#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180833 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016461.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016461_Fobs loop_ _publ_author_name 'Laval, Jean Paul' 'Jennene Boukharrata, Nefla' 'Thomas, Philippe' _publ_section_title ; New oxyfluorotellurates(IV): MTeO~3~F (M = Fe^III^, Ga^III^ and Cr^III^) ; _journal_coeditor_code SQ3115 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i12 _journal_page_last i14 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.630 _cell_angle_gamma 90.000 _cell_length_a 5.0667 _cell_length_b 5.0550 _cell_length_c 12.3975 _exptl_crystal_F_000 444.00 _reflns_d_resolution_high 0.7111 _cod_data_source_file sq3115Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1fe4te_pt69 in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 29112.26 28185.18 258.65 o 4 0 0 21257.70 21145.60 250.67 o 6 0 0 6149.49 6147.83 211.40 o 1 1 0 5979.60 5960.28 41.78 o 2 1 0 1.35 17.69 20.35 o 3 1 0 959.12 942.45 31.34 o 4 1 0 331.12 256.41 40.79 o 5 1 0 945.29 969.03 86.16 o 6 1 0 3.66 73.07 98.07 o 0 2 0 23275.30 22715.29 193.56 o 1 2 0 4985.72 5411.86 48.10 o 2 2 0 36236.79 36837.71 208.43 o 3 2 0 9.36 64.97 23.58 o 4 2 0 9793.16 9752.84 98.12 o 5 2 0 383.74 348.48 51.04 o 6 2 0 3306.99 3191.93 129.58 o 1 3 0 12791.35 12969.42 96.43 o 2 3 0 1068.06 1034.87 28.46 o 3 3 0 7456.11 7486.88 76.30 o 4 3 0 281.37 384.42 54.82 o 5 3 0 4986.38 5247.41 126.29 o 6 3 0 183.28 319.14 141.92 o 0 4 0 2829.62 2841.18 67.34 o 1 4 0 658.48 715.20 40.99 o 2 4 0 4124.81 4122.25 52.94 o 3 4 0 1051.88 1111.41 48.99 o 4 4 0 1079.06 1083.55 64.36 o 5 4 0 659.32 873.97 147.73 o 1 5 0 6356.63 6366.42 96.52 o 2 5 0 362.69 353.59 45.19 o 3 5 0 6534.88 6423.80 104.26 o 4 5 0 627.45 633.34 111.82 o 5 5 0 3244.33 2809.20 228.56 o 0 6 0 140.09 -125.36 139.53 o 1 6 0 123.56 123.15 94.12 o 2 6 0 562.97 455.45 101.79 o 3 6 0 145.56 234.84 143.77 o 1 7 0 1212.87 1253.21 195.19 o -7 0 1 551.07 704.92 277.18 o -5 0 1 395.57 586.45 108.31 o -3 0 1 302.10 289.51 40.11 o 3 0 1 3288.81 3365.12 60.04 o 5 0 1 744.45 691.06 104.08 o -7 1 1 8455.95 8221.01 200.37 o -6 1 1 442.27 409.87 101.79 o -5 1 1 13603.40 13674.85 218.24 o -4 1 1 20.56 57.82 25.32 o -3 1 1 32428.95 32737.41 222.41 o -2 1 1 391.53 375.37 14.35 o -1 1 1 44855.35 45375.32 213.85 o 1 1 1 23947.64 23956.26 143.88 o 2 1 1 1622.30 1531.72 25.35 o 3 1 1 6468.26 6502.79 66.36 o 4 1 1 1129.16 1205.93 52.16 o 5 1 1 682.64 719.73 64.07 o 6 1 1 346.42 514.19 99.33 o -6 2 1 2064.07 2079.52 119.38 o -5 2 1 278.96 306.99 54.49 o -4 2 1 3713.63 3591.17 62.94 o -3 2 1 0.47 12.60 20.82 o -2 2 1 6322.03 6411.16 55.24 o -1 2 1 74.89 104.52 12.48 o 0 2 1 9068.35 9128.93 63.89 o 1 2 1 121.32 90.14 16.57 o 2 2 1 8047.24 8116.60 66.96 o 3 2 1 100.65 59.82 24.30 o 4 2 1 1178.41 1125.85 45.73 o 5 2 1 1088.30 968.19 70.82 o 6 2 1 1173.55 1173.37 122.32 o -6 3 1 34.13 14.49 150.68 o -5 3 1 7893.75 7856.97 147.20 o -4 3 1 500.80 499.60 50.30 o -3 3 1 8337.46 8352.59 83.06 o -2 3 1 1712.33 1655.01 32.51 o -1 3 1 8995.71 8871.48 65.39 o 0 3 1 4993.45 5002.27 51.08 o 1 3 1 3560.59 3674.30 44.20 o 2 3 1 3720.76 3846.52 48.12 o 3 3 1 641.75 626.67 32.69 o 4 3 1 4302.77 4453.75 73.19 o 5 3 1 68.82 65.63 81.07 o 6 3 1 2279.90 2286.04 156.84 o -5 4 1 0.85 156.90 150.12 o -4 4 1 5660.53 5867.57 102.12 o -3 4 1 44.59 99.14 39.06 o -2 4 1 10595.63 10524.98 87.77 o -1 4 1 1417.53 1417.80 34.48 o 0 4 1 7289.26 7479.94 74.30 o 1 4 1 1415.74 1502.19 37.50 o 2 4 1 5131.74 5290.36 67.44 o 3 4 1 1188.37 1231.35 47.64 o 4 4 1 5924.07 5896.26 106.46 o 5 4 1 211.59 289.13 124.51 o -5 5 1 42.88 90.41 249.83 o -4 5 1 525.12 508.75 125.21 o -3 5 1 297.59 236.04 68.46 o -2 5 1 1443.62 1430.70 52.12 o -1 5 1 34.28 100.83 45.67 o 0 5 1 2450.17 2370.85 66.35 o 1 5 1 0.17 127.78 51.51 o 2 5 1 3333.68 3342.11 77.62 o 3 5 1 809.70 983.36 68.13 o 4 5 1 2460.09 2579.15 121.56 o -3 6 1 506.10 411.46 182.70 o -2 6 1 2030.59 2015.25 118.18 o -1 6 1 2637.39 2547.36 102.05 o 0 6 1 3736.73 3793.27 121.82 o 1 6 1 3133.28 3197.54 113.10 o 2 6 1 2581.25 2542.12 123.75 o 3 6 1 1773.14 1753.13 181.96 o -1 7 1 688.86 470.25 165.18 o 0 7 1 441.46 398.03 190.59 o 1 7 1 1671.17 1318.08 223.26 o -6 0 2 7507.46 7734.80 207.50 o -4 0 2 9058.82 9072.45 141.55 o -2 0 2 6266.41 6214.31 64.30 o 2 0 2 2450.18 2690.75 38.74 o 4 0 2 2869.43 2829.85 85.65 o 6 0 2 61.03 -103.20 136.95 o -7 1 2 615.61 486.83 233.64 o -6 1 2 448.38 396.25 103.60 o -5 1 2 599.57 586.23 59.99 o -4 1 2 832.32 853.71 34.53 o -3 1 2 202.05 211.44 16.82 o -2 1 2 913.84 916.38 18.42 o -1 1 2 2162.31 2169.32 22.53 o 0 1 2 3759.98 3693.68 27.17 o 1 1 2 2506.95 2579.23 27.32 o 2 1 2 12555.28 12899.47 91.74 o 3 1 2 121.99 104.81 25.59 o 4 1 2 9932.76 9766.21 89.26 o 5 1 2 13.14 -48.85 58.04 o 6 1 2 7074.58 7155.50 168.00 o -6 2 2 4479.16 4520.05 132.05 o -5 2 2 1593.60 1688.15 61.79 o -4 2 2 5917.04 5899.44 79.06 o -3 2 2 4346.82 4265.13 50.99 o -2 2 2 2229.44 2201.41 29.84 o -1 2 2 6271.80 6100.23 47.22 o 0 2 2 812.72 833.07 16.38 o 1 2 2 4484.66 4420.74 41.93 o 2 2 2 2099.21 2061.91 32.05 o 3 2 2 11438.14 11438.33 94.26 o 4 2 2 67.86 143.73 46.27 o 5 2 2 1652.19 1763.35 78.39 o 6 2 2 451.05 503.79 125.53 o -6 3 2 36.56 53.61 156.29 o -5 3 2 3207.03 3209.29 95.81 o -4 3 2 232.22 222.41 47.38 o -3 3 2 4607.19 4565.79 59.98 o -2 3 2 7.60 35.97 20.20 o -1 3 2 3464.23 3485.07 37.59 o 0 3 2 105.33 100.36 20.32 o 1 3 2 4285.96 4357.44 48.21 o 2 3 2 298.05 289.34 27.34 o 3 3 2 938.81 917.90 31.22 o 4 3 2 1917.77 1899.16 52.06 o 5 3 2 362.42 281.84 88.31 o 6 3 2 2445.70 2314.90 173.15 o -5 4 2 2149.61 2215.57 140.80 o -4 4 2 220.02 132.31 59.34 o -3 4 2 6318.58 6109.98 82.92 o -2 4 2 101.20 121.75 26.53 o -1 4 2 8052.42 8227.12 74.60 o 0 4 2 909.35 957.46 39.94 o 1 4 2 14239.00 14115.75 113.03 o 2 4 2 1738.65 1811.01 49.92 o 3 4 2 4160.16 4226.49 75.99 o 4 4 2 645.69 738.85 68.17 o 5 4 2 6341.37 6132.61 142.96 o -5 5 2 2250.50 2009.43 240.57 o -4 5 2 1561.18 1452.41 141.38 o -3 5 2 3493.61 3465.23 89.44 o -2 5 2 3928.99 3922.70 74.61 o -1 5 2 3009.84 3019.44 73.06 o 0 5 2 1980.68 2100.50 64.75 o 1 5 2 1331.71 1371.70 63.05 o 2 5 2 1261.69 1155.81 59.86 o 3 5 2 1288.54 1277.84 77.69 o 4 5 2 96.46 60.10 110.02 o -3 6 2 1575.41 1635.51 153.34 o -2 6 2 974.65 805.10 99.24 o -1 6 2 4466.28 4432.03 121.20 o 0 6 2 2124.15 2094.85 109.43 o 1 6 2 2753.89 2691.02 111.13 o 2 6 2 1057.06 1023.04 103.93 o 3 6 2 3728.33 3801.75 235.83 o -1 7 2 928.75 905.75 200.45 o 0 7 2 5316.38 4926.24 204.64 o -7 0 3 709.84 187.69 308.42 o -5 0 3 5676.95 5778.67 120.36 o -3 0 3 6243.01 6219.04 90.93 o -1 0 3 30458.51 30037.96 206.15 o 1 0 3 42553.33 42872.34 354.57 o 3 0 3 28826.12 28905.44 231.15 o 5 0 3 19792.25 19730.88 424.89 o -7 1 3 763.53 516.00 204.49 o -6 1 3 361.68 386.19 88.74 o -5 1 3 288.10 424.85 56.58 o -4 1 3 4782.84 4700.49 54.36 o -3 1 3 2440.77 2433.35 40.82 o -2 1 3 4.86 7.83 11.70 o -1 1 3 1797.48 1680.84 19.25 o 0 1 3 6931.27 6858.08 46.41 o 1 1 3 7162.26 6979.41 53.02 o 2 1 3 2089.45 2111.15 28.41 o 3 1 3 2636.80 2594.01 40.91 o 4 1 3 1687.97 1714.53 43.85 o 5 1 3 1075.99 1095.21 69.72 o 6 1 3 511.32 438.16 122.25 o -6 2 3 1002.14 964.00 116.42 o -5 2 3 559.43 560.41 53.62 o -4 2 3 22.51 -25.78 32.72 o -3 2 3 4859.17 4792.72 57.72 o -2 2 3 633.08 670.18 21.89 o -1 2 3 11828.17 11836.29 82.90 o 0 2 3 107.70 103.19 12.41 o 1 2 3 21362.95 21375.86 134.52 o 2 2 3 44.40 18.45 18.89 o 3 2 3 16254.81 16308.60 123.87 o 4 2 3 26.50 92.35 34.03 o 5 2 3 7818.49 8147.75 137.01 o 6 2 3 928.99 924.33 141.69 o -6 3 3 3904.94 4136.94 228.25 o -5 3 3 368.58 352.99 79.91 o -4 3 3 5970.54 6032.88 108.13 o -3 3 3 22.81 28.26 27.26 o -2 3 3 11773.61 11959.39 87.39 o -1 3 3 6878.82 6939.28 65.95 o 0 3 3 13525.56 13553.91 88.16 o 1 3 3 2670.09 2681.30 33.58 o 2 3 3 9549.89 9567.99 84.86 o 3 3 3 1664.53 1719.82 50.11 o 4 3 3 5425.24 5393.19 93.26 o 5 3 3 164.61 266.11 90.84 o 6 3 3 2987.59 2842.39 184.04 o -5 4 3 526.49 485.42 101.94 o -4 4 3 1428.54 1437.65 72.88 o -3 4 3 7.17 -22.85 46.91 o -2 4 3 352.00 371.64 32.75 o -1 4 3 241.63 241.18 27.85 o 0 4 3 99.71 88.58 27.51 o 1 4 3 1072.75 1040.75 39.34 o 2 4 3 112.41 155.17 37.94 o 3 4 3 2282.90 2223.03 74.44 o 4 4 3 433.27 388.06 81.61 o 5 4 3 1085.47 1040.03 123.47 o -5 5 3 78.89 -46.71 186.65 o -4 5 3 3524.71 3572.87 139.55 o -3 5 3 2303.08 2410.89 92.90 o -2 5 3 10032.42 10002.31 133.78 o -1 5 3 1213.83 1254.22 56.66 o 0 5 3 7036.00 7226.77 98.96 o 1 5 3 1139.61 1102.34 57.74 o 2 5 3 6527.77 6418.95 106.19 o 3 5 3 285.97 164.49 70.94 o 4 5 3 3693.13 3678.30 143.04 o -3 6 3 3034.80 2840.10 173.65 o -2 6 3 271.05 270.44 110.23 o -1 6 3 1898.50 1874.12 128.69 o 0 6 3 23.59 50.31 91.44 o 1 6 3 810.05 901.00 109.11 o 2 6 3 4.81 94.31 122.48 o 3 6 3 149.81 69.50 163.90 o 0 7 3 1445.24 1330.97 197.26 o -6 0 4 1598.70 1424.03 139.34 o -4 0 4 4374.56 4147.09 84.91 o -2 0 4 15109.57 15053.05 116.29 o 0 0 4 7329.05 7221.27 74.15 o 2 0 4 3591.69 3500.85 50.23 o 4 0 4 1357.82 1387.08 76.10 o 6 0 4 1595.05 1767.75 193.53 o -7 1 4 5.45 -199.43 199.43 o -6 1 4 4745.16 4775.95 138.86 o -5 1 4 0.86 43.70 43.62 o -4 1 4 14232.61 14024.03 102.05 o -3 1 4 112.38 101.18 20.17 o -2 1 4 37798.96 38280.39 221.96 o -1 1 4 4076.75 4271.22 32.92 o 0 1 4 33682.69 33331.23 173.18 o 1 1 4 528.74 610.27 16.69 o 2 1 4 34307.85 34619.14 193.97 o 3 1 4 1476.06 1467.89 33.60 o 4 1 4 11252.99 11074.52 106.16 o 5 1 4 655.20 690.80 75.94 o 6 1 4 2629.66 2742.70 158.47 o -6 2 4 1217.60 1478.72 116.95 o -5 2 4 3096.51 2894.83 82.21 o -4 2 4 3404.17 3455.02 58.59 o -3 2 4 6663.84 6549.25 65.70 o -2 2 4 4088.67 4095.16 40.24 o -1 2 4 4745.53 4661.76 39.41 o 0 2 4 6693.65 6743.69 50.83 o 1 2 4 4983.96 5006.61 47.05 o 2 2 4 1321.12 1288.15 30.54 o 3 2 4 3552.07 3662.01 56.58 o 4 2 4 838.22 889.49 60.48 o 5 2 4 1690.75 1886.92 89.56 o 6 2 4 64.87 262.22 137.12 o -6 3 4 1093.34 1204.29 160.45 o -5 3 4 124.91 178.76 74.78 o -4 3 4 2961.17 2870.14 66.89 o -3 3 4 340.38 390.95 36.31 o -2 3 4 6705.85 6651.47 60.39 o -1 3 4 1868.06 1860.42 32.93 o 0 3 4 22509.89 22874.68 136.17 o 1 3 4 3676.00 3661.24 44.66 o 2 3 4 5230.81 5280.97 59.58 o 3 3 4 2781.80 2836.78 59.78 o 4 3 4 3492.63 3567.63 82.82 o 5 3 4 3007.84 3212.37 137.02 o -5 4 4 4705.67 4952.14 133.25 o -4 4 4 1307.52 1315.28 77.03 o -3 4 4 6485.11 6417.81 94.06 o -2 4 4 1019.88 998.00 41.26 o -1 4 4 11089.12 11174.24 100.12 o 0 4 4 188.84 189.17 39.01 o 1 4 4 5907.58 5922.75 64.80 o 2 4 4 51.91 53.20 36.50 o 3 4 4 4645.56 4679.68 83.88 o 4 4 4 375.95 532.71 91.69 o 5 4 4 1332.12 1223.70 137.58 o -4 5 4 4.04 75.20 126.85 o -3 5 4 355.14 401.11 86.68 o -2 5 4 122.22 175.00 64.61 o -1 5 4 431.22 465.39 56.29 o 0 5 4 101.07 35.43 55.26 o 1 5 4 3461.87 3438.85 86.55 o 2 5 4 986.68 1038.18 71.95 o 3 5 4 2212.55 2224.13 102.85 o 4 5 4 35.69 166.43 164.47 o -3 6 4 2790.16 3036.15 153.11 o -2 6 4 142.49 130.76 129.96 o -1 6 4 2198.07 2231.05 132.10 o 0 6 4 264.17 269.28 115.39 o 1 6 4 3163.56 3247.67 140.08 o 2 6 4 922.77 889.76 141.69 o 3 6 4 888.61 764.01 164.23 o -7 0 5 4574.65 4438.55 331.25 o -5 0 5 14265.64 14150.55 196.39 o -3 0 5 26134.71 25993.80 211.80 o -1 0 5 13721.49 12977.95 97.14 o 1 0 5 14670.60 14851.93 135.97 o 3 0 5 1704.59 1709.19 51.63 o 5 0 5 22.87 -13.52 128.97 o -6 1 5 603.14 626.66 106.84 o -5 1 5 3859.04 3804.28 84.85 o -4 1 5 586.60 588.69 43.54 o -3 1 5 5514.40 5461.99 58.20 o -2 1 5 2809.14 2765.64 31.24 o -1 1 5 7182.06 7531.25 47.66 o 0 1 5 362.67 433.41 12.87 o 1 1 5 1427.98 1433.49 25.38 o 2 1 5 1417.09 1391.75 26.83 o 3 1 5 2667.90 2690.28 42.34 o 4 1 5 160.83 197.42 40.95 o 5 1 5 2088.36 2084.86 96.99 o 6 1 5 23.45 83.47 160.81 o -6 2 5 338.85 169.67 144.79 o -5 2 5 6883.91 7056.05 116.99 o -4 2 5 2026.17 2021.51 49.42 o -3 2 5 11684.27 11929.71 93.13 o -2 2 5 7609.00 7692.26 58.65 o -1 2 5 16482.03 16584.76 97.45 o 0 2 5 3471.62 3390.69 36.11 o 1 2 5 5737.05 5734.29 60.64 o 2 2 5 6279.03 6309.35 61.14 o 3 2 5 710.87 710.21 30.02 o 4 2 5 3533.76 3595.66 76.92 o 5 2 5 7.83 -19.12 90.23 o 6 2 5 2092.58 1931.40 173.83 o -6 3 5 1889.09 1744.86 155.98 o -5 3 5 1054.16 974.63 79.75 o -4 3 5 4230.77 4076.99 83.94 o -3 3 5 1076.91 1084.84 40.48 o -2 3 5 2388.93 2417.65 37.65 o -1 3 5 230.94 233.93 25.36 o 0 3 5 4268.28 4249.26 44.95 o 1 3 5 631.12 669.20 29.46 o 2 3 5 1492.63 1528.97 44.25 o 3 3 5 6.02 54.51 39.25 o 4 3 5 422.97 379.84 61.46 o 5 3 5 28.28 156.93 112.71 o -5 4 5 1132.99 1205.85 143.07 o -4 4 5 2872.51 2750.25 97.79 o -3 4 5 1973.70 1904.47 61.68 o -2 4 5 4246.16 4431.17 63.56 o -1 4 5 3170.83 3089.54 60.14 o 0 4 5 9751.88 9613.34 94.47 o 1 4 5 432.26 405.25 36.73 o 2 4 5 8459.11 8545.41 103.52 o 3 4 5 24.43 140.43 58.55 o 4 4 5 5871.93 5564.21 120.82 o 5 4 5 171.22 106.93 163.39 o -4 5 5 1936.02 1910.32 143.24 o -3 5 5 890.07 895.50 96.37 o -2 5 5 2147.66 2366.62 96.03 o -1 5 5 444.87 417.01 58.68 o 0 5 5 2880.36 2734.35 75.71 o 1 5 5 3913.20 3810.18 86.34 o 2 5 5 745.89 757.78 84.95 o 3 5 5 2343.85 2494.28 122.35 o 4 5 5 382.87 310.23 143.67 o -3 6 5 56.16 201.19 199.23 o -2 6 5 2139.91 2163.48 144.59 o -1 6 5 39.17 38.39 135.42 o 0 6 5 3510.48 3438.10 139.01 o 1 6 5 20.55 150.97 144.43 o 2 6 5 2955.67 2878.50 152.46 o -6 0 6 1578.16 1528.11 210.47 o -4 0 6 4961.17 4624.35 81.13 o -2 0 6 4235.47 4351.84 56.73 o 0 0 6 11690.86 11925.98 119.22 o 2 0 6 3997.81 4033.34 61.88 o 4 0 6 8783.67 8445.12 137.72 o 6 0 6 5702.52 5820.09 393.43 o -6 1 6 4021.56 4139.08 151.21 o -5 1 6 1390.70 1357.01 58.44 o -4 1 6 2560.68 2547.33 71.69 o -3 1 6 1350.76 1389.72 37.35 o -2 1 6 1055.15 1025.14 22.35 o -1 1 6 3294.57 3226.89 27.41 o 0 1 6 356.46 338.15 12.93 o 1 1 6 4836.58 4836.69 44.55 o 2 1 6 5147.04 5138.74 48.64 o 3 1 6 54.25 32.36 24.96 o 4 1 6 1966.51 2042.68 71.96 o 5 1 6 2066.86 2115.19 110.30 o 6 1 6 2852.05 2882.41 171.82 o -6 2 6 1680.77 1445.25 164.01 o -5 2 6 847.27 789.85 73.95 o -4 2 6 833.86 860.82 60.89 o -3 2 6 179.35 138.01 27.63 o -2 2 6 1052.22 1075.89 25.34 o -1 2 6 426.28 413.72 16.69 o 0 2 6 1237.82 1238.69 24.54 o 1 2 6 430.65 419.75 25.87 o 2 2 6 4493.63 4441.56 58.95 o 3 2 6 21.07 -24.55 35.21 o 4 2 6 2983.77 2901.87 71.42 o 5 2 6 119.00 119.95 107.25 o 6 2 6 3187.28 3228.59 209.71 o -6 3 6 838.80 865.87 190.72 o -5 3 6 4482.25 4367.84 166.27 o -4 3 6 1453.60 1566.33 65.14 o -3 3 6 7686.11 7692.29 82.30 o -2 3 6 63.41 105.11 25.33 o -1 3 6 11461.43 11366.30 86.39 o 0 3 6 467.04 477.90 25.76 o 1 3 6 10497.62 10540.47 96.09 o 2 3 6 320.46 360.44 32.33 o 3 3 6 7404.75 7680.65 110.76 o 4 3 6 4460.72 4330.10 106.56 o 5 3 6 3610.92 3296.57 145.59 o -5 4 6 254.41 139.86 139.25 o -4 4 6 471.39 513.91 82.18 o -3 4 6 475.59 576.81 57.54 o -2 4 6 682.54 734.64 47.90 o -1 4 6 158.71 218.07 43.58 o 0 4 6 1200.18 1225.10 38.75 o 1 4 6 206.27 155.90 41.50 o 2 4 6 39.65 5.88 50.92 o 3 4 6 318.56 306.67 67.39 o 4 4 6 21.54 44.81 97.40 o -4 5 6 129.81 140.24 117.07 o -3 5 6 6282.98 6457.17 133.37 o -2 5 6 0.46 67.08 76.28 o -1 5 6 7270.90 7220.49 147.73 o 0 5 6 246.58 242.18 71.48 o 1 5 6 6567.72 6378.29 126.80 o 2 5 6 1194.64 1405.63 100.33 o 3 5 6 7443.18 7279.36 150.59 o 4 5 6 209.64 220.34 184.10 o -3 6 6 246.38 304.53 232.70 o -2 6 6 4343.58 4279.86 173.48 o -1 6 6 30.60 11.52 168.59 o 0 6 6 4109.05 3991.09 151.23 o 1 6 6 9.02 223.21 155.45 o 2 6 6 4017.32 3939.88 160.02 o -5 0 7 1024.00 1037.86 86.23 o -3 0 7 1321.12 1344.09 49.72 o -1 0 7 21344.34 21734.01 182.45 o 1 0 7 18006.35 18155.00 198.32 o 3 0 7 9250.29 9159.35 129.21 o 5 0 7 4641.99 4466.37 297.27 o -6 1 7 113.77 -35.50 132.59 o -5 1 7 1502.80 1482.97 77.92 o -4 1 7 163.59 139.21 37.38 o -3 1 7 6062.51 5966.90 58.69 o -2 1 7 730.67 707.40 20.71 o -1 1 7 10245.90 10110.54 62.08 o 0 1 7 125.10 130.22 17.07 o 1 1 7 14351.40 14318.07 93.68 o 2 1 7 1257.89 1241.36 29.45 o 3 1 7 11004.42 11050.80 95.06 o 4 1 7 185.49 115.65 55.15 o 5 1 7 6568.52 6486.26 212.56 o 6 1 7 172.34 165.30 195.12 o -6 2 7 2430.63 2148.21 167.76 o -5 2 7 239.16 403.19 82.23 o -4 2 7 2272.28 2166.02 60.01 o -3 2 7 4647.89 4633.99 68.29 o -2 2 7 10399.95 10318.51 81.25 o -1 2 7 6763.62 6672.90 52.77 o 0 2 7 4542.44 4551.00 47.38 o 1 2 7 9513.03 9696.67 89.68 o 2 2 7 2811.08 2838.06 50.05 o 3 2 7 6483.40 6369.83 84.26 o 4 2 7 1876.67 1893.29 78.08 o 5 2 7 2977.06 3097.72 134.21 o -6 3 7 14.34 -163.16 163.16 o -5 3 7 410.08 375.56 101.22 o -4 3 7 235.53 244.43 64.53 o -3 3 7 4.72 16.29 39.04 o -2 3 7 351.09 401.36 30.81 o -1 3 7 1725.65 1712.76 40.08 o 0 3 7 2471.27 2429.70 39.90 o 1 3 7 2289.99 2303.60 47.29 o 2 3 7 1271.89 1366.40 53.38 o 3 3 7 4760.85 4837.77 91.26 o 4 3 7 2342.08 2298.15 103.42 o 5 3 7 2466.77 2786.29 197.94 o -5 4 7 36.14 220.99 150.99 o -4 4 7 7997.19 8071.27 165.62 o -3 4 7 1526.76 1461.11 70.30 o -2 4 7 5554.30 5455.30 88.34 o -1 4 7 1483.37 1483.10 52.16 o 0 4 7 8060.98 7820.97 87.74 o 1 4 7 2164.95 2290.55 68.49 o 2 4 7 5752.80 5723.74 114.31 o 3 4 7 1352.68 1461.26 114.20 o 4 4 7 2779.96 2994.94 134.63 o -4 5 7 277.80 350.27 162.55 o -3 5 7 768.52 690.55 116.46 o -2 5 7 365.60 314.74 92.66 o -1 5 7 1250.78 1321.54 105.02 o 0 5 7 746.01 649.31 64.95 o 1 5 7 21.19 10.19 81.61 o 2 5 7 1282.65 1412.55 99.63 o 3 5 7 16.33 79.16 125.71 o -2 6 7 3210.59 3209.56 168.20 o -1 6 7 444.14 403.49 156.73 o 0 6 7 3037.61 2943.98 198.19 o 1 6 7 160.48 293.88 182.11 o 2 6 7 1979.94 2098.51 178.66 o -6 0 8 2954.08 3043.76 228.48 o -4 0 8 5074.92 4978.64 99.48 o -2 0 8 16345.87 16190.45 144.53 o 0 0 8 19428.42 19349.76 184.56 o 2 0 8 10095.01 10231.90 115.85 o 4 0 8 2771.96 2771.69 118.77 o -6 1 8 4341.97 4634.77 183.97 o -5 1 8 158.91 -59.69 83.50 o -4 1 8 8707.84 8601.37 96.28 o -3 1 8 1465.44 1452.46 34.80 o -2 1 8 17803.44 17780.45 110.40 o -1 1 8 677.39 674.59 17.05 o 0 1 8 15238.52 15291.88 104.23 o 1 1 8 470.59 488.50 19.36 o 2 1 8 9465.25 9341.77 73.47 o 3 1 8 178.49 201.45 40.21 o 4 1 8 3774.27 3684.98 99.08 o 5 1 8 12.87 -119.55 119.55 o -6 2 8 1032.04 1345.39 233.75 o -5 2 8 1037.57 1003.82 131.10 o -4 2 8 4713.37 4585.27 79.14 o -3 2 8 1357.31 1368.56 42.46 o -2 2 8 6163.24 6210.37 61.53 o -1 2 8 3422.27 3357.10 36.94 o 0 2 8 9432.97 9463.16 80.83 o 1 2 8 5006.83 4933.80 57.03 o 2 2 8 7631.86 7503.51 79.15 o 3 2 8 3736.77 3643.48 65.54 o 4 2 8 3008.31 2933.87 96.44 o 5 2 8 1374.95 1611.30 164.27 o -5 3 8 3157.30 3429.81 132.18 o -4 3 8 5248.76 5179.46 117.82 o -3 3 8 3337.34 3279.78 72.68 o -2 3 8 4617.56 4528.54 68.59 o -1 3 8 2568.72 2499.21 42.08 o 0 3 8 3991.41 3926.97 53.58 o 1 3 8 2329.70 2353.53 54.02 o 2 3 8 1459.32 1499.90 60.87 o 3 3 8 514.17 499.38 69.82 o 4 3 8 242.02 69.41 101.79 o 5 3 8 292.10 382.99 185.44 o -5 4 8 863.57 961.96 162.74 o -4 4 8 116.68 83.01 124.52 o -3 4 8 4318.89 4442.10 104.87 o -2 4 8 1119.96 1077.74 66.78 o -1 4 8 4389.20 4323.92 87.57 o 0 4 8 1726.84 1700.29 54.35 o 1 4 8 4674.61 4701.78 82.18 o 2 4 8 1733.12 1726.99 77.78 o 3 4 8 5085.87 5216.96 124.36 o 4 4 8 1110.88 1183.41 174.84 o -4 5 8 110.67 256.30 226.33 o -3 5 8 2038.49 2046.39 147.99 o -2 5 8 171.46 101.60 90.54 o -1 5 8 2149.55 2150.68 99.75 o 0 5 8 46.83 -2.75 78.91 o 1 5 8 998.54 1213.29 91.98 o 2 5 8 346.10 296.55 108.56 o 3 5 8 628.40 569.62 163.61 o -2 6 8 5.26 69.44 188.91 o -1 6 8 1954.56 2148.09 210.98 o 0 6 8 80.28 65.24 151.17 o 1 6 8 2363.05 2235.01 154.88 o -5 0 9 9839.63 10421.53 391.75 o -3 0 9 10784.39 10680.91 118.27 o -1 0 9 5371.52 5497.12 79.93 o 1 0 9 12058.89 11938.60 143.24 o 3 0 9 1864.22 1962.18 69.53 o 5 0 9 1727.77 2011.53 233.05 o -6 1 9 528.82 275.94 178.88 o -5 1 9 3669.92 3711.38 155.13 o -4 1 9 1346.83 1344.33 52.90 o -3 1 9 4203.02 4078.85 53.87 o -2 1 9 128.90 121.50 19.04 o -1 1 9 7646.18 7472.41 68.51 o 0 1 9 5257.47 5247.61 58.13 o 1 1 9 677.21 673.40 33.21 o 2 1 9 764.49 735.95 30.32 o 3 1 9 0.21 66.06 44.56 o 4 1 9 1151.80 1363.78 92.17 o 5 1 9 613.04 719.27 178.41 o -6 2 9 558.58 274.10 255.55 o -5 2 9 4828.50 5046.20 140.40 o -4 2 9 143.04 78.51 70.25 o -3 2 9 5256.04 5332.14 74.13 o -2 2 9 48.63 16.97 25.78 o -1 2 9 5777.62 5769.28 53.73 o 0 2 9 819.30 773.92 31.61 o 1 2 9 819.41 834.80 32.28 o 2 2 9 470.93 491.64 46.25 o 3 2 9 1105.55 1176.08 70.91 o 4 2 9 41.11 45.29 83.48 o 5 2 9 600.77 727.61 188.99 o -5 3 9 1638.71 1584.61 141.64 o -4 3 9 4474.76 4504.26 114.54 o -3 3 9 4363.40 4303.73 81.28 o -2 3 9 7110.97 7042.30 79.25 o -1 3 9 520.69 544.24 37.69 o 0 3 9 7836.40 7691.78 82.94 o 1 3 9 1978.36 1931.50 62.54 o 2 3 9 7391.07 7383.56 112.30 o 3 3 9 2.14 -74.91 74.91 o 4 3 9 3918.02 3777.70 134.36 o -5 4 9 285.72 390.64 204.66 o -4 4 9 547.23 633.19 143.98 o -3 4 9 276.38 133.11 82.19 o -2 4 9 475.96 502.18 73.08 o -1 4 9 0.19 18.46 54.89 o 0 4 9 190.46 57.19 48.46 o 1 4 9 646.98 747.17 60.83 o 2 4 9 36.57 14.33 78.42 o 3 4 9 256.20 371.73 117.33 o 4 4 9 141.69 272.35 195.08 o -3 5 9 479.26 487.99 172.04 o -2 5 9 6910.43 6953.08 157.89 o -1 5 9 1459.16 1474.33 107.40 o 0 5 9 4473.59 4444.06 118.87 o 1 5 9 165.92 125.08 104.39 o 2 5 9 5721.94 5699.04 150.12 o -1 6 9 3117.50 3185.90 221.90 o 0 6 9 21.07 -186.48 186.48 o -6 0 10 129.66 279.83 237.81 o -4 0 10 433.02 609.06 89.30 o -2 0 10 697.84 812.61 54.00 o 0 0 10 2302.06 2360.22 59.01 o 2 0 10 5418.48 5293.78 94.50 o 4 0 10 9168.85 9167.24 234.41 o -6 1 10 3633.38 3576.45 257.63 o -5 1 10 131.45 280.11 103.51 o -4 1 10 2607.10 2681.90 79.63 o -3 1 10 88.33 85.10 35.47 o -2 1 10 2473.50 2449.35 45.26 o -1 1 10 68.08 80.43 24.60 o 0 1 10 2030.76 1973.06 41.43 o 1 1 10 134.28 122.60 23.09 o 2 1 10 2355.97 2297.49 49.09 o 3 1 10 631.48 692.27 60.15 o 4 1 10 1811.38 1696.48 117.35 o 5 1 10 200.25 70.59 204.34 o -5 2 10 1810.38 1845.24 127.94 o -4 2 10 103.77 80.06 93.85 o -3 2 10 4357.53 4518.12 71.19 o -2 2 10 1.65 13.92 26.24 o -1 2 10 3776.90 3721.32 48.48 o 0 2 10 2461.43 2434.30 46.29 o 1 2 10 3670.69 3738.44 65.03 o 2 2 10 4128.84 4049.15 76.15 o 3 2 10 3339.81 3234.99 87.55 o 4 2 10 3405.15 3636.57 145.24 o -5 3 10 95.06 40.65 167.42 o -4 3 10 331.88 552.33 106.95 o -3 3 10 199.63 166.46 55.69 o -2 3 10 75.37 83.05 34.29 o -1 3 10 1148.74 1219.57 60.90 o 0 3 10 0.21 -41.31 41.31 o 1 3 10 1408.33 1353.99 56.60 o 2 3 10 5.04 172.33 66.48 o 3 3 10 1211.92 1369.51 98.07 o 4 3 10 318.28 388.09 176.28 o -4 4 10 416.80 119.84 185.17 o -3 4 10 5217.01 5380.31 155.12 o -2 4 10 27.23 191.58 97.94 o -1 4 10 8565.21 8783.90 139.29 o 0 4 10 78.55 78.87 81.66 o 1 4 10 5098.86 5200.27 106.83 o 2 4 10 961.48 876.92 90.23 o 3 4 10 2750.02 2929.53 167.90 o -3 5 10 316.61 -82.86 192.09 o -2 5 10 2611.79 2653.93 161.68 o -1 5 10 723.46 780.17 137.09 o 0 5 10 1876.88 1690.45 125.35 o 1 5 10 1172.22 1186.36 135.25 o 2 5 10 896.39 691.91 199.81 o -5 0 11 1190.26 1097.11 171.08 o -3 0 11 1081.44 1066.87 69.88 o -1 0 11 1903.03 1863.76 60.96 o 1 0 11 2549.10 2700.37 88.42 o 3 0 11 4363.55 4203.27 154.96 o -5 1 11 1769.70 1763.74 179.99 o -4 1 11 786.26 841.20 96.43 o -3 1 11 7655.92 7430.80 93.78 o -2 1 11 306.44 306.87 32.87 o -1 1 11 12948.37 13004.78 119.76 o 0 1 11 209.55 272.24 40.36 o 1 1 11 13321.67 13154.94 158.64 o 2 1 11 1147.45 1037.68 46.73 o 3 1 11 12679.98 12739.94 178.16 o 4 1 11 2.02 155.95 150.52 o -5 2 11 241.89 125.72 139.46 o -4 2 11 1273.12 1189.68 94.94 o -3 2 11 529.15 506.09 41.47 o -2 2 11 2024.43 2011.93 43.48 o -1 2 11 596.40 581.70 33.99 o 0 2 11 2133.70 2061.88 43.51 o 1 2 11 1931.53 1967.13 56.87 o 2 2 11 1840.56 1919.36 72.98 o 3 2 11 994.72 1093.13 97.30 o 4 2 11 2690.99 2738.66 185.34 o -5 3 11 425.12 584.87 168.63 o -4 3 11 3333.28 3489.47 122.35 o -3 3 11 1410.55 1444.05 81.58 o -2 3 11 2838.82 2932.10 71.32 o -1 3 11 4836.45 4712.93 68.52 o 0 3 11 2500.22 2524.20 64.95 o 1 3 11 7433.92 7435.17 128.38 o 2 3 11 1102.04 1028.61 89.98 o 3 3 11 2157.56 2142.12 125.62 o 4 3 11 409.62 266.52 234.47 o -4 4 11 1376.78 1550.66 180.45 o -3 4 11 380.55 443.08 128.25 o -2 4 11 3239.78 3171.40 113.65 o -1 4 11 5.75 100.47 79.94 o 0 4 11 3270.31 3396.59 100.27 o 1 4 11 0.26 119.78 86.56 o 2 4 11 4908.71 4773.51 140.38 o 3 4 11 259.21 161.44 162.54 o -2 5 11 3154.26 3012.14 168.66 o -1 5 11 228.63 293.96 171.89 o 0 5 11 2002.11 1944.81 146.51 o 1 5 11 107.50 184.92 168.01 o -4 0 12 17704.64 17982.67 367.54 o -2 0 12 12731.68 13226.67 216.28 o 0 0 12 18800.09 18943.76 246.97 o 2 0 12 8199.85 8439.90 209.78 o 4 0 12 4142.32 4172.87 282.31 o -5 1 12 503.52 928.90 250.68 o -4 1 12 740.56 886.18 91.49 o -3 1 12 1406.69 1398.47 80.07 o -2 1 12 1071.95 1126.05 62.00 o -1 1 12 677.10 716.98 49.55 o 0 1 12 2095.22 2176.77 66.97 o 1 1 12 894.40 929.80 54.34 o 2 1 12 1247.08 1225.75 58.81 o 3 1 12 664.66 702.85 134.39 o 4 1 12 511.42 632.26 197.14 o -5 2 12 1155.27 986.92 231.10 o -4 2 12 5456.06 5440.64 198.37 o -3 2 12 1.39 92.83 76.60 o -2 2 12 12226.23 12106.35 129.82 o -1 2 12 397.18 347.46 50.39 o 0 2 12 8301.88 8251.37 132.02 o 1 2 12 19.18 62.19 55.45 o 2 2 12 5668.72 5540.58 115.75 o 3 2 12 5.59 -47.33 149.20 o 4 2 12 1875.33 1500.57 239.82 o -4 3 12 42.35 186.15 157.80 o -3 3 12 3634.74 3728.30 123.53 o -2 3 12 1107.31 1070.30 82.01 o -1 3 12 4925.92 4949.39 94.39 o 0 3 12 1031.24 1039.62 64.36 o 1 3 12 5436.45 5520.60 117.35 o 2 3 12 889.50 982.22 115.79 o 3 3 12 3589.53 3262.72 160.91 o -3 4 12 1303.24 1079.26 197.63 o -2 4 12 1899.91 2014.26 153.29 o -1 4 12 30.52 -94.65 94.65 o 0 4 12 896.86 833.95 105.00 o 1 4 12 33.07 153.00 135.74 o 2 4 12 308.58 264.75 155.45 o -1 5 12 4296.13 3931.24 284.94 o 0 5 12 329.29 270.69 228.69 o -5 0 13 376.67 -371.93 371.93 o -3 0 13 577.09 503.48 162.97 o -1 0 13 63.17 -10.74 59.74 o 1 0 13 13.37 24.51 74.94 o 3 0 13 984.75 707.36 297.76 o -5 1 13 6669.66 7394.87 289.58 o -4 1 13 3.63 -21.54 162.56 o -3 1 13 8117.46 8199.98 156.70 o -2 1 13 113.53 56.95 61.78 o -1 1 13 6200.67 6005.27 91.82 o 0 1 13 580.97 539.56 60.69 o 1 1 13 1832.77 1746.60 77.17 o 2 1 13 45.50 41.98 98.24 o 3 1 13 1042.36 1035.22 151.32 o -4 2 13 2166.51 2090.23 141.75 o -3 2 13 404.04 295.75 104.28 o -2 2 13 4078.24 4012.33 99.11 o -1 2 13 624.52 527.35 64.22 o 0 2 13 1647.16 1673.22 87.95 o 1 2 13 47.79 110.87 88.52 o 2 2 13 2426.90 2570.24 138.08 o 3 2 13 169.30 -82.39 257.63 o -4 3 13 116.36 146.92 246.00 o -3 3 13 1546.17 1388.07 170.67 o -2 3 13 334.30 564.73 147.42 o -1 3 13 656.41 637.12 111.91 o 0 3 13 1031.98 1060.08 111.15 o 1 3 13 631.68 610.61 117.79 o 2 3 13 1017.88 1181.70 167.53 o -3 4 13 490.36 195.87 329.16 o -2 4 13 3690.21 3604.01 219.66 o -1 4 13 1072.56 1127.91 149.07 o 0 4 13 6251.58 6543.53 185.19 o 1 4 13 366.39 246.99 178.18 o -4 0 14 1898.03 1314.05 297.32 o -2 0 14 1972.99 2128.55 139.23 o 0 0 14 1.17 -96.03 110.05 o 2 0 14 248.27 148.72 216.08 o -4 1 14 194.10 465.29 213.73 o -3 1 14 538.94 456.00 122.75 o -2 1 14 1482.24 1356.25 93.68 o -1 1 14 596.41 574.58 64.76 o 0 1 14 3886.47 4015.45 97.17 o 1 1 14 136.96 306.03 114.33 o 2 1 14 5653.72 5531.84 174.58 o 3 1 14 97.45 -99.06 222.48 o -4 2 14 890.83 782.11 183.14 o -3 2 14 880.37 899.16 167.88 o -2 2 14 19.26 -48.52 120.77 o -1 2 14 2907.82 2914.15 101.98 o 0 2 14 164.03 334.38 94.95 o 1 2 14 1141.48 1147.38 146.73 o 2 2 14 5.61 123.50 201.02 o -3 3 14 2728.51 3272.13 273.88 o -2 3 14 68.84 96.35 196.93 o -1 3 14 1797.22 1999.31 133.63 o 0 3 14 441.80 371.84 172.66 o 1 3 14 1762.49 1826.55 196.56 o 2 3 14 1797.47 1654.34 215.17 o -2 4 14 317.98 231.17 293.67 o -1 4 14 1460.96 1337.79 229.46 o 0 4 14 388.73 307.12 193.54 o -3 0 15 5913.02 5846.06 283.94 o -1 0 15 11244.09 11980.62 268.41 o 1 0 15 15002.47 15173.08 312.76 o -4 1 15 732.66 730.03 286.47 o -3 1 15 56.88 -90.10 182.04 o -2 1 15 426.64 461.27 117.12 o -1 1 15 3.63 28.84 113.91 o 0 1 15 1075.48 1190.19 103.59 o 1 1 15 15.87 209.60 140.73 o 2 1 15 709.02 975.58 214.33 o -3 2 15 3991.17 4373.68 373.01 o -2 2 15 360.49 470.19 206.36 o -1 2 15 6188.35 6239.46 182.91 o 0 2 15 173.44 54.62 154.92 o 1 2 15 6318.81 6241.90 225.54 o 2 2 15 153.35 47.75 225.11 o -2 3 15 3182.84 2993.48 356.55 o -1 3 15 340.14 379.22 162.00 o 0 3 15 3694.72 3617.60 191.92 o 1 3 15 2.26 -199.98 209.23 o -2 0 16 37.47 144.78 226.43 o 0 0 16 42.17 -169.81 226.86 o -3 1 16 86.95 513.68 436.75 o -2 1 16 10596.32 11068.38 243.63 o -1 1 16 212.14 97.68 170.95 o 0 1 16 7984.52 8017.73 189.81 o 1 1 16 68.03 -74.02 223.05 o -2 2 16 70.02 278.04 240.31 o -1 2 16 2275.02 2307.09 186.31 o 0 2 16 24.01 -8.28 160.22 o 1 2 16 1895.33 1477.66 213.08 o -1 0 17 2328.99 1704.79 391.47 o -2 1 17 419.71 648.83 230.85 o -1 1 17 314.46 54.93 211.07 o 0 1 17 307.74 599.54 232.45 o