#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016411.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016411_Fobs loop_ _publ_author_name 'Wang, Xin-Qiang' 'Yu, Wen-Tao' 'Xu, Dong' 'Fan, Jian-Dong' 'Zhang, Guang-Hui' 'Ren, Quan' _publ_section_title ; Tetraphenylphosphonium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)aurate(III) acetone solvate and ethyltriphenylphosphonium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)aurate(III) ; _journal_coeditor_code SK3168 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m46 _journal_page_last m49 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.959 _cell_angle_gamma 90.000 _cell_length_a 17.3058 _cell_length_b 9.9306 _cell_length_c 19.0668 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.7692 _[local]_cod_data_source_file sk3168IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' TPEADT in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 416.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 78569.68 81343.95 1140.00 o 4 0 0 57269.66 58319.37 832.28 o 6 0 0 1458.99 1593.80 34.59 o 8 0 0 27642.44 28102.55 478.42 o 10 0 0 2407.96 2251.26 58.21 o 12 0 0 3009.98 3039.95 76.03 o 14 0 0 36.86 21.87 38.12 o 16 0 0 56.63 10.72 54.56 o 18 0 0 79.44 157.22 73.69 o 20 0 0 670.52 777.83 98.66 o 1 1 0 13498.71 13963.22 146.20 o 2 1 0 1220.01 1195.74 22.11 o 3 1 0 21706.54 22406.66 234.22 o 4 1 0 1268.37 1064.88 28.34 o 5 1 0 326.83 316.53 18.43 o 6 1 0 2910.35 3101.43 47.62 o 7 1 0 2441.47 2330.42 39.41 o 8 1 0 20091.18 20395.26 178.76 o 9 1 0 1849.15 1963.06 48.90 o 10 1 0 8759.46 8600.54 96.72 o 11 1 0 2774.77 2886.35 54.98 o 12 1 0 23024.26 22709.60 222.83 o 13 1 0 5060.42 4885.56 95.99 o 14 1 0 1361.50 1395.95 53.50 o 15 1 0 94.49 29.94 32.90 o 16 1 0 4016.46 4029.71 121.59 o 17 1 0 530.78 449.09 44.93 o 18 1 0 1189.49 1105.31 67.63 o 19 1 0 764.34 894.86 69.77 o 20 1 0 1564.50 1625.75 103.85 o 21 1 0 225.82 141.60 73.24 o 0 2 0 5863.41 5939.31 145.72 o 1 2 0 15840.92 16274.10 197.59 o 2 2 0 34182.23 36361.11 366.10 o 3 2 0 81.08 131.83 22.22 o 4 2 0 25469.28 26092.72 280.15 o 5 2 0 5320.19 5270.86 69.11 o 6 2 0 14071.25 14537.24 158.72 o 7 2 0 34024.64 34213.86 300.03 o 8 2 0 30468.27 30628.67 300.28 o 9 2 0 31368.87 31552.87 262.56 o 10 2 0 216.95 183.83 28.76 o 11 2 0 12060.18 11567.28 133.11 o 12 2 0 555.06 533.49 34.42 o 13 2 0 6459.57 6255.86 87.41 o 14 2 0 1.65 -9.49 23.77 o 15 2 0 4517.08 4657.58 102.76 o 16 2 0 403.44 384.46 43.37 o 17 2 0 2570.36 2741.91 84.14 o 18 2 0 107.26 55.54 41.68 o 19 2 0 1867.27 1957.64 78.85 o 20 2 0 224.03 414.66 80.25 o 21 2 0 819.32 1051.33 126.98 o 1 3 0 13651.22 14104.08 138.54 o 2 3 0 5093.49 5049.13 66.94 o 3 3 0 32140.46 32693.92 276.75 o 4 3 0 6777.12 7105.69 71.98 o 5 3 0 63114.99 63815.08 489.24 o 6 3 0 236.64 179.71 17.18 o 7 3 0 8264.90 8261.23 111.36 o 8 3 0 2740.99 2898.21 49.34 o 9 3 0 13366.31 12910.86 154.90 o 10 3 0 1.84 -7.41 21.78 o 11 3 0 416.90 393.07 37.51 o 12 3 0 79.79 54.17 23.13 o 13 3 0 12.94 10.55 24.08 o 14 3 0 18.60 -11.32 27.76 o 15 3 0 57.88 13.53 25.16 o 16 3 0 82.18 -2.30 32.16 o 17 3 0 652.59 482.98 75.31 o 18 3 0 161.59 115.75 48.68 o 19 3 0 666.43 671.66 65.00 o 20 3 0 0.61 74.60 52.22 o 21 3 0 234.51 180.09 63.24 o 0 4 0 11538.48 11717.00 202.89 o 1 4 0 1048.96 1075.64 22.51 o 2 4 0 8080.39 8222.80 101.44 o 3 4 0 35133.09 35691.01 371.82 o 4 4 0 21492.20 22084.03 201.07 o 5 4 0 9331.72 9506.81 104.55 o 6 4 0 64.46 37.29 17.92 o 7 4 0 8196.91 7866.05 95.47 o 8 4 0 6628.69 6683.80 132.87 o 9 4 0 4364.64 4245.30 101.90 o 10 4 0 29.38 -3.55 23.16 o 11 4 0 11513.47 11314.70 178.65 o 12 4 0 770.01 765.27 44.23 o 13 4 0 10050.93 9743.16 173.30 o 14 4 0 601.86 544.06 47.04 o 15 4 0 4523.34 4577.51 140.44 o 16 4 0 30.64 1.22 38.89 o 17 4 0 3944.83 4204.79 112.48 o 18 4 0 53.47 80.31 48.00 o 19 4 0 1026.95 935.95 71.25 o 20 4 0 33.60 24.42 52.71 o 1 5 0 15639.14 15978.79 186.03 o 2 5 0 25.58 36.78 11.74 o 3 5 0 6620.41 6705.38 93.27 o 4 5 0 1603.00 1483.44 38.38 o 5 5 0 3171.37 3146.94 52.98 o 6 5 0 9386.75 9296.52 109.02 o 7 5 0 3259.62 3255.35 64.61 o 8 5 0 1145.98 1178.50 50.35 o 9 5 0 4006.22 3950.36 74.49 o 10 5 0 4440.26 4288.99 81.62 o 11 5 0 23.32 21.04 27.49 o 12 5 0 5321.13 5234.43 99.80 o 13 5 0 370.41 391.31 41.52 o 14 5 0 4212.37 4176.21 96.40 o 15 5 0 192.98 213.27 49.65 o 16 5 0 2845.13 2964.58 101.05 o 17 5 0 79.87 80.69 57.18 o 18 5 0 469.44 430.31 80.87 o 19 5 0 7.61 -48.42 48.42 o 20 5 0 126.19 149.44 57.03 o 0 6 0 12971.68 12507.75 336.77 o 1 6 0 247.18 210.82 19.94 o 2 6 0 29841.62 29929.82 289.09 o 3 6 0 193.69 227.32 18.54 o 4 6 0 23538.52 22861.21 259.84 o 5 6 0 3864.83 3931.24 76.62 o 6 6 0 21576.37 20967.01 226.89 o 7 6 0 138.47 94.32 25.91 o 8 6 0 3068.36 3133.16 79.74 o 9 6 0 3.03 -17.73 28.63 o 10 6 0 2625.73 2617.77 81.83 o 11 6 0 204.40 177.80 40.95 o 12 6 0 1022.46 1060.11 50.71 o 13 6 0 17.71 87.13 39.18 o 14 6 0 120.89 111.26 43.78 o 15 6 0 19.89 86.08 45.82 o 16 6 0 4.25 -34.89 56.01 o 17 6 0 180.64 255.31 73.63 o 18 6 0 166.85 60.65 89.05 o 19 6 0 76.82 119.11 54.80 o 1 7 0 114.37 134.85 20.62 o 2 7 0 40.01 54.24 19.91 o 3 7 0 1885.12 1817.37 47.16 o 4 7 0 2096.09 2038.02 51.32 o 5 7 0 1103.68 1047.98 40.36 o 6 7 0 6718.79 6591.29 105.19 o 7 7 0 75.87 101.04 28.67 o 8 7 0 4662.71 4719.65 102.01 o 9 7 0 56.60 -27.93 33.10 o 10 7 0 2647.92 2514.61 82.38 o 11 7 0 361.26 351.29 54.01 o 12 7 0 434.52 433.48 60.92 o 13 7 0 4.72 -7.79 49.24 o 14 7 0 3737.33 3743.58 174.99 o 15 7 0 86.42 64.02 51.45 o 16 7 0 622.48 671.67 75.17 o 17 7 0 56.57 18.45 60.40 o 18 7 0 467.79 345.48 72.16 o 0 8 0 463.71 349.80 83.50 o 1 8 0 693.90 740.95 69.63 o 2 8 0 5896.02 5902.57 100.52 o 3 8 0 820.76 773.75 41.81 o 4 8 0 2493.45 2490.47 82.99 o 5 8 0 1079.63 1057.31 51.87 o 6 8 0 7010.81 7242.36 142.47 o 7 8 0 3939.58 3893.58 87.42 o 8 8 0 774.51 874.66 49.76 o 9 8 0 1890.98 1692.07 78.99 o 10 8 0 1712.65 1846.99 86.86 o 11 8 0 2530.58 2669.76 105.72 o 12 8 0 614.82 613.81 92.34 o 13 8 0 888.10 985.47 107.76 o 14 8 0 302.36 249.16 90.02 o 15 8 0 1228.71 1238.95 121.41 o 16 8 0 8.45 -22.12 57.80 o 17 8 0 304.66 262.18 72.14 o 1 9 0 3440.24 3604.11 140.64 o 2 9 0 15.15 8.33 27.01 o 3 9 0 5524.03 5603.64 104.30 o 4 9 0 241.66 212.42 36.82 o 5 9 0 1836.91 1864.76 67.02 o 6 9 0 500.99 574.42 52.65 o 7 9 0 1398.27 1439.95 59.38 o 8 9 0 89.01 80.95 39.69 o 9 9 0 223.01 212.50 68.40 o 10 9 0 3.85 60.70 65.34 o 11 9 0 134.06 20.52 73.10 o 12 9 0 38.09 45.60 72.87 o 13 9 0 1.39 -129.66 129.66 o 14 9 0 26.72 162.27 87.55 o 15 9 0 47.61 25.63 90.19 o 0 10 0 1290.15 1222.84 134.53 o 1 10 0 111.16 -29.82 166.09 o 2 10 0 175.95 92.08 66.94 o 3 10 0 126.57 138.89 31.01 o 4 10 0 43.24 23.86 30.19 o 5 10 0 669.72 753.35 49.32 o 6 10 0 321.81 234.42 85.38 o 7 10 0 300.96 238.05 61.99 o 8 10 0 165.31 117.97 58.64 o 9 10 0 1935.31 2094.01 130.00 o 10 10 0 4.26 9.81 68.79 o 11 10 0 811.84 734.24 154.16 o 12 10 0 135.21 6.27 100.76 o 13 10 0 1180.64 1447.27 188.48 o 1 11 0 917.06 1106.95 101.87 o 2 11 0 303.56 344.16 79.77 o 3 11 0 777.00 857.94 210.23 o 4 11 0 217.37 273.09 81.25 o 5 11 0 226.61 133.57 61.49 o 6 11 0 492.96 518.08 99.62 o 7 11 0 82.46 13.04 61.77 o 8 11 0 105.46 41.56 74.85 o 9 11 0 15.41 61.33 76.01 o 10 11 0 318.39 408.26 138.47 o 11 11 0 246.41 196.57 90.44 o 0 12 0 535.94 762.01 149.39 o 1 12 0 80.07 161.54 81.09 o 2 12 0 1313.88 1410.04 173.07 o 3 12 0 298.12 293.64 133.06 o 4 12 0 478.06 536.50 100.70 o 5 12 0 77.57 75.69 83.89 o 6 12 0 722.59 672.98 108.66 o 7 12 0 3.92 -0.25 69.06 o 8 12 0 449.54 430.08 100.77 o -21 0 1 2.47 -70.25 70.25 o -19 0 1 0.69 41.18 67.62 o -17 0 1 650.58 769.60 81.02 o -15 0 1 1528.93 1439.76 69.45 o -13 0 1 16257.68 15894.65 235.34 o -11 0 1 17451.86 17440.68 215.43 o -9 0 1 23659.53 22788.50 256.43 o -7 0 1 22320.51 22402.20 257.67 o -5 0 1 102111.80 103926.41 1459.09 o -3 0 1 33035.94 34829.66 499.63 o -1 0 1 96374.52 96830.65 1943.37 o 1 0 1 116031.47 115050.88 2339.06 o 3 0 1 27734.23 27605.87 473.68 o 5 0 1 5540.11 5485.01 95.50 o 7 0 1 1437.50 1497.34 50.44 o 9 0 1 1593.63 1620.87 48.94 o 11 0 1 492.82 571.37 36.59 o 13 0 1 6093.02 6043.83 459.92 o 15 0 1 43.27 47.08 55.15 o 17 0 1 2780.62 3000.90 245.01 o 19 0 1 1878.26 1927.26 156.64 o 21 0 1 1156.49 1350.84 117.40 o -21 1 1 924.88 954.44 82.14 o -20 1 1 532.71 542.50 78.85 o -19 1 1 2896.59 3185.06 104.96 o -18 1 1 93.29 57.01 39.56 o -17 1 1 3705.57 3753.40 87.72 o -16 1 1 91.55 98.44 35.34 o -15 1 1 3105.96 3069.23 86.16 o -14 1 1 274.30 215.49 34.20 o -13 1 1 6392.14 6281.55 114.82 o -12 1 1 6064.64 5998.66 89.03 o -11 1 1 17322.31 17292.54 165.78 o -10 1 1 10271.27 10400.91 135.26 o -9 1 1 5530.27 5239.83 65.43 o -8 1 1 20863.41 21269.98 169.56 o -7 1 1 18036.99 18786.20 177.82 o -6 1 1 9529.38 9511.80 114.79 o -5 1 1 726.38 779.61 26.49 o -4 1 1 36577.07 38076.85 319.34 o -3 1 1 3981.25 4145.39 50.72 o -2 1 1 9560.53 9883.13 107.43 o -1 1 1 6724.51 7679.87 82.36 o 0 1 1 40019.68 41555.39 629.79 o 1 1 1 223.90 222.19 12.96 o 2 1 1 1927.59 2165.57 30.42 o 3 1 1 21590.80 22293.75 197.53 o 4 1 1 303.11 417.01 30.78 o 5 1 1 9753.18 9986.74 119.12 o 6 1 1 5338.14 5615.78 63.17 o 7 1 1 24125.44 24452.95 204.99 o 8 1 1 7111.08 7216.37 75.54 o 9 1 1 28092.30 28016.78 235.10 o 10 1 1 726.15 717.93 28.87 o 11 1 1 15792.66 15566.91 164.03 o 12 1 1 1152.59 1072.14 41.29 o 13 1 1 9041.91 9168.50 171.84 o 14 1 1 226.17 205.14 34.18 o 15 1 1 3637.23 3669.05 83.45 o 16 1 1 754.57 780.32 49.40 o 17 1 1 1991.98 2196.83 85.76 o 18 1 1 345.63 441.41 54.80 o 19 1 1 871.63 952.75 69.89 o 20 1 1 468.97 594.78 117.61 o 21 1 1 64.44 34.70 71.02 o -21 2 1 59.66 3.30 84.35 o -20 2 1 2210.61 2445.63 89.82 o -19 2 1 1.28 -18.84 43.69 o -18 2 1 847.00 835.63 66.15 o -17 2 1 1265.01 1332.53 85.03 o -16 2 1 2751.95 2766.61 80.00 o -15 2 1 307.75 334.31 34.01 o -14 2 1 140.57 100.44 26.79 o -13 2 1 3617.30 3483.14 70.22 o -12 2 1 8615.95 8688.69 128.05 o -11 2 1 1424.47 1510.07 45.16 o -10 2 1 812.72 743.57 28.52 o -9 2 1 16889.11 16884.10 145.67 o -8 2 1 11502.27 11646.19 116.96 o -7 2 1 39916.97 40378.39 321.92 o -6 2 1 1975.23 2078.69 39.99 o -5 2 1 3441.61 3474.19 49.47 o -4 2 1 1194.03 1305.57 27.16 o -3 2 1 4785.70 4831.19 50.14 o -2 2 1 141.84 140.45 8.71 o -1 2 1 12273.85 12314.12 116.11 o 0 2 1 11892.34 12061.78 267.03 o 1 2 1 44519.94 47244.08 552.86 o 2 2 1 42111.00 44569.73 446.24 o 3 2 1 4866.93 4996.69 52.00 o 4 2 1 51546.48 52585.42 402.61 o 5 2 1 5254.47 5029.94 63.64 o 6 2 1 18486.46 18264.74 158.67 o 7 2 1 1977.38 1877.07 37.98 o 8 2 1 36859.29 36728.73 278.29 o 9 2 1 1062.25 1070.56 30.40 o 10 2 1 24396.96 24023.66 249.58 o 11 2 1 5293.39 5250.49 115.07 o 12 2 1 29917.63 29741.48 277.99 o 13 2 1 569.87 608.91 35.87 o 14 2 1 289.95 345.23 33.23 o 15 2 1 815.95 870.42 46.91 o 16 2 1 2417.74 2416.60 85.78 o 17 2 1 9.06 -30.51 30.51 o 18 2 1 401.34 445.71 56.23 o 19 2 1 227.12 299.38 71.83 o 20 2 1 719.32 1058.83 93.10 o 21 2 1 305.96 379.93 105.38 o -21 3 1 54.32 -16.34 53.92 o -20 3 1 107.79 150.96 55.02 o -19 3 1 12.43 9.87 48.36 o -18 3 1 9.82 -20.97 39.06 o -17 3 1 9.22 -28.03 37.22 o -16 3 1 30.58 6.42 35.03 o -15 3 1 141.14 82.27 35.73 o -14 3 1 714.67 743.47 47.47 o -13 3 1 407.42 400.10 39.58 o -12 3 1 3381.67 3366.36 77.61 o -11 3 1 1363.01 1336.78 50.73 o -10 3 1 16745.84 16269.38 205.94 o -9 3 1 2625.31 2654.93 59.42 o -8 3 1 51749.72 50798.63 401.78 o -7 3 1 360.32 321.25 21.67 o -6 3 1 29431.98 29828.74 265.35 o -5 3 1 34.22 48.81 17.83 o -4 3 1 53951.60 55147.29 422.25 o -3 3 1 43755.99 45287.30 374.35 o -2 3 1 7344.24 7394.65 90.94 o -1 3 1 11571.92 12121.71 138.92 o 0 3 1 90239.98 90148.59 1257.61 o 1 3 1 11983.41 12642.58 162.59 o 2 3 1 13428.70 13878.91 254.36 o 3 3 1 12432.56 12391.48 108.06 o 4 3 1 35777.39 36722.89 289.00 o 5 3 1 31.56 38.86 13.84 o 6 3 1 11127.00 11137.03 118.13 o 7 3 1 665.55 717.94 24.44 o 8 3 1 4824.14 4716.48 65.09 o 9 3 1 30.62 48.77 22.56 o 10 3 1 1080.12 992.97 42.37 o 11 3 1 42.89 26.27 27.16 o 12 3 1 6.64 20.04 28.21 o 13 3 1 693.07 687.90 57.56 o 14 3 1 211.19 169.75 33.04 o 15 3 1 957.50 831.00 49.61 o 16 3 1 422.18 435.35 46.08 o 17 3 1 240.87 202.20 48.35 o 18 3 1 501.04 530.96 68.00 o 19 3 1 0.84 -18.11 48.87 o 20 3 1 742.52 821.04 74.65 o -20 4 1 541.97 508.71 63.68 o -19 4 1 5.17 -45.55 45.55 o -18 4 1 1474.77 1637.33 92.53 o -17 4 1 245.00 307.93 46.19 o -16 4 1 3363.04 3519.54 95.58 o -15 4 1 97.15 27.84 36.48 o -14 4 1 3989.63 3939.54 91.82 o -13 4 1 454.57 520.24 42.46 o -12 4 1 1116.10 1080.93 52.30 o -11 4 1 2037.88 1803.40 104.02 o -10 4 1 1775.50 1685.20 58.24 o -9 4 1 55.53 23.00 20.13 o -8 4 1 2918.38 2966.63 58.23 o -7 4 1 2052.03 1923.19 68.67 o -6 4 1 4357.09 4360.89 61.95 o -5 4 1 9408.46 9473.71 104.09 o -4 4 1 48.45 55.35 13.14 o -3 4 1 12833.71 13273.15 139.63 o -2 4 1 30.99 56.94 13.09 o -1 4 1 17734.94 18521.28 180.65 o 1 4 1 105.48 127.08 24.85 o 2 4 1 16780.54 16837.77 185.94 o 3 4 1 41818.62 42730.79 393.46 o 4 4 1 45756.60 46845.57 396.04 o 5 4 1 2143.40 2051.93 41.66 o 6 4 1 26157.27 25999.09 220.93 o 7 4 1 788.49 719.20 28.43 o 8 4 1 23842.51 23754.26 246.35 o 9 4 1 11629.01 11281.09 141.94 o 10 4 1 10777.66 10417.56 142.23 o 11 4 1 59.82 60.74 28.29 o 12 4 1 6464.83 6335.93 140.16 o 13 4 1 247.17 198.63 36.79 o 14 4 1 8683.71 8459.53 138.89 o 15 4 1 93.80 69.16 43.29 o 16 4 1 2157.14 2295.12 84.98 o 17 4 1 339.06 351.89 73.96 o 18 4 1 1520.49 1591.83 79.49 o 19 4 1 291.35 360.54 62.01 o 20 4 1 260.94 232.63 60.44 o -20 5 1 2.15 -34.26 54.98 o -19 5 1 459.98 520.63 60.44 o -18 5 1 8.28 18.85 54.29 o -17 5 1 2434.48 2490.82 95.72 o -16 5 1 444.86 363.96 79.51 o -15 5 1 8403.63 8682.38 336.82 o -14 5 1 749.76 688.70 55.52 o -13 5 1 6336.58 6150.93 125.03 o -12 5 1 1140.12 1103.35 56.54 o -11 5 1 2547.05 2552.48 75.32 o -10 5 1 174.59 127.80 46.62 o -9 5 1 2014.21 1909.99 74.45 o -8 5 1 1551.17 1496.39 64.49 o -7 5 1 3717.36 3699.73 77.22 o -6 5 1 11565.48 11372.25 125.79 o -5 5 1 2958.24 2962.41 50.89 o -4 5 1 17638.45 17401.53 167.44 o -3 5 1 2171.68 2319.61 60.67 o -2 5 1 28706.68 28481.11 272.73 o -1 5 1 2111.30 2099.85 35.45 o 0 5 1 2408.49 2463.50 100.39 o 1 5 1 13375.34 13527.51 648.31 o 2 5 1 5940.39 5876.50 74.45 o 3 5 1 4302.61 4396.07 63.91 o 4 5 1 156.93 145.18 16.66 o 5 5 1 3481.12 3413.50 55.91 o 6 5 1 6476.10 6452.90 86.01 o 7 5 1 19543.47 19050.09 257.11 o 8 5 1 2734.76 2631.53 71.28 o 9 5 1 215.17 192.42 27.66 o 10 5 1 292.93 228.95 30.81 o 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