#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:12:38 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180831 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016260.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016260_Fobs loop_ _publ_author_name 'Portalone, Gustavo' 'Colapietro, Marcello' _publ_section_title ; Hydrogen-bonded supramolecular motifs in the 1:1 monohydrated molecular adduct of acetoguanaminium chloride with acetoguanamine and in 2,4,6-triaminopyrimidinediium dichloride dihydrate ; _journal_coeditor_code GZ3095 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o655 _journal_page_last o658 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.742 _cell_angle_gamma 90.000 _cell_length_a 9.4045 _cell_length_b 8.6089 _cell_length_c 13.7420 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.7090 _cod_data_source_file gz3095IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title '2,4,6-triaminopyrimidinediium dichloride dihydrate' _shelx_refln_list_code 4 _shelx_f_calc_maximum 140.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1614.83 1406.42 9.79 o 4 0 0 547.27 515.67 4.11 o 6 0 0 465.06 451.65 3.84 o 8 0 0 41.62 41.06 1.16 o 10 0 0 189.15 184.11 2.45 o 12 0 0 6.42 6.66 1.24 o 1 1 0 1239.52 1226.51 8.44 o 3 1 0 0.39 6.25 0.50 o 5 1 0 581.24 552.80 4.72 o 7 1 0 116.84 105.98 1.45 o 9 1 0 219.48 220.35 2.68 o 11 1 0 3.35 2.21 1.07 o 0 2 0 582.68 664.69 5.18 o 2 2 0 4855.96 5037.76 34.22 o 4 2 0 2514.18 2336.68 17.48 o 6 2 0 85.09 75.13 1.22 o 8 2 0 46.36 45.15 1.21 o 10 2 0 108.65 101.88 2.03 o 12 2 0 23.58 23.43 1.46 o 1 3 0 2544.79 2625.72 18.53 o 3 3 0 2608.56 2573.49 18.34 o 5 3 0 872.35 844.82 7.01 o 7 3 0 395.31 398.66 3.61 o 9 3 0 344.04 343.00 3.72 o 11 3 0 16.42 17.54 1.26 o 0 4 0 127.30 155.85 1.76 o 2 4 0 195.07 178.97 1.88 o 4 4 0 168.08 158.62 1.77 o 6 4 0 39.56 37.04 1.10 o 8 4 0 2.65 3.12 0.85 o 1 5 0 1732.27 2006.49 14.40 o 3 5 0 1020.62 1036.80 8.41 o 5 5 0 2204.02 2159.56 16.80 o 7 5 0 89.42 91.42 1.54 o 9 5 0 270.33 270.64 3.30 o 11 5 0 24.87 26.34 1.34 o 0 6 0 348.20 398.26 3.61 o 2 6 0 400.24 379.64 3.52 o 4 6 0 12.68 15.90 0.80 o 6 6 0 324.01 322.84 3.25 o 8 6 0 250.30 243.28 3.13 o 10 6 0 14.67 12.43 1.20 o 1 7 0 21.08 25.02 1.00 o 3 7 0 33.49 38.03 1.11 o 5 7 0 229.56 229.39 2.74 o 7 7 0 140.94 131.32 2.07 o 9 7 0 11.79 13.81 1.12 o 0 8 0 525.60 511.57 4.54 o 2 8 0 244.83 255.65 2.89 o 4 8 0 151.34 146.47 2.19 o 6 8 0 0.76 0.51 0.95 o 8 8 0 7.01 7.35 1.09 o 1 9 0 246.44 224.85 2.71 o 3 9 0 3.43 3.64 1.00 o 0 10 0 93.88 110.36 1.90 o 2 10 0 60.19 55.69 1.50 o 4 10 0 28.22 24.32 1.29 o 6 10 0 38.65 37.29 1.47 o 3 11 0 18.01 16.38 1.30 o 5 11 0 28.71 28.44 1.50 o 0 12 0 5.82 5.38 1.26 o -12 1 1 29.29 30.96 1.45 o -10 1 1 87.28 88.75 1.70 o -8 1 1 289.01 283.01 3.04 o -6 1 1 3123.75 2996.13 21.99 o -4 1 1 8039.03 8161.49 50.81 o -2 1 1 15.31 27.70 0.63 o 0 1 1 3949.39 4108.48 20.60 o 2 1 1 1677.77 1675.03 12.33 o 4 1 1 270.62 247.37 2.53 o 6 1 1 2042.34 2017.30 15.34 o 8 1 1 740.52 719.10 6.46 o 10 1 1 102.66 106.18 1.86 o 12 1 1 11.87 13.29 1.32 o -11 2 1 72.51 72.71 1.71 o -9 2 1 120.59 117.87 1.96 o -7 2 1 240.11 259.20 2.91 o -5 2 1 1993.98 2127.02 15.75 o -3 2 1 5631.25 5748.39 39.60 o -1 2 1 3948.43 3851.27 26.18 o 1 2 1 997.19 956.90 7.46 o 3 2 1 3747.27 3603.58 25.32 o 5 2 1 1448.92 1398.15 10.52 o 7 2 1 529.15 537.79 4.66 o 9 2 1 87.67 83.53 1.65 o 11 2 1 30.70 26.44 1.34 o -12 3 1 5.35 6.51 1.18 o -10 3 1 4.42 6.01 0.98 o -8 3 1 489.44 476.75 4.39 o -6 3 1 127.64 115.70 1.51 o -4 3 1 8.10 8.96 0.54 o -2 3 1 2814.61 2737.01 19.97 o 0 3 1 4030.16 4016.30 28.01 o 2 3 1 3354.39 3359.46 24.45 o 4 3 1 649.63 590.25 4.88 o 6 3 1 76.05 89.89 1.33 o 8 3 1 56.96 56.29 1.36 o 10 3 1 93.98 88.18 1.89 o -11 4 1 86.90 90.27 1.91 o -9 4 1 160.57 157.61 2.27 o -7 4 1 187.56 202.82 2.29 o -5 4 1 232.37 222.14 2.40 o -3 4 1 1015.99 921.81 7.32 o -1 4 1 8229.31 8085.45 52.38 o 1 4 1 238.73 169.16 1.83 o 3 4 1 3903.31 3826.38 27.34 o 5 4 1 538.76 507.04 4.52 o 7 4 1 87.05 88.75 1.51 o 9 4 1 43.00 42.23 1.31 o 11 4 1 30.41 30.51 1.44 o -10 5 1 22.89 22.09 1.32 o -6 5 1 1.60 3.45 0.71 o -4 5 1 14.75 13.22 0.73 o -2 5 1 321.77 292.89 2.75 o 0 5 1 2.41 3.99 0.64 o 2 5 1 22.96 19.89 0.81 o 4 5 1 235.07 230.61 2.44 o 6 5 1 5.73 8.31 0.81 o -11 6 1 30.38 27.80 1.38 o -9 6 1 174.49 169.69 2.62 o -7 6 1 154.17 153.85 2.24 o -5 6 1 3.23 3.60 0.76 o -3 6 1 15.94 13.51 0.74 o -1 6 1 1137.70 1077.95 9.23 o 1 6 1 2726.73 2723.36 19.92 o 3 6 1 570.36 546.21 4.69 o 5 6 1 63.01 60.12 1.25 o 7 6 1 5.59 7.68 0.95 o 9 6 1 29.79 28.33 1.28 o -10 7 1 10.64 10.39 1.17 o -8 7 1 7.21 7.80 1.01 o -6 7 1 1414.18 1420.77 11.36 o -4 7 1 6.95 6.46 0.82 o -2 7 1 211.09 224.85 2.41 o 0 7 1 186.45 172.58 2.11 o 2 7 1 202.95 192.94 2.51 o 4 7 1 67.26 68.66 1.33 o 6 7 1 9.34 6.30 0.96 o 8 7 1 546.79 541.53 5.14 o 10 7 1 5.07 3.16 1.14 o -7 8 1 29.81 28.12 1.28 o -5 8 1 8.61 6.30 0.96 o -3 8 1 323.23 305.05 3.16 o -1 8 1 15.64 10.01 0.89 o 1 8 1 182.79 148.66 2.20 o 3 8 1 7.30 5.57 0.90 o 5 8 1 105.41 100.27 1.81 o 9 8 1 8.29 8.84 1.19 o -8 9 1 44.90 48.02 1.53 o -6 9 1 61.24 64.24 1.61 o -4 9 1 75.60 74.60 1.56 o -2 9 1 196.13 197.14 2.54 o 0 9 1 48.96 54.20 1.48 o 2 9 1 36.65 43.67 1.33 o 4 9 1 119.28 116.79 1.95 o 6 9 1 34.22 35.71 1.32 o 8 9 1 24.73 27.38 1.37 o -3 10 1 4.39 5.48 1.08 o -1 10 1 0.00 1.68 0.99 o 1 10 1 43.10 51.86 1.45 o 5 10 1 7.02 7.14 1.18 o -4 11 1 33.18 30.07 1.43 o 0 11 1 2.94 2.58 1.13 o 2 11 1 1.29 1.98 1.13 o 4 11 1 4.01 4.49 1.19 o -1 12 1 96.18 100.87 2.22 o 1 12 1 24.13 24.52 1.49 o -12 0 2 422.15 416.50 4.51 o -10 0 2 114.69 111.21 1.91 o -8 0 2 789.52 750.13 6.60 o -6 0 2 0.18 0.68 0.56 o -4 0 2 1051.35 1008.54 7.65 o -2 0 2 244.12 303.30 2.45 o 0 0 2 678.76 563.24 4.29 o 4 0 2 156.02 217.68 2.07 o 6 0 2 389.44 401.87 3.62 o 8 0 2 143.16 138.32 1.89 o 10 0 2 32.50 30.62 1.33 o 12 0 2 29.03 27.28 1.47 o -11 1 2 14.99 15.34 1.18 o -9 1 2 31.70 29.63 1.09 o -7 1 2 867.44 870.11 7.11 o -5 1 2 291.46 264.40 2.61 o -3 1 2 1606.16 1618.79 11.31 o -1 1 2 1083.96 1209.68 9.08 o 1 1 2 2965.43 2913.15 20.60 o 3 1 2 145.20 132.94 1.39 o 5 1 2 16.52 16.30 0.73 o 7 1 2 176.91 180.58 2.16 o 9 1 2 19.86 19.53 1.15 o 11 1 2 40.20 38.90 1.50 o -12 2 2 36.76 36.68 1.46 o -10 2 2 114.51 117.00 1.96 o -8 2 2 361.10 366.06 3.46 o -6 2 2 325.95 311.75 2.84 o -4 2 2 344.82 301.20 2.79 o -2 2 2 6214.92 6176.41 37.89 o 0 2 2 6204.70 6494.55 35.61 o 2 2 2 546.66 558.01 4.27 o 4 2 2 1626.82 1547.66 11.85 o 6 2 2 585.93 593.19 5.38 o 8 2 2 10.50 12.78 0.93 o 10 2 2 2.56 5.06 0.99 o -11 3 2 3.02 5.20 1.05 o -9 3 2 76.55 75.30 1.57 o -7 3 2 1421.32 1428.35 11.39 o -5 3 2 781.11 744.64 6.03 o -3 3 2 1329.52 1294.25 10.12 o -1 3 2 6308.45 5901.69 40.12 o 1 3 2 1391.90 1499.83 11.67 o 3 3 2 906.26 973.76 7.52 o 5 3 2 613.53 578.60 4.83 o 7 3 2 332.98 336.70 3.32 o 9 3 2 127.52 127.44 2.04 o 11 3 2 54.53 60.59 1.72 o -12 4 2 34.82 32.54 1.49 o -10 4 2 6.29 6.25 1.00 o -8 4 2 42.56 39.03 1.25 o -6 4 2 35.21 32.09 0.91 o -4 4 2 48.13 45.15 0.94 o -2 4 2 803.74 731.00 5.97 o 0 4 2 9.58 9.95 0.63 o 2 4 2 209.63 243.28 2.51 o 4 4 2 160.30 144.77 1.69 o 6 4 2 19.49 29.85 0.99 o 8 4 2 12.79 12.43 0.99 o 10 4 2 0.01 0.99 1.02 o -9 5 2 98.11 94.52 1.76 o -7 5 2 682.73 696.13 6.36 o -5 5 2 414.26 395.46 3.60 o -3 5 2 4287.71 4199.10 31.24 o -1 5 2 932.69 961.26 7.47 o 1 5 2 1026.87 1194.36 9.02 o 3 5 2 852.96 892.77 7.20 o 5 5 2 544.06 558.96 4.75 o 7 5 2 705.77 704.63 6.40 o 9 5 2 9.12 11.59 1.09 o 11 5 2 70.18 67.83 1.82 o -10 6 2 60.21 62.64 1.59 o -8 6 2 49.23 45.82 1.36 o -6 6 2 782.59 771.74 6.70 o -4 6 2 566.26 549.97 4.71 o -2 6 2 6.22 7.35 0.76 o 0 6 2 277.69 253.41 2.56 o 2 6 2 275.51 300.85 3.14 o 4 6 2 293.13 292.89 3.09 o 6 6 2 17.13 16.46 0.98 o 8 6 2 143.70 137.61 2.12 o 10 6 2 61.87 58.42 1.69 o -9 7 2 18.37 18.22 1.20 o -7 7 2 32.11 34.17 1.17 o -5 7 2 338.90 322.84 3.61 o -3 7 2 475.64 484.67 4.42 o -1 7 2 13.25 16.46 0.90 o 1 7 2 24.48 30.85 1.00 o 3 7 2 25.35 27.70 1.06 o 5 7 2 27.98 29.85 1.10 o 7 7 2 69.17 71.68 1.70 o 9 7 2 35.88 32.31 1.48 o -8 8 2 5.11 5.57 1.09 o -6 8 2 29.52 30.18 1.21 o -4 8 2 0.98 1.60 0.89 o -2 8 2 291.82 304.00 3.15 o 0 8 2 125.90 130.40 1.84 o 2 8 2 433.06 418.14 4.11 o 4 8 2 210.99 209.75 2.62 o 6 8 2 44.09 41.83 1.43 o -7 9 2 35.21 32.31 1.37 o -5 9 2 13.99 14.87 1.08 o -3 9 2 7.78 8.31 0.98 o 1 9 2 162.84 143.08 2.16 o 3 9 2 181.91 171.52 2.37 o 5 9 2 4.70 3.91 1.07 o -6 10 2 53.99 55.54 1.65 o -4 10 2 54.67 55.69 1.50 o -2 10 2 44.69 40.16 1.40 o 0 10 2 92.88 89.13 1.90 o 2 10 2 71.32 81.89 1.82 o 4 10 2 25.72 24.52 1.29 o 6 10 2 10.31 11.25 1.21 o -5 11 2 12.14 10.85 1.26 o -3 11 2 37.84 44.21 1.60 o -1 11 2 27.26 31.52 1.35 o 0 12 2 42.44 42.62 1.70 o -12 1 3 88.14 82.25 2.00 o -10 1 3 125.52 130.17 2.06 o -8 1 3 312.00 296.68 3.11 o -6 1 3 498.10 461.09 4.31 o -4 1 3 9563.23 10075.02 56.45 o 0 1 3 289.08 248.95 2.22 o 2 1 3 3059.32 2938.14 21.78 o 4 1 3 507.47 524.37 4.60 o 6 1 3 182.81 177.63 2.14 o 8 1 3 405.46 394.66 3.99 o 10 1 3 135.29 137.14 2.35 o -11 2 3 131.46 136.44 2.11 o -9 2 3 222.61 229.08 2.74 o -7 2 3 415.43 432.64 4.18 o -5 2 3 507.81 611.43 4.97 o -3 2 3 3772.57 3910.08 28.89 o -1 2 3 9134.10 8937.65 45.58 o 1 2 3 704.83 725.58 5.95 o 3 2 3 739.74 617.90 4.99 o 5 2 3 1267.55 1236.38 9.89 o 7 2 3 293.36 299.46 3.13 o 9 2 3 101.34 97.67 1.79 o 11 2 3 23.37 20.15 1.35 o -10 3 3 6.08 5.62 1.00 o -8 3 3 49.66 49.43 1.27 o -6 3 3 1792.13 1896.47 14.00 o -4 3 3 85.48 76.70 1.06 o -2 3 3 6.93 11.12 0.54 o 0 3 3 3751.52 3571.09 25.21 o 2 3 3 1043.33 1020.69 7.70 o 4 3 3 870.49 863.61 7.08 o 6 3 3 78.16 75.65 1.40 o 8 3 3 71.56 67.83 1.49 o 10 3 3 9.87 10.72 1.18 o -11 4 3 39.69 40.16 1.53 o -9 4 3 312.47 311.39 3.54 o -7 4 3 515.71 518.86 4.58 o -5 4 3 497.77 520.70 4.58 o -3 4 3 279.20 267.02 2.63 o -1 4 3 1039.29 936.51 7.38 o 1 4 3 7018.77 7087.00 50.73 o 3 4 3 204.51 177.63 1.87 o 5 4 3 1129.97 1089.19 8.62 o 7 4 3 182.11 183.57 2.45 o 9 4 3 17.49 21.90 1.22 o 11 4 3 5.58 1.89 1.19 o -10 5 3 2.15 1.40 1.02 o -8 5 3 64.19 66.67 1.48 o -6 5 3 1.23 0.44 0.68 o -4 5 3 0.15 2.78 0.64 o -2 5 3 18.03 12.50 0.78 o 0 5 3 137.46 120.07 1.54 o 2 5 3 61.02 60.12 1.09 o 4 5 3 32.26 31.30 1.01 o 6 5 3 83.84 89.70 1.52 o -11 6 3 24.66 27.17 1.36 o -9 6 3 156.69 154.10 2.24 o -7 6 3 524.99 546.21 5.16 o -5 6 3 546.10 544.80 4.69 o -3 6 3 4.14 3.53 0.72 o -1 6 3 0.35 2.30 0.70 o 1 6 3 1330.97 1305.84 10.16 o 3 6 3 1177.56 1169.50 8.93 o 5 6 3 212.10 210.62 2.62 o 7 6 3 56.23 55.69 1.50 o 9 6 3 5.85 5.15 1.09 o -8 7 3 35.55 35.11 1.31 o -6 7 3 11.32 14.41 0.99 o -4 7 3 2248.39 2224.45 17.05 o -2 7 3 0.43 0.15 2.31 o 0 7 3 351.32 377.68 3.51 o 2 7 3 73.95 64.72 1.29 o 4 7 3 91.47 92.58 1.55 o 6 7 3 17.39 18.48 1.12 o 8 7 3 6.46 6.25 1.11 o -9 8 3 4.38 1.87 1.12 o -5 8 3 74.23 71.85 1.53 o -3 8 3 17.85 17.12 1.00 o -1 8 3 480.49 463.68 4.33 o 1 8 3 20.91 15.98 1.04 o 3 8 3 147.97 131.09 2.07 o 5 8 3 3.70 4.62 0.95 o 7 8 3 17.43 17.46 1.17 o -8 9 3 41.72 35.23 1.43 o -6 9 3 125.66 122.94 2.23 o -4 9 3 99.69 101.88 1.82 o -2 9 3 100.99 102.29 1.83 o 0 9 3 200.54 194.05 2.52 o 2 9 3 29.68 31.97 1.25 o 4 9 3 12.38 13.88 1.12 o 6 9 3 45.99 44.47 1.61 o -7 10 3 31.38 32.09 1.48 o -1 10 3 0.74 2.33 1.01 o 1 10 3 1.86 3.72 1.05 o 3 10 3 21.49 25.02 1.31 o -4 11 3 69.89 71.85 1.87 o -2 11 3 42.74 34.76 1.54 o 0 11 3 0.38 1.03 1.14 o 2 11 3 5.37 7.14 1.18 o -12 0 4 4.46 3.57 1.14 o -10 0 4 1410.96 1423.80 11.37 o -8 0 4 757.62 727.20 5.96 o -6 0 4 2189.46 2149.31 16.76 o -4 0 4 442.84 433.48 3.76 o -2 0 4 403.62 406.31 3.24 o 0 0 4 432.43 515.67 4.11 o 2 0 4 9.81 12.93 0.58 o 4 0 4 19681.89 20179.56 97.02 o 6 0 4 3.34 3.38 0.74 o 8 0 4 173.07 169.95 2.36 o 10 0 4 27.81 30.85 1.34 o -13 1 4 36.88 33.23 1.51 o -11 1 4 120.71 119.63 1.98 o -9 1 4 48.31 48.16 1.25 o -7 1 4 137.16 153.60 1.74 o -5 1 4 2400.30 2458.63 17.93 o -3 1 4 94.02 97.47 1.19 o -1 1 4 2835.19 2596.98 18.43 o 1 1 4 1584.22 1755.72 13.47 o 3 1 4 1191.61 1232.14 9.87 o 5 1 4 17.81 19.71 0.80 o 7 1 4 6.30 7.80 0.84 o 9 1 4 56.78 52.15 1.45 o 11 1 4 0.52 1.24 1.14 o -12 2 4 97.46 100.87 2.02 o -10 2 4 158.05 151.86 2.23 o -8 2 4 314.47 328.28 3.28 o -6 2 4 855.06 903.61 7.25 o -4 2 4 1036.66 1121.24 8.74 o -2 2 4 485.69 461.95 3.89 o 0 2 4 4917.78 4921.53 35.23 o 2 2 4 2570.08 2583.69 19.40 o 4 2 4 397.81 379.64 3.52 o 6 2 4 402.95 396.65 4.00 o 8 2 4 121.99 124.06 2.01 o -11 3 4 30.65 28.33 1.28 o -9 3 4 0.72 0.44 0.88 o -7 3 4 233.71 214.43 2.35 o -5 3 4 3914.84 4184.79 29.89 o -3 3 4 768.79 610.43 4.96 o -1 3 4 1510.47 1520.12 10.96 o 1 3 4 4143.24 4099.47 29.58 o 3 3 4 361.69 369.15 3.47 o 5 3 4 213.13 227.26 2.42 o 7 3 4 91.71 118.75 1.97 o 9 3 4 89.33 90.08 1.91 o 11 3 4 22.29 23.53 1.36 o -12 4 4 8.47 8.14 1.20 o -10 4 4 133.18 130.17 2.06 o -8 4 4 12.30 13.00 0.94 o -6 4 4 155.27 156.35 1.76 o -4 4 4 213.34 213.84 2.06 o -2 4 4 13.85 17.29 0.67 o 0 4 4 805.70 767.28 6.12 o 2 4 4 112.49 120.07 1.54 o 4 4 4 164.71 185.20 2.19 o 6 4 4 42.30 41.32 1.16 o -9 5 4 0.20 0.41 0.93 o -7 5 4 206.25 202.25 2.29 o -5 5 4 1170.24 1170.88 9.62 o -3 5 4 1127.14 1097.82 8.65 o -1 5 4 3829.91 3796.61 27.23 o 1 5 4 569.31 590.25 4.88 o 3 5 4 232.79 263.09 2.93 o 5 5 4 198.01 201.97 2.28 o 7 5 4 167.36 164.24 2.32 o 9 5 4 154.43 156.86 2.52 o -10 6 4 46.19 47.19 1.52 o -8 6 4 195.28 196.30 2.53 o -6 6 4 119.39 115.49 1.73 o -4 6 4 1617.61 1616.36 12.11 o -2 6 4 648.82 625.41 5.53 o 0 6 4 2.36 2.95 0.72 o 2 6 4 89.38 85.38 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