#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180833 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016412.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016412_Fobs loop_ _publ_author_name 'Che, Xi-Quan' _publ_section_title ; Bis[1-(2-hydroxyethyl)-4,10-diazapyrazolo[4,3-b]fluoren-5(1H)-one thiosemicarbazonato]zinc(II) dimethylformamide trisolvate monohydrate ; _journal_coeditor_code SQ3102 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m5 _journal_page_last m7 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.191 _cell_angle_gamma 90.000 _cell_length_a 16.5300 _cell_length_b 12.1040 _cell_length_c 23.6010 _exptl_crystal_F_000 2032.00 _reflns_d_resolution_high 0.7491 _cod_data_source_file sq3102Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' che08 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 369.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 136778.19 154548.44 5626.47 o 4 0 0 19357.65 16658.32 302.94 o 5 0 0 47557.67 51163.60 906.11 o 6 0 0 2076.10 1815.56 41.24 o 7 0 0 15148.94 15499.92 237.38 o 8 0 0 1317.74 1368.50 38.54 o 9 0 0 18.71 14.02 13.17 o 10 0 0 324.45 342.30 22.77 o 11 0 0 2839.64 3090.53 71.83 o 12 0 0 754.31 773.04 34.90 o 13 0 0 328.47 421.13 113.23 o 14 0 0 1685.00 1716.16 117.64 o 15 0 0 1759.23 1847.09 126.93 o 16 0 0 84.79 203.70 66.35 o 17 0 0 15.23 5.61 49.36 o 18 0 0 230.73 388.33 83.66 o 19 0 0 12.48 57.86 58.98 o 20 0 0 69.05 136.71 72.60 o 21 0 0 210.95 129.34 72.92 o 1 1 0 45637.63 43269.41 1020.59 o 2 1 0 5188.10 5975.91 334.56 o 3 1 0 719.45 685.92 20.26 o 4 1 0 71250.88 77876.19 1932.69 o 5 1 0 16778.45 18493.03 213.70 o 6 1 0 12311.22 13046.04 141.89 o 7 1 0 7453.59 7220.68 85.32 o 8 1 0 12839.38 13253.01 147.55 o 9 1 0 2865.76 2723.92 42.80 o 10 1 0 42.10 52.58 10.86 o 11 1 0 1313.81 1388.65 39.74 o 12 1 0 498.73 525.24 24.36 o 13 1 0 2071.84 2251.23 70.04 o 14 1 0 3.32 13.85 24.82 o 15 1 0 290.89 456.13 53.09 o 16 1 0 389.19 426.23 53.82 o 17 1 0 251.55 279.55 51.00 o 18 1 0 13.75 20.85 40.15 o 19 1 0 48.52 111.50 53.37 o 20 1 0 95.08 120.25 91.35 o 21 1 0 0.44 -39.75 42.26 o 0 2 0 8371.81 8324.03 213.80 o 1 2 0 3861.12 3756.92 61.44 o 2 2 0 26775.17 26316.18 1073.38 o 3 2 0 215.31 200.39 10.98 o 4 2 0 79732.77 80493.91 3577.71 o 5 2 0 30924.76 32630.87 1162.60 o 6 2 0 6755.58 6598.54 255.73 o 7 2 0 29039.81 29447.32 549.51 o 8 2 0 202.45 192.08 19.79 o 9 2 0 658.52 647.76 24.35 o 10 2 0 2419.40 2220.68 68.29 o 11 2 0 28.64 27.33 11.80 o 12 2 0 836.95 826.16 39.89 o 13 2 0 75.30 104.27 26.72 o 14 2 0 6.94 -23.03 23.03 o 15 2 0 8.96 17.53 26.25 o 16 2 0 337.36 346.12 71.08 o 17 2 0 164.24 136.88 44.67 o 18 2 0 8.60 18.62 38.11 o 19 2 0 184.67 119.71 47.32 o 20 2 0 0.65 9.77 41.64 o 21 2 0 5.17 -41.75 43.62 o 2 3 0 196.76 244.16 13.21 o 3 3 0 357.52 295.88 15.06 o 4 3 0 2735.31 2229.44 36.64 o 5 3 0 298.78 258.10 18.28 o 6 3 0 1629.21 1760.70 50.31 o 7 3 0 6.75 13.43 14.61 o 8 3 0 3001.44 2863.98 71.05 o 9 3 0 6446.80 6537.64 108.25 o 10 3 0 62.71 30.11 15.08 o 11 3 0 2320.50 2243.62 78.40 o 12 3 0 122.96 118.27 17.05 o 13 3 0 41.41 59.96 20.46 o 14 3 0 171.54 238.50 34.05 o 15 3 0 103.51 99.18 37.37 o 16 3 0 14.97 10.09 26.85 o 17 3 0 303.79 279.41 69.64 o 18 3 0 129.70 64.11 61.22 o 19 3 0 2.30 27.23 42.18 o 20 3 0 60.17 143.92 73.72 o 21 3 0 2.73 81.42 73.40 o 0 4 0 1537.39 1491.14 65.87 o 1 4 0 462.89 431.53 17.56 o 2 4 0 325.12 292.27 22.02 o 3 4 0 3.76 7.74 10.36 o 4 4 0 19.92 24.66 11.84 o 5 4 0 4653.48 4071.45 122.86 o 6 4 0 682.86 657.53 21.31 o 7 4 0 2311.19 2410.74 79.90 o 8 4 0 1435.04 1281.76 48.60 o 9 4 0 4869.24 4743.16 130.81 o 10 4 0 2369.42 2541.79 105.45 o 11 4 0 21.62 47.57 14.91 o 12 4 0 274.13 342.00 27.37 o 13 4 0 847.09 763.24 37.49 o 14 4 0 37.24 42.72 26.10 o 15 4 0 24.27 13.51 25.47 o 16 4 0 320.57 412.84 83.48 o 17 4 0 73.68 12.31 47.36 o 18 4 0 18.24 5.45 65.23 o 19 4 0 96.10 163.47 73.24 o 20 4 0 33.33 -52.41 62.67 o 21 4 0 7.93 79.81 75.01 o 1 5 0 2.85 29.71 10.54 o 2 5 0 12.26 70.20 28.37 o 3 5 0 588.58 624.02 24.30 o 4 5 0 302.07 326.82 19.19 o 5 5 0 545.44 717.85 26.78 o 6 5 0 905.50 937.77 40.95 o 7 5 0 1827.21 1869.56 54.27 o 8 5 0 349.95 414.51 37.24 o 9 5 0 1.01 47.62 13.46 o 10 5 0 32.69 52.39 14.40 o 11 5 0 82.25 54.44 20.30 o 12 5 0 1.31 -12.12 17.51 o 13 5 0 413.82 353.78 43.99 o 14 5 0 470.60 529.52 85.18 o 15 5 0 492.27 430.72 52.48 o 16 5 0 166.28 173.71 44.41 o 17 5 0 72.88 154.64 44.36 o 18 5 0 66.47 7.53 57.38 o 19 5 0 14.26 46.64 64.11 o 20 5 0 1.36 -2.72 65.39 o 0 6 0 6777.07 6244.41 132.26 o 1 6 0 1717.31 1771.89 39.68 o 2 6 0 3369.41 3649.82 64.94 o 3 6 0 10.77 17.07 13.09 o 4 6 0 255.52 245.38 21.70 o 5 6 0 1050.13 1279.87 51.70 o 6 6 0 25.67 26.38 16.41 o 7 6 0 1030.66 948.21 49.83 o 8 6 0 310.86 277.11 24.38 o 9 6 0 11.52 23.16 16.82 o 10 6 0 542.50 629.80 31.94 o 11 6 0 287.44 214.69 24.86 o 12 6 0 488.29 522.67 39.76 o 13 6 0 92.75 75.53 27.41 o 14 6 0 1111.66 1236.95 77.98 o 15 6 0 200.25 185.26 46.38 o 16 6 0 13.63 86.25 42.56 o 17 6 0 0.03 -14.01 36.65 o 18 6 0 5.22 0.74 41.65 o 19 6 0 30.12 54.33 68.76 o 20 6 0 0.02 -47.60 58.50 o 1 7 0 858.92 875.55 26.74 o 2 7 0 49.19 7.47 15.57 o 3 7 0 1351.56 1180.48 49.09 o 4 7 0 1922.93 2020.67 56.58 o 5 7 0 75.52 79.53 18.02 o 6 7 0 403.91 429.66 42.15 o 7 7 0 259.18 228.24 23.90 o 8 7 0 193.99 205.63 24.27 o 9 7 0 4.59 -25.61 25.61 o 10 7 0 156.46 123.56 22.63 o 11 7 0 121.89 136.06 23.21 o 12 7 0 0.08 34.95 25.09 o 13 7 0 1.59 3.49 42.58 o 14 7 0 15.83 8.09 38.08 o 15 7 0 26.24 66.93 40.18 o 16 7 0 18.84 56.26 60.66 o 17 7 0 17.68 72.29 44.93 o 18 7 0 55.38 150.32 51.05 o 19 7 0 22.76 -19.07 61.22 o 0 8 0 1807.61 1930.27 98.89 o 1 8 0 69.83 20.97 17.01 o 2 8 0 176.09 162.67 33.13 o 3 8 0 1572.64 1621.12 83.33 o 4 8 0 116.68 94.14 19.61 o 5 8 0 1160.10 1174.12 56.68 o 6 8 0 285.58 236.64 25.86 o 7 8 0 2.71 7.39 18.42 o 8 8 0 752.19 723.40 36.64 o 9 8 0 488.86 547.11 47.08 o 10 8 0 98.89 128.35 23.86 o 11 8 0 1.19 16.77 20.37 o 12 8 0 488.82 604.81 45.21 o 13 8 0 5.65 -24.72 24.72 o 14 8 0 112.55 65.23 41.61 o 15 8 0 65.04 191.74 50.99 o 16 8 0 233.40 315.31 57.67 o 17 8 0 79.83 101.71 46.05 o 18 8 0 9.07 1.66 42.87 o 19 8 0 18.26 14.35 46.95 o 1 9 0 2692.04 2578.93 87.40 o 2 9 0 1600.90 1592.45 68.93 o 3 9 0 70.76 67.91 28.67 o 4 9 0 741.95 678.36 43.77 o 5 9 0 48.11 48.39 20.29 o 6 9 0 229.70 357.08 41.34 o 7 9 0 97.71 88.54 24.02 o 8 9 0 1524.74 1688.23 75.04 o 9 9 0 47.58 51.55 22.85 o 10 9 0 98.93 95.99 25.00 o 11 9 0 512.64 602.72 37.67 o 12 9 0 55.18 58.04 30.10 o 13 9 0 210.68 216.30 36.69 o 14 9 0 78.30 78.38 43.91 o 15 9 0 129.96 221.12 51.89 o 16 9 0 28.38 58.18 45.32 o 17 9 0 15.01 -2.58 43.08 o 18 9 0 30.78 35.65 48.25 o 0 10 0 765.45 868.17 78.69 o 1 10 0 234.55 239.76 38.75 o 2 10 0 10.43 -19.85 47.28 o 3 10 0 98.01 94.39 33.82 o 4 10 0 67.81 176.88 35.41 o 5 10 0 372.92 416.30 44.42 o 6 10 0 114.25 112.85 34.68 o 7 10 0 1487.52 1602.54 101.00 o 8 10 0 768.93 782.75 41.40 o 9 10 0 16.96 12.06 24.90 o 10 10 0 86.64 86.43 26.79 o 11 10 0 125.30 115.92 34.90 o 12 10 0 222.36 229.56 39.04 o 13 10 0 63.88 42.99 45.13 o 14 10 0 231.39 237.49 56.44 o 15 10 0 120.09 153.96 50.63 o 16 10 0 79.23 31.61 67.63 o 17 10 0 27.86 -42.00 42.00 o 1 11 0 438.15 409.89 47.15 o 2 11 0 16.60 90.11 55.85 o 3 11 0 709.56 925.23 61.37 o 4 11 0 521.79 494.22 50.68 o 5 11 0 568.29 695.31 58.26 o 6 11 0 450.25 474.83 49.37 o 7 11 0 19.70 58.98 34.22 o 8 11 0 384.25 471.06 50.59 o 9 11 0 216.56 244.22 37.31 o 10 11 0 30.97 45.06 30.10 o 11 11 0 28.17 18.71 30.29 o 12 11 0 153.26 195.17 39.10 o 13 11 0 128.65 210.17 42.19 o 14 11 0 5.41 41.79 81.42 o 15 11 0 185.77 163.20 68.19 o 16 11 0 55.80 116.88 52.44 o 0 12 0 626.73 770.57 85.10 o 1 12 0 81.32 104.61 39.67 o 2 12 0 411.39 498.54 51.79 o 3 12 0 63.30 140.07 41.02 o 4 12 0 160.98 207.56 42.91 o 5 12 0 264.23 199.54 43.80 o 6 12 0 97.59 84.71 39.32 o 7 12 0 103.76 32.19 36.14 o 8 12 0 26.66 35.79 37.37 o 9 12 0 193.08 149.48 50.40 o 10 12 0 99.21 76.36 40.97 o 11 12 0 160.37 216.20 65.71 o 12 12 0 157.43 174.85 65.71 o 13 12 0 12.34 -14.42 51.93 o 1 13 0 485.28 447.84 54.47 o 2 13 0 118.50 39.46 53.93 o 3 13 0 246.68 303.98 102.01 o 4 13 0 202.91 146.78 42.81 o 5 13 0 41.02 7.06 37.04 o 6 13 0 124.00 76.29 39.89 o 7 13 0 30.20 35.40 55.69 o 8 13 0 114.18 33.89 42.21 o 9 13 0 0.70 52.78 42.37 o 10 13 0 139.93 162.19 64.11 o 11 13 0 126.37 121.96 61.22 o 12 13 0 1.63 26.28 54.97 o 0 14 0 204.40 89.59 62.02 o 1 14 0 15.59 -10.69 38.89 o 2 14 0 275.35 222.78 72.12 o 3 14 0 143.75 157.32 118.44 o 4 14 0 24.10 6.28 80.94 o 5 14 0 330.34 316.95 53.19 o 6 14 0 96.86 96.64 54.41 o 7 14 0 123.05 110.75 46.96 o 8 14 0 6.23 29.86 43.05 o 9 14 0 41.53 30.04 45.38 o 1 15 0 192.14 116.99 50.70 o 2 15 0 0.23 -40.91 40.91 o 3 15 0 33.66 28.11 83.82 o 4 15 0 95.09 167.00 73.88 o 5 15 0 7.92 85.58 68.59 o 6 15 0 119.02 18.11 65.07 o -21 1 1 50.92 38.82 48.20 o -20 1 1 25.41 70.06 48.27 o -19 1 1 5.54 -17.36 48.72 o -18 1 1 0.07 43.46 39.85 o -17 1 1 17.19 -32.94 32.94 o -16 1 1 4.26 51.29 36.17 o -15 1 1 328.56 325.17 50.64 o -14 1 1 595.98 585.56 41.44 o -13 1 1 109.50 130.55 17.76 o -12 1 1 22.23 37.00 12.33 o -11 1 1 30.30 19.99 11.52 o -10 1 1 724.24 755.98 27.14 o -9 1 1 2703.09 3017.80 47.30 o -8 1 1 421.08 451.62 16.35 o -7 1 1 1610.31 1530.79 27.70 o -6 1 1 2355.30 2867.83 40.05 o -5 1 1 45.74 26.81 12.99 o -4 1 1 47253.38 47700.55 531.36 o -3 1 1 31393.13 30134.42 1816.58 o -2 1 1 48.97 58.56 11.78 o -1 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11714.61 202.53 o -7 2 1 12354.43 13605.99 322.66 o -6 2 1 3563.93 3275.95 84.05 o -5 2 1 23652.35 25894.50 463.02 o -4 2 1 47780.53 49789.42 1769.87 o -3 2 1 427.40 307.49 13.81 o -2 2 1 5987.48 5692.56 338.20 o -1 2 1 46352.89 45328.18 739.78 o 0 2 1 1865.09 1988.69 44.71 o 1 2 1 4264.10 3826.13 62.51 o 2 2 1 8.78 30.62 12.01 o 3 2 1 407.86 541.30 16.92 o 4 2 1 6875.74 7425.79 234.74 o 5 2 1 20138.94 21968.43 373.81 o 6 2 1 10303.90 10430.76 202.90 o 7 2 1 774.97 731.38 24.09 o 8 2 1 525.13 614.35 28.42 o 9 2 1 721.21 715.82 23.44 o 10 2 1 23.58 13.01 9.98 o 11 2 1 522.29 608.55 21.55 o 12 2 1 811.13 782.25 42.86 o 13 2 1 1260.40 1309.64 55.75 o 14 2 1 1248.56 1328.95 58.59 o 15 2 1 734.67 776.61 49.10 o 16 2 1 232.26 148.10 43.53 o 17 2 1 22.45 32.23 57.14 o 18 2 1 16.05 1.73 38.74 o 19 2 1 7.75 19.65 41.19 o 20 2 1 164.67 223.20 56.21 o 21 2 1 39.91 31.92 71.00 o -21 3 1 29.65 40.39 68.92 o -20 3 1 0.57 -7.27 42.44 o -19 3 1 162.47 161.18 50.49 o -18 3 1 64.01 124.67 74.20 o -17 3 1 33.05 46.38 38.87 o -16 3 1 215.11 241.89 47.92 o -15 3 1 52.69 7.24 26.73 o -14 3 1 798.53 771.80 47.34 o -13 3 1 915.18 960.01 41.64 o -12 3 1 711.16 708.89 34.06 o -11 3 1 1924.32 1983.09 74.29 o -10 3 1 153.52 173.08 13.98 o -9 3 1 7676.85 7578.93 182.88 o -8 3 1 3847.79 3816.38 183.05 o -7 3 1 3621.22 3350.91 53.97 o -6 3 1 8270.89 8482.21 200.46 o -5 3 1 2336.05 2698.69 78.20 o -4 3 1 14.54 4.22 8.96 o -3 3 1 3826.53 4344.48 101.97 o -2 3 1 930.25 782.04 26.37 o -1 3 1 71.15 26.86 14.99 o 0 3 1 104.84 130.39 12.28 o 1 3 1 3653.47 3659.10 55.76 o 2 3 1 2146.42 1906.65 52.42 o 3 3 1 11632.75 11152.89 371.10 o 4 3 1 3107.93 3260.55 77.18 o 5 3 1 8931.18 8452.58 282.82 o 6 3 1 37.04 62.31 11.37 o 7 3 1 16684.28 16919.23 377.26 o 8 3 1 2919.90 3113.40 95.35 o 9 3 1 3241.61 3384.61 56.99 o 10 3 1 3453.73 3754.53 94.86 o 11 3 1 99.19 114.36 15.72 o 12 3 1 1684.93 1816.82 75.55 o 13 3 1 222.60 266.41 33.39 o 14 3 1 162.81 182.23 35.66 o 15 3 1 454.30 430.90 41.15 o 16 3 1 116.44 108.45 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