#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180833 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016463.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016463_Fobs loop_ _publ_author_name 'Bucher, Jolanta' 'Blacque, Olivier' 'Schmalle, Helmut W.' 'Berke, Heinz' _publ_section_title ; Bis(glycinato-\k^2^N,O)dinitrosylmolybdenum(0) and bis(2-aminoethanethiolato-\k^2^N,S)dinitrosylmolybdenum(0) acetonitrile monosolvate ; _journal_coeditor_code SQ3117 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m87 _journal_page_last m90 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.051 _cell_angle_gamma 90.000 _cell_length_a 12.9088 _cell_length_b 7.5727 _cell_length_c 9.6922 _exptl_crystal_F_000 600.00 _reflns_d_resolution_high 0.7040 _cod_data_source_file sq3117Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JOLA287 Stoe IPDS measurement' _shelx_refln_list_code 4 _shelx_f_calc_maximum 159.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 9400.11 8735.43 63.80 o 4 0 0 4818.68 4504.61 41.35 o 5 0 0 4989.15 5086.55 38.66 o 6 0 0 11538.34 11362.66 51.81 o 7 0 0 1573.27 1502.51 19.67 o 8 0 0 15085.94 14495.36 52.88 o 9 0 0 869.53 884.41 17.76 o 10 0 0 2451.52 2621.47 24.42 o 11 0 0 138.53 149.41 16.37 o 12 0 0 2296.01 2384.03 23.59 o 13 0 0 462.07 489.52 16.74 o 14 0 0 1208.95 1166.53 18.94 o 15 0 0 763.94 752.90 21.49 o 16 0 0 833.83 866.05 24.42 o 17 0 0 343.23 332.80 25.68 o 1 1 0 69.07 71.43 19.55 o 2 1 0 175.13 154.25 16.69 o 3 1 0 3664.41 3286.36 39.10 o 4 1 0 1212.99 1139.14 22.19 o 5 1 0 972.46 968.00 18.65 o 6 1 0 1410.77 1416.56 20.95 o 7 1 0 334.73 354.24 13.49 o 8 1 0 1247.01 1278.01 18.07 o 9 1 0 27.52 30.35 15.19 o 10 1 0 425.99 427.12 13.78 o 11 1 0 0.36 4.97 13.03 o 12 1 0 29.01 22.31 12.31 o 13 1 0 224.19 226.87 18.46 o 14 1 0 55.50 53.92 15.14 o 15 1 0 29.17 26.23 18.85 o 16 1 0 129.48 130.32 22.09 o 17 1 0 65.38 57.97 22.07 o 0 2 0 8147.35 6985.42 61.24 o 1 2 0 0.71 3.59 13.90 o 2 2 0 12693.51 10977.37 62.40 o 3 2 0 175.79 210.86 13.01 o 4 2 0 3955.40 3445.29 32.89 o 5 2 0 1491.20 1448.71 21.05 o 6 2 0 11120.71 10623.81 49.05 o 7 2 0 383.21 354.92 13.42 o 8 2 0 8739.09 8852.96 41.69 o 9 2 0 864.48 886.20 17.39 o 10 2 0 6260.62 6241.84 34.32 o 11 2 0 1189.39 1237.48 18.34 o 12 2 0 2691.37 2821.40 26.91 o 13 2 0 2383.40 2342.44 24.08 o 14 2 0 3284.49 3659.52 30.91 o 15 2 0 1008.11 1028.05 22.77 o 16 2 0 1232.51 1245.60 25.68 o 17 2 0 1071.14 1020.78 25.63 o 1 3 0 342.06 370.52 16.64 o 2 3 0 1044.13 1128.84 21.56 o 3 3 0 3206.91 3416.66 32.97 o 4 3 0 266.30 295.23 13.47 o 5 3 0 410.04 402.51 14.22 o 6 3 0 807.02 795.58 16.08 o 7 3 0 11.05 14.90 11.72 o 8 3 0 135.94 144.90 13.44 o 9 3 0 306.45 299.20 13.42 o 10 3 0 107.38 124.12 12.84 o 11 3 0 319.72 330.21 15.79 o 12 3 0 53.94 58.64 15.67 o 13 3 0 6.18 6.95 14.87 o 14 3 0 340.49 365.53 22.45 o 15 3 0 54.03 43.31 17.32 o 16 3 0 0.05 1.72 19.74 o 17 3 0 19.16 15.45 24.10 o 0 4 0 12882.88 12933.38 61.48 o 1 4 0 195.87 196.88 12.04 o 2 4 0 6320.64 6133.03 41.20 o 3 4 0 1089.70 1049.73 18.60 o 4 4 0 12537.60 11707.94 53.05 o 5 4 0 370.70 363.83 14.73 o 6 4 0 10228.62 10021.46 45.52 o 7 4 0 3167.10 3264.03 27.35 o 8 4 0 6015.90 6163.36 35.07 o 9 4 0 217.34 213.55 13.03 o 10 4 0 606.60 630.28 16.01 o 11 4 0 460.13 468.13 15.62 o 12 4 0 2598.61 2611.49 24.83 o 13 4 0 458.41 481.51 20.69 o 14 4 0 2056.73 2147.35 27.71 o 15 4 0 525.79 511.45 22.24 o 16 4 0 1284.85 1354.82 30.76 o 1 5 0 29.52 30.30 14.29 o 2 5 0 1223.06 1258.60 19.72 o 3 5 0 1698.06 1683.57 22.62 o 4 5 0 34.84 45.71 14.95 o 5 5 0 743.02 774.41 18.46 o 6 5 0 0.54 7.17 12.16 o 7 5 0 143.20 144.66 15.43 o 8 5 0 2.55 9.16 12.77 o 9 5 0 1360.37 1411.02 21.12 o 10 5 0 313.22 293.78 14.95 o 11 5 0 1188.10 1177.05 22.04 o 12 5 0 0.31 6.23 16.76 o 13 5 0 40.85 49.58 22.67 o 14 5 0 0.48 -2.33 19.84 o 15 5 0 190.11 171.28 22.55 o 0 6 0 3092.86 3344.91 31.51 o 1 6 0 77.34 93.23 14.90 o 2 6 0 3814.74 4005.91 33.26 o 3 6 0 51.59 59.76 11.82 o 4 6 0 1586.57 1607.03 22.43 o 5 6 0 277.95 300.54 16.42 o 6 6 0 5705.19 5645.11 35.32 o 7 6 0 70.18 69.67 13.47 o 8 6 0 2468.98 2631.15 27.13 o 9 6 0 1174.99 1195.26 21.36 o 10 6 0 2629.50 2672.02 27.76 o 11 6 0 263.08 272.75 20.11 o 12 6 0 1300.11 1301.84 23.57 o 13 6 0 707.33 690.24 21.49 o 14 6 0 1524.00 1595.69 31.03 o 1 7 0 340.18 351.84 15.82 o 2 7 0 43.61 36.24 13.23 o 3 7 0 1004.13 1031.32 19.81 o 4 7 0 4.46 2.54 12.81 o 5 7 0 680.09 718.29 20.01 o 6 7 0 641.18 643.24 18.94 o 7 7 0 402.21 410.99 17.59 o 8 7 0 698.22 691.35 18.53 o 9 7 0 102.30 112.69 17.37 o 10 7 0 206.43 197.61 18.60 o 11 7 0 441.80 475.89 27.83 o 12 7 0 0.24 1.96 18.39 o 13 7 0 378.26 358.94 25.87 o 0 8 0 4621.30 4472.47 34.49 o 1 8 0 21.61 23.38 18.72 o 2 8 0 3591.89 3727.95 33.50 o 3 8 0 1.87 -0.44 13.47 o 4 8 0 2661.62 2864.81 31.78 o 5 8 0 120.86 116.10 17.22 o 6 8 0 1309.45 1395.22 28.15 o 7 8 0 345.22 340.58 19.11 o 8 8 0 961.77 975.56 23.91 o 9 8 0 13.94 6.32 25.43 o 10 8 0 839.87 812.20 22.43 o 11 8 0 64.07 43.02 24.03 o 1 9 0 371.78 380.37 18.72 o 2 9 0 1.71 3.85 18.58 o 3 9 0 1459.79 1528.98 28.99 o 4 9 0 18.76 16.28 19.48 o 5 9 0 682.47 690.91 23.71 o 6 9 0 52.94 50.17 22.62 o 7 9 0 249.38 255.48 22.09 o 8 9 0 41.03 38.76 24.13 o 9 9 0 841.63 846.64 33.62 o 0 10 0 307.06 307.56 27.37 o 1 10 0 36.92 23.11 25.70 o 2 10 0 1238.82 1197.93 32.02 o 3 10 0 3.89 4.65 18.87 o 4 10 0 597.04 595.16 29.96 o 5 10 0 91.25 69.40 28.46 o 6 10 0 668.15 560.45 32.60 o -18 1 1 734.86 641.55 25.17 o -17 1 1 1131.91 1145.77 27.88 o -16 1 1 697.82 696.15 22.04 o -15 1 1 2614.04 2768.09 29.65 o -14 1 1 440.52 449.56 17.03 o -13 1 1 4163.81 4338.22 30.18 o -12 1 1 1617.08 1648.77 20.27 o -11 1 1 4848.45 4740.69 29.46 o -10 1 1 1109.94 1086.23 18.51 o -9 1 1 7200.50 7303.10 37.23 o -8 1 1 574.13 619.94 15.02 o -7 1 1 6327.25 5915.65 36.72 o -6 1 1 1126.63 1055.95 18.80 o -5 1 1 13245.32 12880.16 60.12 o -4 1 1 2065.63 1948.23 28.15 o -3 1 1 10550.28 9567.40 65.40 o -2 1 1 2877.83 2605.50 43.67 o 0 1 1 15.94 16.28 14.99 o 2 1 1 6.43 -16.71 16.84 o 3 1 1 12843.16 11434.75 63.83 o 4 1 1 4526.44 4713.63 39.05 o 5 1 1 5964.30 5303.03 37.26 o 6 1 1 2453.09 2324.54 23.88 o 7 1 1 8122.04 7698.76 39.65 o 8 1 1 1146.32 1119.83 18.39 o 9 1 1 14298.66 14982.87 52.85 o 10 1 1 478.92 528.28 16.98 o 11 1 1 3777.17 3822.69 28.05 o 12 1 1 1660.28 1722.62 20.73 o 13 1 1 1294.55 1374.71 21.53 o 14 1 1 898.32 877.16 19.57 o 15 1 1 1291.82 1294.84 22.38 o 16 1 1 608.76 606.50 25.85 o 17 1 1 1221.07 1195.75 27.54 o -17 2 1 6.98 6.25 27.81 o -16 2 1 53.85 46.68 18.94 o -15 2 1 111.73 108.47 16.64 o -14 2 1 141.53 130.47 17.15 o -13 2 1 134.37 128.79 15.19 o -12 2 1 66.61 62.81 14.78 o -11 2 1 11.67 21.92 11.82 o -10 2 1 197.70 200.11 12.91 o -9 2 1 23.58 38.97 12.64 o -8 2 1 435.23 503.35 16.64 o -7 2 1 4.44 8.50 10.13 o -6 2 1 107.83 115.81 11.48 o -5 2 1 1137.69 1161.52 20.69 o -4 2 1 130.21 129.76 11.60 o -3 2 1 3127.57 2931.98 34.49 o -2 2 1 1945.55 1753.38 29.65 o -1 2 1 290.03 277.45 16.91 o 0 2 1 734.09 673.76 22.09 o 1 2 1 14587.12 13393.74 70.37 o 2 2 1 2.23 4.07 12.38 o 3 2 1 82.00 84.76 11.24 o 4 2 1 171.28 203.45 12.74 o 5 2 1 60.22 66.18 10.42 o 6 2 1 2488.16 2580.79 25.46 o 7 2 1 1.94 2.86 10.08 o 8 2 1 108.24 117.34 14.95 o 9 2 1 29.80 24.34 11.53 o 10 2 1 28.30 31.22 14.49 o 11 2 1 306.86 323.18 13.95 o 12 2 1 538.07 528.40 17.17 o 13 2 1 2.48 -2.08 16.52 o 14 2 1 13.29 12.38 18.99 o 15 2 1 6.34 7.85 16.42 o 16 2 1 16.14 9.18 20.64 o 17 2 1 50.34 31.95 26.38 o -17 3 1 1507.05 1494.39 30.84 o -16 3 1 305.40 318.78 20.59 o -15 3 1 1506.66 1557.13 24.88 o -14 3 1 569.74 544.82 19.62 o -13 3 1 1757.19 1869.49 24.30 o -12 3 1 1996.92 2028.03 24.71 o -11 3 1 2271.53 2373.13 23.98 o -10 3 1 55.21 72.23 13.03 o -9 3 1 6584.56 6701.16 35.90 o -8 3 1 30.26 21.36 12.33 o -7 3 1 9978.94 9924.13 44.69 o -6 3 1 768.48 739.84 15.96 o -5 3 1 14731.41 14652.54 59.39 o -4 3 1 3.84 6.93 9.01 o -3 3 1 8746.39 8030.57 49.05 o -2 3 1 14.67 10.17 10.44 o -1 3 1 4223.64 3696.68 38.15 o 0 3 1 61.16 65.16 11.65 o 2 3 1 36.23 42.87 11.00 o 3 3 1 16409.78 16040.79 65.31 o 4 3 1 1126.45 1056.92 18.46 o 5 3 1 3247.85 3058.38 27.28 o 6 3 1 103.79 104.57 10.46 o 7 3 1 6739.81 6508.80 35.49 o 8 3 1 276.92 255.48 13.23 o 9 3 1 5434.67 5415.86 32.34 o 10 3 1 2279.19 2289.71 23.16 o 11 3 1 1172.80 1238.09 20.15 o 12 3 1 1582.16 1632.46 22.84 o 13 3 1 1555.48 1565.27 22.89 o 14 3 1 469.79 465.81 20.18 o 15 3 1 2023.77 2037.54 27.40 o 16 3 1 1183.40 1306.03 30.88 o -16 4 1 41.08 34.57 27.37 o -15 4 1 426.85 418.02 23.57 o -14 4 1 17.37 19.33 16.69 o -13 4 1 67.47 67.92 15.72 o -12 4 1 1027.12 1061.53 19.98 o -11 4 1 7.03 11.26 13.90 o -10 4 1 176.35 174.48 12.84 o -9 4 1 26.10 29.62 10.88 o -8 4 1 66.69 64.65 11.94 o -7 4 1 444.41 448.68 15.55 o -6 4 1 719.08 750.91 18.63 o -5 4 1 262.97 263.11 14.87 o -4 4 1 1221.62 1220.19 20.88 o -3 4 1 327.95 311.19 13.37 o -2 4 1 940.03 935.01 18.89 o -1 4 1 7.78 5.84 8.48 o 0 4 1 78.51 49.41 9.69 o 1 4 1 75.76 82.19 10.37 o 2 4 1 210.72 176.37 11.94 o 3 4 1 68.29 58.84 11.19 o 4 4 1 649.10 636.63 15.74 o 5 4 1 94.41 100.57 11.70 o 6 4 1 923.98 895.67 17.73 o 7 4 1 112.92 104.50 13.10 o 8 4 1 11.31 15.55 11.77 o 9 4 1 306.09 306.93 13.88 o 10 4 1 202.47 186.69 13.98 o 11 4 1 2.09 2.88 14.36 o 12 4 1 351.81 341.11 17.39 o 13 4 1 70.29 62.93 17.63 o 14 4 1 259.40 255.36 22.02 o 15 4 1 133.29 124.97 21.70 o 16 4 1 20.81 12.14 26.16 o -16 5 1 201.77 188.53 24.27 o -15 5 1 1268.63 1184.36 27.57 o -14 5 1 408.94 398.49 21.49 o -13 5 1 960.02 983.09 21.22 o -12 5 1 425.88 435.43 17.80 o -11 5 1 2016.46 2126.49 25.31 o -10 5 1 178.12 181.07 14.70 o -9 5 1 3365.62 3330.96 27.13 o -8 5 1 2.37 1.82 12.45 o -7 5 1 6398.53 6799.91 38.83 o -6 5 1 434.73 425.79 16.37 o -5 5 1 8866.84 8986.70 45.59 o -4 5 1 345.51 361.72 16.21 o -3 5 1 8917.61 8832.01 46.14 o -2 5 1 276.80 305.14 15.09 o -1 5 1 7047.63 7165.61 43.48 o 0 5 1 25.70 35.90 12.69 o 1 5 1 6445.61 6272.51 39.85 o 2 5 1 143.99 180.32 15.16 o 3 5 1 11004.72 11693.96 51.74 o 4 5 1 2.80 5.69 15.33 o 5 5 1 6397.06 6426.06 37.52 o 6 5 1 1146.23 1163.36 18.53 o 7 5 1 2510.24 2553.37 23.91 o 8 5 1 287.53 286.39 14.32 o 9 5 1 969.80 1074.17 22.89 o 10 5 1 201.63 204.39 15.48 o 11 5 1 1858.46 1828.48 21.75 o 12 5 1 408.61 399.10 19.11 o 13 5 1 1326.12 1292.59 22.77 o 14 5 1 1051.26 1116.56 30.18 o 15 5 1 1089.78 1083.98 26.69 o -14 6 1 94.18 92.87 26.43 o -13 6 1 24.91 23.62 22.75 o -12 6 1 309.39 294.89 19.16 o -11 6 1 1.00 4.94 15.96 o -10 6 1 701.06 704.16 18.00 o -9 6 1 314.93 327.25 17.85 o -8 6 1 641.84 677.54 19.45 o -7 6 1 100.39 97.30 14.46 o -6 6 1 1023.42 1075.94 21.03 o -5 6 1 342.70 337.69 15.58 o -4 6 1 861.33 861.59 19.16 o -3 6 1 40.68 39.60 12.18 o -2 6 1 3159.81 3112.22 29.16 o -1 6 1 213.30 235.52 16.01 o 0 6 1 1451.86 1510.94 22.07 o 1 6 1 196.47 202.99 15.43 o 2 6 1 345.45 357.27 15.60 o 3 6 1 295.48 281.86 14.82 o 4 6 1 1232.93 1272.61 20.59 o 5 6 1 16.66 17.10 12.50 o 6 6 1 1102.98 1127.70 19.91 o 7 6 1 215.77 219.41 15.24 o 8 6 1 87.02 90.47 14.32 o 9 6 1 37.02 33.82 15.26 o 10 6 1 92.96 98.15 21.34 o 11 6 1 11.97 12.94 17.76 o 12 6 1 320.07 283.80 21.68 o 13 6 1 32.63 23.47 21.12 o 14 6 1 57.90 53.29 23.76 o -13 7 1 1271.79 1277.04 28.39 o -12 7 1 288.89 261.80 21.03 o -11 7 1 2710.35 2723.86 30.84 o -10 7 1 509.43 529.95 21.73 o -9 7 1 896.20 933.89 24.13 o -8 7 1 72.49 67.90 14.73 o -7 7 1 1612.81 1692.20 25.12 o -6 7 1 604.91 603.64 17.83 o -5 7 1 1846.55 1950.44 26.62 o -4 7 1 35.56 37.52 14.46 o -3 7 1 3109.33 3134.61 29.46 o -2 7 1 176.70 175.54 15.24 o -1 7 1 2530.28 2695.88 29.24 o 0 7 1 46.07 41.83 12.31 o 1 7 1 2004.57 2053.68 25.31 o 2 7 1 0.13 0.75 10.49 o 3 7 1 2315.29 2401.76 27.01 o 4 7 1 391.86 408.21 17.85 o 5 7 1 2615.28 2577.84 25.99 o 6 7 1 794.94 788.44 19.06 o 7 7 1 2242.12 2276.77 26.14 o 8 7 1 650.65 659.84 21.24 o 9 7 1 2380.73 2469.93 28.78 o 10 7 1 386.31 407.46 21.80 o 11 7 1 1620.92 1595.33 26.38 o 12 7 1 269.78 262.97 25.82 o 13 7 1 583.51 547.22 25.14 o -12 8 1 135.30 109.37 27.57 o -11 8 1 108.10 106.19 30.23 o -10 8 1 215.18 217.96 24.39 o -9 8 1 250.48 251.17 23.69 o -8 8 1 951.60 953.56 23.57 o -7 8 1 153.89 141.05 20.06 o -6 8 1 268.80 280.94 21.63 o -5 8 1 173.45 156.09 15.84 o -4 8 1 520.54 541.65 20.98 o -3 8 1 145.38 148.71 15.67 o -2 8 1 685.83 695.95 19.40 o -1 8 1 73.06 57.72 17.39 o 0 8 1 817.98 800.45 21.15 o 1 8 1 308.04 286.27 17.27 o 2 8 1 504.04 508.05 18.22 o 3 8 1 94.03 79.52 16.54 o 4 8 1 477.82 511.08 18.12 o 5 8 1 54.43 48.93 16.57 o 6 8 1 810.44 843.59 23.64 o 7 8 1 99.53 93.72 18.63 o 8 8 1 200.65 200.01 20.30 o 9 8 1 118.82 114.70 19.67 o 10 8 1 191.60 185.33 20.08 o 11 8 1 161.72 134.80 29.29 o -9 9 1 934.69 808.08 30.98 o -8 9 1 61.74 45.71 22.33 o -7 9 1 720.18 714.36 24.78 o -6 9 1 189.55 179.44 21.61 o -5 9 1 1109.92 1100.11 24.95 o -4 9 1 26.67 28.90 18.89 o -3 9 1 2135.07 2243.97 31.05 o -2 9 1 12.79 5.64 17.88 o -1 9 1 2104.36 2161.16 31.54 o 0 9 1 50.52 47.86 18.92 o 1 9 1 1776.24 1824.29 30.91 o 2 9 1 188.04 174.33 20.32 o 3 9 1 1058.71 1091.88 23.98 o 4 9 1 18.87 14.46 18.29 o 5 9 1 616.18 663.95 28.07 o 6 9 1 181.80 175.18 20.08 o 7 9 1 1909.93 1929.39 31.47 o 8 9 1 40.70 31.93 22.77 o 9 9 1 830.71 780.05 28.80 o -6 10 1 635.97 553.45 29.14 o -5 10 1 0.26 -0.56 28.00 o -4 10 1 527.28 493.01 31.27 o -3 10 1 21.55 11.34 24.61 o -2 10 1 342.06 336.29 26.28 o -1 10 1 2.99 4.80 23.54 o 0 10 1 595.88 608.77 25.75 o 1 10 1 19.48 20.18 21.99 o 2 10 1 419.44 426.86 25.07 o 3 10 1 229.11 221.40 27.93 o 4 10 1 944.13 933.22 29.48 o 5 10 1 12.75 6.98 27.01 o 6 10 1 481.04 453.79 28.10 o -18 0 2 567.09 474.77 32.73 o -17 0 2 562.95 542.31 22.24 o -16 0 2 1377.74 1382.87 24.08 o -15 0 2 12.98 17.05 22.29 o -14 0 2 3801.53 3758.78 27.93 o -13 0 2 206.96 189.96 14.61 o -12 0 2 4293.19 4603.37 31.66 o -11 0 2 1041.02 1081.97 18.55 o -10 0 2 4923.16 5234.99 32.17 o -9 0 2 846.07 985.90 18.05 o -8 0 2 8658.97 8324.10 41.20 o -7 0 2 59.46 88.34 9.64 o -5 0 2 1494.46 1499.16 24.30 o -3 0 2 72.67 73.61 15.19 o -1 0 2 347.28 336.85 20.81 o 1 0 2 231.25 234.21 15.38 o 2 0 2 12104.57 10238.35 60.97 o 3 0 2 98.99 115.54 13.30 o 4 0 2 5285.70 4571.56 34.95 o 5 0 2 287.85 294.65 15.02 o 6 0 2 4059.22 3761.21 29.02 o 7 0 2 1033.45 1000.99 17.20 o 8 0 2 5160.58 5306.08 32.31 o 9 0 2 769.22 741.83 15.53 o 10 0 2 4325.61 4186.47 27.59 o 11 0 2 407.20 423.83 15.12 o 12 0 2 275.53 286.95 16.88 o 13 0 2 2442.84 2436.26 23.50 o 14 0 2 984.57 993.10 20.93 o 15 0 2 504.36 489.01 18.48 o 16 0 2 1171.31 1113.39 25.72 o 17 0 2 1151.36 1117.58 26.04 o -18 1 2 58.52 45.49 23.71 o -17 1 2 11.24 22.72 18.75 o -16 1 2 0.74 5.04 19.60 o -15 1 2 195.17 191.36 19.31 o -14 1 2 8.61 3.80 13.73 o -13 1 2 0.94 12.09 15.79 o -12 1 2 611.53 583.07 14.82 o -11 1 2 585.65 609.31 16.13 o -10 1 2 664.66 744.98 15.87 o -9 1 2 490.82 487.59 14.49 o -8 1 2 1095.39 1103.29 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