#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016395.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016395_Fobs loop_ _publ_author_name 'Beaurain, M.' 'Astier, R.' 'van der Lee, A.' 'Armand, P.' _publ_section_title ; K~3~Ga~2~(PO~4~)~3~ and Na~3~Ga(PO~4~)~2~ ; _journal_coeditor_code IZ3036 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i5 _journal_page_last i8 _journal_volume 64 _journal_year 2008 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _audit_creation_date 07-11-13 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.67110(15) _cell_length_b 17.0109(3) _cell_length_c 8.38857(16) _[local]_cod_data_source_file iz3036Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 -11 9932.69 10117.16 325.43 o 0 1 -11 2251.69 2293.54 249.68 o 1 1 -11 2189.53 2319.19 270.56 o 2 1 -11 508.75 654.02 273.45 o 1 2 -11 273.23 300.05 276.13 o 2 2 -11 2951.62 2825.49 278.63 o 0 3 -11 602.60 649.68 303.05 o 1 3 -11 6995.87 7005.35 280.60 o 2 3 -11 461.61 489.39 281.19 o 1 4 -11 155.06 228.47 255.49 o 2 4 -11 632.43 635.18 298.16 o 0 5 -11 1737.34 1857.69 316.39 o 1 5 -11 4795.12 4355.30 296.49 o 2 5 -11 144.29 104.17 325.00 o 1 6 -11 752.59 827.26 307.59 o 2 6 -11 5871.09 6124.91 338.87 o 3 6 -11 911.74 803.09 446.65 o 0 7 -11 928.43 1198.87 293.19 o 1 8 -11 551.17 266.17 311.54 o 0 0 -10 5722.37 6035.10 224.19 o 2 0 -10 2250.52 2240.45 180.68 o 4 0 -10 4194.71 3691.56 239.95 o 1 1 -10 203.52 181.27 204.84 o 2 1 -10 1081.20 1212.20 186.43 o 3 1 -10 2100.55 1879.31 205.95 o 4 1 -10 2232.49 2212.36 231.86 o 0 2 -10 1998.56 1828.60 202.80 o 1 2 -10 805.82 885.87 218.15 o 2 2 -10 600.43 593.72 230.66 o 3 2 -10 1.95 16.68 178.91 o 4 2 -10 608.62 595.70 242.35 o 1 3 -10 4925.47 4715.89 226.00 o 2 3 -10 192.76 149.49 231.84 o 3 3 -10 3381.42 3564.84 247.28 o 4 3 -10 82.36 59.53 148.21 o 0 4 -10 6071.91 6325.73 237.29 o 1 4 -10 1525.54 1465.74 216.44 o 2 4 -10 1161.28 1064.43 224.77 o 3 4 -10 142.23 184.43 242.24 o 4 4 -10 1701.66 1923.98 232.22 o 1 5 -10 1750.82 1812.80 223.01 o 2 5 -10 2357.34 2459.35 237.79 o 3 5 -10 400.74 460.99 271.74 o 4 5 -10 270.63 267.17 302.62 o 0 6 -10 2134.22 2033.20 217.37 o 1 6 -10 186.94 109.75 226.93 o 2 6 -10 574.43 566.66 246.58 o 3 6 -10 417.04 351.85 274.49 o 4 6 -10 8653.93 8524.84 348.65 o 5 6 -10 835.95 606.10 357.21 o 1 7 -10 2722.93 2695.88 243.19 o 2 7 -10 1547.05 1626.93 253.95 o 3 7 -10 2404.29 2549.82 265.66 o 4 7 -10 337.51 308.76 399.40 o 5 7 -10 130.79 38.71 1931.95 o 0 8 -10 1346.47 1247.47 294.08 o 1 8 -10 122.68 148.20 208.67 o 2 8 -10 1156.59 1156.55 278.36 o 3 8 -10 400.99 363.87 331.42 o 4 8 -10 585.70 765.43 447.84 o 1 9 -10 3733.19 3840.60 269.43 o 2 9 -10 408.26 271.52 307.73 o 3 9 -10 3881.35 3820.84 313.81 o 0 10 -10 1750.26 1995.69 264.56 o 1 10 -10 2406.12 2282.88 275.13 o 2 10 -10 4535.56 4236.75 295.55 o 1 11 -10 -33.45 39.75 129.51 o 2 11 -10 1755.60 1713.29 316.03 o 2 0 -9 7759.48 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359.02 o 1 11 0 1684.93 1790.11 139.81 o 2 11 0 9924.80 10297.58 249.43 o 3 11 0 7323.90 7434.08 229.58 o 4 11 0 63.95 65.65 140.48 o 5 11 0 430.42 113.10 165.64 o 6 11 0 1786.06 2020.86 177.65 o 7 11 0 1527.24 1830.69 196.20 o 8 11 0 7035.00 7080.29 288.07 o 9 11 0 371.44 332.28 229.57 o 10 11 0 1888.72 1431.83 293.93 o 11 11 0 318.77 276.67 354.91 o 0 12 0 19283.30 19390.97 324.43 o 1 12 0 785.29 41.38 142.01 o 2 12 0 3843.46 3535.22 196.48 o 3 12 0 259.54 223.57 147.77 o 4 12 0 2380.83 2426.69 184.58 o 5 12 0 7372.04 7759.23 265.40 o 6 12 0 2225.19 2299.34 194.91 o 7 12 0 402.99 448.40 203.60 o 8 12 0 3874.29 3652.11 252.29 o 9 12 0 265.09 253.33 244.06 o 10 12 0 1623.43 1515.42 309.31 o 1 13 0 2553.76 2723.30 172.24 o 2 13 0 835.17 814.89 155.69 o 3 13 0 7672.29 8357.16 260.80 o 4 13 0 1452.55 1451.52 177.97 o 5 13 0 524.01 461.00 175.62 o 6 13 0 1311.58 1558.65 195.53 o 7 13 0 11045.33 11160.10 346.53 o 8 13 0 35.88 48.35 219.63 o 9 13 0 684.66 550.76 301.62 o 10 13 0 972.28 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233.45 o 11 3 1 948.81 1137.94 291.03 o 12 3 1 220.30 175.39 349.07 o 1 4 1 6609.79 6733.49 125.85 o 2 4 1 56477.24 59342.06 356.09 o 3 4 1 5330.01 5055.63 139.17 o 4 4 1 21689.93 22183.95 266.40 o 5 4 1 2175.42 1885.01 120.96 o 6 4 1 173.43 144.37 108.90 o 7 4 1 3455.99 3612.63 174.87 o 8 4 1 4141.78 3927.94 198.86 o 9 4 1 3799.25 3684.74 216.81 o 10 4 1 334.29 403.52 237.20 o 11 4 1 320.34 339.14 291.39 o 12 4 1 1085.15 1190.95 362.73 o 0 5 1 7199.13 7577.35 137.34 o 1 5 1 4386.45 4322.07 115.61 o 2 5 1 6548.00 6410.08 149.16 o 3 5 1 3177.79 2906.52 128.51 o 4 5 1 4767.37 4664.18 154.21 o 5 5 1 233.00 180.46 105.11 o 6 5 1 514.29 538.21 116.41 o 7 5 1 6421.41 6498.53 212.24 o 8 5 1 2614.20 2429.34 178.32 o 9 5 1 3023.73 3121.24 204.98 o 10 5 1 1946.01 2240.42 253.97 o 11 5 1 200.15 216.63 276.42 o 12 5 1 1041.22 1158.99 351.11 o 1 6 1 1808.52 1675.28 102.76 o 2 6 1 20105.55 21494.15 249.82 o 3 6 1 1594.48 888.57 115.83 o 4 6 1 626.44 383.05 108.47 o 5 6 1 314.78 12.68 119.46 o 6 6 1 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1427.62 1469.39 226.86 o 1 6 10 242.04 174.38 210.44 o 2 6 10 487.72 490.24 223.05 o 3 6 10 517.30 324.49 234.44 o 4 6 10 8773.42 8458.20 329.74 o 5 6 10 631.32 500.44 284.50 o 6 6 10 645.02 733.93 325.72 o 1 7 10 2809.87 2858.07 216.03 o 2 7 10 1428.69 1547.69 242.23 o 3 7 10 2601.95 2573.34 254.77 o 4 7 10 310.37 270.84 275.29 o 5 7 10 151.45 57.98 297.52 o 6 7 10 163.20 161.78 384.03 o 0 8 10 956.14 910.02 276.75 o 1 8 10 171.99 204.34 238.19 o 2 8 10 1128.65 1076.12 258.60 o 3 8 10 428.58 430.74 255.53 o 4 8 10 905.93 940.93 302.19 o 5 8 10 1413.82 1388.28 340.04 o 6 8 10 115.99 228.96 410.63 o 1 9 10 3813.88 3858.30 257.10 o 2 9 10 451.38 259.10 250.66 o 3 9 10 4428.98 4319.53 280.15 o 4 9 10 933.51 885.47 304.15 o 5 9 10 93.87 62.03 304.30 o 0 10 10 1999.21 2026.11 274.90 o 1 10 10 2288.80 2189.88 285.49 o 2 10 10 4401.59 4275.67 279.03 o 3 10 10 220.90 311.00 274.96 o 4 10 10 2694.78 2860.79 311.90 o 5 10 10 758.88 696.53 392.79 o 1 11 10 187.00 71.16 298.89 o 2 11 10 1659.16 1568.12 304.22 o 3 11 10 893.73 943.01 320.23 o 4 11 10 16.01 20.89 191.43 o 0 12 10 3789.02 4031.87 325.68 o 1 12 10 1138.73 1209.03 342.59 o 2 12 10 268.88 318.82 317.27 o 3 12 10 257.95 148.84 315.16 o 1 13 10 1230.27 1241.04 359.80 o 2 13 10 466.96 851.87 302.53 o 3 13 10 284.00 587.88 329.05 o 2 0 11 10290.30 9706.18 319.69 o 4 0 11 3314.67 3326.96 260.29 o 0 1 11 2392.34 2329.51 238.41 o 1 1 11 2832.91 2667.79 235.59 o 2 1 11 718.79 739.04 245.21 o 3 1 11 206.58 178.50 237.26 o 4 1 11 375.12 360.98 260.76 o 5 1 11 2547.49 2474.35 332.98 o 1 2 11 280.73 392.61 236.37 o 2 2 11 2843.43 2654.06 249.28 o 3 2 11 1174.29 1162.42 260.65 o 4 2 11 822.23 582.95 285.61 o 5 2 11 1847.01 2924.41 338.27 o 0 3 11 647.06 618.89 253.28 o 1 3 11 6830.37 6700.70 274.16 o 2 3 11 438.80 469.74 246.75 o 3 3 11 1644.78 1676.24 257.91 o 4 3 11 601.66 676.08 296.38 o 5 3 11 2802.07 3279.08 354.41 o 1 4 11 191.25 230.85 248.97 o 2 4 11 624.02 637.70 267.66 o 3 4 11 557.90 565.97 272.47 o 4 4 11 371.51 422.96 295.25 o 5 4 11 638.53 796.47 388.20 o 0 5 11 2109.50 2031.04 266.43 o 1 5 11 5110.26 4542.40 257.82 o 2 5 11 70.60 135.79 237.80 o 3 5 11 185.42 157.06 270.83 o 4 5 11 677.10 617.51 308.62 o 5 5 11 1438.99 1189.13 391.68 o 1 6 11 899.39 903.52 291.94 o 2 6 11 6152.14 6118.74 284.92 o 3 6 11 596.07 686.14 285.49 o 4 6 11 2348.72 2370.54 325.13 o 0 7 11 1574.62 1570.57 279.26 o 1 7 11 1641.27 1651.88 316.92 o 2 7 11 167.68 166.14 1329.59 o 3 7 11 107.97 94.19 6891.76 o 4 7 11 1690.74 1826.18 332.21 o 1 8 11 402.00 165.76 314.83 o 2 8 11 570.08 677.43 310.28 o 3 8 11 2226.73 2208.29 339.18 o 4 8 11 317.97 581.20 384.13 o 0 9 11 929.67 765.31 358.22 o 1 9 11 1256.27 1318.24 329.89 o 2 9 11 555.32 600.84 303.90 o 3 9 11 1328.43 1244.95 355.73 o 1 10 11 320.71 416.84 329.18 o 2 0 12 543.02 774.26 315.02 o 1 1 12 -90.23 43.17 282.15 o 2 1 12 1078.92 1485.00 326.16 o 0 2 12 1510.31 1421.73 326.18 o 1 2 12 -59.99 80.20 232.96 o 2 2 12 119.56 153.41 349.47 o 3 2 12 570.95 647.21 346.20 o 1 3 12 1027.70 1003.83 347.28 o 2 3 12 82.64 118.71 313.24 o 0 4 12 1490.90 1382.03 345.86 o 1 4 12 24.70 149.76 329.68 o 2 4 12 543.83 866.11 303.42 o 2 5 12 511.84 631.61 297.95 o 0 6 12 2220.16 3427.75 379.33 o 1 6 12 175.32 128.69 382.96 o