#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016366.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016366_Fobs loop_ _publ_author_name 'Bera, Manindranath' 'Noll, Bruce C.' _publ_section_title ; Two new oximate-bridged square-planar dinuclear nickel(II) complexes ; _journal_coeditor_code TR3024 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m553 _journal_page_last m556 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.622 _cell_angle_gamma 90.000 _cell_length_a 13.1320 _cell_length_b 12.2045 _cell_length_c 17.2959 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.6801 _[local]_cod_data_source_file tr3024Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bcn220t4 in P2(1)/n; Bera/Lappin' _shelx_refln_list_code 4 _shelx_f_calc_maximum 295.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 8190.17 8197.24 60.49 o 8 0 0 441.11 358.62 10.17 o 10 0 0 690.03 535.84 14.86 o 12 0 0 627.13 597.72 20.69 o 14 0 0 2851.04 2662.07 46.07 o 16 0 0 7789.70 7846.53 143.59 o 16 0 0 7791.62 7962.74 166.10 o 17 1 1 2.79 23.38 55.45 o 18 0 0 303.88 304.21 41.37 o 19 1 1 12.58 20.25 36.07 o 1 1 0 2771.32 3065.62 22.25 o 2 1 0 5922.60 6428.75 38.59 o 3 1 0 12.49 20.77 2.87 o 4 1 0 2104.01 2014.46 16.69 o 5 1 0 8690.98 9368.17 61.45 o 6 1 0 7774.02 7880.95 46.93 o 7 1 0 3870.24 4173.19 31.12 o 8 1 0 394.77 344.97 8.00 o 9 1 0 1932.70 1795.69 15.12 o 10 1 0 158.92 157.49 8.17 o 11 1 0 1614.38 1671.57 18.25 o 12 1 0 1370.54 1196.49 19.47 o 13 1 0 818.73 856.82 18.08 o 14 1 0 22.93 11.13 8.17 o 15 1 0 129.26 149.15 13.30 o 16 1 0 466.64 522.71 69.36 o 16 1 0 54.85 64.58 16.51 o 17 1 0 312.02 334.54 68.23 o 17 1 0 2.18 -8.52 15.73 o 17 1 0 1028.28 1259.50 84.13 o 18 1 0 637.78 748.61 49.98 o 18 1 0 247.82 213.90 39.55 o 19 1 0 81.29 50.24 39.55 o 19 1 0 533.75 583.47 49.80 o 0 2 0 100.90 105.43 8.43 o 1 2 0 19357.41 22442.71 90.39 o 2 2 0 116.53 171.22 7.39 o 3 2 0 17905.33 18759.29 111.08 o 3 2 0 11731.54 12413.28 76.14 o 4 2 0 2162.20 2339.87 20.16 o 5 2 0 144.86 168.36 6.00 o 6 2 0 130.71 123.16 5.30 o 7 2 0 292.15 264.49 8.60 o 8 2 0 408.01 349.40 8.78 o 9 2 0 206.86 205.99 8.95 o 10 2 0 222.04 238.58 9.82 o 11 2 0 125.20 121.68 8.69 o 12 2 0 191.81 224.24 10.43 o 13 2 0 98.69 139.07 10.52 o 14 2 0 405.12 384.26 13.47 o 15 2 0 571.20 579.21 15.99 o 16 2 0 32.69 44.76 13.30 o 16 2 0 145.03 198.17 65.10 o 17 2 0 1253.86 1353.46 40.42 o 17 2 0 1497.53 1595.52 91.96 o 18 2 0 44.77 59.28 38.68 o 18 2 0 64.26 31.03 36.07 o 19 2 0 364.13 1009.27 57.45 o 19 2 0 376.71 405.81 46.76 o 1 3 0 4478.32 4709.20 33.46 o 2 3 0 638.99 622.93 12.86 o 3 3 0 5502.47 5593.66 50.32 o 3 3 0 8398.17 8482.49 64.14 o 4 3 0 63.79 93.43 5.48 o 5 3 0 10286.14 9834.13 38.33 o 6 3 0 441.35 387.04 7.91 o 7 3 0 680.85 559.39 9.30 o 8 3 0 433.16 443.10 8.78 o 9 3 0 250.86 212.42 8.43 o 10 3 0 2986.96 2818.26 24.68 o 11 3 0 69.56 102.30 7.91 o 12 3 0 4798.48 4760.66 34.85 o 13 3 0 575.20 556.78 13.21 o 14 3 0 2708.03 2613.22 27.99 o 15 3 0 1.45 -7.13 7.91 o 16 3 0 215.51 253.88 16.95 o 16 3 0 273.68 322.02 64.14 o 17 3 0 53.62 47.46 15.12 o 17 3 0 56.10 69.36 60.49 o 18 3 0 178.73 251.80 32.25 o 18 3 0 199.74 165.92 63.80 o 18 3 0 568.69 530.88 57.54 o 19 3 0 1210.02 1244.20 59.71 o 19 3 0 756.55 867.42 55.80 o 0 4 0 29.23 35.55 8.08 o 1 4 0 267.92 258.05 16.08 o 2 4 0 4020.82 4170.32 35.46 o 2 4 0 2634.44 2728.47 26.68 o 3 4 0 0.06 5.48 3.04 o 4 4 0 1094.12 939.30 12.78 o 5 4 0 2117.86 1984.21 17.21 o 6 4 0 13525.34 13536.67 46.41 o 7 4 0 20.63 31.12 3.65 o 8 4 0 21020.00 19765.43 54.50 o 9 4 0 235.37 236.24 8.60 o 10 4 0 9108.27 8402.62 39.03 o 11 4 0 966.75 954.25 15.64 o 12 4 0 878.61 821.18 14.25 o 13 4 0 1791.96 1655.32 19.64 o 14 4 0 904.09 927.13 17.30 o 15 4 0 213.84 241.89 15.04 o 15 4 0 536.73 664.39 66.84 o 16 4 0 1276.04 1230.12 28.16 o 16 4 0 1522.07 1519.03 89.70 o 17 4 0 335.62 370.70 19.82 o 17 4 0 946.95 1098.62 85.79 o 18 4 0 661.73 690.46 52.50 o 18 4 0 436.46 502.11 38.42 o 18 4 0 474.49 506.55 58.06 o 1 5 0 1256.41 1244.29 14.60 o 2 5 0 5.88 9.82 3.82 o 3 5 0 1269.32 1333.21 15.64 o 4 5 0 124.59 107.60 5.74 o 5 5 0 2801.87 2950.28 21.03 o 6 5 0 32.39 59.28 4.35 o 7 5 0 823.03 773.21 10.43 o 8 5 0 36.40 58.23 5.65 o 9 5 0 1461.75 1232.12 16.25 o 10 5 0 24.81 38.24 5.91 o 11 5 0 162.93 186.00 8.87 o 12 5 0 565.03 544.01 11.91 o 13 5 0 12.63 1.74 5.82 o 14 5 0 1233.39 1151.29 18.34 o 15 5 0 75.21 127.07 10.86 o 16 5 0 231.04 266.48 16.77 o 17 5 0 86.31 107.34 15.82 o 17 5 0 89.49 152.71 69.97 o 18 5 0 177.16 213.73 24.51 o 18 5 0 198.17 190.26 39.98 o 18 5 0 180.80 190.43 68.58 o 0 6 0 194.81 241.37 11.39 o 1 6 0 3464.14 4031.78 28.07 o 2 6 0 4915.21 4767.79 31.20 o 3 6 0 321.95 404.68 9.39 o 3 6 0 491.38 595.72 35.90 o 4 6 0 463.02 495.94 8.78 o 5 6 0 6252.74 6212.68 27.03 o 6 6 0 35.35 60.41 4.78 o 7 6 0 10665.81 10352.58 44.15 o 8 6 0 790.65 709.41 13.65 o 9 6 0 3424.53 3307.33 26.16 o 10 6 0 1.89 0.52 5.04 o 11 6 0 361.09 379.82 10.86 o 12 6 0 90.37 92.39 7.04 o 13 6 0 1519.30 1489.74 18.86 o 14 6 0 484.37 446.49 14.60 o 15 6 0 433.36 404.25 15.99 o 16 6 0 49.66 55.19 11.30 o 17 6 0 1295.61 1371.28 33.55 o 18 6 0 546.48 549.05 77.79 o 18 6 0 321.22 338.89 28.51 o 18 6 0 321.22 628.58 85.70 o 1 7 0 2247.13 2346.30 20.16 o 2 7 0 4015.98 3949.30 22.60 o 2 7 0 6129.42 6470.04 91.44 o 3 7 0 1784.83 1844.01 17.04 o 3 7 0 2724.11 2953.85 67.71 o 4 7 0 10830.23 10450.28 36.07 o 5 7 0 1189.37 1221.61 13.56 o 6 7 0 4764.78 4624.20 25.99 o 7 7 0 309.02 256.40 9.13 o 8 7 0 19.01 21.12 5.91 o 9 7 0 431.33 326.63 10.34 o 10 7 0 1244.16 1216.91 15.38 o 11 7 0 3146.85 3035.89 22.16 o 12 7 0 3377.68 3186.43 21.99 o 13 7 0 1272.60 1231.60 17.99 o 14 7 0 340.95 341.58 12.52 o 15 7 0 797.64 766.08 19.64 o 16 7 0 0.04 -14.99 10.00 o 17 7 0 3.37 -7.82 11.56 o 0 8 0 977.40 1000.40 43.81 o 0 8 0 638.00 611.98 20.43 o 1 8 0 118.55 127.25 8.34 o 1 8 0 180.94 203.38 32.85 o 2 8 0 818.21 854.56 12.78 o 2 8 0 1248.80 1391.53 53.45 o 3 8 0 441.28 477.08 9.73 o 3 8 0 673.50 728.97 45.20 o 4 8 0 52.27 43.81 4.95 o 5 8 0 261.94 223.03 7.91 o 6 8 0 142.09 141.15 7.65 o 7 8 0 3.32 5.74 4.95 o 8 8 0 1263.33 1224.39 17.47 o 9 8 0 28.86 28.77 6.34 o 10 8 0 759.79 661.52 11.65 o 11 8 0 900.07 794.85 11.73 o 12 8 0 342.72 340.71 10.00 o 13 8 0 4.00 1.56 6.00 o 14 8 0 74.92 80.31 9.47 o 15 8 0 0.68 -1.13 8.69 o 16 8 0 78.51 95.43 13.21 o 17 8 0 112.30 123.42 15.30 o 1 9 0 143.98 142.72 7.91 o 1 9 0 219.76 217.20 35.90 o 2 9 0 466.67 432.23 10.60 o 2 9 0 712.26 689.07 46.24 o 3 9 0 479.84 461.00 11.30 o 3 9 0 732.35 707.67 50.15 o 4 9 0 766.38 750.52 13.04 o 5 9 0 529.32 477.34 11.04 o 6 9 0 43.89 43.37 6.00 o 7 9 0 719.91 614.32 12.78 o 8 9 0 472.28 470.48 10.95 o 9 9 0 24.51 30.86 6.08 o 10 9 0 204.81 214.68 8.08 o 11 9 0 527.49 487.86 10.60 o 12 9 0 323.92 317.50 9.91 o 13 9 0 476.92 464.57 11.73 o 14 9 0 3.52 -0.70 7.30 o 15 9 0 444.15 463.00 15.82 o 16 9 0 1.01 -5.65 11.56 o 0 10 0 2223.52 2181.42 41.11 o 0 10 0 3393.65 3806.58 85.61 o 1 10 0 10261.94 10549.79 137.15 o 1 10 0 6723.60 6437.10 43.28 o 2 10 0 3.90 15.56 6.00 o 2 10 0 5.95 7.39 36.59 o 3 10 0 1096.92 1050.56 15.30 o 4 10 0 6.51 11.47 5.30 o 5 10 0 589.76 587.81 12.34 o 6 10 0 329.12 283.43 9.21 o 7 10 0 3987.27 3734.53 24.68 o 8 10 0 390.95 337.15 8.95 o 9 10 0 2579.80 2343.26 19.21 o 10 10 0 507.33 487.43 10.86 o 11 10 0 807.50 760.52 12.78 o 12 10 0 150.71 147.24 8.87 o 13 10 0 772.67 754.95 14.95 o 14 10 0 6.41 -4.87 7.56 o 15 10 0 564.14 546.18 18.77 o 16 10 0 170.71 198.43 14.17 o 1 11 0 0.32 -9.26 6.17 o 1 11 0 0.32 -38.16 39.98 o 2 11 0 727.68 718.71 17.64 o 2 11 0 727.85 662.74 56.32 o 3 11 0 214.08 178.27 9.65 o 3 11 0 597.03 522.45 55.54 o 4 11 0 1812.15 1885.65 19.21 o 5 11 0 979.11 898.97 13.47 o 6 11 0 1942.72 1857.14 17.73 o 7 11 0 458.65 411.03 9.73 o 8 11 0 6.93 -3.56 5.21 o 9 11 0 396.10 355.75 10.17 o 10 11 0 790.35 733.83 13.04 o 11 11 0 211.51 210.68 9.39 o 12 11 0 420.92 405.03 11.99 o 13 11 0 8.82 -1.56 7.65 o 14 11 0 6.90 -12.65 8.43 o 15 11 0 28.05 22.69 10.08 o 0 12 0 1212.35 1126.00 25.81 o 0 12 0 1225.81 1123.74 63.88 o 1 12 0 25.58 18.60 7.04 o 1 12 0 663.58 692.29 59.10 o 2 12 0 823.92 849.17 14.69 o 2 12 0 837.38 868.47 62.84 o 3 12 0 441.05 402.07 12.08 o 3 12 0 874.64 873.51 65.10 o 4 12 0 82.58 85.61 6.95 o 5 12 0 11.21 3.13 5.30 o 6 12 0 461.52 462.48 9.91 o 7 12 0 12.14 4.78 5.74 o 8 12 0 406.80 398.60 10.52 o 9 12 0 133.44 127.94 8.26 o 10 12 0 308.26 330.98 10.86 o 11 12 0 24.93 14.25 7.04 o 12 12 0 34.70 29.99 7.74 o 13 12 0 198.19 215.29 11.47 o 14 12 0 2.73 -6.08 9.04 o 1 13 0 709.80 683.42 11.99 o 1 13 0 709.80 709.32 62.49 o 2 13 0 87.88 90.39 8.78 o 2 13 0 461.41 467.35 30.68 o 3 13 0 3471.03 3443.01 55.89 o 3 13 0 3424.78 3331.67 30.07 o 4 13 0 105.52 144.54 9.82 o 4 13 0 1907.83 2007.07 44.94 o 5 13 0 1884.66 1882.78 20.51 o 5 13 0 1940.19 2000.38 46.85 o 6 13 0 519.39 496.12 10.95 o 7 13 0 152.92 176.01 8.78 o 8 13 0 45.13 39.46 7.13 o 9 13 0 91.95 98.82 8.34 o 10 13 0 106.92 115.08 8.87 o 11 13 0 619.55 623.45 14.08 o 12 13 0 542.33 529.23 13.65 o 13 13 0 605.78 588.60 15.47 o 0 14 0 57.76 78.05 10.60 o 1 14 0 2098.10 2046.61 23.64 o 1 14 0 2128.49 2163.52 47.28 o 2 14 0 24.46 26.42 8.34 o 2 14 0 1128.59 1146.42 39.20 o 3 14 0 683.52 684.64 16.51 o 3 14 0 696.39 703.33 36.42 o 4 14 0 288.18 293.60 13.91 o 4 14 0 647.88 627.80 26.07 o 5 14 0 158.31 192.08 11.73 o 5 14 0 309.96 306.99 24.77 o 6 14 0 99.07 97.69 9.13 o 6 14 0 182.38 170.27 31.81 o 7 14 0 433.13 450.14 12.17 o 8 14 0 482.33 457.53 12.78 o 9 14 0 426.10 478.56 12.86 o 10 14 0 3.09 -1.22 7.56 o 11 14 0 293.97 330.63 12.60 o 12 14 0 2.52 -1.83 8.08 o 1 15 0 68.97 77.79 27.03 o 1 15 0 131.05 118.55 21.21 o 1 15 0 131.05 160.79 17.90 o 1 15 0 236.13 266.40 30.16 o 2 15 0 268.64 260.57 19.82 o 2 15 0 199.95 192.26 56.41 o 2 15 0 199.67 228.68 18.43 o 3 15 0 0.53 2.43 10.52 o 3 15 0 105.61 76.14 21.99 o 3 15 0 30.29 24.77 38.24 o 4 15 0 56.83 31.20 22.42 o 4 15 0 56.55 64.67 11.39 o 5 15 0 4.16 -6.78 8.78 o 5 15 0 33.92 25.03 20.77 o 6 15 0 14.66 10.69 9.47 o 6 15 0 16.85 -28.42 22.08 o 7 15 0 8.30 -36.24 27.99 o 7 15 0 0.58 -7.47 9.21 o 8 15 0 224.75 237.19 11.99 o 9 15 0 255.27 288.21 12.43 o 10 15 0 276.35 294.30 12.86 o 0 16 0 5093.25 5125.53 52.24 o 1 16 0 2682.60 2748.55 44.59 o 1 16 0 275.13 243.97 25.29 o 2 16 0 518.54 485.77 22.77 o 2 16 0 516.90 458.57 35.20 o 2 16 0 572.48 586.60 36.50 o 3 16 0 377.64 345.49 21.82 o 3 16 0 105.62 110.47 18.77 o 3 16 0 163.67 114.03 43.54 o 4 16 0 165.89 124.20 22.08 o 4 16 0 110.31 106.82 15.04 o 4 16 0 146.48 137.94 44.50 o 5 16 0 126.77 116.99 23.29 o 5 16 0 68.72 88.92 13.73 o 6 16 0 225.01 248.32 22.69 o 6 16 0 188.84 194.52 17.38 o 7 16 0 320.74 325.67 24.25 o 7 16 0 221.36 251.10 20.34 o 8 16 0 5.03 4.78 10.34 o 8 16 0 121.52 102.39 37.29 o 1 17 0 146.02 143.41 24.25 o 1 17 0 280.77 255.01 26.51 o 1 17 0 272.43 273.70 24.94 o 2 17 0 159.22 157.32 23.64 o 2 17 0 272.49 231.02 28.86 o 2 17 0 15.85 24.60 35.11 o 3 17 0 496.02 508.89 25.81 o 3 17 0 493.23 419.28 40.24 o 3 17 0 487.68 485.86 33.38 o 4 17 0 267.20 278.65 22.42 o 4 17 0 10.56 21.99 17.38 o 4 17 0 462.13 395.56 51.63 o 5 17 0 863.64 923.31 32.25 o 5 17 0 858.08 839.09 24.77 o 6 17 0 547.73 589.12 27.90 o 6 17 0 96.16 106.99 16.25 o -19 0 1 111.10 -6.34 37.63 o 18 1 0 130.42 143.32 37.72 o -17 0 1 544.07 488.90 66.66 o -17 0 1 542.92 637.18 50.06 o -15 0 1 130.06 156.71 21.99 o -13 0 1 195.96 206.34 15.91 o -11 0 1 542.78 556.96 15.91 o -9 0 1 1880.61 1782.22 20.08 o -7 0 1 972.03 860.64 23.47 o -5 0 1 169.51 172.44 10.17 o -3 0 1 4176.25 4009.44 35.98 o -1 0 1 13076.67 13501.99 87.70 o 1 0 1 10040.26 10387.70 192.17 o 7 0 1 13490.36 13885.81 66.23 o 9 0 1 905.53 952.77 20.77 o 11 0 1 47.85 83.87 8.26 o 13 0 1 1730.73 1607.43 32.77 o 15 0 1 5926.07 5685.88 69.36 o 16 1 2 379.42 531.93 70.66 o 17 0 1 1978.14 2075.64 99.52 o 17 0 1 1949.82 1858.79 76.14 o 18 1 2 8.92 12.43 35.29 o 19 0 1 284.73 264.83 42.07 o -19 1 1 3.22 -42.68 36.50 o -19 1 1 194.85 237.11 41.89 o -18 1 1 174.69 181.13 39.20 o -18 1 1 300.80 309.77 40.16 o -17 1 1 326.73 330.63 27.90 o -17 1 1 986.58 1173.98 84.13 o -17 1 1 326.73 304.73 62.67 o -16 1 1 228.45 197.13 59.62 o -16 1 1 211.25 327.15 23.38 o -15 1 1 1489.73 1455.06 32.77 o -14 1 1 34.02 24.68 8.95 o -13 1 1 0.74 -8.17 6.78 o -12 1 1 1265.87 1258.72 19.90 o -11 1 1 201.63 183.91 8.78 o -10 1 1 3538.40 3413.81 26.94 o -9 1 1 1932.06 1826.02 14.78 o -8 1 1 1237.48 1070.37 13.30 o -7 1 1 5085.27 5119.88 32.33 o -6 1 1 447.17 553.74 17.38 o -5 1 1 7938.45 8780.27 62.93 o -4 1 1 2719.02 2745.16 22.42 o -3 1 1 1170.92 1375.97 14.95 o -2 1 1 1117.82 1191.88 13.04 o -1 1 1 15410.33 15848.46 94.22 o 0 1 1 1578.60 1558.58 13.73 o 1 1 1 12623.47 11919.42 74.57 o 2 1 1 4163.27 4623.68 68.23 o 2 1 1 2727.77 2893.70 44.85 o 3 1 1 4750.16 5132.92 41.81 o 4 1 1 4108.20 4333.03 39.20 o 5 1 1 6048.79 6338.88 47.54 o 6 1 1 18656.44 18866.19 77.62 o 7 1 1 6465.85 6286.82 33.12 o 8 1 1 7128.53 7039.43 30.25 o 9 1 1 7401.66 6983.97 33.81 o 10 1 1 791.34 871.77 13.91 o 11 1 1 2502.89 2443.21 21.73 o 12 1 1 58.98 49.19 7.13 o 13 1 1 147.07 190.95 11.30 o 14 1 1 456.35 460.39 15.21 o 15 1 1 497.28 477.00 18.34 o 16 1 1 3.66 3.22 12.60 o 16 1 1 646.95 830.14 76.83 o 16 1 1 4.07 1.22 50.85 o 17 1 1 5.30 -5.13 52.76 o 17 1 1 5.30 10.95 17.38 o 17 1 1 15.29 4.26 59.28 o 18 1 1 213.53 180.35 39.98 o 18 1 1 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