#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016384_Fobs loop_ _publ_author_name 'Insuasty, Henry' 'Mier, Paola' 'Suarez, Gina' 'Low, John N.' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Three 4,7-diaryl-2-ethylsulfanylpyrazolo[1,5-a][1,3,5]triazines ; _journal_coeditor_code GG3133 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o27 _journal_page_last o30 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.978 _cell_angle_gamma 90.000 _cell_length_a 7.7120 _cell_length_b 8.3260 _cell_length_c 27.6780 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file gg3133IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' PG-11' _shelx_refln_list_code 4 _shelx_f_calc_maximum 263.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12744.49 13124.46 127.37 o 4 0 0 421.11 376.03 12.08 o 6 0 0 329.42 297.62 18.82 o 8 0 0 183.93 144.08 36.08 o 2 1 0 69550.53 68296.80 423.01 o 3 1 0 1177.31 1152.70 11.83 o 4 1 0 43.84 19.58 5.34 o 5 1 0 1122.36 1184.30 17.88 o 6 1 0 868.28 954.19 22.03 o 7 1 0 252.27 284.69 23.11 o 8 1 0 0.05 0.34 26.74 o 9 1 0 75.59 40.23 38.81 o 0 2 0 7275.20 7298.71 62.22 o 1 2 0 17492.02 17619.39 117.03 o 2 2 0 4748.29 4902.99 40.91 o 3 2 0 2544.15 2528.65 23.27 o 4 2 0 6515.71 7333.29 58.57 o 5 2 0 218.62 236.40 9.24 o 6 2 0 702.38 732.52 19.41 o 7 2 0 8.54 26.47 15.63 o 8 2 0 2.17 2.54 20.37 o 9 2 0 6.71 6.87 45.32 o 1 3 0 396.99 356.18 6.04 o 2 3 0 478.41 450.90 9.24 o 3 3 0 0.00 4.76 5.87 o 4 3 0 218.99 209.45 10.68 o 5 3 0 164.25 159.63 12.44 o 6 3 0 4222.18 4800.85 66.04 o 7 3 0 111.92 99.21 26.59 o 8 3 0 204.44 171.20 40.50 o 9 3 0 60.74 100.49 47.43 o 0 4 0 6209.36 6349.56 66.51 o 1 4 0 6411.47 6909.67 48.55 o 2 4 0 1074.55 1024.92 15.15 o 3 4 0 10.78 10.48 6.67 o 4 4 0 1488.20 1628.45 26.45 o 5 4 0 1060.20 1202.64 28.56 o 6 4 0 0.91 25.85 15.22 o 7 4 0 1.17 -3.49 21.04 o 8 4 0 559.03 261.78 55.34 o 9 4 0 28.01 4.52 43.38 o 1 5 0 3980.81 4356.47 36.16 o 2 5 0 88.83 60.93 7.12 o 3 5 0 638.97 648.94 15.08 o 4 5 0 1119.66 1176.06 22.84 o 5 5 0 562.77 621.36 18.90 o 6 5 0 986.41 1106.66 29.75 o 7 5 0 174.95 142.78 29.51 o 8 5 0 101.09 29.61 43.07 o 0 6 0 26.56 30.78 12.64 o 1 6 0 442.13 475.44 12.53 o 2 6 0 1343.16 1273.21 18.91 o 3 6 0 219.72 225.41 10.45 o 4 6 0 274.34 240.75 16.13 o 5 6 0 33.45 38.30 18.07 o 6 6 0 1.09 -16.94 21.22 o 7 6 0 88.69 60.38 31.86 o 8 6 0 98.54 83.97 41.63 o 1 7 0 49.85 19.42 10.74 o 2 7 0 244.42 211.86 13.15 o 3 7 0 7.51 -13.72 13.22 o 4 7 0 388.28 361.95 21.88 o 5 7 0 3.90 10.03 21.59 o 6 7 0 2.66 -3.19 26.70 o 7 7 0 406.73 334.57 52.64 o 0 8 0 816.03 861.38 42.82 o 1 8 0 173.00 142.30 20.49 o 2 8 0 6.70 11.21 17.26 o 3 8 0 0.94 14.14 23.61 o 4 8 0 42.56 15.72 23.22 o 5 8 0 554.96 612.35 36.17 o 6 8 0 0.04 35.96 36.73 o 1 9 0 251.54 221.90 25.66 o 2 9 0 173.42 128.97 25.61 o 3 9 0 280.73 156.56 36.95 o 4 9 0 77.05 53.83 38.86 o 5 9 0 5.21 14.55 35.44 o 0 10 0 29.80 46.40 44.40 o 1 10 0 16.23 42.32 42.23 o 2 10 0 680.71 821.89 46.97 o 3 10 0 131.01 136.96 40.43 o -7 0 1 87.01 63.67 22.13 o -5 0 1 532.90 456.44 16.81 o -3 0 1 1274.54 1096.41 17.82 o 3 0 1 31016.31 32628.38 327.86 o 5 0 1 163.39 135.15 12.25 o 7 0 1 357.51 376.42 36.05 o 9 0 1 412.95 481.29 112.01 o -9 1 1 13.92 -40.01 48.07 o -8 1 1 12.60 -4.84 21.60 o -7 1 1 16.86 12.31 17.41 o -6 1 1 371.12 374.74 15.50 o -5 1 1 430.34 377.42 11.32 o -4 1 1 745.99 801.09 9.97 o -3 1 1 16.30 9.26 3.31 o -2 1 1 28460.63 29792.15 190.62 o 2 1 1 23822.27 24729.30 162.70 o 3 1 1 2177.97 2303.66 20.13 o 4 1 1 807.76 809.14 12.39 o 5 1 1 2271.90 2469.78 29.01 o 6 1 1 1769.72 1802.19 31.47 o 7 1 1 140.17 138.88 21.63 o 8 1 1 0.30 -12.47 23.71 o 9 1 1 97.10 106.13 33.38 o -9 2 1 2.71 38.82 42.58 o -8 2 1 183.65 178.68 27.95 o -7 2 1 9.48 27.86 16.83 o -6 2 1 15.49 -5.61 9.24 o -5 2 1 123.89 119.10 6.78 o -4 2 1 1438.41 1615.01 17.52 o -3 2 1 78.28 80.70 5.49 o -2 2 1 540.89 530.81 8.85 o -1 2 1 15190.03 15559.01 104.00 o 0 2 1 8773.47 8731.62 52.70 o 1 2 1 30.12 33.97 3.04 o 2 2 1 127.17 99.98 5.39 o 3 2 1 242.95 220.33 5.91 o 4 2 1 28397.35 30499.21 222.46 o 5 2 1 3937.46 4348.68 44.01 o 6 2 1 225.74 205.63 13.43 o 7 2 1 164.47 165.27 26.12 o 8 2 1 13.48 -18.85 22.33 o 9 2 1 1.90 -15.97 36.84 o -9 3 1 15.01 -8.77 46.83 o -8 3 1 290.04 266.94 22.81 o -7 3 1 4.04 -12.94 14.88 o -6 3 1 466.28 538.22 19.90 o -5 3 1 85.04 70.40 11.95 o -4 3 1 410.29 384.87 11.39 o -3 3 1 3621.26 4007.22 35.89 o -2 3 1 7541.81 7858.45 64.85 o -1 3 1 279.60 234.55 5.69 o 0 3 1 4888.25 4971.95 33.65 o 1 3 1 16.11 10.23 3.47 o 2 3 1 255.36 228.34 7.13 o 3 3 1 5515.74 6428.30 56.76 o 4 3 1 318.01 309.49 12.02 o 5 3 1 393.66 375.21 11.01 o 6 3 1 5618.77 6261.95 74.82 o 7 3 1 629.52 642.57 30.35 o 8 3 1 65.82 3.99 28.52 o 9 3 1 463.46 688.92 94.67 o -9 4 1 236.14 176.23 62.65 o -8 4 1 118.24 61.83 39.80 o -7 4 1 60.96 51.30 19.96 o -6 4 1 75.35 47.45 13.96 o -5 4 1 49.92 44.10 11.51 o -4 4 1 121.39 112.97 9.74 o -3 4 1 22.08 9.96 6.23 o -2 4 1 569.31 537.59 10.69 o -1 4 1 1414.56 1532.55 15.34 o 0 4 1 54.17 68.54 5.16 o 1 4 1 513.06 649.52 9.55 o 2 4 1 3366.47 3315.07 28.75 o 3 4 1 1468.95 1410.12 20.09 o 4 4 1 83.94 82.26 16.26 o 5 4 1 892.80 1020.50 26.18 o 6 4 1 379.62 405.84 21.12 o 7 4 1 71.63 -4.65 21.77 o 8 4 1 397.36 181.85 59.16 o 9 4 1 179.88 109.55 49.73 o -8 5 1 170.63 135.13 32.60 o -7 5 1 398.85 579.32 58.16 o -6 5 1 19.37 -6.47 17.13 o -5 5 1 87.67 73.94 13.01 o -4 5 1 76.96 47.61 9.62 o -3 5 1 35.11 24.87 7.19 o -2 5 1 47.14 41.17 5.75 o -1 5 1 571.61 589.81 10.86 o 0 5 1 80.57 92.67 6.43 o 1 5 1 12.91 13.25 5.21 o 2 5 1 17.37 -3.94 6.00 o 3 5 1 9.81 2.35 9.36 o 4 5 1 290.77 297.67 13.73 o 5 5 1 80.49 68.03 13.61 o 6 5 1 210.94 189.74 23.22 o 7 5 1 94.25 46.09 27.66 o 8 5 1 275.98 342.67 74.16 o -8 6 1 41.10 106.53 42.36 o -7 6 1 83.47 11.48 36.02 o -6 6 1 223.46 236.55 26.85 o -5 6 1 413.64 384.49 22.46 o -4 6 1 0.28 -0.57 10.08 o -3 6 1 241.99 242.82 11.78 o -2 6 1 0.26 12.19 7.83 o -1 6 1 1052.35 1026.41 18.20 o 0 6 1 2169.47 2177.00 27.93 o 1 6 1 356.42 391.63 11.86 o 2 6 1 26.17 17.42 8.66 o 3 6 1 45.93 38.89 8.90 o 4 6 1 920.44 951.64 23.49 o 5 6 1 454.24 474.49 21.11 o 6 6 1 10.05 -7.65 20.59 o 7 6 1 81.82 52.98 30.46 o 8 6 1 7.36 7.98 40.51 o -7 7 1 254.38 151.83 112.89 o -6 7 1 104.39 86.32 27.40 o -5 7 1 157.43 113.14 21.06 o -4 7 1 673.07 805.04 30.17 o -3 7 1 22.49 -20.18 14.48 o -2 7 1 1819.25 1881.57 34.14 o -1 7 1 279.44 245.85 14.04 o 0 7 1 68.74 50.09 12.18 o 1 7 1 1200.99 1227.74 23.48 o 2 7 1 125.85 92.03 10.84 o 3 7 1 123.86 80.94 17.31 o 4 7 1 241.68 201.15 20.11 o 5 7 1 603.47 657.63 28.98 o 6 7 1 0.53 39.51 36.07 o 7 7 1 7.21 -6.85 34.91 o -6 8 1 38.83 -2.83 42.74 o -5 8 1 339.63 402.62 40.87 o -4 8 1 452.29 489.37 27.32 o -3 8 1 248.55 296.66 36.52 o -2 8 1 558.25 685.18 26.01 o -1 8 1 792.61 915.16 37.22 o 0 8 1 150.45 70.51 20.07 o 1 8 1 0.75 -2.98 17.72 o 2 8 1 784.64 778.45 30.05 o 3 8 1 26.62 21.26 18.65 o 4 8 1 11.77 22.79 26.59 o 5 8 1 0.28 8.03 26.00 o 6 8 1 280.10 326.98 63.09 o -5 9 1 3.37 -1.28 33.00 o -4 9 1 76.78 45.92 31.54 o -3 9 1 3.42 -3.59 31.11 o -2 9 1 71.48 69.80 33.94 o -1 9 1 36.18 22.90 23.14 o 0 9 1 39.29 -18.46 21.28 o 1 9 1 6.56 17.86 20.62 o 2 9 1 39.81 28.56 20.97 o 3 9 1 54.13 57.02 45.69 o 4 9 1 17.08 10.84 31.76 o 5 9 1 24.00 19.92 55.72 o -3 10 1 14.06 32.31 38.12 o -2 10 1 2.62 -5.21 35.65 o -1 10 1 145.15 109.29 35.01 o 0 10 1 28.23 42.58 30.41 o 1 10 1 65.02 8.94 32.47 o 2 10 1 54.39 75.71 32.23 o 3 10 1 4.72 -13.25 47.20 o -10 0 2 350.21 517.97 127.53 o -8 0 2 1.69 68.70 38.09 o -6 0 2 2488.96 2748.66 67.87 o -4 0 2 616.47 642.74 14.87 o -2 0 2 20.19 24.67 3.60 o 2 0 2 362.11 375.11 9.33 o 4 0 2 9143.26 9328.08 119.41 o 6 0 2 365.82 397.25 27.46 o 8 0 2 251.22 217.19 41.21 o -9 1 2 56.60 11.04 36.44 o -8 1 2 2.08 42.48 27.60 o -7 1 2 332.66 320.57 19.47 o -6 1 2 48.11 43.48 9.96 o -5 1 2 204.50 189.68 8.15 o -4 1 2 2955.58 2912.42 24.01 o -3 1 2 132.98 132.89 4.18 o -2 1 2 1774.64 1618.11 13.17 o -1 1 2 62.06 56.08 1.98 o 1 1 2 2462.22 2353.62 19.75 o 2 1 2 23239.85 24029.25 161.92 o 3 1 2 4.78 5.49 3.38 o 4 1 2 38.12 32.70 5.73 o 5 1 2 860.97 880.82 22.18 o 6 1 2 255.74 273.25 14.80 o 7 1 2 192.29 150.33 25.03 o 8 1 2 6.27 -10.70 24.91 o 9 1 2 126.68 42.76 43.11 o -9 2 2 12.46 -9.92 38.84 o -8 2 2 19.89 41.50 22.66 o -7 2 2 47.94 50.10 16.55 o -6 2 2 47.49 56.62 7.75 o -5 2 2 1357.88 1345.60 16.24 o -4 2 2 3199.20 3399.84 27.72 o -3 2 2 1539.53 1488.00 17.24 o -2 2 2 1076.25 1087.29 12.79 o -1 2 2 573.52 527.34 6.43 o 0 2 2 1.23 4.08 2.09 o 1 2 2 1494.82 1492.75 13.63 o 2 2 2 338.38 387.97 6.82 o 3 2 2 543.72 495.07 8.74 o 4 2 2 4834.54 5223.51 45.57 o 5 2 2 355.23 338.78 15.37 o 6 2 2 1.77 -14.16 11.41 o 7 2 2 1726.64 1980.62 80.20 o 8 2 2 28.82 -17.58 24.39 o 9 2 2 2.37 43.79 33.01 o -9 3 2 16.50 0.34 89.12 o -8 3 2 300.74 327.71 54.83 o -7 3 2 21.68 15.15 13.94 o -6 3 2 998.43 1086.06 27.11 o -5 3 2 22.80 22.58 9.63 o -4 3 2 23.99 12.08 6.92 o -3 3 2 233.24 237.50 7.02 o -2 3 2 2.95 7.13 4.24 o -1 3 2 606.40 585.56 7.50 o 0 3 2 1357.00 1326.93 12.41 o 1 3 2 225.04 236.55 5.62 o 2 3 2 87.65 108.49 5.45 o 3 3 2 1598.38 1704.23 22.46 o 4 3 2 255.25 208.89 10.88 o 5 3 2 388.73 362.32 13.77 o 6 3 2 432.87 400.62 20.15 o 7 3 2 68.50 31.93 24.35 o 8 3 2 11.92 14.71 27.87 o 9 3 2 661.93 609.61 57.65 o -9 4 2 0.41 -55.80 55.22 o -8 4 2 668.83 619.12 40.27 o -7 4 2 29.12 13.93 20.30 o -6 4 2 984.99 1093.96 32.14 o -5 4 2 393.02 361.10 17.35 o -4 4 2 167.59 161.22 10.26 o -3 4 2 167.76 166.00 7.81 o -2 4 2 1233.65 1190.66 15.33 o -1 4 2 7.66 7.21 4.67 o 0 4 2 788.71 707.01 9.40 o 1 4 2 702.28 758.91 9.87 o 2 4 2 25.84 24.69 5.44 o 3 4 2 634.75 584.17 14.46 o 4 4 2 1810.50 1762.94 37.60 o 5 4 2 55.66 48.28 15.81 o 6 4 2 11.47 21.50 16.96 o 7 4 2 417.33 425.25 37.71 o 8 4 2 1519.62 1599.77 101.05 o 9 4 2 133.49 81.61 40.70 o -8 5 2 37.77 22.76 32.25 o -7 5 2 807.59 940.82 55.10 o -6 5 2 35.12 24.96 17.52 o -5 5 2 19.08 18.89 13.94 o -4 5 2 777.68 787.30 28.47 o -3 5 2 20.81 19.24 7.16 o -2 5 2 3957.49 4104.57 39.26 o -1 5 2 471.04 499.02 9.91 o 0 5 2 1160.42 971.98 13.72 o 1 5 2 11.61 7.86 4.71 o 2 5 2 2272.79 2189.99 23.14 o 3 5 2 22.81 9.32 9.20 o 4 5 2 36.44 33.30 12.58 o 5 5 2 2907.60 3347.34 53.70 o 6 5 2 5.89 -10.59 17.96 o 7 5 2 2.16 -23.22 23.27 o 8 5 2 2.08 16.05 41.01 o -8 6 2 81.81 42.16 42.73 o -7 6 2 24.21 28.11 31.90 o -6 6 2 75.01 71.51 25.47 o -5 6 2 595.53 620.06 23.19 o -4 6 2 1660.17 1825.74 31.92 o -3 6 2 2.04 -0.53 11.08 o -2 6 2 576.26 554.85 13.13 o -1 6 2 206.51 198.45 9.64 o 0 6 2 30.78 27.35 8.60 o 1 6 2 59.54 80.13 10.63 o 2 6 2 1078.34 1114.07 17.02 o 3 6 2 3308.77 3450.39 45.42 o 4 6 2 35.84 33.31 12.60 o 5 6 2 3.17 -4.66 16.82 o 6 6 2 317.95 335.17 29.66 o 7 6 2 4.14 -14.15 38.20 o 8 6 2 3.30 -32.04 46.37 o -7 7 2 7.42 54.14 38.11 o -6 7 2 175.83 148.85 36.74 o -5 7 2 60.32 88.95 25.28 o -4 7 2 460.08 472.67 23.60 o -3 7 2 15.06 8.96 14.45 o -2 7 2 3.81 11.61 11.00 o -1 7 2 65.57 77.19 12.45 o 0 7 2 4.10 -2.60 11.61 o 1 7 2 1838.08 1913.95 29.25 o 2 7 2 0.00 3.19 9.60 o 3 7 2 4.59 -0.72 14.26 o 4 7 2 156.36 137.70 17.03 o 5 7 2 65.81 81.18 21.90 o 6 7 2 46.94 23.72 25.77 o 7 7 2 32.44 48.54 49.79 o -6 8 2 128.69 81.64 31.65 o -5 8 2 82.73 68.39 58.09 o -4 8 2 90.49 67.77 28.04 o -3 8 2 475.86 507.28 28.90 o -2 8 2 116.15 134.70 18.80 o -1 8 2 3034.53 3382.92 56.93 o 0 8 2 55.97 40.14 18.35 o 1 8 2 11.34 5.18 16.16 o 2 8 2 15.35 0.74 17.63 o 3 8 2 1.59 8.86 19.84 o 4 8 2 132.31 57.82 25.36 o 5 8 2 411.17 474.54 38.71 o 6 8 2 32.38 0.22 30.76 o -5 9 2 0.64 -30.08 34.51 o -4 9 2 189.13 199.37 38.82 o -3 9 2 783.13 804.61 105.86 o -2 9 2 309.84 304.74 31.58 o -1 9 2 64.82 29.43 27.11 o 0 9 2 71.56 38.27 24.68 o 1 9 2 498.16 512.06 30.39 o 2 9 2 538.43 605.55 31.09 o 3 9 2 504.84 528.96 39.43 o 4 9 2 0.59 26.05 32.62 o 5 9 2 191.34 137.18 49.41 o -3 10 2 89.83 6.68 40.70 o -2 10 2 377.21 335.59 41.98 o -1 10 2 436.49 567.85 45.59 o 0 10 2 180.56 174.59 32.64 o 1 10 2 741.68 835.97 61.75 o 2 10 2 210.59 210.62 60.90 o 3 10 2 13.69 24.07 55.50 o -9 0 3 16.82 27.95 39.07 o -7 0 3 713.89 675.49 31.53 o -5 0 3 533.99 568.22 17.86 o -3 0 3 1778.99 1622.15 19.69 o 3 0 3 106.70 79.55 7.49 o 5 0 3 51.22 39.18 11.59 o 7 0 3 197.07 239.22 33.20 o 9 0 3 518.76 617.00 56.79 o -9 1 3 135.00 81.41 40.94 o -8 1 3 914.82 1107.51 72.72 o -7 1 3 224.47 173.89 17.45 o -6 1 3 105.87 114.76 10.04 o -5 1 3 90.46 84.03 6.90 o -4 1 3 515.79 505.94 7.91 o -3 1 3 2578.04 2460.45 18.90 o -2 1 3 6424.81 6286.34 41.18 o -1 1 3 1876.92 1885.10 14.04 o 1 1 3 18.72 16.00 2.23 o 2 1 3 387.89 370.87 6.61 o 3 1 3 5440.30 5512.63 40.98 o 4 1 3 1904.07 1806.58 20.95 o 5 1 3 0.62 -7.33 8.38 o 6 1 3 43.38 45.05 13.96 o 7 1 3 771.92 860.41 36.90 o 8 1 3 104.15 107.98 26.85 o 9 1 3 10.78 -23.12 47.10 o -9 2 3 1.28 5.89 33.16 o -8 2 3 3.52 18.98 18.72 o -7 2 3 0.61 -14.08 16.38 o -6 2 3 2621.75 2823.98 43.14 o -5 2 3 223.76 183.38 6.92 o -4 2 3 1128.54 1025.20 12.27 o -3 2 3 473.88 431.47 8.11 o -2 2 3 7531.15 7310.37 57.97 o -1 2 3 2977.99 2945.00 21.12 o 0 2 3 90.51 101.43 3.12 o 1 2 3 7.58 11.96 4.03 o 2 2 3 1234.28 1124.46 12.14 o 3 2 3 106.73 89.06 4.58 o 4 2 3 1058.46 1037.55 14.57 o 5 2 3 62.17 63.73 9.34 o 6 2 3 40.57 18.40 13.26 o 7 2 3 162.13 162.46 48.89 o 8 2 3 493.30 475.37 39.63 o 9 2 3 2.88 31.16 30.21 o -9 3 3 33.97 11.01 108.38 o -8 3 3 119.41 65.46 24.24 o -7 3 3 551.72 601.15 39.67 o -6 3 3 603.15 583.54 20.02 o -5 3 3 140.40 151.33 10.22 o -4 3 3 331.75 367.91 10.56 o -3 3 3 1087.34 1166.44 16.30 o -2 3 3 15.68 3.05 4.04 o -1 3 3 835.79 789.36 9.30 o 0 3 3 2542.13 2443.41 19.82 o 1 3 3 621.76 648.61 8.74 o 2 3 3 5604.97 5804.79 46.53 o 3 3 3 1348.11 1281.48 15.35 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