#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180833 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016450.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016450_Fobs loop_ _publ_author_name 'Rubin-Preminger, Janice M.' 'Kozlov, Leonid' 'Goldberg, Israel' _publ_section_title ; Hydrogen-bonding and \p--\p stacking interactions in aquachloridobis(1,10-phenanthroline)cobalt(II) chloride dichloridobis(1,10-phenanthroline)cobalt(II) hexahydrate ; _journal_coeditor_code SK3176 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m83 _journal_page_last m86 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.792 _cell_angle_gamma 90.000 _cell_length_a 14.0905 _cell_length_b 23.9088 _cell_length_c 14.2504 _exptl_crystal_F_000 2272.00 _reflns_d_resolution_high 0.7604 _cod_data_source_file sk3176Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound KL8 P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 534.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20034.71 24593.80 711.12 o 3 0 0 76581.70 77133.60 2086.88 o 4 0 0 285893.44 303517.78 7422.93 o 5 0 0 60371.30 48705.70 1386.67 o 6 0 0 26640.68 29122.76 862.28 o 7 0 0 43588.01 43912.08 1221.67 o 8 0 0 10326.07 12689.23 452.43 o 9 0 0 49266.69 52108.34 1552.62 o 10 0 0 2286.13 2118.14 175.92 o 11 0 0 9027.22 8913.56 422.01 o 12 0 0 45562.05 50174.82 1842.78 o 13 0 0 1303.88 1059.49 185.57 o 14 0 0 1874.96 1937.40 196.69 o 15 0 0 719.86 921.02 237.91 o 16 0 0 2814.85 3644.75 461.46 o 17 0 0 2952.17 3927.67 369.46 o 18 0 0 1625.36 1112.88 276.62 o 2 1 0 57564.79 57024.79 1082.78 o 3 1 0 1052.99 557.44 32.10 o 4 1 0 92990.42 82699.59 1583.36 o 5 1 0 98949.11 99577.38 1880.54 o 6 1 0 5757.25 5091.01 157.14 o 7 1 0 38723.62 42819.45 857.87 o 8 1 0 1988.95 2053.10 105.63 o 9 1 0 590.53 883.99 69.34 o 10 1 0 3086.43 3146.79 138.05 o 11 1 0 8874.11 9561.01 310.40 o 12 1 0 23.10 138.26 67.03 o 13 1 0 498.45 519.88 110.77 o 14 1 0 5249.42 5239.96 267.29 o 15 1 0 97.45 161.23 129.13 o 16 1 0 2983.91 3875.11 310.50 o 17 1 0 747.79 889.76 177.81 o 18 1 0 581.41 576.01 175.71 o 2 2 0 2118.62 2266.78 70.91 o 3 2 0 28965.03 29100.62 607.79 o 4 2 0 53868.05 53762.61 1066.41 o 5 2 0 1738.56 1488.01 69.97 o 6 2 0 3189.01 3992.91 126.93 o 7 2 0 19389.33 18734.20 407.85 o 8 2 0 10988.04 10694.77 261.31 o 9 2 0 8012.03 8288.88 241.79 o 10 2 0 1465.94 1540.88 91.58 o 11 2 0 0.68 70.39 69.02 o 12 2 0 7619.53 8389.48 290.68 o 13 2 0 377.59 373.86 95.14 o 14 2 0 419.52 414.98 81.82 o 15 2 0 85.96 358.97 170.57 o 16 2 0 656.22 838.36 187.56 o 17 2 0 113.53 194.90 149.17 o 18 2 0 987.87 1053.20 180.74 o 1 3 0 8961.76 9598.98 215.78 o 2 3 0 8217.59 7709.63 193.33 o 3 3 0 2102.13 2481.30 80.67 o 4 3 0 3237.61 3421.42 113.71 o 5 3 0 1425.79 1460.63 69.34 o 6 3 0 1547.98 1894.81 78.99 o 7 3 0 3437.16 3695.73 125.98 o 8 3 0 731.18 684.89 76.26 o 9 3 0 4434.51 4962.40 173.40 o 10 3 0 206.21 247.77 66.30 o 11 3 0 0.88 14.58 62.84 o 12 3 0 113.27 30.32 74.16 o 13 3 0 4759.46 4741.38 227.53 o 14 3 0 236.55 226.79 88.75 o 15 3 0 358.83 110.15 119.59 o 16 3 0 13.73 -27.17 156.09 o 17 3 0 22.66 41.96 146.86 o 18 3 0 52.88 -47.10 144.55 o 0 4 0 1874.58 2372.84 91.47 o 1 4 0 6328.25 5997.03 150.53 o 2 4 0 2842.69 2385.53 75.95 o 3 4 0 9109.70 8514.52 215.15 o 4 4 0 8256.46 8962.55 239.17 o 5 4 0 198.90 185.04 40.49 o 6 4 0 1310.29 1448.25 81.40 o 7 4 0 8274.74 7915.75 213.26 o 8 4 0 1098.80 1108.58 75.53 o 9 4 0 406.68 522.82 78.47 o 10 4 0 0.00 -8.29 56.44 o 11 4 0 1023.78 1076.48 93.47 o 12 4 0 329.27 288.06 63.78 o 13 4 0 85.33 134.48 66.09 o 14 4 0 0.47 -85.81 82.77 o 15 4 0 874.90 878.22 176.65 o 16 4 0 40.19 185.04 176.23 o 17 4 0 82.91 68.18 159.45 o 18 4 0 8.07 -27.17 179.06 o 1 5 0 10518.74 10701.48 247.98 o 2 5 0 8086.70 7921.52 196.06 o 3 5 0 7593.70 8658.55 217.04 o 4 5 0 2144.11 2178.25 78.57 o 5 5 0 9026.08 9459.88 245.68 o 6 5 0 3610.04 3566.91 119.90 o 7 5 0 9968.77 9485.06 271.27 o 8 5 0 9081.54 10388.88 270.75 o 9 5 0 1350.23 1294.78 86.23 o 10 5 0 366.24 433.66 72.80 o 11 5 0 937.76 926.90 96.61 o 12 5 0 3444.21 3459.50 167.63 o 13 5 0 40.94 -22.03 84.86 o 14 5 0 1413.63 1428.63 129.76 o 15 5 0 29.41 -36.72 118.43 o 16 5 0 730.71 922.91 196.79 o 17 5 0 101.95 280.40 220.19 o 18 5 0 464.26 684.89 235.61 o 1 6 0 111.76 98.82 24.44 o 2 6 0 22.08 37.87 23.08 o 3 6 0 6237.71 5966.92 160.08 o 4 6 0 12750.73 15052.00 357.60 o 5 6 0 4023.13 2722.47 94.62 o 6 6 0 413.91 440.48 54.34 o 7 6 0 156.14 94.41 42.17 o 8 6 0 3527.86 3774.93 135.32 o 9 6 0 9223.71 9681.64 280.40 o 10 6 0 211.23 261.20 73.33 o 11 6 0 7351.14 8014.05 284.17 o 12 6 0 12759.38 13853.09 457.47 o 13 6 0 1.72 81.61 81.93 o 14 6 0 212.79 204.97 84.34 o 15 6 0 482.92 560.59 161.02 o 16 6 0 1278.50 1358.46 241.17 o 17 6 0 30.04 15.63 212.21 o 1 7 0 4993.17 5008.14 137.52 o 2 7 0 205.23 506.67 35.04 o 3 7 0 450.15 318.48 38.18 o 4 7 0 10706.85 9554.61 240.64 o 5 7 0 18747.61 17814.75 397.68 o 6 7 0 3745.38 4046.31 140.15 o 7 7 0 12882.29 13587.49 354.88 o 8 7 0 3726.43 3984.73 143.08 o 9 7 0 801.05 897.52 81.51 o 10 7 0 275.37 226.79 65.35 o 11 7 0 3358.30 3448.06 197.84 o 12 7 0 253.70 317.32 90.00 o 13 7 0 358.86 202.14 77.42 o 14 7 0 4422.45 4750.29 249.98 o 15 7 0 2.87 -41.96 90.21 o 16 7 0 2623.69 3096.12 277.57 o 17 7 0 229.78 -3.15 134.80 o 0 8 0 16485.58 14391.86 466.28 o 1 8 0 329.55 279.35 28.11 o 2 8 0 7674.41 6503.91 177.60 o 3 8 0 16402.51 16218.17 371.24 o 4 8 0 160.48 54.55 37.76 o 5 8 0 45.49 195.74 46.26 o 6 8 0 3221.33 3017.34 106.79 o 7 8 0 16775.06 16859.63 403.76 o 8 8 0 341.81 317.32 54.23 o 9 8 0 12860.64 13272.16 388.03 o 10 8 0 152.93 125.57 55.18 o 11 8 0 436.74 398.10 85.28 o 12 8 0 2673.90 2692.15 171.41 o 13 8 0 1172.29 1110.68 131.65 o 14 8 0 870.65 1046.90 129.97 o 15 8 0 0.22 -76.47 165.43 o 16 8 0 803.62 604.33 179.90 o 17 8 0 218.60 361.49 190.92 o 1 9 0 24.81 19.93 21.08 o 2 9 0 103154.63 105867.28 1917.99 o 3 9 0 433.32 328.97 38.81 o 4 9 0 8481.02 8737.12 224.07 o 5 9 0 7579.00 7244.81 204.03 o 6 9 0 6461.95 7439.09 195.53 o 7 9 0 8357.91 7967.68 242.84 o 8 9 0 2418.01 2608.76 115.81 o 9 9 0 15.79 -67.14 51.51 o 10 9 0 8.52 54.55 51.19 o 11 9 0 4891.03 5008.14 206.23 o 12 9 0 59.31 55.49 62.73 o 13 9 0 1582.76 1435.98 144.87 o 14 9 0 1586.17 1443.32 152.63 o 15 9 0 177.93 -28.22 162.39 o 16 9 0 413.05 354.14 190.18 o 17 9 0 74.36 260.15 197.42 o 0 10 0 324.48 223.86 40.70 o 1 10 0 6996.57 6933.89 172.56 o 2 10 0 466.18 512.54 39.55 o 3 10 0 95.71 132.17 35.77 o 4 10 0 79.51 85.18 33.46 o 5 10 0 3056.45 3505.34 126.51 o 6 10 0 520.48 441.84 61.26 o 7 10 0 188.21 153.89 45.84 o 8 10 0 653.97 765.04 69.86 o 9 10 0 429.50 439.11 62.42 o 10 10 0 799.30 781.30 85.07 o 11 10 0 230.59 324.25 78.15 o 12 10 0 103.82 90.00 67.03 o 13 10 0 10.77 -41.96 88.96 o 14 10 0 12.50 44.90 89.06 o 15 10 0 539.97 232.67 133.43 o 16 10 0 447.77 230.78 139.73 o 17 10 0 257.30 362.64 182.53 o 1 11 0 3919.01 4768.13 134.17 o 2 11 0 16264.05 17462.07 385.19 o 3 11 0 2597.66 2491.06 87.28 o 4 11 0 663.25 715.73 46.79 o 5 11 0 1041.31 1099.98 64.41 o 6 11 0 13968.37 14602.50 360.12 o 7 11 0 2490.03 2967.73 120.01 o 8 11 0 132.49 66.09 46.37 o 9 11 0 47.63 -10.49 57.69 o 10 11 0 2619.41 2539.73 130.60 o 11 11 0 641.44 565.20 87.80 o 12 11 0 72.29 205.81 84.55 o 13 11 0 332.04 375.12 95.35 o 14 11 0 5.54 267.49 159.97 o 15 11 0 501.80 409.74 140.36 o 16 11 0 44.69 12.69 171.72 o 17 11 0 7.34 -137.42 150.43 o 0 12 0 24530.54 29001.28 827.35 o 1 12 0 1426.69 1551.16 58.64 o 2 12 0 1340.05 1772.81 68.19 o 3 12 0 1691.27 1937.40 77.00 o 4 12 0 12171.21 13481.96 330.96 o 5 12 0 928.60 784.86 59.90 o 6 12 0 287.79 386.45 52.24 o 7 12 0 4564.36 5040.34 165.53 o 8 12 0 4119.04 4665.85 172.56 o 9 12 0 1309.93 1201.00 94.31 o 10 12 0 646.18 599.50 93.57 o 11 12 0 877.30 786.75 96.30 o 12 12 0 2077.96 2166.19 144.76 o 13 12 0 708.42 605.90 108.47 o 14 12 0 53.03 358.97 187.77 o 15 12 0 79.51 42.80 105.53 o 16 12 0 261.01 380.16 197.00 o 1 13 0 2297.36 1811.20 71.65 o 2 13 0 4000.97 4464.54 116.86 o 3 13 0 1699.85 1553.67 68.92 o 4 13 0 3452.56 2672.01 97.14 o 5 13 0 5726.48 5558.86 164.17 o 6 13 0 130.39 69.23 44.16 o 7 13 0 6458.77 7551.23 219.56 o 8 13 0 330.39 590.06 73.95 o 9 13 0 45.65 97.56 51.19 o 10 13 0 403.30 292.46 71.96 o 11 13 0 3590.06 3830.84 192.49 o 12 13 0 89.29 -16.68 79.30 o 13 13 0 786.40 741.96 107.63 o 14 13 0 957.40 997.18 194.27 o 15 13 0 132.71 218.09 133.01 o 16 13 0 414.73 719.19 192.81 o 0 14 0 3300.88 1780.99 90.21 o 1 14 0 1041.61 1269.29 57.69 o 2 14 0 152.53 197.63 38.29 o 3 14 0 122.63 199.41 36.61 o 4 14 0 11.07 29.27 41.02 o 5 14 0 6261.71 5997.03 190.60 o 6 14 0 23.55 7.45 41.02 o 7 14 0 3623.69 3668.25 145.18 o 8 14 0 9.47 -47.10 50.25 o 9 14 0 1131.06 1001.27 94.31 o 10 14 0 185.38 141.30 70.07 o 11 14 0 5.64 3.15 73.74 o 12 14 0 935.21 970.74 112.98 o 13 14 0 229.49 119.80 78.68 o 14 14 0 17.60 345.65 155.36 o 15 14 0 63.56 118.43 141.72 o 16 14 0 52.08 380.16 183.16 o 1 15 0 1601.84 1332.33 59.16 o 2 15 0 4408.10 5104.85 148.12 o 3 15 0 207.51 221.97 39.55 o 4 15 0 2323.74 2112.27 86.33 o 5 15 0 2055.09 1906.14 87.70 o 6 15 0 0.20 24.23 46.26 o 7 15 0 6852.92 7200.76 219.87 o 8 15 0 1019.66 944.73 79.62 o 9 15 0 3345.78 3249.38 155.04 o 10 15 0 249.91 263.30 78.88 o 11 15 0 2297.86 2064.85 138.36 o 12 15 0 13.83 -71.44 70.07 o 13 15 0 186.29 373.86 108.99 o 14 15 0 406.22 469.53 138.99 o 15 15 0 15.16 -9.44 121.79 o 16 15 0 461.40 48.04 204.24 o 0 16 0 522.31 560.59 64.41 o 1 16 0 40.95 69.23 33.46 o 2 16 0 1155.23 1084.98 59.79 o 3 16 0 355.17 414.98 47.52 o 4 16 0 254.72 193.96 44.16 o 5 16 0 1719.34 1589.65 82.66 o 6 16 0 495.40 684.89 66.09 o 7 16 0 1416.07 1753.72 97.66 o 8 16 0 2.31 60.95 66.19 o 9 16 0 82.93 52.66 58.74 o 10 16 0 312.88 236.65 66.82 o 11 16 0 35.88 -73.64 55.60 o 12 16 0 477.16 428.31 92.52 o 13 16 0 31.56 113.50 93.15 o 14 16 0 524.44 420.33 131.44 o 15 16 0 3.15 -82.87 110.25 o 1 17 0 967.67 1139.00 69.97 o 2 17 0 15.54 24.23 35.67 o 3 17 0 976.20 1019.84 62.10 o 4 17 0 223.27 139.73 42.90 o 5 17 0 103.21 31.37 41.02 o 6 17 0 2255.62 2193.35 100.07 o 7 17 0 55.07 85.81 49.20 o 8 17 0 1763.00 1633.82 107.31 o 9 17 0 130.78 153.89 69.86 o 10 17 0 21.28 6.19 62.52 o 11 17 0 1.37 2.10 80.25 o 12 17 0 0.58 -3.15 96.93 o 13 17 0 95.07 324.25 102.70 o 14 17 0 259.22 310.40 166.58 o 15 17 0 51.87 244.73 152.00 o 0 18 0 777.80 424.32 64.09 o 1 18 0 8.07 51.19 44.06 o 2 18 0 61.66 74.27 37.97 o 3 18 0 986.48 1216.73 70.07 o 4 18 0 1377.97 1239.50 73.01 o 5 18 0 284.61 327.81 53.92 o 6 18 0 2.70 62.94 56.54 o 7 18 0 187.13 171.20 60.21 o 8 18 0 369.63 319.63 62.52 o 9 18 0 32.29 70.39 70.07 o 10 18 0 1410.42 1119.39 104.06 o 11 18 0 749.48 874.45 107.31 o 12 18 0 318.91 583.77 104.90 o 13 18 0 41.85 69.23 108.89 o 14 18 0 1.13 -220.45 146.96 o 15 18 0 448.21 264.35 182.21 o 1 19 0 1677.81 2272.97 89.58 o 2 19 0 11.94 53.60 45.00 o 3 19 0 121.29 159.55 49.09 o 4 19 0 1520.73 1625.95 86.23 o 5 19 0 715.60 799.44 67.77 o 6 19 0 649.60 582.20 65.67 o 7 19 0 806.90 779.41 79.62 o 8 19 0 620.97 602.76 69.97 o 9 19 0 294.47 252.91 79.30 o 10 19 0 490.68 398.10 75.00 o 11 19 0 527.60 601.08 98.50 o 12 19 0 62.19 194.90 101.23 o 13 19 0 242.93 378.90 132.38 o 14 19 0 40.80 22.97 122.31 o 0 20 0 2637.40 3735.28 193.96 o 1 20 0 95.41 77.63 42.80 o 2 20 0 73.99 82.87 40.70 o 3 20 0 1514.12 1675.99 90.21 o 4 20 0 702.17 618.70 59.58 o 5 20 0 503.74 639.89 72.07 o 6 20 0 20.47 -36.72 47.10 o 7 20 0 93.43 145.92 50.04 o 8 20 0 13.99 -7.45 62.21 o 9 20 0 46.69 104.06 55.49 o 10 20 0 94.75 98.82 63.78 o 11 20 0 107.70 106.79 68.92 o 12 20 0 540.43 512.54 108.57 o 13 20 0 65.58 227.84 134.90 o 14 20 0 190.25 439.11 203.61 o 1 21 0 2066.14 2178.25 96.72 o 2 21 0 504.78 551.35 57.80 o 3 21 0 0.74 36.72 43.11 o 4 21 0 1638.22 1914.63 102.07 o 5 21 0 3515.40 3727.31 154.20 o 6 21 0 36.88 -17.73 48.04 o 7 21 0 1863.96 1903.31 110.25 o 8 21 0 493.82 597.93 69.65 o 9 21 0 44.27 88.22 70.60 o 10 21 0 141.17 108.05 77.42 o 11 21 0 1437.61 1406.71 121.47 o 12 21 0 214.68 111.51 94.41 o 13 21 0 85.63 -13.64 155.25 o 0 22 0 13.94 -24.23 49.41 o 1 22 0 98.13 63.99 39.86 o 2 22 0 2181.86 2251.36 104.48 o 3 22 0 430.57 358.97 54.02 o 4 22 0 43.29 85.18 44.27 o 5 22 0 608.99 497.96 60.74 o 6 22 0 386.18 172.04 50.98 o 7 22 0 1131.71 1230.37 106.79 o 8 22 0 4.09 -86.39 57.59 o 9 22 0 1306.99 1214.53 115.18 o 10 22 0 267.19 273.89 85.81 o 11 22 0 181.80 90.00 77.42 o 12 22 0 225.46 321.94 127.87 o 13 22 0 84.87 -177.18 142.24 o 1 23 0 1.15 60.95 46.05 o 2 23 0 1496.49 1358.46 81.19 o 3 23 0 406.48 328.97 54.02 o 4 23 0 149.86 88.22 53.50 o 5 23 0 355.25 294.66 61.16 o 6 23 0 37.90 10.49 60.84 o 7 23 0 102.85 111.51 55.39 o 8 23 0 35.63 -2.10 67.56 o 9 23 0 8.20 -14.58 62.84 o 10 23 0 195.20 285.85 84.34 o 11 23 0 56.88 -92.52 116.54 o 12 23 0 56.75 38.71 138.15 o 0 24 0 843.38 696.75 92.31 o 1 24 0 54.89 54.55 44.06 o 2 24 0 350.95 247.77 68.29 o 3 24 0 46.48 60.95 47.00 o 4 24 0 6.89 47.10 52.45 o 5 24 0 559.26 542.33 58.85 o 6 24 0 134.20 134.48 63.04 o 7 24 0 827.46 793.99 78.47 o 8 24 0 124.72 75.32 66.93 o 9 24 0 129.48 -24.23 74.58 o 10 24 0 486.51 568.24 115.81 o 11 24 0 267.01 302.53 148.75 o 1 25 0 641.79 477.92 62.31 o 2 25 0 3099.10 3128.64 141.30 o 3 25 0 706.27 451.38 66.09 o 4 25 0 1074.32 733.15 71.96 o 5 25 0 559.57 399.35 69.86 o 6 25 0 851.18 724.44 85.39 o 7 25 0 729.20 634.96 86.54 o 8 25 0 12.53 61.89 87.17 o 9 25 0 98.87 76.47 79.83 o 10 25 0 40.75 -47.10 102.70 o 11 25 0 1097.66 750.77 186.41 o 0 26 0 4876.13 4953.27 282.71 o 1 26 0 409.06 278.19 52.97 o 2 26 0 11.48 -35.56 45.21 o 3 26 0 30.16 86.96 51.40 o 4 26 0 303.74 122.00 60.84 o 5 26 0 33.52 28.22 62.94 o 6 26 0 107.46 127.77 90.11 o 7 26 0 702.49 613.87 117.17 o 8 26 0 69.42 -66.09 97.45 o 9 26 0 394.03 443.20 124.10 o 10 26 0 79.72 -1.05 118.85 o 1 27 0 80.73 15.63 63.78 o 2 27 0 36.96 -127.61 85.07 o 3 27 0 326.38 182.42 80.46 o 4 27 0 641.96 512.54 98.29 o 5 27 0 1286.02 1087.08 130.29 o 6 27 0 5.56 -18.88 84.86 o 7 27 0 76.07 258.05 92.63 o 8 27 0 228.34 19.93 167.11 o 9 27 0 91.19 188.61 102.28 o 0 28 0 394.62 381.42 93.57 o 1 28 0 115.07 51.19 100.60 o 2 28 0 198.17 47.10 94.31 o -18 1 1 1.42 88.22 125.98 o -17 1 1 2017.04 1983.24 253.86 o -16 1 1 2399.56 2313.25 299.07 o -15 1 1 905.85 743.74 150.11 o -14 1 1 176.11 60.95 88.96 o -13 1 1 1376.28 1167.54 139.41 o -12 1 1 8922.43 9535.62 347.95 o -11 1 1 9627.84 9938.33 309.98 o -10 1 1 1371.09 1304.12 102.91 o -9 1 1 9499.75 9732.73 281.13 o -8 1 1 13093.45 13898.83 328.34 o -7 1 1 25578.38 26996.33 596.04 o -6 1 1 6300.54 6042.24 171.20 o -5 1 1 38.30 60.95 31.37 o -4 1 1 91989.18 90747.52 1697.70 o -3 1 1 17413.85 16986.04 388.34 o -2 1 1 317.06 236.65 23.92 o 1 1 1 18.68 28.22 13.74 o 2 1 1 18465.56 16884.81 370.40 o 3 1 1 100.67 169.52 37.97 o 4 1 1 5940.75 6092.70 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