#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016309.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016309_Fobs loop_ _publ_author_name 'Chen, Min' 'Chen, Xu-Dong' 'Du, Miao' _publ_section_title ; An unusual chain cadmium(II) coordination polymer: catena-poly[[(2,2'-bipyridyl-\k^2^N,N')cadmium(II)]-di-\m-chlorido-[(2,2'-bipyridyl-\k^2^N,N')cadmium(II)]-di-\m-thiocyanato-\k^2^N:S;\k^2^S:N] ; _journal_coeditor_code DN3068 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m570 _journal_page_last m572 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 103.031 _cell_angle_beta 106.938 _cell_angle_gamma 106.303 _cell_length_a 8.0149 _cell_length_b 9.2527 _cell_length_c 9.5534 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file dn3068Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 186.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13223.67 12054.04 235.07 o 2 0 0 142.21 177.36 3.53 o 3 0 0 1648.13 1595.26 23.00 o 4 0 0 3045.72 2875.70 40.76 o 5 0 0 2183.20 2102.03 30.96 o 6 0 0 379.62 371.18 8.12 o 7 0 0 79.61 88.54 6.94 o -8 1 0 136.01 115.75 8.35 o -7 1 0 255.45 273.57 10.92 o -6 1 0 47.86 48.99 4.81 o -5 1 0 7.63 8.42 1.52 o -4 1 0 68.00 67.25 2.73 o -3 1 0 365.58 352.90 5.99 o -2 1 0 313.10 310.32 4.96 o -1 1 0 902.61 890.53 18.21 o 0 1 0 272.04 286.86 8.47 o 1 1 0 277.50 291.98 6.85 o 2 1 0 1181.17 1221.45 25.32 o 3 1 0 2746.93 2798.85 39.51 o 4 1 0 1016.45 1010.63 16.05 o 5 1 0 243.94 237.95 7.16 o 6 1 0 361.28 338.57 8.12 o 7 1 0 324.19 323.27 12.87 o 8 1 0 146.81 120.98 9.12 o -8 2 0 456.26 471.55 16.03 o -7 2 0 465.55 448.35 14.28 o -6 2 0 271.09 272.51 14.28 o -5 2 0 1521.27 1545.68 22.34 o -4 2 0 2113.97 2094.27 30.00 o -3 2 0 4668.91 4729.62 64.71 o -2 2 0 34812.48 28807.99 731.87 o -1 2 0 9809.67 9939.75 175.05 o 0 2 0 169.28 163.49 2.57 o 1 2 0 3929.24 3964.89 52.09 o 2 2 0 2612.01 2578.65 36.41 o 3 2 0 1433.41 1360.23 20.62 o 4 2 0 294.77 310.97 6.96 o 5 2 0 68.89 65.94 3.67 o 6 2 0 408.99 391.25 9.18 o 7 2 0 205.81 202.04 7.42 o -9 3 0 12.93 10.51 6.49 o -8 3 0 2.00 2.54 5.11 o -7 3 0 156.16 152.03 8.56 o -6 3 0 82.46 91.39 4.33 o -5 3 0 23.78 22.53 2.32 o -4 3 0 315.68 318.17 5.07 o -3 3 0 2605.65 2677.87 32.12 o -2 3 0 5462.80 5638.49 66.34 o -1 3 0 1462.31 1473.53 17.93 o 0 3 0 73.70 60.93 2.16 o 1 3 0 5625.38 5653.16 67.09 o 2 3 0 7015.61 7150.21 103.31 o 3 3 0 1171.26 1182.41 18.66 o 4 3 0 363.76 380.15 8.40 o 5 3 0 821.57 791.10 14.54 o 6 3 0 926.03 922.83 32.24 o 7 3 0 262.83 259.76 14.62 o -9 4 0 174.90 187.95 10.92 o -8 4 0 1.04 1.18 5.19 o -7 4 0 162.01 164.97 6.28 o -6 4 0 1416.86 1464.85 24.73 o -5 4 0 1986.38 2064.90 32.85 o -4 4 0 4064.52 4271.86 51.07 o -3 4 0 1952.54 2130.76 25.91 o -2 4 0 1386.75 1464.53 18.06 o -1 4 0 4166.86 4209.95 105.11 o 0 4 0 47.19 41.35 3.35 o 1 4 0 236.78 291.42 6.20 o 2 4 0 297.49 306.96 5.52 o 3 4 0 769.31 782.63 13.77 o 4 4 0 231.14 223.66 6.75 o 5 4 0 20.56 23.12 7.85 o 6 4 0 28.45 26.63 4.24 o -9 5 0 2.45 6.38 5.90 o -8 5 0 32.71 42.82 5.00 o -7 5 0 412.06 439.06 10.62 o -6 5 0 1143.26 1153.81 20.32 o -5 5 0 413.29 423.90 12.79 o -4 5 0 776.50 795.74 21.90 o -3 5 0 3257.77 3334.61 40.10 o -2 5 0 2481.83 2532.11 39.39 o -1 5 0 4111.40 4186.96 64.24 o 0 5 0 4671.56 4837.25 74.06 o 1 5 0 1757.65 1758.51 22.39 o 2 5 0 1120.31 1124.67 18.25 o 3 5 0 1288.37 1266.43 20.82 o 4 5 0 1457.69 1444.03 23.82 o 5 5 0 571.22 576.13 12.89 o -8 6 0 195.97 197.25 11.67 o -7 6 0 397.37 422.88 10.32 o -6 6 0 653.11 647.49 13.10 o -5 6 0 144.29 148.69 5.23 o -4 6 0 53.87 62.53 5.74 o -3 6 0 1042.93 1063.56 13.97 o -2 6 0 40.22 48.21 2.85 o -1 6 0 1089.86 1143.88 19.72 o 0 6 0 197.95 192.36 6.73 o 1 6 0 315.83 321.09 10.68 o 2 6 0 108.64 113.39 6.97 o 3 6 0 384.21 372.56 13.05 o 4 6 0 370.34 358.36 13.93 o 5 6 0 9.28 7.26 6.11 o -8 7 0 616.02 658.68 15.02 o -7 7 0 217.44 236.63 8.06 o -6 7 0 76.48 74.08 7.02 o -5 7 0 1535.82 1543.15 41.82 o -4 7 0 2858.37 2875.96 72.19 o -3 7 0 1883.08 1942.77 31.69 o -2 7 0 772.11 802.90 15.07 o -1 7 0 852.36 846.53 22.45 o 0 7 0 2646.20 2603.69 42.14 o 1 7 0 1978.72 1959.42 43.53 o 2 7 0 552.06 568.98 17.38 o 3 7 0 205.04 211.50 10.86 o 4 7 0 203.00 210.17 11.42 o -8 8 0 36.89 35.09 7.88 o -7 8 0 267.23 251.23 13.46 o -6 8 0 27.09 28.33 6.70 o -5 8 0 94.68 109.79 8.59 o -4 8 0 301.20 313.09 13.69 o -3 8 0 320.86 317.50 8.29 o -2 8 0 154.07 153.59 10.70 o -1 8 0 54.61 57.49 4.21 o 0 8 0 112.67 104.16 7.08 o 1 8 0 513.47 524.32 16.71 o 2 8 0 493.43 459.12 16.20 o 3 8 0 139.97 147.51 10.09 o -7 9 0 270.79 283.81 15.82 o -6 9 0 448.84 467.59 19.21 o -5 9 0 689.97 736.56 24.85 o -4 9 0 668.77 702.76 23.64 o -3 9 0 309.22 312.82 13.87 o -2 9 0 624.62 633.96 13.85 o -1 9 0 824.54 825.71 16.98 o 0 9 0 344.03 342.57 13.10 o 1 9 0 105.50 101.12 8.50 o -6 10 0 500.75 501.77 21.01 o -5 10 0 101.55 86.12 9.62 o -4 10 0 10.88 5.99 6.02 o -3 10 0 322.84 330.77 15.94 o -2 10 0 923.32 933.61 27.14 o -1 10 0 525.81 555.75 17.94 o 0 -10 1 330.07 333.48 14.17 o 1 -10 1 882.87 937.08 25.35 o 2 -10 1 1241.62 1278.37 37.81 o 3 -10 1 423.83 421.61 18.24 o 4 -10 1 59.47 64.58 8.94 o 5 -10 1 247.26 264.54 15.11 o 6 -10 1 600.33 604.63 23.32 o -2 -9 1 0.19 0.59 5.61 o -1 -9 1 117.82 102.89 7.85 o 0 -9 1 56.03 51.95 5.93 o 1 -9 1 676.79 671.93 14.53 o 2 -9 1 181.71 172.56 6.85 o 3 -9 1 16.24 14.96 6.02 o 4 -9 1 59.03 55.99 7.11 o 5 -9 1 688.85 680.24 23.76 o 6 -9 1 236.40 233.40 13.93 o 7 -9 1 27.29 32.44 8.74 o -3 -8 1 435.49 449.12 16.38 o -2 -8 1 1376.96 1312.50 32.41 o -1 -8 1 912.28 916.56 23.91 o 0 -8 1 317.94 316.21 8.89 o 1 -8 1 537.30 558.19 12.20 o 2 -8 1 1105.35 1108.46 20.20 o 3 -8 1 789.23 810.45 29.01 o 4 -8 1 306.60 300.72 13.13 o 5 -8 1 180.05 162.59 10.15 o 6 -8 1 130.58 115.52 9.50 o 7 -8 1 121.97 118.53 10.48 o -4 -7 1 118.70 109.50 8.65 o -3 -7 1 6.99 6.79 4.37 o -2 -7 1 116.58 113.10 7.38 o -1 -7 1 1234.33 1240.72 29.46 o 0 -7 1 1876.12 1879.30 31.34 o 1 -7 1 429.64 429.90 9.63 o 2 -7 1 92.79 90.73 4.22 o 3 -7 1 1494.23 1512.03 25.40 o 4 -7 1 1717.41 1672.93 44.54 o 5 -7 1 545.98 567.38 19.24 o 6 -7 1 540.51 545.95 19.60 o 7 -7 1 482.77 508.86 19.15 o 8 -7 1 369.99 417.12 17.97 o -5 -6 1 270.28 282.54 12.37 o -4 -6 1 927.77 954.52 25.03 o -3 -6 1 638.72 654.86 18.36 o -2 -6 1 44.41 55.93 5.14 o -1 -6 1 263.40 265.60 7.17 o 0 -6 1 2278.55 2242.02 36.14 o 1 -6 1 1329.02 1290.52 21.87 o 2 -6 1 68.60 63.16 3.11 o 3 -6 1 263.16 257.60 4.69 o 4 -6 1 403.32 421.50 8.76 o 5 -6 1 1298.33 1327.23 22.45 o 6 -6 1 49.58 47.86 4.01 o 7 -6 1 171.60 170.72 8.53 o 8 -6 1 21.66 22.32 4.78 o -6 -5 1 148.60 145.30 9.71 o -5 -5 1 446.32 460.66 13.22 o -4 -5 1 665.06 694.17 20.25 o -3 -5 1 679.04 682.34 17.27 o -2 -5 1 1417.83 1475.95 19.38 o -1 -5 1 3121.29 3030.45 41.37 o 0 -5 1 2347.93 2207.16 35.09 o 1 -5 1 2374.00 2277.55 46.75 o 2 -5 1 1825.89 1820.24 22.45 o 3 -5 1 2148.73 2198.84 27.02 o 4 -5 1 4563.02 4779.07 57.20 o 5 -5 1 1546.83 1618.71 26.62 o 6 -5 1 473.69 498.38 21.75 o 7 -5 1 501.62 512.86 15.29 o 8 -5 1 177.88 176.64 9.65 o -6 -4 1 84.97 83.62 5.23 o -5 -4 1 76.28 79.38 4.29 o -4 -4 1 146.22 144.52 7.13 o -3 -4 1 177.79 178.66 5.14 o -2 -4 1 128.72 127.62 3.42 o -1 -4 1 1.43 5.45 1.63 o 0 -4 1 79.14 89.93 12.82 o 1 -4 1 372.42 369.74 5.26 o 2 -4 1 193.78 209.83 3.63 o 3 -4 1 546.50 569.49 8.02 o 4 -4 1 6.10 8.99 1.60 o 5 -4 1 810.04 824.65 14.99 o 6 -4 1 271.38 295.85 7.98 o 7 -4 1 21.40 57.38 5.76 o 8 -4 1 48.50 53.95 6.43 o -7 -3 1 246.37 254.20 10.67 o -6 -3 1 376.36 407.61 14.96 o -5 -3 1 708.38 708.10 13.05 o -4 -3 1 1505.63 1558.95 37.60 o -3 -3 1 3751.78 3747.53 52.78 o -2 -3 1 3602.01 3336.35 40.28 o -1 -3 1 2575.60 2501.30 118.50 o 0 -3 1 786.23 732.14 12.43 o 1 -3 1 2032.12 2053.22 24.71 o 2 -3 1 19158.42 18899.61 504.38 o 3 -3 1 7543.41 7752.78 91.44 o 4 -3 1 78.04 81.59 3.54 o 5 -3 1 263.71 286.67 5.28 o 6 -3 1 901.69 898.53 27.20 o 7 -3 1 631.48 609.68 17.38 o 8 -3 1 72.02 74.43 7.59 o -7 -2 1 108.28 121.89 8.56 o -6 -2 1 7.21 5.73 2.65 o -5 -2 1 367.43 364.19 7.93 o -4 -2 1 0.14 0.87 1.69 o -3 -2 1 3206.91 3360.19 47.14 o -2 -2 1 2848.55 3022.33 50.37 o -1 -2 1 7.71 7.70 1.32 o 0 -2 1 1262.36 1297.06 20.34 o 1 -2 1 378.70 394.40 6.52 o 2 -2 1 484.69 486.52 6.61 o 3 -2 1 1624.66 1675.93 20.75 o 4 -2 1 570.11 582.99 8.36 o 5 -2 1 1351.50 1361.94 29.51 o 6 -2 1 1201.45 1178.27 27.54 o 7 -2 1 442.24 440.00 14.31 o 8 -2 1 328.45 282.07 12.19 o -8 -1 1 42.08 35.36 6.43 o -7 -1 1 512.44 514.23 16.06 o -6 -1 1 1747.71 1696.67 26.15 o -5 -1 1 1327.24 1322.56 20.55 o -4 -1 1 132.48 97.77 6.39 o -3 -1 1 1460.03 1393.16 20.37 o -2 -1 1 6787.71 6768.94 142.24 o -1 -1 1 2592.09 2653.89 36.39 o 0 -1 1 7551.15 6801.24 102.36 o 1 -1 1 6950.21 6963.16 94.92 o 2 -1 1 830.27 857.90 10.91 o 3 -1 1 1203.09 1253.56 17.69 o 4 -1 1 743.41 748.34 10.46 o 5 -1 1 333.09 338.18 7.03 o 6 -1 1 20.90 24.76 4.22 o 7 -1 1 0.90 1.03 4.52 o 8 -1 1 51.01 50.17 6.73 o -8 0 1 2.93 8.65 5.64 o -7 0 1 0.14 0.53 3.95 o -6 0 1 163.11 163.27 5.50 o -5 0 1 2707.90 2701.45 38.67 o -4 0 1 3388.56 3285.62 45.96 o -3 0 1 98.60 87.89 2.43 o -2 0 1 1771.12 1740.69 24.24 o -1 0 1 3504.51 3671.14 51.47 o 0 0 1 4056.66 4144.36 81.52 o 1 0 1 6835.50 6298.46 194.85 o 2 0 1 114.54 105.30 2.70 o 3 0 1 2864.12 2873.98 53.16 o 4 0 1 6717.33 6663.46 119.58 o 5 0 1 1972.72 1911.35 28.75 o 6 0 1 476.45 469.73 12.85 o 7 0 1 261.05 258.04 11.19 o 8 0 1 242.56 269.67 13.16 o -9 1 1 54.18 45.63 7.29 o -8 1 1 551.77 558.17 17.59 o -7 1 1 679.58 662.12 18.42 o -6 1 1 4.43 3.60 3.22 o -5 1 1 9.47 7.31 1.52 o -4 1 1 1964.24 1914.51 27.20 o -3 1 1 2111.91 2076.01 28.93 o -2 1 1 1019.17 1062.48 21.40 o -1 1 1 1109.32 1105.90 15.45 o 0 1 1 1880.58 1892.93 26.49 o 1 1 1 2900.16 2969.66 58.91 o 2 1 1 4.01 5.12 1.16 o 3 1 1 758.00 767.31 12.56 o 4 1 1 67.49 73.24 3.69 o 5 1 1 87.50 86.75 4.15 o 6 1 1 41.50 41.26 5.11 o 7 1 1 67.08 62.25 7.35 o -9 2 1 137.14 147.54 10.21 o -8 2 1 371.42 392.36 14.08 o -7 2 1 418.28 437.81 14.08 o -6 2 1 513.56 525.56 14.52 o -5 2 1 1480.27 1459.48 31.11 o -4 2 1 7520.01 7406.66 141.52 o -3 2 1 2851.81 2786.56 54.25 o -2 2 1 300.61 359.35 5.57 o -1 2 1 5503.89 5401.90 105.54 o 0 2 1 6275.48 6148.48 83.83 o 1 2 1 6874.90 6977.72 82.57 o 2 2 1 7411.52 7584.36 104.01 o 3 2 1 2303.41 2366.25 37.72 o 4 2 1 1211.44 1184.15 19.17 o 5 2 1 792.16 778.00 14.29 o 6 2 1 465.51 473.42 10.77 o 7 2 1 339.37 326.84 15.19 o -9 3 1 47.16 40.08 6.91 o -8 3 1 2.50 3.93 5.02 o -7 3 1 1.75 1.43 2.79 o -6 3 1 28.69 36.80 4.13 o -5 3 1 167.91 173.87 6.82 o -4 3 1 313.93 333.57 9.00 o -3 3 1 7.57 10.93 0.99 o -2 3 1 56.59 61.68 2.77 o -1 3 1 37.07 39.90 2.63 o 1 3 1 1447.80 1484.09 39.61 o 2 3 1 1555.85 1558.81 23.54 o 3 3 1 93.58 95.43 4.29 o 4 3 1 0.45 10.08 5.37 o 5 3 1 409.99 401.53 9.81 o 6 3 1 537.72 550.16 12.41 o -9 4 1 200.12 216.52 11.45 o -8 4 1 154.61 157.19 9.44 o -7 4 1 449.94 485.98 11.03 o -6 4 1 3097.18 3130.13 63.22 o -5 4 1 1813.08 1849.86 38.19 o -4 4 1 241.39 247.18 7.20 o -3 4 1 1563.63 1567.35 22.28 o -2 4 1 8928.48 8803.97 119.52 o -1 4 1 6452.34 6413.30 125.88 o 0 4 1 2087.08 2173.71 26.89 o 1 4 1 513.65 538.30 11.99 o 2 4 1 2490.01 2475.49 36.35 o 3 4 1 2497.67 2556.46 38.02 o 4 4 1 252.72 252.62 7.30 o 5 4 1 40.90 41.30 4.44 o 6 4 1 22.91 20.50 4.52 o -9 5 1 21.88 23.43 6.35 o -8 5 1 9.77 11.24 3.70 o -7 5 1 383.00 410.19 10.04 o -6 5 1 114.82 121.18 5.83 o -5 5 1 110.82 109.62 5.52 o -4 5 1 21.99 24.97 2.74 o -3 5 1 1333.82 1248.75 70.01 o -2 5 1 2909.33 2925.16 35.48 o -1 5 1 1017.36 1046.91 17.77 o 0 5 1 913.75 931.91 16.25 o 1 5 1 1159.75 1165.91 15.79 o 2 5 1 676.36 670.01 13.24 o 3 5 1 796.03 846.43 18.77 o 4 5 1 634.11 651.14 13.66 o 5 5 1 280.77 287.64 9.28 o -9 6 1 122.35 142.36 7.49 o -8 6 1 368.67 366.22 10.31 o -7 6 1 484.68 519.69 18.64 o -6 6 1 20.66 33.80 3.37 o -5 6 1 249.30 252.08 7.44 o -4 6 1 1297.62 1315.82 21.66 o -3 6 1 1695.03 1736.73 21.93 o -2 6 1 1597.35 1652.83 20.99 o -1 6 1 368.09 375.70 9.61 o 0 6 1 597.37 595.52 12.34 o 1 6 1 1008.30 1031.09 17.36 o 2 6 1 97.52 97.19 6.85 o 3 6 1 0.51 -0.68 4.37 o 4 6 1 0.87 -1.45 4.66 o -8 7 1 102.31 118.73 6.46 o -7 7 1 5.28 7.60 3.71 o -6 7 1 4.24 4.78 2.86 o -5 7 1 943.12 928.28 27.45 o -4 7 1 2866.02 3022.82 75.62 o -3 7 1 730.54 729.22 13.81 o -2 7 1 194.57 206.41 6.27 o -1 7 1 1444.13 1469.76 25.11 o 0 7 1 2351.09 2388.26 51.56 o 1 7 1 1290.62 1261.85 30.43 o 2 7 1 238.26 249.28 11.39 o 3 7 1 234.47 238.56 12.04 o -8 8 1 3.47 6.05 7.38 o -7 8 1 248.07 283.37 14.61 o -6 8 1 217.69 194.56 11.19 o -5 8 1 0.10 -0.83 4.75 o -4 8 1 113.46 106.31 8.62 o -3 8 1 458.92 439.08 16.20 o -2 8 1 174.74 185.97 6.62 o -1 8 1 0.04 2.53 3.00 o 0 8 1 37.38 36.24 5.22 o 1 8 1 1.87 6.64 5.08 o 2 8 1 2.62 7.59 5.73 o -7 9 1 148.66 146.95 11.57 o -6 9 1 360.17 369.28 16.76 o -5 9 1 527.06 550.82 20.51 o -4 9 1 791.27 800.34 25.88 o -3 9 1 1004.45 1007.56 30.31 o -2 9 1 621.15 662.60 14.45 o -1 9 1 519.28 542.68 16.94 o 0 9 1 361.43 369.19 14.05 o 1 9 1 372.05 376.66 15.38 o -5 10 1 89.12 82.52 9.47 o -4 10 1 63.38 58.79 8.59 o -3 10 1 144.27 135.71 10.51 o -2 10 1 425.42 456.20 16.23 o 0 -10 2 220.60 218.11 11.78 o 1 -10 2 878.11 869.29 32.88 o 2 -10 2 957.34 938.74 22.78 o 3 -10 2 391.16 390.09 17.71 o 4 -10 2 179.35 172.78 12.81 o 5 -10 2 395.16 410.75 18.36 o 6 -10 2 549.74 558.65 23.17 o -1 -9 2 100.82 121.78 8.53 o 0 -9 2 10.58 8.13 3.87 o 1 -9 2 18.22 19.00 6.77 o 2 -9 2 161.70 168.23 11.57 o 3 -9 2 129.80 125.78 6.24 o 4 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