#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:12:38 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180831 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016269.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016269_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Bhuiyan, M. Delower H.' 'Kay, Andrew J.' _publ_section_title ; Geometry and bond-length alternation in nonlinear optical materials. I. Standard parameters in two precursors ; _journal_coeditor_code JZ3086 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o633 _journal_page_last o637 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.5731 _cell_length_b 9.6510 _cell_length_c 22.7965 _exptl_crystal_F_000 1552.00 _reflns_d_resolution_high 0.7022 _cod_data_source_file jz3086Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' d66brf in Pbca RElabelled & centred Jun 14th, 2007 (like BZTT)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 324.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 105026.94 104298.98 1394.84 o 6 0 0 10494.52 10666.94 136.49 o 8 0 0 2995.46 3402.00 91.61 o 10 0 0 4230.05 4310.44 80.95 o 12 0 0 625.84 635.21 32.19 o 14 0 0 658.38 639.08 44.16 o 16 0 0 3966.83 3879.64 102.46 o 18 0 0 326.27 229.46 67.98 o 20 0 0 677.07 627.03 94.91 o 22 0 0 1.83 -70.59 70.59 o 24 0 0 297.91 301.14 97.85 o 2 1 0 622.71 522.56 17.20 o 4 1 0 6391.15 6249.83 60.93 o 6 1 0 11681.47 11653.89 118.59 o 8 1 0 74.27 98.51 10.80 o 10 1 0 650.94 663.41 22.69 o 12 1 0 455.58 487.68 21.51 o 14 1 0 106.39 115.92 19.29 o 16 1 0 160.42 170.83 32.62 o 18 1 0 362.50 317.64 37.45 o 20 1 0 326.05 320.15 59.01 o 22 1 0 44.99 15.20 54.27 o 24 1 0 52.51 19.98 54.87 o 0 2 0 5884.65 5515.14 49.05 o 2 2 0 17210.29 16793.05 140.80 o 4 2 0 5860.82 5650.81 63.59 o 6 2 0 226.97 254.78 19.29 o 8 2 0 414.73 382.53 32.55 o 10 2 0 11.53 21.12 13.04 o 12 2 0 187.53 184.33 28.52 o 14 2 0 3471.86 3469.51 83.15 o 16 2 0 783.66 822.93 46.24 o 18 2 0 173.66 186.75 37.53 o 20 2 0 328.72 339.65 41.44 o 22 2 0 310.28 336.75 63.40 o 24 2 0 26.91 -4.62 54.21 o 2 3 0 56.60 62.98 9.39 o 4 3 0 20356.07 20658.42 196.69 o 6 3 0 2540.63 2421.10 65.45 o 8 3 0 72.60 57.44 25.73 o 10 3 0 1.86 -30.41 30.41 o 12 3 0 513.20 464.68 36.95 o 14 3 0 230.27 224.45 35.79 o 16 3 0 179.06 184.67 36.28 o 18 3 0 2523.84 2598.48 95.88 o 20 3 0 752.30 845.78 90.75 o 22 3 0 31.18 53.00 60.76 o 24 3 0 17.49 -74.61 74.61 o 0 4 0 41.39 28.40 12.33 o 2 4 0 3837.83 3795.30 33.05 o 4 4 0 2065.03 2049.45 36.24 o 6 4 0 4723.46 4795.50 72.42 o 8 4 0 876.95 818.12 48.42 o 10 4 0 1216.88 1157.89 63.40 o 12 4 0 41.52 8.01 40.89 o 14 4 0 1078.73 1186.23 57.63 o 16 4 0 158.23 84.45 43.85 o 18 4 0 599.56 695.53 66.70 o 20 4 0 62.25 71.51 38.88 o 22 4 0 36.75 29.23 155.02 o 2 5 0 1299.87 1295.73 26.37 o 4 5 0 3123.88 3191.44 50.17 o 6 5 0 60.01 53.94 17.71 o 8 5 0 672.71 740.93 49.14 o 10 5 0 359.47 326.61 40.38 o 12 5 0 0.50 -51.37 54.52 o 14 5 0 73.36 45.40 38.49 o 16 5 0 1248.75 1224.04 63.12 o 18 5 0 706.80 649.33 51.04 o 20 5 0 644.78 597.09 57.84 o 22 5 0 292.75 299.92 83.02 o 0 6 0 7563.93 7728.74 110.47 o 2 6 0 337.55 337.31 26.55 o 4 6 0 477.99 532.65 24.52 o 6 6 0 61.62 52.73 21.13 o 8 6 0 489.61 418.71 41.98 o 10 6 0 126.41 143.77 67.28 o 12 6 0 1446.27 1426.03 67.24 o 14 6 0 1293.09 1267.49 72.16 o 16 6 0 160.18 189.09 78.68 o 18 6 0 1079.98 1057.56 115.68 o 20 6 0 92.10 8.08 40.08 o 22 6 0 103.10 0.76 85.90 o 2 7 0 563.59 542.28 33.31 o 4 7 0 14.37 -1.50 24.16 o 6 7 0 816.34 813.90 40.77 o 8 7 0 559.16 585.03 49.47 o 10 7 0 3584.89 3447.06 99.18 o 12 7 0 461.03 432.03 50.61 o 14 7 0 792.13 796.31 61.03 o 16 7 0 1184.15 1233.59 141.50 o 18 7 0 50.20 41.87 62.90 o 20 7 0 443.44 413.07 68.67 o 0 8 0 166.53 182.86 39.63 o 2 8 0 133.05 129.63 28.83 o 4 8 0 9.59 -24.09 24.09 o 6 8 0 2805.23 2753.70 67.55 o 8 8 0 178.89 182.90 29.33 o 10 8 0 36.98 7.91 26.47 o 12 8 0 2096.56 2168.93 90.23 o 14 8 0 1.78 -1.76 41.62 o 16 8 0 151.54 154.78 49.41 o 18 8 0 181.90 121.54 52.80 o 2 9 0 0.57 -26.45 26.45 o 4 9 0 92.47 98.00 29.91 o 6 9 0 7.66 -26.18 26.18 o 8 9 0 0.97 -5.66 28.12 o 10 9 0 193.90 220.70 32.48 o 12 9 0 99.04 131.00 46.68 o 14 9 0 16.31 -16.30 41.70 o 16 9 0 0.38 -17.21 44.17 o 18 9 0 2.42 -24.33 63.31 o 2 10 0 589.08 602.74 82.70 o 4 10 0 1213.94 1099.51 51.22 o 6 10 0 2875.60 2685.59 108.45 o 8 10 0 1528.67 1585.96 94.30 o 10 10 0 472.20 510.40 59.87 o 12 10 0 118.86 132.36 50.40 o 14 10 0 253.42 170.77 54.17 o 16 10 0 0.72 -18.57 68.42 o 2 11 0 0.33 -33.23 51.58 o 4 11 0 587.15 575.13 50.83 o 6 11 0 29.54 53.96 56.74 o 8 11 0 68.78 57.77 64.40 o 10 11 0 826.77 780.70 94.59 o 12 11 0 613.01 444.27 84.60 o 14 11 0 251.54 426.24 91.55 o 4 12 0 144.88 88.40 67.66 o 6 12 0 122.08 197.86 70.91 o 8 12 0 812.30 783.30 91.55 o 10 12 0 408.51 359.78 83.51 o 12 12 0 89.80 0.00 64.18 o 4 13 0 92.42 84.38 69.50 o 6 13 0 50.88 -61.47 61.47 o 1 1 1 1298.70 1018.31 23.46 o 2 1 1 8216.20 7090.63 139.78 o 3 1 1 450.20 454.39 10.88 o 4 1 1 4753.21 4462.50 35.96 o 5 1 1 6409.17 6742.82 51.06 o 6 1 1 2709.96 2827.15 22.93 o 7 1 1 5159.55 5346.03 39.31 o 8 1 1 1745.14 1771.23 19.91 o 9 1 1 1574.26 1664.70 19.32 o 10 1 1 36.24 52.72 8.68 o 11 1 1 1207.30 1239.94 24.79 o 12 1 1 85.92 121.61 10.98 o 13 1 1 165.66 195.55 13.41 o 14 1 1 0.04 9.71 12.19 o 15 1 1 261.71 249.90 20.46 o 16 1 1 481.17 441.59 25.75 o 17 1 1 476.47 462.57 23.23 o 18 1 1 9.63 -4.06 24.51 o 19 1 1 393.35 349.76 32.54 o 20 1 1 2.65 -32.29 32.29 o 21 1 1 309.58 293.53 41.01 o 22 1 1 60.34 60.06 39.31 o 23 1 1 44.44 -19.96 36.94 o 24 1 1 24.36 -29.89 39.48 o 0 2 1 12499.21 11725.10 71.28 o 1 2 1 803.03 797.83 8.85 o 2 2 1 6598.76 6116.45 39.97 o 3 2 1 364.38 335.00 10.48 o 4 2 1 2283.92 2239.05 26.49 o 5 2 1 39.44 45.10 8.56 o 6 2 1 2264.11 2385.18 27.51 o 7 2 1 1098.55 1177.47 27.46 o 8 2 1 7388.21 7698.97 85.98 o 9 2 1 1021.99 972.95 23.62 o 10 2 1 143.25 149.99 14.47 o 11 2 1 1262.54 1231.46 26.62 o 12 2 1 389.90 376.01 15.44 o 13 2 1 4.45 13.66 11.71 o 14 2 1 180.03 196.52 21.58 o 15 2 1 1020.86 1041.73 34.41 o 16 2 1 439.18 422.81 27.54 o 17 2 1 1.61 7.27 21.53 o 18 2 1 96.54 88.57 24.02 o 19 2 1 578.79 569.10 37.27 o 20 2 1 0.12 -26.98 26.98 o 21 2 1 685.40 701.67 50.22 o 22 2 1 114.12 128.21 40.78 o 23 2 1 1.40 3.49 39.66 o 24 2 1 11.90 -39.28 39.28 o 1 3 1 4012.06 3958.15 21.38 o 2 3 1 4728.62 4690.83 28.08 o 3 3 1 165.39 170.31 7.71 o 4 3 1 3239.12 3256.89 38.19 o 5 3 1 2917.10 2881.64 36.95 o 6 3 1 3.28 1.58 12.68 o 7 3 1 480.15 472.11 19.04 o 8 3 1 1107.40 1205.02 43.72 o 9 3 1 206.14 222.44 23.02 o 10 3 1 677.30 729.73 33.28 o 11 3 1 800.53 840.45 44.02 o 12 3 1 242.22 259.16 24.67 o 13 3 1 103.41 101.82 22.13 o 14 3 1 3.22 43.76 21.82 o 15 3 1 1219.22 1363.06 41.57 o 16 3 1 897.76 982.85 47.46 o 17 3 1 41.80 -16.30 23.00 o 18 3 1 51.85 38.45 24.36 o 19 3 1 292.25 303.27 30.18 o 20 3 1 17.67 -12.38 29.15 o 21 3 1 2.34 -28.13 28.13 o 22 3 1 11.73 -31.34 72.98 o 23 3 1 31.91 -20.09 51.37 o 24 3 1 6.94 -56.24 56.24 o 0 4 1 13045.70 13364.34 84.53 o 1 4 1 4665.27 4697.86 25.64 o 2 4 1 970.10 1020.07 13.03 o 3 4 1 1607.68 1575.62 19.83 o 4 4 1 1884.45 1839.30 22.49 o 5 4 1 47.88 35.36 11.18 o 6 4 1 1059.08 993.66 24.93 o 7 4 1 36.82 16.71 12.23 o 8 4 1 1007.35 978.99 35.19 o 9 4 1 4768.45 4851.42 80.40 o 10 4 1 75.71 79.52 26.46 o 11 4 1 1239.36 1296.36 46.65 o 12 4 1 136.92 156.14 28.43 o 13 4 1 1375.47 1453.72 46.69 o 14 4 1 1151.26 1058.24 64.33 o 15 4 1 23.96 24.41 22.44 o 16 4 1 681.93 622.98 32.81 o 17 4 1 675.79 695.88 35.58 o 18 4 1 18.45 -24.29 24.29 o 19 4 1 0.23 -24.93 24.93 o 20 4 1 157.70 153.88 32.62 o 21 4 1 227.06 195.04 35.26 o 22 4 1 219.50 203.02 36.51 o 23 4 1 8.75 -10.07 41.93 o 1 5 1 10948.46 11248.55 64.27 o 2 5 1 607.95 649.72 15.32 o 3 5 1 1253.36 1230.76 27.02 o 4 5 1 183.92 193.67 12.22 o 5 5 1 584.36 653.16 23.03 o 6 5 1 29.88 16.73 14.88 o 7 5 1 213.91 184.89 13.36 o 8 5 1 3044.82 2914.13 47.58 o 9 5 1 583.16 539.34 32.02 o 10 5 1 44.25 43.53 26.81 o 11 5 1 262.28 258.97 30.33 o 12 5 1 3.05 -24.05 24.05 o 13 5 1 424.23 343.59 38.53 o 14 5 1 310.55 304.50 37.17 o 15 5 1 1092.64 1134.90 49.19 o 16 5 1 6.24 0.91 23.60 o 17 5 1 44.69 31.22 25.26 o 18 5 1 343.92 353.92 48.44 o 19 5 1 70.35 20.21 27.32 o 20 5 1 333.26 309.54 54.69 o 21 5 1 295.00 262.46 58.20 o 22 5 1 340.30 366.08 63.26 o 23 5 1 51.12 -63.80 63.80 o 0 6 1 2119.32 2093.84 34.80 o 1 6 1 45.97 49.68 10.85 o 2 6 1 197.92 200.43 17.01 o 3 6 1 240.21 242.77 16.50 o 4 6 1 865.36 834.92 22.06 o 5 6 1 237.15 241.12 16.17 o 6 6 1 421.57 427.89 20.39 o 7 6 1 1117.57 1120.42 26.88 o 8 6 1 52.08 53.23 13.45 o 9 6 1 135.98 89.15 25.50 o 10 6 1 6.21 2.60 25.57 o 11 6 1 1036.63 1025.19 42.77 o 12 6 1 100.77 92.44 26.98 o 13 6 1 22.64 -22.17 25.51 o 14 6 1 6.20 -24.97 24.97 o 15 6 1 7.51 18.70 27.99 o 16 6 1 219.86 218.84 29.18 o 17 6 1 66.54 47.54 26.31 o 18 6 1 4.52 -25.68 25.68 o 19 6 1 296.76 299.65 43.74 o 20 6 1 19.30 -7.22 32.30 o 21 6 1 41.51 -10.78 44.90 o 22 6 1 7.80 -55.34 55.34 o 1 7 1 476.91 518.38 17.62 o 2 7 1 4.97 -10.10 14.18 o 3 7 1 189.64 194.26 17.46 o 4 7 1 984.70 916.15 28.78 o 5 7 1 340.84 358.34 30.28 o 6 7 1 1915.87 1774.06 37.75 o 7 7 1 956.47 911.50 25.24 o 8 7 1 381.01 377.91 26.19 o 9 7 1 19.92 -15.85 23.38 o 10 7 1 3359.93 3347.96 70.06 o 11 7 1 515.21 513.79 36.13 o 12 7 1 28.56 21.69 26.73 o 13 7 1 9.49 -26.34 26.34 o 14 7 1 185.36 186.72 34.62 o 15 7 1 10.30 -0.98 29.21 o 16 7 1 326.41 307.17 37.56 o 17 7 1 39.94 -16.08 29.47 o 18 7 1 28.30 -0.68 27.99 o 19 7 1 107.12 32.53 33.26 o 20 7 1 115.34 86.76 40.96 o 21 7 1 95.16 0.79 88.45 o 0 8 1 2640.07 2564.92 54.41 o 1 8 1 159.59 160.74 19.17 o 2 8 1 4.76 -6.98 16.27 o 3 8 1 745.92 653.41 27.35 o 4 8 1 1101.77 1013.62 31.69 o 5 8 1 902.25 891.13 30.45 o 6 8 1 3394.34 3336.63 52.44 o 7 8 1 1.61 -11.46 17.86 o 8 8 1 55.77 60.03 19.28 o 9 8 1 448.42 413.02 24.61 o 10 8 1 197.53 212.67 25.17 o 11 8 1 142.72 159.73 23.87 o 12 8 1 102.17 90.90 30.47 o 13 8 1 810.21 752.35 53.87 o 14 8 1 92.16 72.20 31.56 o 15 8 1 234.67 239.39 36.96 o 16 8 1 18.20 -18.28 31.15 o 17 8 1 29.29 -2.00 61.03 o 18 8 1 188.62 196.34 39.73 o 19 8 1 385.85 424.88 51.11 o 20 8 1 340.57 316.26 118.80 o 1 9 1 1284.96 1148.60 41.64 o 2 9 1 1148.98 1113.02 37.36 o 3 9 1 697.87 587.82 33.05 o 4 9 1 7.74 0.31 18.84 o 5 9 1 703.78 723.86 29.62 o 6 9 1 14.78 -5.52 19.62 o 7 9 1 2144.64 1899.05 45.34 o 8 9 1 1009.41 991.68 47.18 o 9 9 1 67.70 44.44 20.68 o 10 9 1 0.27 5.62 19.19 o 11 9 1 20.88 9.70 24.00 o 12 9 1 22.12 12.38 23.42 o 13 9 1 43.89 19.45 30.92 o 14 9 1 93.81 134.43 34.75 o 15 9 1 30.32 9.64 37.49 o 16 9 1 222.29 271.82 44.29 o 17 9 1 182.14 116.61 42.84 o 18 9 1 24.16 54.38 52.78 o 1 10 1 32.87 22.72 29.51 o 2 10 1 32.23 -0.87 26.58 o 3 10 1 128.67 118.27 24.33 o 4 10 1 4.57 5.32 22.63 o 5 10 1 637.18 607.04 32.12 o 6 10 1 90.82 64.90 23.41 o 7 10 1 52.18 83.06 23.60 o 8 10 1 210.77 185.93 25.55 o 9 10 1 349.15 402.89 35.36 o 10 10 1 16.53 7.56 26.84 o 11 10 1 12.66 -14.55 34.66 o 12 10 1 103.37 108.95 40.19 o 13 10 1 2.64 -16.43 34.67 o 14 10 1 2.14 6.93 36.86 o 15 10 1 29.00 -36.08 37.85 o 16 10 1 115.42 87.47 54.28 o 2 11 1 226.22 218.68 34.79 o 3 11 1 74.91 88.96 31.34 o 4 11 1 27.14 18.31 31.87 o 5 11 1 338.66 378.58 31.14 o 6 11 1 86.22 114.95 25.12 o 7 11 1 211.73 295.20 35.36 o 8 11 1 613.09 574.28 63.69 o 9 11 1 63.79 46.83 36.10 o 10 11 1 0.79 11.67 36.08 o 11 11 1 29.18 53.82 38.77 o 12 11 1 34.40 53.72 38.60 o 13 11 1 142.85 125.84 43.41 o 14 11 1 276.04 282.21 56.42 o 3 12 1 3.26 -40.89 40.89 o 4 12 1 0.11 5.17 34.32 o 5 12 1 3.79 3.32 33.18 o 6 12 1 51.33 45.52 40.06 o 7 12 1 341.78 511.26 70.15 o 8 12 1 5.15 29.86 123.80 o 9 12 1 50.80 8.66 44.60 o 10 12 1 177.35 162.24 51.94 o 11 12 1 607.17 533.18 64.79 o 4 13 1 305.82 263.76 55.86 o 5 13 1 8.92 -9.46 44.42 o 6 13 1 9.28 -48.60 48.60 o 7 13 1 0.01 -41.38 41.38 o 2 0 2 1733.13 1519.77 18.65 o 3 0 2 15797.48 15355.49 166.24 o 4 0 2 18857.23 18992.05 180.33 o 5 0 2 22000.41 22153.29 194.75 o 6 0 2 16291.50 16669.39 137.06 o 7 0 2 3784.34 3872.46 40.88 o 8 0 2 3812.65 3934.89 42.50 o 9 0 2 2800.04 2879.03 37.89 o 10 0 2 7090.70 7559.39 80.99 o 11 0 2 14.66 34.51 13.12 o 12 0 2 834.45 904.98 36.26 o 13 0 2 40.63 40.15 18.83 o 14 0 2 172.05 188.06 29.17 o 15 0 2 1563.65 1476.71 52.83 o 16 0 2 26.77 15.84 26.64 o 17 0 2 161.30 137.71 31.27 o 18 0 2 2.67 -28.57 28.57 o 19 0 2 23.69 -44.00 44.00 o 20 0 2 75.17 17.42 49.31 o 21 0 2 33.73 -7.61 87.80 o 22 0 2 0.30 -18.37 51.98 o 23 0 2 2263.45 2644.80 129.22 o 24 0 2 23.67 -53.48 53.48 o 1 1 2 12354.10 10779.71 209.34 o 2 1 2 28.00 26.09 4.57 o 3 1 2 17147.86 16380.29 110.54 o 4 1 2 29315.85 28963.69 194.99 o 5 1 2 32146.31 32915.35 200.26 o 6 1 2 65.93 59.32 7.35 o 7 1 2 305.05 370.23 11.13 o 8 1 2 7612.27 8060.77 60.61 o 9 1 2 648.54 670.10 16.67 o 10 1 2 14.87 29.21 9.41 o 11 1 2 57.27 67.92 11.16 o 12 1 2 469.41 450.29 15.46 o 13 1 2 1.36 -10.98 11.45 o 14 1 2 114.56 95.94 13.61 o 15 1 2 64.89 64.52 19.31 o 16 1 2 0.04 -10.77 18.82 o 17 1 2 51.88 46.01 19.92 o 18 1 2 107.67 75.82 26.41 o 19 1 2 93.73 98.06 27.96 o 20 1 2 2.77 -33.14 33.14 o 21 1 2 247.59 193.20 40.66 o 22 1 2 3.06 -35.56 35.56 o 23 1 2 92.82 90.97 41.80 o 24 1 2 94.06 66.75 40.88 o 0 2 2 35.27 35.06 7.14 o 1 2 2 1827.74 1801.50 14.34 o 2 2 2 378.86 400.53 9.02 o 3 2 2 328.00 332.26 9.24 o 4 2 2 1149.67 1139.79 14.80 o 5 2 2 6620.29 6635.91 52.24 o 6 2 2 121.30 118.00 10.24 o 7 2 2 139.37 132.30 12.23 o 8 2 2 1433.70 1504.78 32.85 o 9 2 2 26.97 37.05 12.53 o 10 2 2 67.48 79.24 13.67 o 11 2 2 241.14 246.63 17.48 o 12 2 2 315.93 305.28 20.02 o 13 2 2 48.51 69.02 16.31 o 14 2 2 20.41 17.97 16.96 o 15 2 2 441.13 443.86 21.95 o 16 2 2 175.37 163.88 18.78 o 17 2 2 660.89 572.08 34.19 o 18 2 2 256.37 278.93 31.51 o 19 2 2 3.15 -25.05 25.05 o 20 2 2 4.06 -12.67 28.23 o 21 2 2 77.08 70.37 37.04 o 22 2 2 0.26 -12.45 37.79 o 23 2 2 1115.64 1221.53 87.18 o 24 2 2 18.04 -39.15 39.15 o 1 3 2 2682.72 2452.44 17.14 o 2 3 2 12702.04 12600.67 65.97 o 3 3 2 18.46 8.12 6.33 o 4 3 2 166.13 181.61 8.94 o 5 3 2 7411.82 7870.72 70.85 o 6 3 2 2613.30 2489.60 46.82 o 7 3 2 2632.39 2864.76 47.99 o 8 3 2 53.43 45.14 12.48 o 9 3 2 113.38 79.82 13.10 o 10 3 2 4360.64 4560.35 61.99 o 11 3 2 125.73 171.59 15.06 o 12 3 2 227.91 243.34 24.56 o 13 3 2 1297.20 1283.51 41.76 o 14 3 2 55.05 64.69 22.95 o 15 3 2 904.79 930.34 34.98 o 16 3 2 28.39 -3.14 21.91 o 17 3 2 2684.43 2764.78 57.37 o 18 3 2 28.17 2.14 26.41 o 19 3 2 1.96 -26.83 26.83 o 20 3 2 554.05 516.92 38.80 o 21 3 2 0.38 -28.26 28.26 o 22 3 2 54.66 -36.90 36.90 o 23 3 2 18.98 -28.84 43.10 o 24 3 2 169.84 79.01 61.40 o 0 4 2 326.27 406.04 14.09 o 1 4 2 274.22 294.39 8.06 o 2 4 2 110.76 107.55 7.93 o 3 4 2 346.97 342.95 10.17 o 4 4 2 4302.78 4441.04 38.39 o 5 4 2 0.88 5.69 9.38 o 6 4 2 69.87 65.84 10.55 o 7 4 2 499.66 520.27 21.31 o 8 4 2 336.86 383.54 17.24 o 9 4 2 174.55 184.63 11.38 o 10 4 2 1102.68 1129.19 46.17 o 11 4 2 1616.41 1571.06 49.79 o 12 4 2 116.41 124.32 26.16 o 13 4 2 24.36 32.16 24.19 o 14 4 2 353.32 354.83 31.44 o 15 4 2 1355.26 1296.72 42.41 o 16 4 2 20.50 -16.39 23.53 o 17 4 2 178.13 135.17 26.80 o 18 4 2 102.29 105.71 32.69 o 19 4 2 15.22 -22.02 28.63 o 20 4 2 317.11 331.85 71.82 o 21 4 2 185.69 174.52 41.09 o 22 4 2 3.60 -20.53 41.67 o 23 4 2 57.44 -20.70 55.52 o 1 5 2 861.27 858.58 15.38 o 2 5 2 509.87 534.61 13.69 o 3 5 2 1152.75 1160.18 19.00 o 4 5 2 10.65 11.09 10.46 o 5 5 2 693.94 708.23 16.51 o 6 5 2 268.70 277.77 15.24 o 7 5 2 256.98 254.70 14.13 o 8 5 2 391.63 384.93 24.42 o 9 5 2 1574.49 1583.44 43.55 o 10 5 2 526.07 523.41 32.25 o 11 5 2 68.32 56.28 25.56 o 12 5 2 223.96 195.39 29.62 o 13 5 2 24.33 17.33 25.01 o 14 5 2 823.76 879.68 37.89 o 15 5 2 594.77 636.73 35.66 o 16 5 2 748.44 779.01 43.23 o 17 5 2 9.35 11.15 27.18 o 18 5 2 28.85 -33.31 33.31 o 19 5 2 21.62 19.01 33.53 o 20 5 2 194.96 205.50 39.82 o 21 5 2 216.84 128.11 57.01 o 22 5 2 115.47 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8 9 55.74 64.14 89.58 o 1 9 9 1139.75 1220.59 38.42 o 2 9 9 772.27 788.66 31.11 o 3 9 9 639.52 632.12 29.14 o 4 9 9 8.08 -4.40 18.55 o 5 9 9 227.71 234.68 23.49 o 6 9 9 33.63 -12.32 20.16 o 7 9 9 30.83 -13.06 25.72 o 8 9 9 93.05 66.18 33.49 o 9 9 9 6.91 -21.05 30.40 o 10 9 9 121.39 103.02 34.71 o 11 9 9 94.58 79.34 35.13 o 12 9 9 403.39 402.28 58.96 o 13 9 9 0.69 -39.01 39.01 o 14 9 9 126.66 101.54 49.79 o 15 9 9 324.64 261.91 45.41 o 16 9 9 19.30 87.98 41.25 o 17 9 9 2.31 5.10 60.71 o 0 10 9 401.53 459.13 51.23 o 1 10 9 78.98 69.85 27.36 o 2 10 9 22.37 24.65 21.85 o 3 10 9 73.07 67.84 21.63 o 4 10 9 31.17 13.32 19.92 o 5 10 9 1208.93 1199.64 43.58 o 6 10 9 2.41 16.32 26.76 o 7 10 9 0.38 18.54 27.79 o 8 10 9 31.68 21.26 28.70 o 9 10 9 0.00 -9.87 28.31 o 10 10 9 13.85 3.14 28.67 o 11 10 9 5.06 -0.79 37.08 o 12 10 9 259.26 239.79 42.57 o 13 10 9 84.56 42.11 37.71 o 14 10 9 25.26 49.68 89.42 o 15 10 9 7.94 50.61 58.10 o 1 11 9 0.97 -18.03 27.36 o 2 11 9 827.22 855.30 45.02 o 3 11 9 137.79 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29 8.72 -25.44 27.66 o 3 3 29 83.22 37.42 29.30 o 4 3 29 23.10 -26.63 26.63 o 5 3 29 222.65 196.40 39.51 o 6 3 29 165.71 113.36 38.03 o 7 3 29 4.47 -19.42 35.57 o 8 3 29 0.37 -47.89 47.89 o 9 3 29 12.93 -67.98 67.98 o 0 4 29 45.22 -73.47 73.47 o 1 4 29 84.57 23.21 29.64 o 2 4 29 112.65 123.95 55.89 o 3 4 29 153.92 106.91 31.32 o 4 4 29 60.88 49.34 32.37 o 5 4 29 23.50 21.97 49.20 o 6 4 29 1.89 -28.19 44.37 o 7 4 29 368.40 318.64 57.71 o 1 5 29 16.23 -24.04 36.06 o 2 5 29 113.36 105.34 38.68 o 3 5 29 0.08 -32.32 32.32 o 4 5 29 148.65 91.39 34.84 o 5 5 29 0.02 -39.12 39.12 o 6 5 29 4.73 1.58 71.67 o 0 6 29 238.23 207.40 53.32 o 1 6 29 96.70 187.64 37.81 o 2 6 29 5.24 121.74 67.66 o 0 0 30 1017.09 1025.91 108.16 o 1 0 30 110.56 72.09 50.60 o 2 0 30 1.07 -23.27 45.99 o 3 0 30 260.75 267.54 54.20 o 4 0 30 262.89 267.24 53.72 o 5 0 30 2.59 46.65 48.94 o 6 0 30 2.39 -47.06 47.06 o 7 0 30 42.11 -28.88 47.51 o 8 0 30 42.12 68.74 70.59 o 9 0 30 61.40 49.74 69.50 o 1 1 30 23.83 12.35 34.12 o 2 1 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-31.89 51.78 o 6 1 31 56.37 -43.80 68.04 o 7 1 31 8.24 -47.95 47.95 o 0 2 31 47.45 41.14 51.70 o 1 2 31 11.52 -1.52 35.35 o 2 2 31 3.22 -34.59 34.59 o 3 2 31 97.57 -14.63 63.74 o 4 2 31 171.25 113.03 60.92 o 5 2 31 3.29 -59.08 59.08 o 6 2 31 27.77 -8.04 59.95 o 1 3 31 17.36 -31.66 45.70 o 2 3 31 22.63 22.37 69.07 o 3 3 31 0.43 2.17 63.85 o 4 3 31 34.76 -16.83 64.18 o