#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016444.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016444_Fobs loop_ _publ_author_name 'Hirasawa, Kai' 'Yuge, Hidetaka' 'Miyamoto, Takeshi Ken' _publ_section_title ; Enantiomorphs of a carbene--ruthenium(II)--porphyrin complex with four `chiral pillars' ; _journal_coeditor_code LN3081 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m97 _journal_page_last m100 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.7694 _cell_length_b 23.6914 _cell_length_c 26.7936 _exptl_crystal_F_000 3720.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file ln3081IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' [(EtOH)Ru(D4por(-)):C(COPh)2].2EtOH.2(CH2Cl2) in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 488.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5816.95 5558.20 143.55 o 6 0 0 158063.31 162882.17 705.18 o 8 0 0 37207.99 39088.98 759.14 o 10 0 0 1425.26 1848.60 232.29 o 12 0 0 518.32 488.38 68.38 o 14 0 0 3622.61 3533.81 344.73 o 16 0 0 4640.41 3937.58 542.51 o 2 1 0 9257.32 7274.35 73.58 o 3 1 0 3777.90 4011.61 88.20 o 4 1 0 16959.40 16970.97 188.66 o 5 1 0 14085.90 14363.08 160.55 o 6 1 0 7578.38 8449.46 319.25 o 7 1 0 3872.94 4467.11 113.83 o 8 1 0 302.82 649.74 52.20 o 9 1 0 293.07 260.53 30.06 o 10 1 0 42.73 71.71 20.20 o 11 1 0 2532.45 2540.82 202.58 o 12 1 0 141.40 156.62 40.36 o 13 1 0 7742.06 8222.53 207.80 o 14 1 0 790.29 890.31 67.46 o 15 1 0 120.66 124.29 23.54 o 16 1 0 52.67 139.73 47.54 o 17 1 0 0.07 153.16 68.29 o 2 2 0 15398.23 14074.58 154.62 o 3 2 0 5019.04 5854.38 87.86 o 4 2 0 18384.54 17175.74 162.17 o 5 2 0 2663.70 2217.68 47.64 o 6 2 0 6702.75 7497.69 139.13 o 7 2 0 2313.72 2399.82 110.07 o 8 2 0 12595.16 14292.02 259.94 o 9 2 0 6229.42 6598.37 179.74 o 10 2 0 3278.74 3582.23 205.69 o 11 2 0 578.23 794.56 87.67 o 12 2 0 1003.22 1125.39 77.57 o 13 2 0 943.22 1044.08 79.76 o 14 2 0 389.29 374.40 56.40 o 15 2 0 58.70 76.47 27.32 o 16 2 0 1059.49 1075.00 84.79 o 17 2 0 1128.28 951.79 113.91 o 2 3 0 12652.01 10586.49 117.34 o 3 3 0 325.50 754.34 45.96 o 4 3 0 7064.95 7424.65 76.84 o 5 3 0 10293.11 9541.40 111.49 o 6 3 0 9291.26 9045.20 164.69 o 7 3 0 1258.80 1527.79 139.46 o 8 3 0 166.25 92.45 19.47 o 9 3 0 2433.13 2229.93 244.22 o 10 3 0 3.43 83.53 19.01 o 11 3 0 462.50 494.37 47.44 o 12 3 0 2800.35 3216.22 241.64 o 13 3 0 1338.82 1311.64 92.49 o 14 3 0 1635.40 2004.64 150.27 o 15 3 0 90.96 99.96 42.46 o 16 3 0 45.26 35.81 28.05 o 17 3 0 55.20 51.21 32.77 o 0 4 0 25758.53 28289.54 141.11 o 1 4 0 51707.77 54175.41 435.17 o 2 4 0 25047.25 27447.07 144.58 o 3 4 0 11.33 31.67 17.00 o 4 4 0 76.88 169.69 15.28 o 5 4 0 15693.89 14570.71 209.63 o 6 4 0 116.13 101.18 13.81 o 7 4 0 13174.05 12581.91 167.01 o 8 4 0 261.13 302.15 25.17 o 9 4 0 4625.94 4502.75 138.15 o 10 4 0 3633.82 3916.54 161.80 o 11 4 0 3.48 98.20 27.34 o 12 4 0 1002.26 881.01 94.00 o 13 4 0 1254.72 1342.39 104.47 o 14 4 0 7.10 58.27 21.78 o 15 4 0 141.82 207.35 74.00 o 16 4 0 179.24 196.54 32.72 o 17 4 0 1637.05 1492.26 127.80 o 1 5 0 79988.85 76232.47 389.73 o 2 5 0 8364.73 7491.98 122.27 o 3 5 0 1485.79 813.14 40.86 o 4 5 0 8288.82 7325.20 125.87 o 5 5 0 3.95 91.17 12.42 o 6 5 0 1448.69 1261.63 85.43 o 7 5 0 2668.14 2585.19 84.44 o 8 5 0 1638.69 1363.79 111.24 o 9 5 0 25.94 -1.86 17.59 o 10 5 0 14.64 63.97 28.14 o 11 5 0 27.67 53.33 23.23 o 12 5 0 3766.04 3837.86 286.56 o 13 5 0 3522.20 3694.41 277.33 o 14 5 0 109.71 171.60 36.41 o 15 5 0 2529.81 2601.12 221.46 o 16 5 0 451.41 476.10 56.69 o 17 5 0 230.47 190.34 41.69 o 0 6 0 231410.73 237317.56 1770.02 o 1 6 0 4521.96 5565.95 102.79 o 2 6 0 1712.73 1274.12 63.26 o 3 6 0 1863.88 2086.25 41.62 o 4 6 0 3742.36 3709.55 118.51 o 5 6 0 6383.56 6254.42 141.80 o 6 6 0 4219.24 4709.14 110.21 o 7 6 0 6284.13 6947.65 137.91 o 8 6 0 2963.59 2614.81 102.23 o 9 6 0 79.69 55.16 17.92 o 10 6 0 1163.08 1262.65 136.19 o 11 6 0 2053.93 2261.99 224.59 o 12 6 0 11.17 48.59 37.88 o 13 6 0 112.28 85.28 44.91 o 14 6 0 4287.73 4650.79 363.10 o 15 6 0 54.98 -28.05 53.21 o 16 6 0 1223.78 1271.98 131.26 o 17 6 0 907.93 782.52 116.14 o 1 7 0 41.97 130.90 25.29 o 2 7 0 4173.38 4162.12 90.37 o 3 7 0 4923.16 4975.50 119.19 o 4 7 0 5344.05 4492.79 92.78 o 5 7 0 21058.63 21873.68 252.65 o 6 7 0 843.12 963.00 63.18 o 7 7 0 16461.42 19302.63 238.65 o 8 7 0 193.46 190.50 21.04 o 9 7 0 848.95 845.11 74.61 o 10 7 0 407.56 413.24 40.81 o 11 7 0 1156.10 1710.06 139.15 o 12 7 0 327.62 278.82 33.63 o 13 7 0 1937.31 2305.93 184.39 o 14 7 0 44.62 63.17 52.85 o 15 7 0 399.23 384.78 56.99 o 16 7 0 303.41 326.97 90.86 o 17 7 0 12.51 53.88 35.60 o 0 8 0 74725.21 74437.04 1083.86 o 1 8 0 53736.12 52462.62 499.67 o 2 8 0 28661.41 25221.64 410.46 o 3 8 0 1618.42 1600.01 85.53 o 4 8 0 478.90 480.73 29.78 o 5 8 0 12665.40 13461.42 458.35 o 6 8 0 22219.37 22076.36 436.40 o 7 8 0 3697.38 3013.82 113.93 o 8 8 0 9772.77 8960.39 200.23 o 9 8 0 352.39 158.96 53.75 o 10 8 0 6727.71 6846.25 220.79 o 11 8 0 2.42 82.43 22.95 o 12 8 0 5270.82 5579.61 220.30 o 13 8 0 1036.90 1054.21 99.94 o 14 8 0 4582.39 4916.95 430.90 o 15 8 0 194.86 213.65 50.78 o 16 8 0 1635.48 1852.30 171.37 o 17 8 0 1.63 150.98 36.75 o 1 9 0 1513.78 1253.04 84.37 o 2 9 0 8.27 -7.11 15.64 o 3 9 0 12.96 -19.24 19.24 o 4 9 0 24207.48 25596.86 261.73 o 5 9 0 14780.53 16154.62 372.38 o 6 9 0 5916.79 5604.88 432.98 o 7 9 0 57.27 68.44 35.68 o 8 9 0 371.21 499.30 71.56 o 9 9 0 15.38 -0.01 6.37 o 10 9 0 1341.35 1218.01 176.37 o 11 9 0 1.37 77.71 49.02 o 12 9 0 6365.20 6663.49 295.24 o 13 9 0 288.46 209.63 36.72 o 14 9 0 4938.84 5028.09 474.88 o 15 9 0 219.40 207.45 59.22 o 16 9 0 116.55 111.30 37.92 o 17 9 0 11.57 56.61 38.23 o 0 10 0 2636.69 2334.17 141.59 o 1 10 0 6621.85 6500.57 179.62 o 2 10 0 36.34 18.53 11.26 o 3 10 0 58.66 10.75 17.02 o 4 10 0 3231.62 3219.25 71.11 o 5 10 0 478.26 311.56 63.06 o 6 10 0 1179.16 1187.01 154.29 o 7 10 0 1292.73 1224.31 138.22 o 8 10 0 73.68 39.39 65.25 o 9 10 0 6945.60 7180.88 320.58 o 10 10 0 43.53 66.61 32.13 o 11 10 0 2099.04 1951.53 201.12 o 12 10 0 350.60 242.87 61.80 o 13 10 0 52.50 104.74 40.50 o 14 10 0 881.48 1155.76 122.22 o 15 10 0 483.80 378.31 106.41 o 16 10 0 26.82 145.61 83.99 o 1 11 0 1897.56 1397.39 163.44 o 2 11 0 1892.48 1637.26 83.18 o 3 11 0 8746.92 9002.68 151.75 o 4 11 0 19109.85 21104.99 244.30 o 5 11 0 116.32 32.46 18.38 o 6 11 0 7355.94 7629.43 196.10 o 7 11 0 377.85 380.30 69.93 o 8 11 0 14.38 30.43 60.62 o 9 11 0 2948.67 2807.70 391.49 o 10 11 0 2034.58 2252.52 230.21 o 11 11 0 10.62 -55.84 55.84 o 12 11 0 3664.79 3694.87 375.95 o 13 11 0 2882.28 3126.47 263.69 o 14 11 0 1716.40 1541.58 136.52 o 15 11 0 719.26 750.10 123.81 o 16 11 0 403.87 292.89 77.52 o 0 12 0 20391.70 20314.82 419.37 o 1 12 0 13022.88 13020.11 176.01 o 2 12 0 6816.24 6411.62 116.11 o 3 12 0 735.83 749.82 62.58 o 4 12 0 0.83 -20.27 24.26 o 5 12 0 2937.85 3138.26 86.17 o 6 12 0 7901.70 7954.47 266.80 o 7 12 0 2208.57 2114.57 233.99 o 8 12 0 14648.54 15321.37 253.98 o 9 12 0 2556.48 2977.22 412.78 o 10 12 0 7887.30 8514.57 337.09 o 11 12 0 380.00 292.13 54.96 o 12 12 0 0.13 106.16 61.60 o 13 12 0 968.08 1056.86 96.87 o 14 12 0 1128.28 1227.47 104.53 o 15 12 0 605.67 684.67 94.43 o 16 12 0 1902.28 1934.67 180.48 o 1 13 0 581.13 514.66 57.95 o 2 13 0 337.48 298.97 31.43 o 3 13 0 652.19 519.33 48.76 o 4 13 0 504.82 572.81 53.08 o 5 13 0 5996.96 5594.67 141.36 o 6 13 0 1350.17 1559.34 205.80 o 7 13 0 408.10 226.61 70.30 o 8 13 0 158.02 110.72 42.12 o 9 13 0 1165.03 1157.14 160.01 o 10 13 0 652.41 733.60 122.58 o 11 13 0 4622.68 4801.90 412.74 o 12 13 0 1012.24 1040.32 116.79 o 13 13 0 6398.66 6657.92 609.46 o 14 13 0 152.68 111.05 64.10 o 15 13 0 975.38 1102.42 113.06 o 16 13 0 97.51 164.92 52.14 o 0 14 0 214.43 302.33 72.49 o 1 14 0 2434.15 2535.33 152.78 o 2 14 0 110.01 77.06 22.79 o 3 14 0 182.85 137.99 23.24 o 4 14 0 139.41 85.44 33.94 o 5 14 0 600.74 633.18 74.56 o 6 14 0 4374.98 4554.88 225.64 o 7 14 0 299.64 33.65 80.54 o 8 14 0 1476.97 1523.98 196.01 o 9 14 0 778.03 566.73 138.34 o 10 14 0 4298.71 5062.25 224.31 o 11 14 0 59.84 137.05 44.61 o 12 14 0 67.30 118.24 62.54 o 13 14 0 72.79 84.80 66.22 o 14 14 0 894.96 645.87 100.01 o 15 14 0 107.83 247.04 56.62 o 1 15 0 3676.42 3775.43 124.58 o 2 15 0 118.92 105.24 32.02 o 3 15 0 1044.60 952.70 78.84 o 4 15 0 8374.60 8904.96 161.86 o 5 15 0 4085.09 4330.17 118.80 o 6 15 0 8797.82 10967.26 330.95 o 7 15 0 995.40 1028.72 116.35 o 8 15 0 1400.17 1564.47 164.93 o 9 15 0 373.93 281.91 76.51 o 10 15 0 2682.19 2702.40 256.01 o 11 15 0 508.94 649.87 97.35 o 12 15 0 1326.72 1468.52 173.19 o 13 15 0 1383.65 1501.93 118.26 o 14 15 0 1252.82 1088.92 107.15 o 15 15 0 978.46 848.01 103.04 o 0 16 0 3098.38 3393.76 230.61 o 1 16 0 3526.63 3485.72 209.57 o 2 16 0 2859.64 3303.53 157.93 o 3 16 0 496.55 432.76 39.78 o 4 16 0 14.76 27.50 18.27 o 5 16 0 6277.02 5919.60 176.62 o 6 16 0 1194.25 1167.51 127.79 o 7 16 0 1934.95 2037.68 205.27 o 8 16 0 2344.37 2518.94 276.12 o 9 16 0 7527.91 8043.79 349.81 o 10 16 0 16.30 90.81 100.60 o 11 16 0 440.43 374.47 66.53 o 12 16 0 160.39 254.36 54.37 o 13 16 0 2.27 82.64 81.42 o 14 16 0 137.90 109.25 40.90 o 15 16 0 946.34 957.20 111.24 o 1 17 0 626.86 762.71 85.83 o 2 17 0 3568.37 3637.10 140.24 o 3 17 0 71.89 208.67 42.74 o 4 17 0 8296.04 7904.16 236.16 o 5 17 0 75.99 77.56 57.23 o 6 17 0 3623.09 3225.67 275.76 o 7 17 0 2240.99 2270.78 278.13 o 8 17 0 29.13 94.99 45.59 o 9 17 0 518.67 396.11 77.30 o 10 17 0 94.89 106.33 79.11 o 11 17 0 182.12 129.13 41.53 o 12 17 0 3767.66 4181.51 364.01 o 13 17 0 653.50 534.83 126.51 o 14 17 0 2517.91 2815.06 230.94 o 0 18 0 1042.11 1021.99 121.86 o 1 18 0 1268.01 1196.78 115.37 o 2 18 0 1939.58 1882.09 156.89 o 3 18 0 4791.57 5073.36 169.12 o 4 18 0 2043.80 1738.70 182.11 o 5 18 0 5539.50 5714.20 143.45 o 6 18 0 9369.02 10352.01 250.85 o 7 18 0 32.13 54.77 49.51 o 8 18 0 764.32 760.97 258.03 o 9 18 0 6495.41 7855.39 446.52 o 10 18 0 4927.82 5099.12 462.03 o 11 18 0 67.61 130.95 98.90 o 12 18 0 217.22 182.45 57.29 o 13 18 0 87.03 130.21 57.59 o 14 18 0 728.42 839.92 104.96 o 1 19 0 136.86 206.39 38.72 o 2 19 0 733.26 551.73 108.57 o 3 19 0 4363.27 4929.17 253.58 o 4 19 0 4342.40 4196.42 293.74 o 5 19 0 26.28 -15.56 31.96 o 6 19 0 166.22 127.38 107.88 o 7 19 0 117.37 132.89 93.78 o 8 19 0 15.79 60.66 44.69 o 9 19 0 3.71 -9.08 86.60 o 10 19 0 96.47 19.88 45.04 o 11 19 0 338.12 377.24 142.84 o 12 19 0 1109.62 1222.15 137.67 o 13 19 0 2781.74 2953.49 264.33 o 14 19 0 250.99 256.30 65.34 o 0 20 0 13053.44 14406.41 654.91 o 1 20 0 6318.96 6409.82 209.95 o 2 20 0 1638.19 1618.69 146.75 o 3 20 0 1362.43 1688.02 188.47 o 4 20 0 19.52 61.89 71.48 o 5 20 0 4656.68 5029.12 349.32 o 6 20 0 5695.04 5934.77 480.98 o 7 20 0 421.20 270.56 54.99 o 8 20 0 1773.79 2156.94 225.92 o 9 20 0 42.89 80.03 50.08 o 10 20 0 3404.32 4101.39 381.44 o 11 20 0 85.44 42.55 61.11 o 12 20 0 24.64 201.90 104.65 o 13 20 0 173.11 119.11 46.72 o 1 21 0 503.51 336.73 58.35 o 2 21 0 7210.13 6670.92 197.52 o 3 21 0 1432.30 1538.39 157.31 o 4 21 0 267.05 276.44 38.85 o 5 21 0 886.97 992.39 170.63 o 6 21 0 4228.38 4056.01 465.29 o 7 21 0 1030.31 1164.24 154.15 o 8 21 0 758.00 947.87 107.67 o 9 21 0 93.25 219.38 88.88 o 10 21 0 219.01 152.92 47.88 o 11 21 0 1910.04 2088.29 324.90 o 12 21 0 971.66 1262.56 141.58 o 13 21 0 1725.33 1891.31 198.01 o 0 22 0 199.62 224.89 35.34 o 1 22 0 59.43 85.97 46.37 o 2 22 0 171.41 173.82 60.51 o 3 22 0 176.73 53.28 25.40 o 4 22 0 581.11 683.65 71.68 o 5 22 0 265.94 376.26 133.92 o 6 22 0 1156.90 1047.74 94.55 o 7 22 0 1658.05 1828.06 137.71 o 8 22 0 2887.47 3083.23 285.80 o 9 22 0 3482.71 3411.64 372.75 o 10 22 0 595.96 720.75 172.98 o 11 22 0 982.27 1320.74 111.91 o 12 22 0 61.33 89.13 64.54 o 1 23 0 236.24 307.73 71.16 o 2 23 0 5058.52 4969.03 243.13 o 3 23 0 7.31 54.57 57.43 o 4 23 0 5915.55 6094.21 359.76 o 5 23 0 536.49 433.82 116.94 o 6 23 0 5249.42 5779.10 560.83 o 7 23 0 207.51 173.57 57.08 o 8 23 0 151.81 -4.16 61.61 o 9 23 0 312.86 226.11 59.61 o 10 23 0 268.04 113.82 80.16 o 11 23 0 203.12 178.19 139.95 o 0 24 0 24.21 111.90 66.17 o 1 24 0 1662.25 1792.08 185.89 o 2 24 0 211.50 355.43 45.36 o 3 24 0 755.73 866.26 147.69 o 4 24 0 21.33 153.49 103.16 o 5 24 0 10.84 61.69 116.37 o 6 24 0 148.58 160.05 77.06 o 7 24 0 710.22 1127.50 121.82 o 8 24 0 189.85 318.77 73.07 o 9 24 0 618.62 817.01 125.62 o 10 24 0 852.85 901.74 142.87 o 11 24 0 1353.58 1422.69 138.06 o 1 25 0 791.37 1009.32 115.54 o 2 25 0 294.41 347.48 43.78 o 3 25 0 1467.25 1680.31 157.98 o 4 25 0 858.84 1144.82 126.21 o 5 25 0 1625.40 1463.38 119.58 o 6 25 0 1568.04 1532.07 154.02 o 7 25 0 1129.08 1135.48 93.44 o 8 25 0 3.21 14.41 135.23 o 9 25 0 98.43 134.89 47.57 o 10 25 0 160.98 133.41 40.98 o 0 26 0 5009.62 5406.83 317.68 o 1 26 0 140.26 95.00 48.48 o 2 26 0 276.58 107.00 102.70 o 3 26 0 2.04 125.15 77.12 o 4 26 0 155.55 138.89 56.78 o 5 26 0 48.96 162.31 63.08 o 6 26 0 140.68 129.32 89.48 o 7 26 0 197.84 216.20 69.41 o 8 26 0 3977.25 4126.18 447.24 o 9 26 0 400.28 268.74 57.33 o 1 27 0 881.59 844.86 89.54 o 2 27 0 1690.81 2085.84 219.26 o 3 27 0 1630.11 1935.02 194.54 o 4 27 0 466.09 494.87 81.49 o 5 27 0 2992.93 3707.28 414.69 o 6 27 0 253.48 329.30 92.64 o 7 27 0 579.14 443.52 85.33 o 8 27 0 615.23 291.81 85.32 o 0 28 0 4781.37 4475.31 693.88 o 1 28 0 154.69 128.00 48.94 o 2 28 0 231.17 350.20 78.46 o 3 28 0 195.62 150.01 57.38 o 4 28 0 272.60 165.23 52.03 o 5 28 0 11.91 37.71 39.30 o 6 28 0 2643.72 3032.59 247.86 o 7 28 0 1.38 121.71 49.04 o 1 29 0 491.69 471.01 86.36 o 2 29 0 1973.55 1968.05 191.91 o 3 29 0 202.00 185.19 68.41 o 4 29 0 2439.76 2780.48 283.95 o 5 29 0 656.32 650.59 154.49 o 0 30 0 92.01 -109.85 153.67 o 1 30 0 1026.12 678.38 157.08 o 2 30 0 1.44 92.88 57.89 o 3 30 0 935.75 917.01 100.48 o 2 0 1 58070.29 63404.09 389.39 o 3 0 1 9181.21 8569.33 134.86 o 4 0 1 8705.06 8038.34 118.28 o 5 0 1 8506.32 7923.14 103.84 o 6 0 1 2434.91 2010.55 227.90 o 7 0 1 53448.42 55734.75 625.85 o 8 0 1 5282.84 5164.67 137.28 o 9 0 1 12036.05 12632.49 314.22 o 10 0 1 535.06 656.08 67.18 o 11 0 1 33.63 53.99 34.10 o 12 0 1 844.79 1059.88 78.77 o 13 0 1 75.91 66.64 27.99 o 14 0 1 81.46 62.58 23.02 o 15 0 1 2951.61 2620.75 173.82 o 16 0 1 3.34 56.38 54.11 o 17 0 1 2572.58 2106.44 270.63 o -17 1 1 38.00 183.48 46.52 o -16 1 1 73.41 65.34 29.65 o -15 1 1 549.82 485.94 66.76 o 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108.64 o -3 12 4 9962.25 10174.81 240.08 o -2 12 4 7718.65 7405.97 187.36 o -1 12 4 753.36 511.89 53.45 o 0 12 4 47074.62 51733.95 581.52 o 1 12 4 766.46 483.70 59.59 o 2 12 4 7664.61 7625.93 128.27 o 3 12 4 9514.26 9816.00 159.23 o 4 12 4 3650.25 3798.47 117.49 o 5 12 4 5789.30 6133.54 167.38 o 6 12 4 177.14 223.10 99.99 o 7 12 4 789.12 905.28 94.84 o 8 12 4 7322.22 7816.74 404.03 o 9 12 4 202.42 162.29 50.09 o 10 12 4 2512.01 2638.99 364.78 o 11 12 4 5076.03 5319.23 333.25 o 12 12 4 762.11 810.81 140.17 o 13 12 4 2246.29 2493.68 281.22 o 14 12 4 2440.06 2659.53 231.69 o 15 12 4 649.20 419.65 71.85 o 16 12 4 951.94 938.72 111.01 o -16 13 4 451.56 351.22 86.74 o -15 13 4 409.94 291.04 71.03 o -14 13 4 139.46 179.70 42.11 o -13 13 4 5290.07 5644.70 490.57 o -12 13 4 27.74 29.69 59.04 o -11 13 4 2869.73 3028.09 251.19 o -10 13 4 466.67 352.99 58.38 o -9 13 4 5771.52 5724.75 254.07 o -8 13 4 11208.24 11022.08 261.66 o -7 13 4 1720.40 1761.38 116.64 o -6 13 4 2761.25 3041.72 123.66 o -5 13 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124.14 o -6 14 4 2444.04 2350.62 118.00 o -5 14 4 176.87 223.55 37.94 o -4 14 4 730.04 580.60 63.15 o -3 14 4 2742.74 2737.94 150.46 o -2 14 4 4705.08 4446.00 124.84 o -1 14 4 7847.72 7719.99 158.90 o 0 14 4 41395.77 44441.89 525.23 o 1 14 4 7680.95 7589.51 192.33 o 2 14 4 4816.23 4413.67 134.74 o 3 14 4 2840.76 2785.81 105.25 o 4 14 4 654.43 609.70 50.91 o 5 14 4 164.73 179.26 33.29 o 6 14 4 2613.83 2427.59 225.52 o 7 14 4 3786.67 3537.26 192.40 o 8 14 4 14622.75 16104.92 516.63 o 9 14 4 2787.58 2762.07 397.71 o 10 14 4 2488.45 2434.10 271.38 o 11 14 4 908.08 1111.53 157.26 o 12 14 4 384.67 296.09 109.35 o 13 14 4 1160.29 1138.56 145.37 o 14 14 4 1564.74 1640.07 140.54 o 15 14 4 825.79 1058.31 129.96 o -15 15 4 476.92 531.75 108.50 o -14 15 4 1479.26 1468.88 120.27 o -13 15 4 750.53 675.60 93.38 o -12 15 4 64.22 92.02 101.00 o -11 15 4 1645.82 1885.49 140.28 o -10 15 4 553.44 557.30 83.57 o -9 15 4 1786.22 1822.93 146.26 o -8 15 4 1897.29 1786.71 178.57 o -7 15 4 2517.83 2623.05 245.95 o -6 15 4 2467.82 2288.50 161.26 o -5 15 4 3635.45 3340.57 203.36 o -4 15 4 374.88 235.15 54.43 o -3 15 4 1941.83 1988.40 211.59 o -2 15 4 4644.73 5089.13 136.73 o -1 15 4 2872.92 3315.41 160.99 o 0 15 4 1615.95 1948.82 188.67 o 1 15 4 2772.58 3025.86 177.67 o 2 15 4 4584.03 4665.56 192.64 o 3 15 4 1941.89 1859.49 140.92 o 4 15 4 308.48 291.80 39.61 o 5 15 4 3724.40 3369.12 99.75 o 6 15 4 2371.37 2463.66 255.89 o 7 15 4 2582.52 2320.63 176.78 o 8 15 4 1934.91 1423.27 377.10 o 9 15 4 1716.99 1777.48 279.11 o 10 15 4 482.94 487.40 221.00 o 11 15 4 1576.81 1685.59 217.98 o 12 15 4 43.39 116.17 54.94 o 13 15 4 775.28 454.22 145.21 o 14 15 4 1508.96 1813.06 144.74 o 15 15 4 443.16 447.44 143.67 o -15 16 4 675.15 665.86 123.99 o -14 16 4 438.65 369.60 105.79 o -13 16 4 910.01 1019.91 108.20 o -12 16 4 438.35 578.30 82.64 o -11 16 4 1229.38 1411.82 102.88 o -10 16 4 3711.98 3758.08 323.43 o -9 16 4 2949.72 3381.80 291.54 o -8 16 4 786.66 491.97 153.91 o -7 16 4 3098.07 3198.69 300.26 o 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3157.95 285.11 o -4 17 4 2593.44 2351.27 256.51 o -3 17 4 995.74 1027.73 105.63 o -2 17 4 9287.74 9483.83 281.39 o -1 17 4 3107.74 2712.56 273.32 o 0 17 4 3045.41 3442.13 244.06 o 1 17 4 2887.34 2456.37 264.42 o 2 17 4 9467.75 10003.29 305.20 o 3 17 4 916.95 800.94 87.48 o 4 17 4 2674.61 2586.29 135.84 o 5 17 4 3245.68 2990.24 136.17 o 6 17 4 5182.51 5504.02 278.30 o 7 17 4 870.23 828.70 187.53 o 8 17 4 367.09 505.24 99.58 o 9 17 4 3656.61 3969.42 510.59 o 10 17 4 771.29 1089.67 148.00 o 11 17 4 255.57 399.04 86.45 o 12 17 4 288.79 162.57 98.25 o 13 17 4 603.66 478.78 84.99 o 14 17 4 482.90 297.22 101.36 o -14 18 4 688.10 793.49 134.75 o -13 18 4 95.19 13.06 39.13 o -12 18 4 930.14 1087.73 80.87 o -11 18 4 3926.30 3942.54 298.59 o -10 18 4 1496.57 1662.68 141.96 o -9 18 4 228.18 200.50 41.06 o -8 18 4 2898.27 2992.58 245.89 o -7 18 4 1271.59 1172.18 115.15 o -6 18 4 1935.72 2094.35 206.24 o -5 18 4 2219.02 2389.16 229.89 o -4 18 4 108.98 94.95 73.95 o -3 18 4 412.00 332.57 60.74 o -2 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292.36 53.65 o 2 2 28 2827.00 2782.37 221.10 o 3 2 28 1890.92 2034.28 160.71 o 4 2 28 3325.19 3257.01 279.01 o 5 2 28 292.47 297.93 54.34 o 6 2 28 909.26 947.25 92.12 o 7 2 28 208.99 175.63 62.34 o 8 2 28 326.13 184.20 35.82 o 9 2 28 238.00 229.98 45.91 o 10 2 28 1174.39 1373.25 146.15 o -10 3 28 432.07 476.47 211.58 o -9 3 28 655.67 696.11 206.54 o -8 3 28 348.66 221.45 91.35 o -7 3 28 1863.37 1789.90 277.44 o -6 3 28 308.07 241.99 67.27 o -5 3 28 565.46 256.61 122.18 o -4 3 28 1053.38 1078.26 159.61 o -3 3 28 553.64 764.41 121.93 o -2 3 28 1617.80 1441.98 154.03 o -1 3 28 3922.45 3571.54 395.01 o 0 3 28 220.25 210.77 35.14 o 1 3 28 3825.33 3088.63 284.49 o 2 3 28 1731.81 1419.28 126.07 o 3 3 28 571.08 686.71 90.09 o 4 3 28 1061.54 1296.40 99.85 o 5 3 28 606.94 476.26 76.32 o 6 3 28 301.75 221.84 46.84 o 7 3 28 1895.35 2097.32 177.29 o 8 3 28 342.25 265.96 53.53 o 9 3 28 659.55 632.82 93.39 o 10 3 28 425.71 447.31 95.00 o -10 4 28 1593.98 1745.31 193.39 o -9 4 28 423.45 529.27 186.39 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2722.12 231.55 o 3 5 28 1808.20 1753.34 145.84 o 4 5 28 2062.26 1928.59 158.20 o 5 5 28 2286.85 2588.86 162.41 o 6 5 28 629.63 509.57 93.87 o 7 5 28 587.88 846.21 178.66 o 8 5 28 2319.78 2425.46 204.80 o 9 5 28 1319.98 1595.62 140.63 o 10 5 28 236.84 251.94 84.63 o -10 6 28 1634.49 1545.47 252.93 o -9 6 28 278.38 187.88 41.38 o -8 6 28 673.25 597.22 141.38 o -7 6 28 544.83 491.66 192.12 o -6 6 28 15.12 87.42 110.10 o -5 6 28 1396.84 1493.93 185.65 o -4 6 28 888.43 677.74 185.25 o -3 6 28 3014.36 3077.04 376.32 o -2 6 28 1649.30 1577.90 175.55 o -1 6 28 1177.03 1083.08 161.82 o 0 6 28 501.44 401.61 71.79 o 1 6 28 1145.42 921.90 88.93 o 2 6 28 1695.40 1636.13 135.44 o 3 6 28 3042.66 3326.94 250.77 o 4 6 28 863.48 843.79 120.05 o 5 6 28 1457.29 1642.71 167.93 o 6 6 28 29.82 113.73 53.78 o 7 6 28 548.56 613.57 71.00 o 8 6 28 655.77 626.60 85.83 o 9 6 28 307.53 514.41 100.45 o 10 6 28 1599.79 1396.00 189.09 o -9 7 28 129.43 188.22 92.33 o -8 7 28 2616.14 2503.96 285.10 o -7 7 28 266.24 211.25 76.73 o -6 7 28 466.75 404.53 297.19 o -5 7 28 1535.49 1610.60 142.20 o -4 7 28 134.52 169.99 82.59 o -3 7 28 1294.07 1447.04 183.77 o -2 7 28 1819.41 2106.95 286.67 o -1 7 28 187.42 160.29 83.76 o 0 7 28 2751.96 3024.30 246.69 o 1 7 28 197.12 263.75 41.23 o 2 7 28 1729.91 1842.32 160.55 o 3 7 28 1309.63 1365.80 143.84 o 4 7 28 143.64 208.04 56.43 o 5 7 28 1598.37 1394.99 132.79 o 6 7 28 513.52 476.32 76.22 o 7 7 28 221.53 216.92 61.22 o 8 7 28 2621.58 2328.57 194.36 o 9 7 28 138.35 97.32 64.19 o -9 8 28 61.91 245.90 90.89 o -8 8 28 1697.43 2131.36 253.58 o -7 8 28 635.12 686.72 110.80 o -6 8 28 1132.19 1146.30 148.42 o -5 8 28 86.45 86.43 48.20 o -4 8 28 815.30 774.22 187.44 o -3 8 28 313.50 540.50 117.95 o -2 8 28 3521.52 3732.01 536.46 o -1 8 28 825.24 690.02 161.02 o 0 8 28 2138.01 2458.81 216.66 o 1 8 28 817.87 751.41 80.75 o 2 8 28 3489.12 3444.84 261.54 o 3 8 28 377.20 314.89 50.35 o 4 8 28 801.91 897.63 85.17 o 5 8 28 119.60 170.74 65.39 o 6 8 28 1141.12 1281.15 120.49 o 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