#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016409.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2016409_Fobs
loop_
_publ_author_name
'Copolovici, Dana'
'Silvestru, Cristian'
'Varga, Richard A.'
_publ_section_title
;
 Tris[2-(morpholin-4-ylmethyl)phenyl-\k^2^<i>C</i>^1^,<i>N</i>]antimony(III)
;
_journal_coeditor_code           SF3067
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m37
_journal_page_last               m39
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           148
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   19.02600
_cell_length_b                   19.0260
_cell_length_c                   14.5210
_exptl_crystal_F_000             2016.00
_reflns_d_resolution_high        0.8001
_[local]_cod_data_source_file    sf3067Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
' 149rich   R-3          R = 0.04                    '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            598.01
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-y,x-y,z
-x+y,-x,z
-x,-y,-z
y,-x+y,-z
x-y,x,-z
1/3+x,2/3+y,2/3+z
1/3-y,2/3+x-y,2/3+z
1/3-x+y,2/3-x,2/3+z
1/3-x,2/3-y,2/3-z
1/3+y,2/3-x+y,2/3-z
1/3+x-y,2/3+x,2/3-z
2/3+x,1/3+y,1/3+z
2/3-y,1/3+x-y,1/3+z
2/3-x+y,1/3-x,1/3+z
2/3-x,1/3-y,1/3-z
2/3+y,1/3-x+y,1/3-z
2/3+x-y,1/3+x,1/3-z
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
_refln_sint/lambda
-1 2 0 100313.24 100313.24 316.72 o 0.05256
0 3 0 16119.50 16119.50 126.96 o 0.09104
-2 4 0 432.76 432.76 20.80 o 0.10512
-4 5 0 139468.86 139468.86 373.46 o 0.13906
-1 5 0 139766.66 139766.66 373.85 o 0.13906
-3 6 0 16450.99 16450.99 128.26 o 0.15768
0 6 0 31136.66 31136.66 176.46 o 0.18207
-5 7 0 138589.16 138589.16 372.28 o 0.18951
-2 7 0 17133.50 17133.50 130.89 o 0.18951
-7 8 0 22032.40 22032.40 148.43 o 0.22910
-4 8 0 42519.68 42519.68 206.20 o 0.21024
-1 8 0 41052.72 41052.72 202.61 o 0.22910
-6 9 0 34455.99 34455.99 185.62 o 0.24086
-3 9 0 51929.36 51929.36 227.88 o 0.24086
0 9 0 21094.34 21094.34 145.24 o 0.27311
-8 10 0 83452.15 83452.15 288.88 o 0.27812
-5 10 0 27245.81 27245.81 165.06 o 0.26280
-2 10 0 24752.14 24752.14 157.33 o 0.27812
-10 11 0 29013.71 29013.71 170.33 o 0.31971
-7 11 0 17387.23 17387.23 131.86 o 0.29264
-4 11 0 27847.64 27847.64 166.88 o 0.29264
-1 11 0 22062.20 22062.20 148.53 o 0.31971
-9 12 0 45301.25 45301.25 212.84 o 0.32823
-6 12 0 38818.22 38818.22 197.02 o 0.31536
-3 12 0 41970.72 41970.72 204.87 o 0.32823
0 12 0 13690.13 13690.13 117.00 o 0.36414
-11 13 0 20701.68 20701.68 143.88 o 0.36792
-8 13 0 44752.09 44752.09 211.55 o 0.34466
-5 13 0 15970.87 15970.87 126.38 o 0.34466
-2 13 0 31999.78 31999.78 178.88 o 0.36792
-13 14 0 18119.99 18119.99 134.61 o 0.41050
-10 14 0 24873.58 24873.58 157.71 o 0.37901
-7 14 0 19443.71 19443.71 139.44 o 0.36792
-4 14 0 13396.56 13396.56 115.74 o 0.37901
-1 14 0 9791.33 9791.33 98.95 o 0.41050
-12 15 0 7363.97 7363.97 85.81 o 0.41718
-9 15 0 13503.63 13503.63 116.21 o 0.39682
-6 15 0 7128.37 7128.37 84.43 o 0.39682
-3 15 0 9740.58 9740.58 98.69 o 0.41718
0 15 0 12441.49 12441.49 111.54 o 0.45518
-14 16 0 6501.55 6501.55 80.63 o 0.45820
-11 16 0 3184.79 3184.79 56.43 o 0.43022
-8 16 0 2045.31 2045.31 45.23 o 0.42048
-5 16 0 6388.44 6388.44 79.93 o 0.43022
-2 16 0 12315.91 12315.91 110.98 o 0.45820
-16 17 0 9415.04 9415.04 97.03 o 0.50139
-13 17 0 8338.69 8338.69 91.32 o 0.46716
-10 17 0 7426.22 7426.22 86.18 o 0.44907
-7 17 0 10986.40 10986.40 104.82 o 0.44907
-4 17 0 6303.15 6303.15 79.39 o 0.46716
-1 17 0 18234.28 18234.28 135.03 o 0.50139
-15 18 0 5259.71 5259.71 72.52 o 0.50687
-12 18 0 9436.42 9436.42 97.14 o 0.48172
-9 18 0 14330.16 14330.16 119.71 o 0.47304
-6 18 0 18179.52 18179.52 134.83 o 0.48172
-3 18 0 6433.68 6433.68 80.21 o 0.50687
0 18 0 4101.78 4101.78 64.05 o 0.54622
-17 19 0 3415.69 3415.69 58.44 o 0.54874
-14 19 0 8084.17 8084.17 89.91 o 0.51765
-11 19 0 12210.03 12210.03 110.50 o 0.50139
-8 19 0 15819.67 15819.67 125.78 o 0.50139
-5 19 0 4575.47 4575.47 67.64 o 0.51765
-2 19 0 3372.09 3372.09 58.07 o 0.54874
-19 20 0 1538.65 1538.65 39.23 o 0.59232
-16 20 0 5846.98 5846.98 76.47 o 0.55624
-13 20 0 5171.08 5171.08 71.91 o 0.53342
-10 20 0 6656.55 6656.55 81.59 o 0.52560
-7 20 0 7345.90 7345.90 85.71 o 0.53342
-4 20 0 3287.83 3287.83 57.34 o 0.55624
-1 20 0 3969.54 3969.54 63.00 o 0.59232
-18 21 0 4125.46 4125.46 64.23 o 0.59696
-15 21 0 3654.76 3654.76 60.45 o 0.56852
-12 21 0 2611.89 2611.89 51.11 o 0.55375
-9 21 0 5558.07 5558.07 74.55 o 0.55375
-6 21 0 3681.70 3681.70 60.68 o 0.56852
-3 21 0 3631.41 3631.41 60.26 o 0.59696
0 21 0 3310.69 3310.69 57.54 o 0.63725
-20 22 0 3159.61 3159.61 56.21 o 0.63942
-17 22 0 3388.21 3388.21 58.21 o 0.60615
-14 22 0 4884.16 4884.16 69.89 o 0.58528
-11 22 0 4878.39 4878.39 69.85 o 0.57816
-8 22 0 4001.43 4001.43 63.26 o 0.58528
-5 22 0 3937.68 3937.68 62.75 o 0.60615
-2 22 0 2210.44 2210.44 47.02 o 0.63942
-19 23 0 6077.70 6077.70 77.96 o 0.64586
-16 23 0 1885.16 1885.16 43.42 o 0.61967
-13 23 0 3010.94 3010.94 54.87 o 0.60615
-10 23 0 5675.95 5675.95 75.34 o 0.60615
-7 23 0 2135.21 2135.21 46.21 o 0.61967
-4 23 0 1754.24 1754.24 41.88 o 0.64586
-15 24 0 3428.61 3428.61 58.55 o 0.63725
-12 24 0 2277.66 2277.66 47.72 o 0.63072
-9 24 0 1476.57 1476.57 38.43 o 0.63725
-1 1 1 148.74 148.74 12.20 o 0.04590
-3 2 1 4688.13 4688.13 68.47 o 0.08736
0 2 1 6524.54 6524.54 80.77 o 0.06978
-5 3 1 34761.71 34761.71 186.44 o 0.13668
-2 3 1 192.45 192.45 13.87 o 0.08736
1 3 1 10523.58 10523.58 102.58 o 0.11470
-7 4 1 363.44 363.44 19.06 o 0.18777
-4 4 1 1117.21 1117.21 33.42 o 0.12617
-1 4 1 25757.36 25757.36 160.49 o 0.11470
2 4 1 8568.31 8568.31 92.57 o 0.16422
-9 5 1 2967.62 2967.62 54.48 o 0.23949
-6 5 1 70134.52 70134.52 264.83 o 0.17243
-3 5 1 46080.17 46080.17 214.66 o 0.13668
0 5 1 2258.07 2258.07 47.52 o 0.15558
3 5 1 2161.82 2161.82 46.50 o 0.21519
-11 6 1 9405.14 9405.14 96.98 o 0.29152
-8 6 1 29486.91 29486.91 171.72 o 0.22152
-5 6 1 8973.88 8973.88 94.73 o 0.17243
-2 6 1 8512.98 8512.98 92.27 o 0.16422
1 6 1 3256.52 3256.52 57.07 o 0.20194
4 6 1 9979.95 9979.95 99.90 o 0.26678
-13 7 1 284.88 284.88 16.88 o 0.34370
-10 7 1 8.32 8.32 2.88 o 0.27190
-7 7 1 6293.00 6293.00 79.33 o 0.21519
-4 7 1 4467.08 4467.08 66.84 o 0.18777
-1 7 1 1265.33 1265.33 35.57 o 0.20194
2 7 1 13.32 13.32 3.65 o 0.25076
5 7 1 282.85 282.85 16.82 o 0.31868
-15 8 1 140.04 140.04 11.83 o 0.39599
-12 8 1 263.19 263.19 16.22 o 0.32299
-9 8 1 822.10 822.10 28.67 o 0.26155
-6 8 1 11446.17 11446.17 106.99 o 0.22152
-3 8 1 23537.42 23537.42 153.42 o 0.21519
0 8 1 3398.13 3398.13 58.29 o 0.24519
3 8 1 472.01 472.01 21.73 o 0.30084
6 8 1 924.34 924.34 30.40 o 0.37077
-17 9 1 982.30 982.30 31.34 o 0.44834
-14 9 1 2.06 2.06 1.43 o 0.37448
-11 9 1 2.70 2.70 1.64 o 0.30989
-8 9 1 13839.52 13839.52 117.64 o 0.26155
-5 9 1 13.57 13.57 3.68 o 0.23949
-2 9 1 1230.04 1230.04 35.07 o 0.25076
1 9 1 9831.24 9831.24 99.15 o 0.29152
4 9 1 552.13 552.13 23.50 o 0.35165
7 9 1 4692.39 4692.39 68.50 o 0.42297
-19 10 1 250.47 250.47 15.83 o 0.50073
-16 10 1 668.43 668.43 25.85 o 0.42623
-13 10 1 71.44 71.44 8.45 o 0.35942
-10 10 1 3388.00 3388.00 58.21 o 0.30540
-7 10 1 9968.25 9968.25 99.84 o 0.27190
-4 10 1 2048.91 2048.91 45.26 o 0.26678
-1 10 1 375.42 375.42 19.38 o 0.29152
2 10 1 5542.96 5542.96 74.45 o 0.33966
5 10 1 933.44 933.44 30.55 o 0.40291
8 10 1 968.84 968.84 31.13 o 0.47526
-21 11 1 0.22 0.22 0.47 o 0.55316
-18 11 1 26.77 26.77 5.17 o 0.47816
-15 11 1 17.20 17.20 4.15 o 0.40970
-12 11 1 956.16 956.16 30.92 o 0.35165
-9 11 1 0.77 0.77 0.88 o 0.30989
-6 11 1 39.65 39.65 6.30 o 0.29152
-3 11 1 11513.54 11513.54 107.30 o 0.30084
0 11 1 5399.11 5399.11 73.48 o 0.33557
3 11 1 146.07 146.07 12.09 o 0.38895
6 11 1 1307.33 1307.33 36.16 o 0.45446
9 11 1 403.25 403.25 20.08 o 0.52760
-23 12 1 19.63 19.63 4.43 o 0.60561
-20 12 1 32.83 32.83 5.73 o 0.53021
-17 12 1 37.19 37.19 6.10 o 0.46050
-14 12 1 1112.07 1112.07 33.35 o 0.39946
-11 12 1 124.18 124.18 11.14 o 0.35165
-8 12 1 1715.10 1715.10 41.41 o 0.32299
-5 12 1 1021.52 1021.52 31.96 o 0.31868
-2 12 1 1215.12 1215.12 34.86 o 0.33966
1 12 1 1896.19 1896.19 43.55 o 0.38178
4 12 1 934.52 934.52 30.57 o 0.43900
7 12 1 401.18 401.18 20.03 o 0.50622
10 12 1 45.26 45.26 6.73 o 0.57998
-22 13 1 0.18 0.18 0.42 o 0.58235
-19 13 1 15.96 15.96 4.00 o 0.51165
-16 13 1 295.96 295.96 17.20 o 0.44834
-13 13 1 811.82 811.82 28.49 o 0.39599
-10 13 1 3571.22 3571.22 59.76 o 0.35942
-7 13 1 35.74 35.74 5.98 o 0.34370
-4 13 1 1992.67 1992.67 44.64 o 0.35165
-1 13 1 3557.32 3557.32 59.64 o 0.38178
2 13 1 733.88 733.88 27.09 o 0.42946
5 13 1 398.28 398.28 19.96 o 0.48957
8 13 1 172.66 172.66 13.14 o 0.55813
11 13 1 23.21 23.21 4.82 o 0.63238
-24 14 1 206.91 206.91 14.38 o 0.63456
-21 14 1 136.74 136.74 11.69 o 0.56306
-18 14 1 183.85 183.85 13.56 o 0.49797
-15 14 1 9.73 9.73 3.12 o 0.44213
-12 14 1 1006.82 1006.82 31.73 o 0.39946
-9 14 1 158.85 158.85 12.60 o 0.37448
-6 14 1 5292.73 5292.73 72.75 o 0.37077
-3 14 1 1770.17 1770.17 42.07 o 0.38895
0 14 1 948.09 948.09 30.79 o 0.42623
3 14 1 1364.21 1364.21 36.94 o 0.47816
6 14 1 210.71 210.71 14.52 o 0.54053
9 14 1 2.05 2.05 1.43 o 0.61015
-23 15 1 3.21 3.21 1.79 o 0.61466
-20 15 1 392.74 392.74 19.82 o 0.54814
-17 15 1 1374.54 1374.54 37.07 o 0.48957
-14 15 1 0.78 0.78 0.88 o 0.44213
-11 15 1 1045.58 1045.58 32.34 o 0.40970
-8 15 1 396.17 396.17 19.90 o 0.39599
-5 15 1 3051.25 3051.25 55.24 o 0.40291
-2 15 1 191.90 191.90 13.85 o 0.42946
1 15 1 1506.34 1506.34 38.81 o 0.47234
4 15 1 1.04 1.04 1.02 o 0.52760
7 15 1 621.61 621.61 24.93 o 0.59176
-22 16 1 193.00 193.00 13.89 o 0.59872
-19 16 1 515.58 515.58 22.71 o 0.53797
-16 16 1 11.20 11.20 3.35 o 0.48674
-13 16 1 113.07 113.07 10.63 o 0.44834
-10 16 1 189.74 189.74 13.77 o 0.42623
-7 16 1 106.57 106.57 10.32 o 0.42297
-4 16 1 4728.72 4728.72 68.77 o 0.43900
-1 16 1 403.04 403.04 20.08 o 0.47234
2 16 1 320.58 320.58 17.90 o 0.51968
5 16 1 1465.35 1465.35 38.28 o 0.57759
8 16 1 277.73 277.73 16.67 o 0.64321
-24 17 1 19.17 19.17 4.38 o 0.64962
-21 17 1 97.42 97.42 9.87 o 0.58708
-18 17 1 151.16 151.16 12.29 o 0.53281
-15 17 1 123.02 123.02 11.09 o 0.48957
-12 17 1 447.45 447.45 21.15 o 0.46050
-9 17 1 2.38 2.38 1.54 o 0.44834
-6 17 1 1473.48 1473.48 38.39 o 0.45446
-3 17 1 523.32 523.32 22.88 o 0.47816
0 17 1 405.92 405.92 20.15 o 0.51702
3 17 1 0.87 0.87 0.93 o 0.56794
6 17 1 48.91 48.91 6.99 o 0.62800
-23 18 1 34.51 34.51 5.87 o 0.63674
-20 18 1 3.18 3.18 1.78 o 0.57998
-17 18 1 272.75 272.75 16.52 o 0.53281
-14 18 1 80.22 80.22 8.96 o 0.49797
-11 18 1 60.69 60.69 7.79 o 0.47816
-8 18 1 21.48 21.48 4.64 o 0.47526
-5 18 1 26.39 26.39 5.14 o 0.48957
-2 18 1 482.80 482.80 21.97 o 0.51968
1 18 1 734.39 734.39 27.10 o 0.56306
4 18 1 72.28 72.28 8.50 o 0.61690
-22 19 1 73.87 73.87 8.59 o 0.62800
-19 19 1 177.38 177.38 13.32 o 0.57759
-16 19 1 91.07 91.07 9.54 o 0.53797
-13 19 1 18.99 18.99 4.36 o 0.51165
-10 19 1 65.91 65.91 8.12 o 0.50073
-7 19 1 268.35 268.35 16.38 o 0.50622
-4 19 1 95.93 95.93 9.79 o 0.52760
-1 19 1 1.68 1.68 1.30 o 0.56306
2 19 1 3.19 3.19 1.79 o 0.61015
-21 20 1 10.85 10.85 3.29 o 0.62359
-18 20 1 686.04 686.04 26.19 o 0.57998
-15 20 1 34.63 34.63 5.89 o 0.54814
-12 20 1 7.24 7.24 2.69 o 0.53021
-9 20 1 203.79 203.79 14.28 o 0.52760
-6 20 1 32.22 32.22 5.68 o 0.54053
-3 20 1 463.45 463.45 21.53 o 0.56794
0 20 1 333.35 333.35 18.26 o 0.60788
-20 21 1 27.18 27.18 5.21 o 0.62359
-17 21 1 64.20 64.20 8.01 o 0.58708
-14 21 1 108.86 108.86 10.43 o 0.56306
-11 21 1 23.38 23.38 4.84 o 0.55316
-8 21 1 460.82 460.82 21.47 o 0.55813
-5 21 1 279.52 279.52 16.72 o 0.57759
-2 21 1 187.54 187.54 13.69 o 0.61015
-19 22 1 44.02 44.02 6.64 o 0.62800
-16 22 1 0.49 0.49 0.70 o 0.59872
-13 22 1 4.09 4.09 2.02 o 0.58235
-10 22 1 43.02 43.02 6.56 o 0.57998
-7 22 1 488.99 488.99 22.11 o 0.59176
-4 22 1 72.89 72.89 8.54 o 0.61690
-18 23 1 2.79 2.79 1.67 o 0.63674
-15 23 1 112.72 112.72 10.62 o 0.61466
-12 23 1 132.00 132.00 11.49 o 0.60561
-9 23 1 16.16 16.16 4.02 o 0.61015
-6 23 1 197.55 197.55 14.06 o 0.62800
-17 24 1 533.22 533.22 23.09 o 0.64962
-14 24 1 447.10 447.10 21.14 o 0.63456
-11 24 1 116.90 116.90 10.81 o 0.63238
-8 24 1 190.91 190.91 13.82 o 0.64321
0 1 2 245495.36 245495.36 495.47 o 0.07526
-2 2 2 62824.37 62824.37 250.65 o 0.09179
1 2 2 152832.94 152832.94 390.94 o 0.10578
-4 3 2 357617.34 357617.34 598.01 o 0.12928
-1 3 2 24785.39 24785.39 157.43 o 0.10578
2 3 2 1969.41 1969.41 44.38 o 0.14913
-6 4 2 55714.16 55714.16 236.04 o 0.17472
-3 4 2 69224.88 69224.88 263.11 o 0.12928
0 4 2 29379.60 29379.60 171.40 o 0.13956
3 4 2 48030.53 48030.53 219.16 o 0.19701
-8 5 2 27782.07 27782.07 166.68 o 0.22330
-5 5 2 123729.98 123729.98 351.75 o 0.16662
-2 5 2 14896.02 14896.02 122.05 o 0.14913
1 5 2 42531.60 42531.60 206.23 o 0.18245
4 5 2 36198.39 36198.39 190.26 o 0.24681
-10 6 2 19958.46 19958.46 141.27 o 0.27336
-7 6 2 92971.99 92971.99 304.91 o 0.21057
-4 6 2 76142.29 76142.29 275.94 o 0.17472
-1 6 2 51669.42 51669.42 227.31 o 0.18245
2 6 2 62666.33 62666.33 250.33 o 0.22940
5 6 2 20458.22 20458.22 143.03 o 0.29755
-12 7 2 25320.29 25320.29 159.12 o 0.32421
-9 7 2 41093.50 41093.50 202.72 o 0.25776
-6 7 2 24148.04 24148.04 155.40 o 0.21057
-3 7 2 25845.10 25845.10 160.76 o 0.19701
0 7 2 35314.39 35314.39 187.92 o 0.22330
3 7 2 42391.96 42391.96 205.89 o 0.27837
6 7 2 22133.77 22133.77 148.77 o 0.34884
-14 8 2 12102.44 12102.44 110.01 o 0.37554
-11 8 2 11244.89 11244.89 106.04 o 0.30670
-8 8 2 65742.44 65742.44 256.40 o 0.25234
-5 8 2 22710.38 22710.38 150.70 o 0.22330
-2 8 2 65646.64 65646.64 256.22 o 0.22940
1 8 2 20622.67 20622.67 143.61 o 0.26826
4 8 2 23310.09 23310.09 152.68 o 0.32845
7 8 2 6324.95 6324.95 79.53 o 0.40046
-16 9 2 8397.34 8397.34 91.64 o 0.42716
-13 9 2 18709.96 18709.96 136.78 o 0.35667
-10 9 2 10325.77 10325.77 101.62 o 0.29755
-7 9 2 24521.35 24521.35 156.59 o 0.25776
-4 9 2 43125.41 43125.41 207.67 o 0.24681
-1 9 2 34858.49 34858.49 186.70 o 0.26826
2 9 2 51348.20 51348.20 226.60 o 0.31558
5 9 2 17112.54 17112.54 130.81 o 0.37920
8 9 2 15952.02 15952.02 126.30 o 0.45229
-18 10 2 11204.07 11204.07 105.85 o 0.47899
-15 10 2 11356.89 11356.89 106.57 o 0.40730
-12 10 2 22438.78 22438.78 149.80 o 0.34486
-9 10 2 63544.41 63544.41 252.08 o 0.29755
-6 10 2 12460.32 12460.32 111.63 o 0.27336
-3 10 2 9293.68 9293.68 96.40 o 0.27837
0 10 2 14682.21 14682.21 121.17 o 0.31117
3 10 2 33045.60 33045.60 181.78 o 0.36433
6 10 2 14150.89 14150.89 118.96 o 0.43038
9 10 2 9233.49 9233.49 96.09 o 0.50427
-20 11 2 6015.62 6015.62 77.56 o 0.53096
-17 11 2 10730.45 10730.45 103.59 o 0.45836
-14 11 2 19044.97 19044.97 138.00 o 0.39350
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