0 35.17 39.48 19.81 o 13 7 0 33.40 33.07 21.76 o 14 7 0 6.90 9.43 22.49 o 15 7 0 73.19 166.78 46.35 o 0 8 0 115.71 113.12 12.74 o 1 8 0 90.08 58.36 14.76 o 2 8 0 776.01 742.37 23.36 o 3 8 0 796.87 745.01 20.48 o 4 8 0 789.75 749.29 20.84 o 5 8 0 340.32 355.26 15.79 o 6 8 0 101.71 98.31 10.43 o 7 8 0 301.90 332.13 24.58 o 8 8 0 9.68 16.00 12.74 o 9 8 0 637.86 704.98 37.47 o 10 8 0 54.40 38.70 17.63 o 11 8 0 31.86 36.12 18.72 o 12 8 0 74.00 106.38 23.41 o 13 8 0 61.39 37.78 21.68 o 14 8 0 50.31 57.65 26.77 o 1 9 0 190.16 229.68 14.49 o 2 9 0 6062.14 6245.25 129.81 o 3 9 0 209.14 194.63 11.76 o 4 9 0 294.15 288.56 19.47 o 5 9 0 0.01 0.00 7.83 o 6 9 0 43.64 37.75 12.78 o 7 9 0 32.70 14.12 14.13 o 8 9 0 1039.77 1024.08 45.04 o 9 9 0 123.42 138.19 20.68 o 10 9 0 228.18 329.36 30.16 o 11 9 0 7.86 6.15 24.55 o 12 9 0 221.08 321.57 33.54 o 13 9 0 6.53 13.02 24.20 o 14 9 0 27.01 0.00 47.98 o 0 10 0 1021.17 967.71 40.57 o 1 10 0 331.46 307.04 23.88 o 2 10 0 10.72 11.72 7.35 o 3 10 0 1.61 5.23 8.39 o 4 10 0 266.24 279.19 17.79 o 5 10 0 15.18 5.30 12.02 o 6 10 0 1.48 9.71 12.77 o 7 10 0 117.32 153.28 20.22 o 8 10 0 1.18 0.00 14.34 o 9 10 0 6.28 22.03 18.22 o 10 10 0 24.10 40.87 19.82 o 11 10 0 6.36 29.05 19.91 o 12 10 0 0.33 10.25 21.94 o 13 10 0 5.33 13.33 62.68 o 1 11 0 56.03 59.59 10.28 o 2 11 0 56.83 25.47 10.71 o 3 11 0 292.84 294.26 18.97 o 4 11 0 286.86 286.88 19.12 o 5 11 0 1957.94 1946.22 64.13 o 6 11 0 294.89 329.63 27.63 o 7 11 0 141.58 198.32 23.85 o 8 11 0 2.65 0.00 15.86 o 9 11 0 96.82 77.40 21.20 o 10 11 0 17.18 19.59 20.03 o 11 11 0 11.91 5.58 21.22 o 12 11 0 7.92 13.87 24.25 o 0 12 0 120.98 145.91 30.20 o 1 12 0 593.13 642.51 30.34 o 2 12 0 1.07 0.00 10.35 o 3 12 0 558.17 553.58 28.97 o 4 12 0 273.32 258.42 24.91 o 5 12 0 59.70 56.90 18.32 o 6 12 0 118.47 126.92 21.05 o 7 12 0 169.76 239.97 28.29 o 8 12 0 4.17 0.00 18.47 o 9 12 0 2.08 0.00 19.94 o 10 12 0 1.34 17.53 21.74 o 11 12 0 0.87 8.42 25.74 o 1 13 0 105.14 121.62 37.72 o 2 13 0 2.16 2.19 14.37 o 3 13 0 1.50 0.00 16.91 o 4 13 0 71.86 58.18 18.45 o 5 13 0 403.97 366.42 31.71 o 6 13 0 242.88 296.25 30.16 o 7 13 0 162.63 217.04 34.86 o 8 13 0 89.80 89.13 36.22 o 9 13 0 2.14 10.99 22.05 o 10 13 0 13.31 0.00 31.81 o 0 14 0 130.33 146.60 34.84 o 1 14 0 2.00 0.00 18.73 o 2 14 0 85.90 112.11 35.04 o 3 14 0 1.15 0.00 21.92 o 4 14 0 199.92 204.39 26.86 o 5 14 0 39.78 55.73 22.00 o 6 14 0 62.24 117.72 26.03 o 7 14 0 54.81 118.13 30.04 o 8 14 0 15.16 24.06 32.41 o 9 14 0 21.19 47.93 39.96 o 1 15 0 0.24 1.39 24.67 o 2 15 0 116.29 117.61 35.33 o 3 15 0 14.79 0.00 29.82 o 4 15 0 6.92 35.05 33.77 o 5 15 0 23.10 13.62 23.51 o 6 15 0 6.51 30.81 26.11 o 7 15 0 3.99 32.12 30.00 o 0 16 0 73.01 63.08 52.03 o 1 16 0 574.00 627.80 59.85 o 2 16 0 0.65 0.00 34.24 o 3 16 0 122.69 109.52 37.82 o 4 16 0 19.83 10.88 88.29 o 5 16 0 32.56 165.25 64.16 o -15 0 1 47.73 0.00 27.73 o -13 0 1 1.82 34.51 31.27 o -11 0 1 275.72 330.32 34.22 o -9 0 1 0.93 1.85 12.33 o -7 0 1 1194.39 995.02 31.67 o -5 0 1 629.36 618.44 20.93 o -3 0 1 130.08 157.05 8.80 o -1 0 1 6.88 7.30 2.10 o 1 0 1 78.43 37.08 5.37 o 3 0 1 1485.08 1425.34 38.24 o 5 0 1 288.32 239.62 12.75 o 7 0 1 108.22 133.41 14.93 o 9 0 1 0.02 0.00 8.43 o 11 0 1 89.23 31.44 15.29 o 13 0 1 4.79 8.06 37.34 o 15 0 1 44.41 57.42 50.41 o -17 1 1 7.65 62.81 60.92 o -16 1 1 0.35 0.00 29.83 o -15 1 1 16.54 29.56 25.39 o -14 1 1 7.08 0.00 16.68 o -13 1 1 16.43 9.07 14.48 o -12 1 1 0.14 13.52 10.42 o -11 1 1 214.37 211.75 15.36 o -10 1 1 61.00 70.42 8.79 o -9 1 1 0.83 4.22 6.14 o -8 1 1 35.98 15.84 6.03 o -7 1 1 2622.18 2373.74 52.71 o -6 1 1 3559.59 3265.79 68.73 o -5 1 1 3598.67 3436.87 65.25 o -4 1 1 7187.73 7260.93 132.47 o -3 1 1 1306.19 1316.17 26.09 o -2 1 1 1646.81 1577.78 27.85 o -1 1 1 100.30 82.56 4.33 o 0 1 1 491.47 541.41 11.05 o 1 1 1 2962.61 2922.71 53.66 o 2 1 1 8233.13 8220.84 148.38 o 3 1 1 6637.41 6516.74 118.99 o 4 1 1 7113.15 6949.72 127.70 o 5 1 1 883.79 767.70 19.02 o 6 1 1 221.82 194.16 9.78 o 7 1 1 19.14 19.17 5.48 o 8 1 1 120.52 118.64 14.59 o 9 1 1 35.10 29.66 7.18 o 10 1 1 0.76 3.40 8.01 o 11 1 1 42.20 37.31 10.35 o 12 1 1 46.04 37.58 13.49 o 13 1 1 5.68 8.68 16.21 o 14 1 1 0.01 0.00 23.90 o 15 1 1 0.73 5.47 35.31 o 16 1 1 22.25 94.62 55.26 o -16 2 1 28.64 42.96 37.45 o -15 2 1 0.27 1.71 27.90 o -14 2 1 8.75 26.60 24.47 o -13 2 1 32.25 30.28 14.47 o -12 2 1 64.83 29.81 11.08 o -11 2 1 365.25 306.11 18.13 o -10 2 1 86.25 80.78 11.05 o -9 2 1 81.44 74.82 8.32 o -8 2 1 101.05 96.44 8.16 o -7 2 1 9174.33 9347.84 161.22 o -6 2 1 8.10 4.31 4.20 o -5 2 1 3006.68 3040.19 54.76 o -4 2 1 2183.84 2007.13 36.96 o -3 2 1 32401.27 33519.89 558.90 o -2 2 1 2453.15 2394.20 41.99 o -1 2 1 13154.05 14006.33 270.02 o 0 2 1 9.26 0.00 3.44 o 1 2 1 7237.53 7424.39 134.35 o 2 2 1 17.39 21.82 4.45 o 3 2 1 401.99 415.68 13.47 o 4 2 1 272.01 249.63 10.06 o 5 2 1 858.88 788.10 18.22 o 6 2 1 155.37 176.62 10.37 o 7 2 1 202.38 193.25 10.15 o 8 2 1 26.32 18.80 6.48 o 9 2 1 498.27 554.40 27.65 o 10 2 1 15.53 9.56 8.61 o 11 2 1 8.57 34.77 10.37 o 12 2 1 0.46 2.19 14.77 o 13 2 1 86.29 91.72 20.93 o 14 2 1 25.00 33.37 21.48 o 15 2 1 2.91 0.00 59.04 o 16 2 1 39.32 92.46 60.38 o -16 3 1 0.52 0.00 31.42 o -15 3 1 125.83 105.23 45.15 o -14 3 1 0.01 0.00 16.99 o -13 3 1 7.39 37.22 16.56 o -12 3 1 11.98 13.81 11.78 o -11 3 1 795.17 752.23 28.21 o -10 3 1 37.43 44.69 9.18 o -9 3 1 275.68 272.56 12.70 o -8 3 1 312.54 289.29 12.34 o -7 3 1 375.58 329.42 12.21 o -6 3 1 905.87 812.08 19.16 o -5 3 1 1277.67 1101.39 23.12 o -4 3 1 236.50 183.57 7.33 o -3 3 1 7568.27 7272.52 124.05 o -2 3 1 7.70 10.83 3.29 o -1 3 1 332.08 296.28 10.57 o 0 3 1 996.43 912.89 24.06 o 1 3 1 4832.06 4825.39 88.99 o 2 3 1 511.30 472.84 12.98 o 3 3 1 57.05 66.36 4.96 o 4 3 1 826.76 827.77 19.58 o 5 3 1 107.76 98.54 7.01 o 6 3 1 45.02 39.61 6.55 o 7 3 1 2253.10 2168.53 43.02 o 8 3 1 1649.13 1574.71 34.15 o 9 3 1 292.72 302.91 15.61 o 10 3 1 177.16 195.28 14.13 o 11 3 1 50.28 84.77 19.53 o 12 3 1 41.62 35.78 14.84 o 13 3 1 46.86 43.58 19.40 o 14 3 1 2.80 0.00 22.86 o 15 3 1 11.12 0.00 32.34 o 16 3 1 0.70 0.00 48.25 o -16 4 1 1.24 13.12 49.60 o -15 4 1 104.23 152.88 38.31 o -14 4 1 34.11 24.64 19.22 o -13 4 1 0.63 0.00 15.56 o -12 4 1 1.15 3.22 14.37 o -11 4 1 233.72 227.08 17.17 o -10 4 1 404.55 373.06 20.43 o -9 4 1 33.64 30.93 8.07 o -8 4 1 548.01 578.45 17.72 o -7 4 1 64.94 69.56 7.59 o -6 4 1 395.51 352.23 17.27 o -5 4 1 42.29 34.71 4.98 o -4 4 1 93.29 75.44 5.71 o -3 4 1 702.25 637.74 15.34 o -2 4 1 6005.15 6079.68 104.78 o -1 4 1 1332.47 1294.59 25.37 o 0 4 1 1696.35 1816.13 36.31 o 1 4 1 6.92 6.58 3.38 o 2 4 1 178.29 212.85 8.32 o 3 4 1 81.71 82.61 9.61 o 4 4 1 865.23 794.60 18.24 o 5 4 1 867.47 794.03 18.77 o 6 4 1 379.86 396.61 13.31 o 7 4 1 575.61 504.44 22.38 o 8 4 1 881.70 892.44 27.47 o 9 4 1 22.18 20.57 9.95 o 10 4 1 12.91 16.21 11.40 o 11 4 1 73.82 74.47 29.96 o 12 4 1 11.28 7.21 14.68 o 13 4 1 32.71 60.44 26.19 o 14 4 1 6.33 22.55 25.16 o 15 4 1 16.14 34.47 38.05 o -16 5 1 0.35 0.00 34.92 o -15 5 1 2.93 31.71 23.81 o -14 5 1 2.84 12.02 20.28 o -13 5 1 8.78 26.40 25.68 o -12 5 1 2.88 23.63 16.45 o -11 5 1 54.58 60.24 16.03 o -10 5 1 353.74 352.25 21.96 o -9 5 1 218.82 245.67 14.13 o -8 5 1 533.07 514.25 18.96 o -7 5 1 292.34 299.85 12.33 o -6 5 1 505.87 468.73 15.26 o -5 5 1 21.34 16.39 5.24 o -4 5 1 112.60 102.59 6.85 o -3 5 1 547.83 563.40 19.18 o -2 5 1 5773.74 6946.83 120.03 o -1 5 1 270.54 271.56 16.97 o 0 5 1 23.54 26.98 4.45 o 1 5 1 598.66 647.19 18.16 o 2 5 1 12779.19 15255.12 276.14 o 3 5 1 447.87 448.13 13.28 o 4 5 1 1451.01 1323.98 27.51 o 5 5 1 78.41 83.64 6.82 o 6 5 1 7103.01 7434.90 130.37 o 7 5 1 471.68 447.72 17.17 o 8 5 1 0.06 5.83 8.10 o 9 5 1 302.71 344.82 19.24 o 10 5 1 106.97 129.79 17.78 o 11 5 1 63.40 72.14 16.00 o 12 5 1 20.46 7.61 20.57 o 13 5 1 1.69 0.00 17.16 o 14 5 1 6.93 0.00 23.29 o 15 5 1 1.32 0.00 27.07 o -15 6 1 64.33 95.13 27.63 o -14 6 1 15.86 43.75 22.68 o -13 6 1 54.21 71.81 20.46 o -12 6 1 0.19 0.00 16.30 o -11 6 1 182.02 257.37 34.16 o -10 6 1 9.80 0.17 12.45 o -9 6 1 148.14 128.04 17.27 o -8 6 1 11.98 20.23 7.73 o -7 6 1 669.01 624.43 18.36 o -6 6 1 51.76 48.15 6.74 o -5 6 1 102.82 99.22 8.48 o -4 6 1 43.09 42.98 6.03 o -3 6 1 1371.15 1277.44 28.13 o -2 6 1 975.00 901.88 20.71 o -1 6 1 2630.95 2560.25 51.43 o 0 6 1 938.33 975.95 23.32 o 1 6 1 2763.64 2873.24 61.88 o 2 6 1 1328.68 1327.27 32.21 o 3 6 1 1596.02 1633.59 41.39 o 4 6 1 402.04 363.64 12.58 o 5 6 1 28.07 39.34 6.22 o 6 6 1 20.85 18.38 6.15 o 7 6 1 1568.74 1562.88 40.63 o 8 6 1 15.69 11.01 9.24 o 9 6 1 794.45 803.12 36.64 o 10 6 1 48.62 44.72 15.59 o 11 6 1 2.17 0.00 14.85 o 12 6 1 61.12 74.60 20.60 o 13 6 1 55.67 30.70 22.02 o 14 6 1 1.50 10.14 24.99 o 15 6 1 2.93 0.00 35.76 o -15 7 1 168.57 231.38 34.40 o -14 7 1 7.39 25.88 22.48 o -13 7 1 90.17 110.86 24.34 o -12 7 1 74.06 87.49 28.87 o -11 7 1 288.90 280.26 26.53 o -10 7 1 166.81 158.82 20.97 o -9 7 1 29.74 8.41 12.06 o -8 7 1 58.37 87.45 14.38 o -7 7 1 608.78 585.31 22.33 o -6 7 1 1.53 0.00 5.73 o -5 7 1 11.03 11.57 6.20 o -4 7 1 4.71 8.92 5.50 o -3 7 1 619.32 604.93 17.20 o -2 7 1 6.64 6.56 5.04 o -1 7 1 131.12 126.50 8.90 o 0 7 1 5.26 10.88 4.95 o 1 7 1 552.40 602.50 18.13 o 2 7 1 119.15 112.62 8.06 o 3 7 1 98.20 97.87 9.71 o 4 7 1 61.15 64.91 7.10 o 5 7 1 1675.07 1612.85 37.06 o 6 7 1 134.77 146.19 12.28 o 7 7 1 1668.42 1606.31 42.38 o 8 7 1 308.02 312.13 21.05 o 9 7 1 1604.49 1510.31 54.32 o 10 7 1 153.47 189.76 30.62 o 11 7 1 278.54 308.69 28.69 o 12 7 1 26.67 31.06 19.66 o 13 7 1 110.58 91.65 28.72 o 14 7 1 4.26 17.89 24.92 o -15 8 1 33.31 10.41 42.19 o -14 8 1 0.05 24.30 24.12 o -13 8 1 83.89 78.39 23.67 o -12 8 1 0.25 0.00 17.40 o -11 8 1 33.17 25.57 18.03 o -10 8 1 197.10 198.37 28.33 o -9 8 1 4.32 9.08 13.63 o -8 8 1 457.15 508.25 30.31 o -7 8 1 14.15 2.95 13.37 o -6 8 1 61.13 68.75 9.62 o -5 8 1 3.73 3.35 6.82 o -4 8 1 317.54 326.53 13.55 o -3 8 1 485.47 592.43 17.98 o -2 8 1 965.50 916.16 24.40 o -1 8 1 1912.50 1888.93 41.71 o 0 8 1 1208.61 1178.90 31.11 o 1 8 1 2299.56 2159.79 50.26 o 2 8 1 1292.85 1244.60 28.50 o 3 8 1 802.13 740.30 30.90 o 4 8 1 125.22 149.21 12.37 o 5 8 1 0.00 7.00 7.85 o 6 8 1 315.87 295.34 17.04 o 7 8 1 295.54 269.22 21.94 o 8 8 1 358.53 345.39 26.63 o 9 8 1 239.29 250.84 35.17 o 10 8 1 150.69 184.74 24.06 o 11 8 1 68.19 9.90 19.09 o 12 8 1 45.81 66.23 22.83 o 13 8 1 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