#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016398.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016398_Fobs loop_ _publ_author_name 'Liu, Qi Sheng' 'Liu, Lian Dong' 'Shi, Jing Min' _publ_section_title ; Bis[\m-1-(1,10-phenanthrolin-2-yl)-2-pyridone]bis{aqua[1-(1,10-phenanthrolin-2-yl)-2-pyridone]cadmium(II)} tetrakis(perchlorate) ; _journal_coeditor_code LN3071 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m58 _journal_page_last m60 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 107.317 _cell_angle_beta 106.340 _cell_angle_gamma 91.838 _cell_length_a 11.6808 _cell_length_b 12.4371 _cell_length_c 12.7092 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8165 _[local]_cod_data_source_file ln3071Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 70507am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 276.71 254.86 10.51 o 2 0 0 13396.65 14147.27 395.08 o 3 0 0 626.53 668.69 27.06 o 4 0 0 273.75 309.23 19.40 o 6 0 0 226.75 232.22 19.34 o 7 0 0 727.60 715.41 36.72 o 8 0 0 1493.33 1331.73 65.27 o 9 0 0 40.35 46.11 12.83 o 10 0 0 167.02 186.22 28.16 o 11 0 0 64.89 89.54 25.69 o 12 0 0 157.64 168.57 33.03 o 13 0 0 10.11 24.40 26.80 o -13 1 0 0.14 0.00 21.87 o -12 1 0 226.47 244.03 35.95 o -11 1 0 15.61 31.79 19.92 o -10 1 0 241.74 250.90 30.88 o -9 1 0 1175.38 1268.21 60.41 o -8 1 0 2187.96 2118.51 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