#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016229.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016229_Fobs loop_ _publ_author_name 'Xu, Duan-Jun' 'Yang, Qian' 'Ma, Li-Jie' 'Nie, Jing-Jing' _publ_section_title ; Diaquabis(2,5-dihydroxybenzoato-\kO)bis(1,10-phenanthroline-\k^2^N,N')strontium(II) bis(1,10-phenanthroline) tetrahydrate ; _journal_coeditor_code BG3052 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m476 _journal_page_last m478 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.526 _cell_angle_gamma 90.000 _cell_length_a 24.7846 _cell_length_b 13.2694 _cell_length_c 18.9986 _exptl_crystal_F_000 2528.00 _reflns_d_resolution_high 0.8348 _[local]_cod_data_source_file bg3052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mlj-5 in c 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 473.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1435.74 1639.54 66.22 o 6 0 0 426.94 382.96 114.09 o 8 0 0 71740.41 69915.77 1221.90 o 10 0 0 22912.69 22658.65 292.62 o 12 0 0 13396.54 13133.80 245.44 o 14 0 0 2384.48 2335.79 101.82 o 16 0 0 9021.37 9874.97 195.07 o 18 0 0 1652.27 1844.55 84.31 o 20 0 0 5931.40 6106.72 152.92 o 22 0 0 1401.84 1480.75 81.94 o 24 0 0 108.75 136.41 73.88 o 26 0 0 189.48 296.33 293.13 o 3 1 0 28046.77 26334.02 226.95 o 5 1 0 35390.98 33502.03 323.42 o 7 1 0 1951.00 2799.89 51.42 o 9 1 0 18299.93 17749.40 185.73 o 11 1 0 6804.43 6329.72 90.08 o 13 1 0 82.86 179.95 32.72 o 15 1 0 4732.24 4951.35 86.98 o 17 1 0 299.38 382.99 59.13 o 19 1 0 1720.26 1715.91 84.38 o 21 1 0 1638.92 1719.57 59.43 o 23 1 0 184.11 232.38 46.78 o 25 1 0 232.52 109.15 77.78 o 27 1 0 441.46 69.42 107.55 o 0 2 0 3752.09 3028.74 92.38 o 2 2 0 1118.17 933.73 23.65 o 4 2 0 24649.64 23399.82 290.37 o 6 2 0 46483.01 50898.10 504.89 o 8 2 0 279.77 365.62 47.39 o 10 2 0 9835.46 9670.61 159.33 o 12 2 0 9334.98 9053.20 134.71 o 14 2 0 21.86 42.86 15.38 o 16 2 0 1278.49 1177.21 65.05 o 18 2 0 5340.59 5588.06 82.80 o 20 2 0 24.28 81.83 73.14 o 22 2 0 26.46 59.59 62.60 o 24 2 0 22.39 9.73 52.50 o 26 2 0 439.48 4.12 123.41 o 1 3 0 1482.77 1474.78 33.52 o 3 3 0 1336.98 1491.44 47.55 o 5 3 0 30216.18 32021.84 249.23 o 7 3 0 2798.38 2799.47 61.53 o 9 3 0 10286.91 11132.66 171.01 o 11 3 0 1297.69 1350.36 81.73 o 13 3 0 8.91 56.34 43.99 o 15 3 0 5612.93 5692.31 118.59 o 17 3 0 365.62 493.44 73.53 o 19 3 0 2635.65 2528.14 118.37 o 21 3 0 87.09 99.71 64.90 o 23 3 0 192.34 105.27 72.04 o 25 3 0 2.43 59.49 73.63 o 0 4 0 14652.26 15096.19 196.70 o 2 4 0 24949.07 22705.04 199.98 o 4 4 0 7775.70 7576.68 80.95 o 6 4 0 14890.72 14368.77 129.30 o 8 4 0 5031.78 5320.95 87.49 o 10 4 0 16699.97 16788.20 239.59 o 12 4 0 1032.40 951.26 75.29 o 14 4 0 3773.42 3512.51 101.77 o 16 4 0 2809.40 2857.63 113.62 o 18 4 0 1504.63 1484.76 132.27 o 20 4 0 140.29 161.59 68.94 o 22 4 0 59.02 71.59 72.81 o 24 4 0 105.74 36.45 70.97 o 26 4 0 225.98 46.07 87.17 o 1 5 0 655.10 796.72 40.35 o 3 5 0 7885.92 7793.28 87.19 o 5 5 0 10216.62 9622.64 100.63 o 7 5 0 875.89 1205.47 36.79 o 9 5 0 1332.25 1759.78 40.77 o 11 5 0 2574.94 2726.39 97.14 o 13 5 0 6569.78 6440.90 128.98 o 15 5 0 1628.48 1677.26 107.28 o 17 5 0 2364.55 2394.56 108.43 o 19 5 0 136.40 201.75 72.10 o 21 5 0 293.52 368.03 84.34 o 23 5 0 416.71 357.15 133.15 o 25 5 0 583.99 98.21 86.37 o 0 6 0 21616.81 19846.78 272.72 o 2 6 0 44719.90 45001.01 407.43 o 4 6 0 3319.05 2992.79 58.55 o 6 6 0 7963.67 7941.76 99.90 o 8 6 0 4587.83 4260.40 75.57 o 10 6 0 699.31 626.48 34.69 o 12 6 0 3017.73 3393.85 100.53 o 14 6 0 5496.10 5472.82 131.85 o 16 6 0 1938.33 2229.08 162.34 o 18 6 0 1538.04 1582.52 107.10 o 20 6 0 1224.49 1396.82 114.54 o 22 6 0 830.24 1261.05 141.18 o 24 6 0 534.28 394.08 198.19 o 1 7 0 21553.44 20652.80 188.24 o 3 7 0 12358.40 11372.50 121.07 o 5 7 0 6157.16 5738.44 91.32 o 7 7 0 13757.79 12921.62 136.39 o 9 7 0 4472.75 4782.27 99.48 o 11 7 0 4128.94 4108.68 79.86 o 13 7 0 3447.12 3595.76 112.13 o 15 7 0 2224.32 2362.13 116.48 o 17 7 0 1049.09 977.00 119.68 o 19 7 0 176.64 258.98 86.57 o 21 7 0 774.91 802.22 124.45 o 23 7 0 458.44 164.90 90.81 o 0 8 0 405.69 495.78 59.70 o 2 8 0 153.50 162.39 32.73 o 4 8 0 3115.78 3306.52 70.85 o 6 8 0 2451.23 2340.27 63.59 o 8 8 0 1974.30 2003.18 55.64 o 10 8 0 195.65 212.54 33.26 o 12 8 0 1551.86 1706.91 62.56 o 14 8 0 512.00 604.53 86.17 o 16 8 0 534.97 713.32 92.23 o 18 8 0 10.13 0.00 81.86 o 20 8 0 92.11 158.28 95.61 o 22 8 0 45.41 103.09 82.15 o 1 9 0 78.79 80.21 38.37 o 3 9 0 112.89 174.56 39.41 o 5 9 0 2574.93 2773.68 71.26 o 7 9 0 45.90 0.00 30.15 o 9 9 0 72.71 118.26 36.58 o 11 9 0 4047.37 4046.54 87.96 o 13 9 0 95.80 149.93 31.73 o 15 9 0 18.18 58.32 66.39 o 17 9 0 369.15 423.67 90.98 o 19 9 0 100.67 128.74 122.53 o 21 9 0 1.09 45.37 120.05 o 0 10 0 950.04 1104.27 98.43 o 2 10 0 66.02 89.81 37.44 o 4 10 0 200.62 269.55 48.57 o 6 10 0 64.82 57.41 36.56 o 8 10 0 163.28 251.34 44.72 o 10 10 0 27.44 23.72 38.85 o 12 10 0 3491.57 3463.12 94.16 o 14 10 0 52.30 79.78 35.27 o 16 10 0 22.41 84.51 99.06 o 18 10 0 509.95 326.64 162.01 o 20 10 0 44.59 60.83 100.69 o 1 11 0 476.75 467.31 54.72 o 3 11 0 1505.12 1537.72 68.88 o 5 11 0 165.12 245.64 54.20 o 7 11 0 706.40 831.53 62.61 o 9 11 0 5493.84 5727.78 151.51 o 11 11 0 1145.05 1306.38 75.54 o 13 11 0 145.95 241.71 52.16 o 15 11 0 94.86 56.33 78.65 o 17 11 0 357.88 265.53 116.81 o 19 11 0 233.63 36.80 92.59 o 0 12 0 1473.33 1710.13 100.60 o 2 12 0 921.56 1120.88 75.84 o 4 12 0 50.15 126.04 47.11 o 6 12 0 1868.10 2184.59 78.39 o 8 12 0 45.80 45.30 46.46 o 10 12 0 1524.41 1769.01 80.05 o 12 12 0 954.87 1157.27 128.84 o 14 12 0 441.87 400.79 52.89 o 16 12 0 289.97 109.99 91.66 o 1 13 0 1607.29 1933.69 86.21 o 3 13 0 174.25 323.47 67.32 o 5 13 0 3770.66 4084.59 102.10 o 7 13 0 3696.31 4144.32 109.14 o 9 13 0 2491.90 2799.79 98.23 o 11 13 0 251.66 331.15 68.79 o 13 13 0 359.17 78.48 69.04 o 15 13 0 687.69 13.84 100.82 o 0 14 0 1220.81 1297.35 107.31 o 2 14 0 235.41 260.56 57.62 o 4 14 0 716.99 942.04 112.96 o 6 14 0 309.87 406.34 81.91 o 8 14 0 42.72 88.91 60.41 o 10 14 0 1201.53 1197.94 149.31 o 12 14 0 733.32 518.51 155.15 o 1 15 0 4.03 0.00 44.97 o 3 15 0 4.02 0.00 47.88 o 5 15 0 2.95 1.08 47.01 o 7 15 0 5.08 0.00 46.94 o 9 15 0 390.56 244.44 67.87 o -27 1 1 7.10 22.43 100.32 o -25 1 1 131.09 75.92 40.61 o -23 1 1 488.11 571.05 50.31 o -21 1 1 83.69 124.66 55.92 o -19 1 1 3345.92 3572.09 75.53 o -17 1 1 1729.64 1668.89 50.92 o -15 1 1 227.13 211.56 46.73 o -13 1 1 1122.75 1022.53 73.80 o -11 1 1 360.83 356.82 66.41 o -9 1 1 315.60 281.56 69.91 o -7 1 1 42122.28 43799.55 564.42 o -5 1 1 214.61 307.22 32.01 o 3 1 1 5545.37 5083.48 52.83 o 5 1 1 6644.59 6678.67 58.31 o 7 1 1 23274.14 23979.67 191.93 o 9 1 1 1794.27 2048.62 42.50 o 11 1 1 3375.53 3258.45 61.37 o 13 1 1 2201.68 2095.06 55.92 o 15 1 1 473.66 499.79 34.56 o 17 1 1 20.77 0.00 26.40 o 19 1 1 1239.93 1285.63 59.61 o 21 1 1 897.41 840.77 52.67 o 23 1 1 628.90 651.98 39.23 o 25 1 1 27.01 44.04 53.31 o -26 2 1 25.53 0.00 59.00 o -24 2 1 658.27 467.32 144.66 o -22 2 1 1556.61 1531.47 97.01 o -20 2 1 2603.45 2692.41 138.00 o -18 2 1 1409.95 1337.24 51.00 o -16 2 1 1993.39 2071.06 55.65 o -14 2 1 7564.60 7880.65 147.66 o -12 2 1 1945.11 1597.15 32.76 o -10 2 1 110.74 113.93 54.40 o -8 2 1 12238.97 11698.81 112.12 o -6 2 1 141570.23 150207.50 3410.56 o -4 2 1 15033.61 13960.42 100.15 o -2 2 1 31115.35 29093.41 206.44 o 0 2 1 2319.11 1925.92 21.30 o 2 2 1 7775.11 8127.77 68.28 o 4 2 1 13465.06 14237.19 135.17 o 6 2 1 3368.01 3235.78 69.04 o 8 2 1 22215.00 22330.26 227.19 o 10 2 1 78.70 107.70 32.10 o 12 2 1 3717.09 3403.17 77.61 o 14 2 1 991.07 882.43 60.49 o 16 2 1 809.26 830.57 65.01 o 18 2 1 143.31 162.60 62.23 o 20 2 1 58.65 41.77 55.16 o 22 2 1 420.92 356.30 106.45 o 24 2 1 464.99 434.04 157.82 o 26 2 1 706.32 793.76 262.59 o -27 3 1 97.29 42.83 74.96 o -25 3 1 129.03 36.26 67.61 o -23 3 1 23.54 45.09 69.19 o -21 3 1 185.04 329.80 81.23 o -19 3 1 2915.47 2847.57 108.77 o -17 3 1 5058.17 5237.00 129.25 o -15 3 1 10056.88 10240.45 234.91 o -13 3 1 12862.18 13794.11 258.99 o -11 3 1 3376.71 3338.11 95.32 o -9 3 1 3305.03 3080.88 70.69 o -7 3 1 19683.46 17053.46 365.44 o -5 3 1 748.68 472.56 27.63 o -3 3 1 9433.56 8564.12 78.28 o -1 3 1 1225.20 1026.12 26.83 o 1 3 1 15682.66 13410.94 118.96 o 3 3 1 26977.11 24985.96 191.53 o 5 3 1 35466.98 33623.42 268.81 o 7 3 1 15728.73 14808.09 160.27 o 9 3 1 2773.39 2520.47 68.21 o 11 3 1 17876.43 17489.31 211.96 o 13 3 1 20115.87 20529.97 223.49 o 15 3 1 2388.64 2439.00 79.77 o 17 3 1 5668.89 6014.69 140.94 o 19 3 1 1834.04 1916.57 104.92 o 21 3 1 28.66 0.00 52.96 o 23 3 1 317.34 191.14 130.02 o 25 3 1 1401.01 1654.43 151.66 o -26 4 1 105.13 0.00 68.53 o -24 4 1 15.44 41.37 86.89 o -22 4 1 794.37 864.80 97.92 o -20 4 1 1755.22 1819.07 125.72 o -18 4 1 1470.67 1736.63 152.22 o -16 4 1 573.43 673.63 132.46 o -14 4 1 3467.46 3392.93 115.97 o -12 4 1 6497.88 6141.97 161.37 o -10 4 1 9041.49 8523.16 122.92 o -8 4 1 107.32 114.71 26.52 o -6 4 1 8554.74 7303.08 78.39 o -4 4 1 10081.32 9257.02 93.67 o -2 4 1 673.37 490.72 36.28 o 0 4 1 10302.45 8555.47 89.09 o 2 4 1 21858.73 20166.11 170.90 o 4 4 1 1443.05 1156.89 36.98 o 6 4 1 522.97 421.45 32.63 o 8 4 1 22538.79 23334.68 320.05 o 10 4 1 25278.02 26863.56 294.25 o 12 4 1 2059.79 2049.54 82.93 o 14 4 1 3335.53 3370.08 106.46 o 16 4 1 1636.79 1736.35 122.62 o 18 4 1 1468.81 1572.35 100.54 o 20 4 1 129.42 88.65 75.77 o 22 4 1 587.30 488.31 120.80 o 24 4 1 714.11 692.09 248.54 o 26 4 1 813.60 587.08 214.88 o -25 5 1 51.83 9.61 83.15 o -23 5 1 109.73 217.48 98.08 o -21 5 1 495.19 474.78 89.21 o -19 5 1 1283.64 1199.16 126.42 o -17 5 1 42.99 72.86 69.57 o -15 5 1 308.72 331.90 92.61 o -13 5 1 201.07 200.85 73.66 o -11 5 1 6257.37 6516.85 114.16 o -9 5 1 250.09 434.99 33.00 o -7 5 1 4730.35 5110.72 85.67 o -5 5 1 84.97 45.90 25.88 o -3 5 1 662.08 637.13 46.85 o -1 5 1 12365.69 12172.38 113.03 o 1 5 1 2245.71 2069.66 43.19 o 3 5 1 656.76 590.08 31.80 o 5 5 1 2098.21 1845.83 46.39 o 7 5 1 2765.20 2958.40 54.21 o 9 5 1 954.26 953.04 36.81 o 11 5 1 1382.84 1515.61 76.40 o 13 5 1 95.04 96.79 61.76 o 15 5 1 473.60 658.12 75.63 o 17 5 1 109.56 110.90 57.07 o 19 5 1 315.67 380.62 77.48 o 21 5 1 449.95 483.57 96.49 o 23 5 1 356.14 238.58 99.83 o 25 5 1 76.85 52.96 79.20 o -24 6 1 1.86 4.25 71.96 o -22 6 1 3.87 18.01 76.33 o -20 6 1 86.29 164.71 123.16 o -18 6 1 257.66 362.37 83.96 o -16 6 1 23.13 62.09 60.80 o -14 6 1 166.62 148.32 93.74 o -12 6 1 208.29 260.82 57.20 o -10 6 1 2214.35 2252.49 59.49 o -8 6 1 2950.56 2716.11 54.10 o -6 6 1 4701.61 5076.27 76.02 o -4 6 1 147.77 272.94 31.27 o -2 6 1 2044.35 1953.16 49.40 o 0 6 1 27625.86 28156.20 249.63 o 2 6 1 6413.97 6855.01 82.60 o 4 6 1 1361.94 1230.52 42.69 o 6 6 1 130.56 86.53 33.79 o 8 6 1 11070.86 11493.60 119.51 o 10 6 1 419.40 451.07 30.63 o 12 6 1 15.21 86.21 62.39 o 14 6 1 1.25 0.00 60.48 o 16 6 1 167.43 186.87 76.52 o 18 6 1 228.44 180.64 65.48 o 20 6 1 375.47 360.49 83.99 o 22 6 1 186.99 137.95 81.70 o 24 6 1 24.96 0.00 71.79 o -25 7 1 179.81 120.04 93.18 o -23 7 1 131.22 60.54 89.16 o -21 7 1 269.61 205.19 147.85 o -19 7 1 128.49 219.73 109.61 o -17 7 1 590.24 667.51 89.28 o -15 7 1 556.05 571.06 180.48 o -13 7 1 1676.50 1510.56 82.65 o -11 7 1 44.99 22.44 31.44 o -9 7 1 405.79 370.30 58.97 o -7 7 1 1460.72 1500.36 49.31 o -5 7 1 3627.72 3599.63 65.81 o -3 7 1 306.27 313.06 36.74 o -1 7 1 5812.69 6108.64 86.57 o 1 7 1 25275.74 25833.84 244.85 o 3 7 1 5521.23 5769.47 86.83 o 5 7 1 6856.34 6469.57 92.48 o 7 7 1 350.50 439.19 34.41 o 9 7 1 546.50 613.23 50.58 o 11 7 1 45.09 89.24 27.54 o 13 7 1 496.69 466.49 75.98 o 15 7 1 496.94 578.84 81.51 o 17 7 1 800.17 956.28 97.88 o 19 7 1 81.79 223.47 75.80 o 21 7 1 298.01 207.79 98.00 o 23 7 1 127.06 36.05 78.86 o -24 8 1 674.11 671.24 154.28 o -22 8 1 491.79 435.34 155.52 o -20 8 1 650.43 317.50 173.66 o -18 8 1 29.38 78.51 81.00 o -16 8 1 1291.69 1468.33 104.15 o -14 8 1 501.25 484.95 70.36 o -12 8 1 843.50 891.45 54.19 o -10 8 1 980.16 1112.61 48.69 o -8 8 1 887.42 819.79 50.39 o -6 8 1 2338.41 2186.24 60.44 o -4 8 1 6213.18 5948.12 89.20 o -2 8 1 6310.44 6114.88 88.34 o 0 8 1 4842.43 4354.37 74.41 o 2 8 1 833.32 750.33 54.20 o 4 8 1 3340.53 3363.19 65.26 o 6 8 1 6384.72 6439.25 98.77 o 8 8 1 2100.93 2173.20 60.79 o 10 8 1 1228.47 1309.12 48.13 o 12 8 1 34.03 41.29 48.30 o 14 8 1 1380.86 1633.92 114.44 o 16 8 1 2420.63 2312.26 147.24 o 18 8 1 47.45 101.19 76.98 o 20 8 1 740.47 673.32 92.50 o 22 8 1 423.82 350.02 95.87 o -23 9 1 546.28 538.41 141.09 o -21 9 1 253.15 161.09 126.91 o -19 9 1 88.22 75.00 79.60 o -17 9 1 187.74 329.46 87.64 o -15 9 1 1835.38 2002.92 95.16 o -13 9 1 5756.47 5608.46 99.68 o -11 9 1 613.98 730.14 63.25 o -9 9 1 752.40 742.49 53.21 o -7 9 1 4362.53 4295.55 95.70 o -5 9 1 6440.83 6423.10 105.12 o -3 9 1 618.38 670.21 48.24 o -1 9 1 1408.96 1415.21 55.56 o 1 9 1 3434.31 3632.36 75.78 o 3 9 1 3190.32 3248.78 79.30 o 5 9 1 8643.57 8740.79 114.65 o 7 9 1 4185.20 4423.71 85.32 o 9 9 1 709.40 893.80 51.74 o 11 9 1 62.39 63.64 31.21 o 13 9 1 4252.51 4384.27 135.72 o 15 9 1 3760.65 3995.13 168.10 o 17 9 1 1785.36 1882.15 147.38 o 19 9 1 824.77 1111.31 227.25 o 21 9 1 220.86 205.74 80.95 o -20 10 1 311.09 174.66 100.60 o -18 10 1 29.49 36.75 77.52 o -16 10 1 89.15 90.36 75.84 o -14 10 1 208.59 238.14 47.91 o -12 10 1 1070.09 1277.94 68.88 o -10 10 1 4768.13 4850.35 112.76 o -8 10 1 3646.13 3825.92 91.86 o -6 10 1 2855.61 2948.85 78.43 o -4 10 1 1687.81 1765.56 85.89 o -2 10 1 6738.15 6672.53 107.22 o 0 10 1 55.85 44.45 36.20 o 2 10 1 3240.65 3515.92 86.19 o 4 10 1 1386.79 1409.69 69.93 o 6 10 1 3758.20 3609.43 80.81 o 8 10 1 1948.27 2017.80 70.00 o 10 10 1 4051.76 4308.76 88.29 o 12 10 1 3564.99 3542.77 148.14 o 14 10 1 987.55 1042.31 54.89 o 16 10 1 677.43 687.55 101.22 o 18 10 1 1798.09 2017.97 134.98 o 20 10 1 445.90 260.31 152.37 o -19 11 1 124.57 252.67 124.67 o -17 11 1 101.31 53.60 94.44 o -15 11 1 13.51 17.74 58.42 o -13 11 1 655.88 611.16 54.55 o -11 11 1 32.05 8.60 43.37 o -9 11 1 372.75 376.70 56.13 o -7 11 1 107.24 101.60 44.38 o -5 11 1 229.10 243.62 51.44 o -3 11 1 2902.53 3015.40 83.56 o -1 11 1 875.20 794.89 59.28 o 1 11 1 377.14 441.24 51.70 o 3 11 1 1268.30 1211.28 65.66 o 5 11 1 938.74 912.52 59.64 o 7 11 1 59.80 58.52 48.70 o 9 11 1 32.80 16.86 35.10 o 11 11 1 361.95 283.93 46.45 o 13 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