#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:07 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180832 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/63/2016399.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016399_Fobs loop_ _publ_author_name 'Thu\'ery, Pierre' _publ_section_title ; One-dimensional uranium--organic framework in catena-poly[[di-\m~2~-hydroxido-bis[dioxouranium(VI)]]-di-\m~2~-2-pyridylacetato-\k^3^O,N:O';\k^3^O:O',N] ; _journal_coeditor_code LN3075 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m50 _journal_page_last m52 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.946 _cell_angle_beta 96.487 _cell_angle_gamma 110.425 _cell_length_a 6.4056 _cell_length_b 8.2220 _cell_length_c 9.0916 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.8201 _cod_data_source_file ln3075Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1544.58 1428.12 134.95 o 2 0 0 12811.97 12454.60 135.85 o 3 0 0 15580.81 15107.81 190.22 o 4 0 0 787.03 779.36 16.31 o 5 0 0 6348.33 6593.06 111.36 o 6 0 0 4106.63 4190.39 185.15 o 7 0 0 1.80 -4.47 12.93 o -7 1 0 3514.53 3610.53 216.60 o -6 1 0 3787.55 3768.95 239.32 o -5 1 0 2217.04 2215.19 90.78 o -4 1 0 11227.85 10795.95 347.87 o -3 1 0 9700.50 9750.45 305.73 o -2 1 0 9839.77 9402.06 243.59 o -1 1 0 27947.04 25191.17 1361.17 o 1 1 0 9643.88 9171.01 259.13 o 2 1 0 21049.11 20558.41 227.87 o 3 1 0 16.50 31.60 8.64 o 4 1 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