#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:12:38 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180831 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016275.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016275_Fobs loop_ _publ_author_name 'Torre, Jos\'e M. de la' 'Nogueras, Manuel' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Redetermination of 6-amino-5-formyl-1,3-dimethyluracil monohydrate at 120K: a polarized molecular structure and two interwoven hydrogen-bonded frameworks ; _journal_coeditor_code LN3062 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o638 _journal_page_last o640 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.408 _cell_angle_gamma 90.000 _cell_length_a 15.5815 _cell_length_b 7.4458 _cell_length_c 16.8575 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file ln3062Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JTR-208B in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 318.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 287.14 154.23 3.00 o 6 0 0 1953.39 2276.85 23.48 o 8 0 0 67.48 53.65 5.07 o 10 0 0 2032.09 1984.79 30.25 o 12 0 0 2952.45 3095.19 44.88 o 14 0 0 115.11 108.55 14.44 o 16 0 0 476.54 451.42 40.62 o 18 0 0 18.25 11.73 38.37 o 3 1 0 24.43 31.86 1.59 o 5 1 0 169.52 214.72 3.35 o 7 1 0 52.73 20.89 2.16 o 9 1 0 57.53 38.44 3.52 o 11 1 0 1720.92 1739.78 19.34 o 13 1 0 401.29 405.72 15.08 o 15 1 0 134.07 114.69 14.23 o 17 1 0 1171.44 1423.94 43.72 o 0 2 0 7795.87 7834.78 72.88 o 2 2 0 19.11 49.68 2.00 o 4 2 0 4476.41 4507.61 31.87 o 6 2 0 6020.34 6197.88 44.79 o 8 2 0 720.42 727.64 11.35 o 10 2 0 114.01 125.48 5.82 o 12 2 0 596.75 588.01 12.85 o 14 2 0 96.12 90.12 12.47 o 16 2 0 9.08 2.87 15.90 o 1 3 0 3886.65 4037.56 29.83 o 3 3 0 7.00 4.56 2.28 o 5 3 0 651.56 758.36 8.10 o 7 3 0 1.62 3.97 3.28 o 9 3 0 10.12 -2.34 4.96 o 11 3 0 508.24 454.57 11.50 o 13 3 0 3069.38 3398.84 41.03 o 15 3 0 1.32 29.84 14.74 o 17 3 0 335.09 332.52 32.67 o 0 4 0 2052.77 2129.80 24.07 o 2 4 0 1065.47 1000.68 10.25 o 4 4 0 128.16 126.77 5.00 o 6 4 0 333.68 259.40 8.06 o 8 4 0 836.76 804.68 12.80 o 10 4 0 174.92 152.73 8.95 o 12 4 0 62.99 23.08 9.74 o 14 4 0 69.05 52.39 15.03 o 16 4 0 3.15 -20.52 20.52 o 1 5 0 1845.93 1792.62 17.09 o 3 5 0 221.44 233.41 7.63 o 5 5 0 90.80 87.32 6.14 o 7 5 0 4.20 -0.09 5.97 o 9 5 0 190.12 169.40 10.40 o 11 5 0 949.53 946.94 22.29 o 13 5 0 156.68 114.87 13.29 o 15 5 0 23.17 -7.86 20.03 o 0 6 0 9.90 15.20 8.94 o 2 6 0 117.91 116.53 5.87 o 4 6 0 86.20 82.90 6.85 o 6 6 0 8.52 0.05 7.48 o 8 6 0 415.62 478.75 12.92 o 10 6 0 577.33 530.84 22.40 o 12 6 0 372.89 365.32 19.46 o 14 6 0 42.23 31.59 22.87 o 1 7 0 14.68 11.05 7.29 o 3 7 0 1.61 -7.50 7.50 o 5 7 0 59.04 29.23 11.04 o 7 7 0 225.89 240.80 14.75 o 9 7 0 227.87 193.35 14.86 o 11 7 0 177.74 143.41 23.74 o 0 8 0 2.29 -20.32 20.32 o 2 8 0 289.14 253.54 14.89 o 4 8 0 1.04 15.55 11.85 o 6 8 0 21.74 12.59 13.99 o 8 8 0 25.88 10.86 14.62 o 10 8 0 0.60 -15.75 30.91 o 1 9 0 1.06 -7.00 14.36 o 3 9 0 537.37 482.90 24.31 o 5 9 0 181.62 174.83 33.41 o -17 1 1 350.23 294.92 21.40 o -15 1 1 104.43 137.53 14.25 o -13 1 1 409.47 425.37 10.65 o -11 1 1 17.98 13.99 4.53 o -9 1 1 290.69 301.88 5.15 o -7 1 1 10259.73 11393.98 72.08 o -5 1 1 471.67 439.73 4.79 o -3 1 1 112.75 110.58 1.78 o 3 1 1 2895.40 2812.35 20.24 o 5 1 1 1659.07 1728.59 13.31 o 7 1 1 55.99 62.87 2.95 o 9 1 1 6.95 6.39 3.64 o 11 1 1 3466.44 3646.24 34.63 o 13 1 1 1123.74 1215.28 20.49 o 15 1 1 698.10 796.38 26.43 o 17 1 1 304.02 280.56 23.33 o -18 2 1 4.35 10.14 26.77 o -16 2 1 4.29 -7.32 13.76 o -14 2 1 2199.44 2398.19 44.28 o -12 2 1 1138.66 1141.60 15.29 o -10 2 1 19.73 22.04 4.18 o -8 2 1 974.38 1079.84 11.58 o -6 2 1 681.68 785.91 8.11 o -4 2 1 2774.79 2715.28 19.18 o -2 2 1 27245.86 26550.99 206.07 o 0 2 1 3198.01 2942.15 20.95 o 2 2 1 509.10 502.76 5.53 o 4 2 1 4514.56 4584.47 31.80 o 6 2 1 119.51 126.35 3.87 o 8 2 1 733.69 642.01 9.64 o 10 2 1 100.01 79.47 5.95 o 12 2 1 1775.27 1908.51 26.20 o 14 2 1 297.29 297.98 18.64 o 16 2 1 21.35 19.15 17.20 o -17 3 1 268.60 273.44 24.42 o -15 3 1 695.57 728.90 24.16 o -13 3 1 1038.57 1163.87 18.68 o -11 3 1 19.01 16.97 6.68 o -9 3 1 363.22 320.06 8.30 o -7 3 1 37.35 31.26 3.33 o -5 3 1 4719.68 4709.32 33.22 o -3 3 1 647.73 672.65 7.13 o -1 3 1 0.42 -0.12 2.16 o 1 3 1 148.86 108.37 2.88 o 3 3 1 2619.21 2634.14 20.81 o 5 3 1 8060.75 8856.22 59.88 o 7 3 1 5.90 4.47 3.71 o 9 3 1 211.95 205.45 8.49 o 11 3 1 160.60 170.32 8.68 o 13 3 1 1468.56 1645.29 25.33 o 15 3 1 50.92 19.46 16.94 o -16 4 1 232.74 188.34 21.59 o -14 4 1 256.25 277.54 21.29 o -12 4 1 514.53 404.24 13.93 o -10 4 1 0.26 6.00 7.25 o -8 4 1 80.52 69.49 5.88 o -6 4 1 3785.86 4059.43 34.33 o -4 4 1 797.24 763.60 9.07 o -2 4 1 3505.92 3594.89 27.12 o 0 4 1 0.58 1.61 2.54 o 2 4 1 619.61 690.09 7.99 o 4 4 1 609.79 669.60 9.21 o 6 4 1 3935.18 4418.96 42.79 o 8 4 1 1484.29 1490.87 22.28 o 10 4 1 323.05 303.04 11.01 o 12 4 1 118.05 73.47 10.94 o 14 4 1 222.34 230.00 17.23 o 16 4 1 0.02 7.41 24.32 o -15 5 1 655.50 667.71 35.68 o -13 5 1 306.35 321.14 16.19 o -11 5 1 475.24 446.61 16.47 o -9 5 1 4.69 -1.94 7.26 o -7 5 1 197.82 189.45 7.70 o -5 5 1 227.90 211.54 7.39 o -3 5 1 248.58 230.61 6.18 o -1 5 1 1422.98 1379.74 15.61 o 1 5 1 313.66 282.91 5.82 o 3 5 1 164.39 135.53 6.50 o 5 5 1 9.18 3.18 5.90 o 7 5 1 508.73 552.89 13.11 o 9 5 1 3.76 7.03 6.88 o 11 5 1 210.59 186.37 14.77 o 13 5 1 196.96 187.53 18.59 o 15 5 1 349.50 382.47 37.27 o -14 6 1 1.15 -19.73 19.73 o -12 6 1 23.51 33.34 15.22 o -10 6 1 45.90 52.92 10.22 o -8 6 1 439.64 465.71 12.08 o -6 6 1 924.88 990.04 17.83 o -4 6 1 126.18 122.55 8.03 o -2 6 1 425.77 452.88 9.43 o 0 6 1 2656.95 2804.20 32.52 o 2 6 1 102.29 85.00 5.46 o 4 6 1 1957.95 2128.93 35.54 o 6 6 1 1.12 3.67 11.69 o 8 6 1 145.43 125.23 13.17 o 10 6 1 1091.41 1093.75 25.42 o 12 6 1 11.18 22.81 16.50 o -11 7 1 26.80 0.15 15.01 o -9 7 1 54.60 20.01 11.29 o -7 7 1 37.95 23.54 9.82 o -5 7 1 127.25 105.39 12.00 o -3 7 1 96.11 91.88 13.69 o -1 7 1 12.47 13.90 9.01 o 1 7 1 370.09 367.33 12.65 o 3 7 1 30.52 16.80 9.39 o 5 7 1 6.17 6.12 9.92 o 7 7 1 143.45 137.94 13.33 o 9 7 1 73.13 15.99 13.31 o 11 7 1 21.69 -1.49 16.93 o -10 8 1 3.98 6.16 22.14 o -8 8 1 12.61 -7.79 15.91 o -6 8 1 445.92 459.15 19.66 o -4 8 1 24.98 31.22 11.63 o -2 8 1 1038.96 1191.88 26.23 o 0 8 1 80.57 70.60 16.94 o 2 8 1 374.95 382.39 15.72 o 4 8 1 315.39 344.10 16.54 o 6 8 1 9.48 2.09 15.97 o 8 8 1 33.13 8.80 18.14 o -7 9 1 67.53 112.33 25.69 o -5 9 1 143.33 154.07 24.51 o -3 9 1 22.86 11.99 17.23 o -1 9 1 30.97 29.95 16.80 o 1 9 1 71.34 51.66 18.95 o 3 9 1 0.34 -4.17 17.53 o 5 9 1 42.13 3.51 25.30 o -18 0 2 36.83 23.90 33.16 o -16 0 2 754.05 790.10 50.60 o -14 0 2 632.76 698.74 23.79 o -12 0 2 713.60 661.72 20.90 o -10 0 2 3024.24 3114.01 43.25 o -8 0 2 5160.37 5666.29 55.88 o -6 0 2 27760.99 28182.62 255.33 o -4 0 2 5318.74 4787.10 45.32 o 2 0 2 399.51 330.98 4.33 o 4 0 2 13732.50 13730.84 116.11 o 6 0 2 296.04 318.49 5.98 o 8 0 2 2.46 1.77 6.09 o 10 0 2 6720.96 7168.11 90.89 o 12 0 2 4207.56 4605.57 69.12 o 14 0 2 5.17 -13.11 13.11 o 16 0 2 17.09 10.00 24.27 o -17 1 2 17.51 30.88 14.98 o -15 1 2 1.20 1.56 11.87 o -13 1 2 908.97 885.23 15.94 o -11 1 2 7.00 1.58 4.21 o -9 1 2 126.13 132.21 4.14 o -7 1 2 6809.98 7695.60 49.45 o -5 1 2 794.32 773.63 6.32 o -3 1 2 574.06 401.99 3.52 o 1 1 2 1032.93 1053.16 8.51 o 3 1 2 4421.38 3942.78 27.94 o 5 1 2 1710.38 1707.03 13.89 o 7 1 2 158.31 134.58 3.65 o 9 1 2 725.66 702.37 10.54 o 11 1 2 7810.28 8659.10 79.49 o 13 1 2 17.08 10.08 9.74 o 15 1 2 485.92 496.40 24.13 o 17 1 2 79.34 45.16 33.60 o -18 2 2 119.23 50.96 32.03 o -16 2 2 126.29 98.45 15.20 o -14 2 2 465.37 444.95 12.51 o -12 2 2 321.40 308.14 7.75 o -10 2 2 55.78 57.80 4.45 o -8 2 2 18.97 2.34 2.64 o -6 2 2 3095.36 3340.30 24.15 o -4 2 2 156.50 140.33 2.58 o -2 2 2 101607.55 89789.71 1889.80 o 0 2 2 3541.50 3437.20 26.20 o 2 2 2 4968.87 4757.39 33.92 o 4 2 2 3623.85 3949.52 27.94 o 6 2 2 1898.39 1996.66 17.24 o 8 2 2 1456.49 1454.72 16.71 o 10 2 2 995.44 994.35 15.72 o 12 2 2 14.04 6.02 8.41 o 14 2 2 205.69 219.60 19.62 o 16 2 2 1.87 -13.93 19.04 o -17 3 2 0.89 -1.91 20.40 o -15 3 2 16.94 11.57 11.90 o -13 3 2 3402.91 3443.52 38.51 o -11 3 2 99.09 113.30 8.64 o -9 3 2 73.38 83.85 5.13 o -7 3 2 7.18 5.54 3.06 o -5 3 2 669.14 627.55 6.91 o -3 3 2 438.36 405.87 4.77 o -1 3 2 9544.61 9375.85 65.21 o 1 3 2 6.61 4.35 2.34 o 3 3 2 77.68 59.35 2.82 o 5 3 2 597.22 616.39 7.76 o 7 3 2 7.77 5.43 4.29 o 9 3 2 69.62 63.57 6.29 o 11 3 2 827.64 886.70 17.54 o 13 3 2 19.82 3.75 12.25 o 15 3 2 0.31 -10.48 15.74 o -16 4 2 218.89 250.44 25.62 o -14 4 2 1854.58 1963.03 43.63 o -12 4 2 1099.42 980.77 19.98 o -10 4 2 169.47 161.49 8.25 o -8 4 2 3.01 1.64 4.60 o -6 4 2 428.02 430.81 9.13 o -4 4 2 832.34 705.40 7.84 o -2 4 2 14.17 27.45 3.56 o 0 4 2 838.64 836.30 9.46 o 2 4 2 707.04 666.30 8.90 o 4 4 2 2599.70 2754.00 29.67 o 6 4 2 876.50 848.18 12.37 o 8 4 2 201.56 214.52 8.14 o 10 4 2 39.50 30.45 9.54 o 12 4 2 291.68 269.73 16.11 o 14 4 2 103.91 63.28 17.84 o -15 5 2 294.80 290.19 25.38 o -13 5 2 1.26 -1.87 11.54 o -11 5 2 32.85 25.14 10.13 o -9 5 2 57.79 57.28 7.51 o -7 5 2 167.36 130.39 6.93 o -5 5 2 3.16 4.59 4.98 o -3 5 2 516.54 529.06 8.67 o -1 5 2 668.58 681.32 12.44 o 1 5 2 27.62 23.65 4.60 o 3 5 2 1742.49 1761.12 22.68 o 5 5 2 197.67 208.54 8.29 o 7 5 2 208.69 232.16 10.12 o 9 5 2 17.85 16.69 8.69 o 11 5 2 118.05 125.14 12.90 o 13 5 2 260.88 294.78 24.63 o -14 6 2 1.30 -7.77 20.87 o -12 6 2 73.49 40.56 14.87 o -10 6 2 597.23 694.80 23.44 o -8 6 2 996.70 1056.15 21.65 o -6 6 2 279.71 285.65 9.93 o -4 6 2 184.04 182.55 9.82 o -2 6 2 65.96 69.89 6.51 o 0 6 2 703.16 777.86 14.85 o 2 6 2 327.29 316.86 10.72 o 4 6 2 112.23 104.61 8.97 o 6 6 2 8.09 8.31 8.08 o 8 6 2 207.40 164.19 15.30 o 10 6 2 28.36 21.97 13.96 o 12 6 2 21.53 24.49 18.86 o -13 7 2 156.93 85.95 29.64 o -11 7 2 19.16 13.73 20.03 o -9 7 2 92.52 51.63 11.24 o -7 7 2 13.10 14.17 9.09 o -5 7 2 176.74 167.07 12.01 o -3 7 2 716.02 775.39 18.83 o -1 7 2 6.24 7.25 10.61 o 1 7 2 140.19 104.00 9.70 o 3 7 2 21.73 17.74 9.47 o 5 7 2 119.80 121.93 13.23 o 7 7 2 0.42 -4.07 11.77 o 9 7 2 452.34 497.63 25.76 o 11 7 2 2.40 8.63 18.03 o -10 8 2 214.90 249.66 23.99 o -8 8 2 2.52 -8.96 14.14 o -6 8 2 602.08 667.02 29.87 o -4 8 2 500.28 531.46 18.57 o -2 8 2 11.32 10.04 10.77 o 0 8 2 68.53 66.30 11.76 o 2 8 2 122.58 103.02 12.95 o 4 8 2 0.08 5.98 11.52 o 6 8 2 7.64 13.57 14.39 o 8 8 2 47.08 8.15 22.67 o -7 9 2 60.72 70.18 21.96 o -5 9 2 39.81 49.75 25.18 o -3 9 2 1.25 1.25 21.33 o -1 9 2 15.94 12.06 16.63 o 1 9 2 6.17 -15.89 16.78 o 3 9 2 32.41 18.48 16.27 o 5 9 2 88.76 22.18 27.09 o -19 1 3 130.09 128.07 35.99 o -17 1 3 69.37 54.13 14.78 o -15 1 3 25.91 33.08 10.10 o -13 1 3 3.54 7.91 7.22 o -11 1 3 12.73 -2.18 4.97 o -9 1 3 2812.05 2981.98 25.53 o -7 1 3 383.91 443.60 5.66 o -5 1 3 47.18 47.38 1.66 o -3 1 3 12453.81 12216.87 75.34 o -1 1 3 755.05 636.79 5.56 o 1 1 3 104.30 104.13 1.92 o 3 1 3 3311.33 3203.70 22.22 o 5 1 3 816.92 849.53 8.52 o 7 1 3 165.27 157.12 4.75 o 9 1 3 3314.93 3518.82 34.27 o 11 1 3 476.87 476.28 11.11 o 13 1 3 372.89 365.49 13.28 o 15 1 3 49.27 19.06 16.43 o -18 2 3 44.98 29.20 21.69 o -16 2 3 134.46 91.94 14.22 o -14 2 3 105.11 83.73 9.58 o -12 2 3 147.22 114.81 6.16 o -10 2 3 0.11 -0.54 3.63 o -8 2 3 319.78 399.38 5.24 o -6 2 3 197.47 142.60 2.95 o -4 2 3 17890.41 18210.90 115.13 o -2 2 3 35448.58 34275.22 265.57 o 0 2 3 250.02 328.26 4.41 o 2 2 3 10.00 1.84 1.97 o 4 2 3 3968.58 4052.73 30.40 o 6 2 3 4305.83 4480.73 36.06 o 8 2 3 8.97 7.03 4.98 o 10 2 3 1795.82 1973.61 26.17 o 12 2 3 486.48 512.20 14.55 o 14 2 3 1.51 8.94 14.88 o 16 2 3 81.03 30.18 22.40 o -17 3 3 151.95 160.37 23.29 o -15 3 3 51.06 34.01 11.39 o -13 3 3 20.02 1.79 8.08 o -11 3 3 287.21 276.72 8.26 o -9 3 3 428.90 378.74 8.62 o -7 3 3 200.54 182.52 4.33 o -5 3 3 13.50 9.74 2.19 o -3 3 3 398.46 317.12 4.35 o -1 3 3 2713.58 2424.07 19.56 o 1 3 3 122.00 96.04 3.09 o 3 3 3 425.64 315.32 4.98 o 5 3 3 256.74 306.09 5.50 o 7 3 3 34.58 29.57 5.66 o 9 3 3 2.37 3.84 5.74 o 11 3 3 139.53 112.55 9.96 o 13 3 3 778.48 918.97 23.34 o 15 3 3 1517.54 1864.48 44.91 o -16 4 3 603.10 618.20 25.67 o -14 4 3 136.59 158.79 13.50 o -12 4 3 544.12 478.27 13.40 o -10 4 3 0.08 -5.52 5.52 o -8 4 3 2829.09 2843.68 31.10 o -6 4 3 390.24 347.81 6.64 o -4 4 3 8461.96 9047.01 61.20 o -2 4 3 178.00 150.05 4.28 o 0 4 3 431.62 435.12 6.38 o 2 4 3 3362.32 3327.55 28.83 o 4 4 3 21.09 16.38 3.69 o 6 4 3 1751.08 1798.94 19.95 o 8 4 3 582.79 563.72 11.97 o 10 4 3 483.68 526.89 14.56 o 12 4 3 27.54 14.24 11.51 o 14 4 3 80.63 27.57 17.81 o -15 5 3 2022.08 2332.20 58.09 o -13 5 3 273.04 278.90 13.87 o -11 5 3 9.26 9.38 7.76 o -9 5 3 28.34 28.43 9.38 o -7 5 3 1093.02 1134.40 17.31 o -5 5 3 97.06 91.34 5.15 o -3 5 3 704.95 725.50 11.66 o -1 5 3 627.16 568.09 11.26 o 1 5 3 5.18 2.38 4.56 o 3 5 3 1506.95 1470.92 21.03 o 5 5 3 135.32 115.16 8.40 o 7 5 3 24.73 14.19 7.16 o 9 5 3 1298.18 1436.19 26.98 o 11 5 3 45.50 31.18 13.51 o 13 5 3 1.54 28.05 17.73 o -14 6 3 6.35 -12.84 21.25 o -12 6 3 115.07 125.12 19.89 o -10 6 3 129.37 107.33 10.53 o -8 6 3 899.72 933.29 20.29 o -6 6 3 650.73 654.74 14.04 o -4 6 3 364.34 390.62 10.17 o -2 6 3 208.97 207.23 8.82 o 0 6 3 691.62 694.53 14.71 o 2 6 3 100.74 123.71 9.02 o 4 6 3 162.74 158.24 9.13 o 6 6 3 18.18 31.55 10.03 o 8 6 3 14.39 7.44 11.91 o 10 6 3 23.23 18.90 15.07 o 12 6 3 46.51 36.68 18.22 o -13 7 3 205.39 208.42 30.75 o -11 7 3 18.62 -3.43 13.47 o -9 7 3 1.15 6.55 11.28 o -7 7 3 715.22 817.18 18.07 o -5 7 3 175.11 186.00 10.30 o -3 7 3 35.75 27.41 8.27 o -1 7 3 190.08 198.75 16.59 o 1 7 3 255.34 216.65 12.81 o 3 7 3 15.98 3.00 8.73 o 5 7 3 2.27 -11.01 11.01 o 7 7 3 2.66 15.70 12.68 o 9 7 3 554.14 534.74 23.22 o 11 7 3 238.68 316.70 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