#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016468.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016468_Fobs loop_ _publ_author_name 'Ojala, Charles R.' 'Ojala, William H.' 'Britton, Doyle' _publ_section_title ; 4-(4-Chlorobenzylidenehydrazonomethyl)benzonitrile and the bromo and iodo analogs ; _journal_coeditor_code TR3028 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o37 _journal_page_last o40 _journal_volume 64 _journal_year 2008 _space_group_IT_number 1 _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _cell_angle_alpha 99.493 _cell_angle_beta 93.767 _cell_angle_gamma 96.629 _cell_length_a 4.6963 _cell_length_b 6.0023 _cell_length_c 11.5850 _exptl_crystal_F_000 156.00 _reflns_d_resolution_high 0.8384 _[local]_cod_data_source_file tr3028Brsup4.hkl _[local]_cod_data_source_block Br #BEGIN Tags that were not found in dictionaries: _shelx_title 'CN//Br in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 83.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -1 -13 41.67 45.33 3.53 o 1 -1 -13 62.65 57.92 4.22 o -1 0 -13 28.49 30.53 3.02 o 0 0 -13 25.35 27.66 1.88 o 1 0 -13 70.03 73.79 3.28 o 2 0 -13 33.79 35.36 2.21 o -1 1 -13 46.57 47.19 3.58 o 0 1 -13 85.29 82.25 3.38 o 1 1 -13 40.50 42.24 2.34 o 2 1 -13 49.70 50.50 3.76 o -1 2 -13 18.97 21.98 2.57 o 0 2 -13 26.57 24.66 2.66 o 1 2 -13 127.54 119.87 6.55 o 0 3 -13 14.24 12.05 2.23 o 1 3 -13 33.64 35.79 3.15 o 0 -2 -12 42.33 37.72 3.24 o 1 -2 -12 56.54 53.95 3.89 o -1 -1 -12 91.87 101.61 5.54 o 0 -1 -12 118.33 125.81 5.70 o 1 -1 -12 85.42 88.09 5.15 o 2 -1 -12 72.82 66.53 4.42 o -2 0 -12 87.69 83.17 5.28 o -1 0 -12 89.79 85.64 5.06 o 0 0 -12 110.87 115.64 4.39 o 1 0 -12 54.56 57.15 2.70 o 2 0 -12 180.88 184.80 6.30 o 3 0 -12 27.57 28.51 1.99 o -2 1 -12 15.08 17.78 2.46 o -1 1 -12 104.32 104.15 6.05 o 0 1 -12 213.01 207.50 9.59 o 1 1 -12 26.92 26.54 1.79 o 2 1 -12 51.51 52.13 2.56 o 3 1 -12 104.64 97.61 5.64 o -2 2 -12 3.77 4.61 1.64 o -1 2 -12 32.20 32.46 2.91 o 0 2 -12 29.44 31.63 2.86 o 1 2 -12 98.14 97.68 5.61 o 2 2 -12 49.20 56.53 3.89 o -2 3 -12 20.71 25.10 2.72 o -1 3 -12 48.52 51.75 3.73 o 0 3 -12 82.93 84.40 4.94 o 1 3 -12 35.44 34.56 2.97 o 2 3 -12 27.96 25.41 2.73 o -1 4 -12 36.89 37.44 3.28 o 0 4 -12 31.82 33.76 3.19 o 1 4 -12 93.11 93.13 5.70 o 0 -3 -11 26.18 29.83 3.36 o -1 -2 -11 92.94 99.89 5.82 o 0 -2 -11 135.19 136.70 7.62 o 1 -2 -11 57.26 45.80 3.52 o 2 -2 -11 144.07 142.82 7.47 o 3 -2 -11 123.49 136.07 7.38 o -2 -1 -11 29.04 28.75 3.00 o -1 -1 -11 66.19 74.13 3.26 o 0 -1 -11 76.79 77.92 3.17 o 1 -1 -11 11.13 13.02 1.42 o 2 -1 -11 64.35 66.79 2.96 o 3 -1 -11 67.55 63.50 4.24 o -2 0 -11 38.42 39.10 3.39 o -1 0 -11 93.40 95.83 3.69 o 0 0 -11 64.92 64.68 2.84 o 1 0 -11 79.80 74.79 3.10 o 2 0 -11 68.86 69.71 2.99 o 3 0 -11 39.54 44.46 2.41 o -3 1 -11 137.62 136.55 7.58 o -2 1 -11 37.11 39.63 3.28 o -1 1 -11 36.02 39.33 3.03 o 0 1 -11 86.47 91.27 3.47 o 1 1 -11 244.92 240.79 7.62 o 2 1 -11 79.59 75.59 3.22 o 3 1 -11 59.88 62.72 3.92 o -3 2 -11 22.23 27.32 3.15 o -2 2 -11 480.59 434.94 19.50 o -1 2 -11 60.21 61.02 4.02 o 0 2 -11 118.07 106.83 5.52 o 1 2 -11 55.96 52.47 3.56 o 2 2 -11 232.69 214.83 9.94 o 3 2 -11 46.37 47.26 3.45 o -2 3 -11 65.94 71.69 4.71 o -1 3 -11 207.82 197.01 9.73 o 0 3 -11 107.00 109.57 5.95 o 1 3 -11 113.34 100.98 5.74 o 2 3 -11 107.81 97.21 5.49 o -2 4 -11 69.95 70.98 4.76 o -1 4 -11 56.02 58.38 3.95 o 0 4 -11 10.25 12.86 2.17 o 1 4 -11 31.48 35.95 3.13 o 2 4 -11 38.15 39.93 3.38 o -1 5 -11 16.86 21.07 2.67 o 0 5 -11 41.67 43.09 3.47 o -1 -3 -10 51.68 53.93 4.25 o 1 -3 -10 127.40 142.17 7.67 o 2 -3 -10 52.12 60.83 4.31 o -2 -2 -10 29.99 34.46 2.95 o -1 -2 -10 107.36 122.77 6.56 o 0 -2 -10 113.86 124.27 6.71 o 1 -2 -10 186.90 195.96 9.08 o 2 -2 -10 91.45 71.54 4.57 o 3 -2 -10 101.18 106.09 5.81 o -2 -1 -10 86.08 82.05 4.97 o -1 -1 -10 79.52 80.09 3.25 o 0 -1 -10 95.77 92.89 5.66 o 1 -1 -10 398.05 402.29 11.88 o 2 -1 -10 113.53 124.06 4.46 o 3 -1 -10 97.71 101.43 3.87 o -3 0 -10 28.24 29.40 3.05 o -2 0 -10 112.51 112.00 6.38 o -1 0 -10 162.25 164.27 8.19 o 0 0 -10 305.21 302.34 9.18 o 1 0 -10 74.40 70.75 2.98 o 2 0 -10 176.99 167.82 5.55 o 3 0 -10 165.11 162.78 8.60 o 4 0 -10 30.33 35.89 2.99 o -3 1 -10 219.01 203.36 10.18 o -2 1 -10 3.53 5.32 1.55 o -1 1 -10 36.18 37.31 2.93 o 0 1 -10 90.63 97.26 3.61 o 1 1 -10 320.67 303.77 9.45 o 2 1 -10 22.26 25.68 1.65 o 3 1 -10 61.60 66.99 4.16 o 4 1 -10 95.22 90.09 5.38 o -3 2 -10 21.09 25.35 2.82 o -2 2 -10 106.14 95.45 5.75 o 0 2 -10 118.93 113.21 5.79 o 1 2 -10 64.35 58.37 3.75 o 2 2 -10 73.50 71.97 4.25 o 3 2 -10 38.94 43.74 3.17 o -3 3 -10 36.77 37.74 3.56 o -2 3 -10 46.90 50.05 3.73 o -1 3 -10 154.58 156.19 7.58 o 0 3 -10 58.56 58.91 3.74 o 1 3 -10 73.55 70.96 4.31 o 2 3 -10 73.99 76.09 4.41 o 3 3 -10 82.93 77.77 4.64 o -2 4 -10 27.12 27.76 2.75 o -1 4 -10 69.48 75.01 4.49 o 0 4 -10 366.23 366.43 16.54 o 1 4 -10 68.73 67.15 4.20 o 2 4 -10 25.53 27.42 2.65 o -2 5 -10 39.78 43.56 3.45 o -1 5 -10 73.80 80.88 4.93 o 0 5 -10 42.50 46.74 3.53 o 1 5 -10 90.80 98.34 5.60 o -1 -4 -9 48.21 53.39 4.13 o 0 -4 -9 129.73 151.83 8.13 o 1 -4 -9 114.01 125.87 7.05 o 2 -4 -9 58.67 58.24 4.52 o -2 -3 -9 88.40 89.76 5.29 o -1 -3 -9 96.48 100.98 5.84 o 0 -3 -9 146.08 140.45 7.56 o 1 -3 -9 89.31 80.44 5.12 o 2 -3 -9 225.95 234.14 10.82 o 3 -3 -9 115.25 130.30 6.85 o -3 -2 -9 7.76 7.47 1.79 o -2 -2 -9 32.00 32.89 2.78 o -1 -2 -9 83.86 90.88 3.59 o 0 -2 -9 388.20 405.08 11.89 o 1 -2 -9 159.56 166.18 8.59 o 2 -2 -9 143.46 139.37 7.19 o 3 -2 -9 193.08 186.62 8.94 o 4 -2 -9 173.90 178.73 8.79 o -3 -1 -9 76.81 74.13 4.69 o -2 -1 -9 7.94 6.47 1.41 o -1 -1 -9 165.76 163.95 5.51 o 0 -1 -9 96.72 91.84 3.48 o 1 -1 -9 267.81 250.08 7.88 o 2 -1 -9 44.05 44.89 2.11 o 3 -1 -9 138.12 157.72 5.32 o 4 -1 -9 54.72 61.15 2.77 o -3 0 -9 61.46 60.63 4.11 o -2 0 -9 55.43 59.35 3.84 o -1 0 -9 55.79 58.84 3.49 o 0 0 -9 207.00 213.57 6.75 o 1 0 -9 218.91 226.27 7.91 o 2 0 -9 161.01 162.59 5.33 o 3 0 -9 83.74 81.92 3.13 o 4 0 -9 64.16 62.65 3.79 o -3 1 -9 42.34 38.43 3.31 o -2 1 -9 352.33 330.43 14.37 o -1 1 -9 284.97 283.85 8.44 o 0 1 -9 152.87 144.78 4.82 o 1 1 -9 87.61 88.44 3.29 o 2 1 -9 276.74 262.75 11.88 o 3 1 -9 183.44 188.14 8.75 o 4 1 -9 74.50 83.48 4.81 o -3 2 -9 43.60 45.08 3.53 o -2 2 -9 165.09 177.93 8.62 o -1 2 -9 626.74 623.87 26.62 o 0 2 -9 220.31 222.54 9.89 o 1 2 -9 336.42 332.59 14.49 o 2 2 -9 192.05 163.40 7.71 o 3 2 -9 157.58 148.03 7.25 o 4 2 -9 49.67 49.54 3.46 o -3 3 -9 58.49 53.27 4.11 o -2 3 -9 66.42 62.42 4.14 o -1 3 -9 551.91 544.23 22.50 o 0 3 -9 168.62 160.64 8.59 o 1 3 -9 56.85 61.13 3.76 o 2 3 -9 145.02 149.04 7.21 o 3 3 -9 192.81 181.73 8.69 o -3 4 -9 5.32 6.77 1.77 o -2 4 -9 20.33 23.22 2.50 o -1 4 -9 48.59 51.43 3.55 o 0 4 -9 206.15 216.27 10.12 o 1 4 -9 23.31 24.40 2.30 o 2 4 -9 23.65 25.86 2.45 o 3 4 -9 19.50 20.92 2.32 o -2 5 -9 36.90 43.10 3.32 o -1 5 -9 32.98 39.30 3.05 o 0 5 -9 28.42 33.28 2.75 o 1 5 -9 25.20 30.34 2.60 o 2 5 -9 36.85 36.47 2.89 o 0 6 -9 16.69 17.24 2.14 o 1 -5 -8 45.83 45.09 4.08 o -1 -4 -8 39.90 36.82 3.45 o 0 -4 -8 37.69 32.95 3.06 o 1 -4 -8 12.33 18.45 2.67 o 2 -4 -8 91.58 92.89 5.74 o 3 -4 -8 68.39 67.63 4.70 o -2 -3 -8 70.56 77.01 4.97 o -1 -3 -8 99.71 100.96 5.60 o 0 -3 -8 60.11 62.23 4.27 o 1 -3 -8 206.02 204.67 9.47 o 2 -3 -8 87.95 83.28 4.98 o 3 -3 -8 130.71 125.42 6.63 o 4 -3 -8 41.20 40.94 3.47 o -3 -2 -8 73.20 68.66 4.39 o -2 -2 -8 127.96 123.54 4.51 o -1 -2 -8 70.39 71.06 2.96 o 0 -2 -8 166.54 171.37 5.53 o 1 -2 -8 217.66 224.98 10.56 o 2 -2 -8 335.59 360.77 15.23 o 3 -2 -8 113.55 119.82 6.19 o 4 -2 -8 98.22 87.22 5.01 o -3 -1 -8 22.17 27.42 2.67 o -2 -1 -8 288.09 272.97 12.30 o -1 -1 -8 238.98 245.07 10.66 o 0 -1 -8 292.20 292.79 8.85 o 1 -1 -8 181.32 174.96 5.60 o 2 -1 -8 660.18 653.40 19.02 o 3 -1 -8 114.98 111.39 3.93 o 4 -1 -8 169.07 184.91 6.07 o -4 0 -8 105.98 97.47 5.84 o -3 0 -8 88.78 84.53 4.85 o -2 0 -8 132.20 129.71 6.42 o -1 0 -8 197.19 220.51 7.20 o 0 0 -8 131.62 124.38 4.31 o 1 0 -8 408.79 406.77 14.55 o 2 0 -8 340.05 346.09 10.26 o 3 0 -8 281.58 268.06 8.70 o 4 0 -8 77.25 70.48 4.04 o -4 1 -8 56.69 60.37 4.24 o -3 1 -8 31.95 34.25 2.92 o -2 1 -8 209.89 205.79 9.80 o -1 1 -8 172.62 165.75 5.31 o 0 1 -8 50.21 41.94 1.89 o 1 1 -8 116.21 115.64 3.94 o 2 1 -8 183.39 175.88 8.25 o 3 1 -8 118.40 114.05 5.58 o 4 1 -8 9.73 10.95 1.79 o -4 2 -8 30.31 32.53 3.05 o -3 2 -8 89.88 91.67 5.38 o -2 2 -8 139.28 139.70 5.53 o -1 2 -8 56.14 56.27 3.69 o 0 2 -8 86.24 87.09 4.47 o 1 2 -8 144.60 147.26 6.73 o 2 2 -8 164.93 157.07 7.39 o 3 2 -8 60.89 52.95 3.40 o 4 2 -8 44.03 44.57 3.18 o -4 3 -8 67.09 76.04 3.54 o -3 3 -8 40.47 43.55 2.33 o -2 3 -8 87.08 79.78 3.25 o -1 3 -8 116.46 113.27 5.76 o 0 3 -8 583.42 554.62 23.11 o 1 3 -8 91.97 92.06 4.75 o 2 3 -8 45.33 48.87 3.11 o 3 3 -8 54.83 58.61 3.62 o 4 3 -8 110.64 111.52 6.05 o -3 4 -8 209.72 207.51 7.13 o -2 4 -8 97.05 107.72 4.04 o -1 4 -8 36.65 38.18 1.95 o 1 4 -8 772.62 753.73 30.76 o 2 4 -8 96.21 94.70 4.99 o 3 4 -8 49.32 45.25 3.17 o -3 5 -8 37.38 35.38 2.26 o -2 5 -8 134.52 123.83 4.66 o -1 5 -8 105.80 106.59 5.61 o 0 5 -8 96.73 100.39 5.29 o 1 5 -8 88.81 89.87 4.69 o 2 5 -8 118.24 120.69 6.30 o -2 6 -8 22.72 21.48 2.51 o 1 6 -8 79.65 78.38 4.45 o -1 -5 -7 58.75 64.34 4.61 o 0 -5 -7 39.54 49.88 3.94 o 1 -5 -7 147.53 155.80 8.04 o 2 -5 -7 68.88 58.57 4.56 o -2 -4 -7 53.43 57.95 4.16 o -1 -4 -7 59.53 57.80 4.00 o 0 -4 -7 86.73 82.84 5.02 o 1 -4 -7 172.31 165.55 8.32 o 2 -4 -7 209.94 217.66 10.21 o 3 -4 -7 85.04 91.33 5.64 o -3 -3 -7 19.69 21.88 2.42 o -2 -3 -7 33.28 35.07 2.86 o -1 -3 -7 185.36 179.34 8.67 o 0 -3 -7 161.87 165.19 7.98 o 1 -3 -7 83.97 84.87 5.31 o 2 -3 -7 163.56 142.55 7.66 o 3 -3 -7 188.47 173.97 8.33 o 4 -3 -7 182.65 188.43 8.94 o -3 -2 -7 89.13 84.07 4.95 o -2 -2 -7 42.58 38.02 1.98 o -1 -2 -7 168.69 160.18 5.23 o 0 -2 -7 120.23 118.02 4.15 o 1 -2 -7 488.31 490.62 14.26 o 2 -2 -7 12.43 9.23 0.99 o 3 -2 -7 101.14 116.75 6.15 o 4 -2 -7 86.27 81.77 4.87 o -4 -1 -7 37.88 39.84 3.38 o -3 -1 -7 73.37 76.57 4.45 o -2 -1 -7 96.40 107.12 3.87 o -1 -1 -7 51.24 52.11 3.04 o 0 -1 -7 329.80 324.30 9.73 o 1 -1 -7 400.49 397.80 11.58 o 2 -1 -7 284.74 272.29 8.50 o 3 -1 -7 169.41 171.38 5.48 o 4 -1 -7 134.21 142.42 4.82 o -4 0 -7 35.17 32.67 3.12 o -3 0 -7 110.96 103.24 5.63 o -2 0 -7 356.01 321.24 14.19 o -1 0 -7 264.20 251.09 7.56 o 0 0 -7 224.80 215.34 6.51 o 1 0 -7 175.98 179.07 6.12 o 2 0 -7 352.21 354.94 10.47 o 3 0 -7 173.61 181.14 5.83 o 4 0 -7 124.50 131.99 6.26 o -4 1 -7 33.19 37.25 3.20 o -3 1 -7 106.40 108.00 5.74 o -2 1 -7 64.53 68.92 4.11 o -1 1 -7 374.33 359.48 10.88 o 0 1 -7 1049.95 1054.63 29.40 o 1 1 -7 400.64 394.65 11.47 o 2 1 -7 171.78 172.76 7.70 o 3 1 -7 123.74 119.91 5.59 o 4 1 -7 298.41 305.55 13.39 o -4 2 -7 37.49 36.84 3.23 o -3 2 -7 68.19 64.53 4.00 o -2 2 -7 280.05 272.06 12.26 o -1 2 -7 434.94 430.17 12.63 o 0 2 -7 142.98 134.42 4.73 o 1 2 -7 391.98 399.75 12.30 o 2 2 -7 293.68 294.06 8.99 o 3 2 -7 272.28 251.50 10.84 o 4 2 -7 37.41 38.98 2.99 o -4 3 -7 103.78 110.01 5.20 o -3 3 -7 22.65 25.63 1.77 o -2 3 -7 55.79 57.05 2.56 o -1 3 -7 93.02 90.19 3.25 o 0 3 -7 949.57 981.52 28.21 o 2 3 -7 43.45 45.27 2.09 o 3 3 -7 56.40 57.67 3.52 o 4 3 -7 141.85 149.75 7.31 o -4 4 -7 30.03 34.48 2.24 o -3 4 -7 78.94 80.12 3.43 o -2 4 -7 74.80 86.38 3.41 o -1 4 -7 64.04 70.88 2.87 o 0 4 -7 64.78 69.06 2.70 o 1 4 -7 165.82 169.07 5.68 o 2 4 -7 40.75 42.14 2.97 o 3 4 -7 45.29 39.82 2.87 o -3 5 -7 39.74 45.50 3.56 o -2 5 -7 68.10 69.84 2.98 o -1 5 -7 66.77 71.86 2.88 o 0 5 -7 101.20 100.73 3.69 o 1 5 -7 42.87 43.91 2.20 o 2 5 -7 99.49 100.58 3.86 o 3 5 -7 18.65 20.79 2.23 o -2 6 -7 40.98 53.86 3.92 o -1 6 -7 151.21 158.28 7.97 o 0 6 -7 29.40 32.04 3.12 o 1 6 -7 23.18 23.89 2.75 o -1 -5 -6 32.61 28.18 2.96 o 0 -5 -6 83.08 87.00 5.31 o 1 -5 -6 16.81 24.86 2.78 o 2 -5 -6 74.45 80.31 5.30 o 3 -5 -6 75.06 67.10 3.32 o -2 -4 -6 199.28 182.38 9.05 o -1 -4 -6 21.86 21.09 2.53 o 0 -4 -6 143.58 148.55 7.51 o 1 -4 -6 144.50 121.85 6.73 o 3 -4 -6 186.65 176.24 6.08 o 4 -4 -6 47.78 54.93 3.95 o -3 -3 -6 88.52 84.23 4.85 o -2 -3 -6 80.59 80.31 3.18 o -1 -3 -6 146.35 149.26 7.56 o 0 -3 -6 96.01 90.66 4.77 o 1 -3 -6 235.11 252.53 11.28 o 2 -3 -6 167.13 180.05 8.82 o 3 -3 -6 128.87 124.60 4.49 o 4 -3 -6 149.25 136.23 4.91 o -4 -2 -6 8.69 12.75 2.12 o -3 -2 -6 38.67 42.96 3.08 o -2 -2 -6 177.19 173.06 5.57 o -1 -2 -6 323.42 322.60 9.52 o 0 -2 -6 243.32 241.28 7.29 o 1 -2 -6 178.76 168.77 13.26 o 2 -2 -6 306.81 281.03 8.26 o 3 -2 -6 323.62 334.82 8.18 o 4 -2 -6 145.91 158.65 5.25 o -4 -1 -6 58.87 57.32 3.91 o -3 -1 -6 131.68 122.89 6.21 o -2 -1 -6 119.57 120.55 3.97 o -1 -1 -6 222.04 242.15 7.66 o 0 -1 -6 322.90 338.80 11.54 o 1 -1 -6 468.06 493.81 14.08 o 2 -1 -6 432.68 460.63 12.94 o 3 -1 -6 375.40 344.97 8.79 o 4 -1 -6 135.27 122.21 3.53 o 5 -1 -6 148.75 152.30 8.33 o -4 0 -6 127.40 132.56 6.77 o -3 0 -6 114.83 115.05 6.20 o -2 0 -6 146.85 139.16 4.39 o -1 0 -6 969.15 978.49 42.98 o 0 0 -6 86.46 98.89 3.32 o 1 0 -6 162.02 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8 33.28 28.53 3.06 o 1 -6 8 19.41 21.30 2.46 o 2 -6 8 23.47 22.53 2.75 o -2 -5 8 131.39 132.55 7.47 o -1 -5 8 80.64 79.04 5.39 o 0 -5 8 95.14 101.03 5.84 o 1 -5 8 107.03 102.45 5.82 o 2 -5 8 145.37 131.89 7.06 o 3 -5 8 34.47 32.76 3.30 o -3 -4 8 45.98 42.82 3.89 o -2 -4 8 96.08 93.41 5.82 o -1 -4 8 788.28 751.82 31.11 o 0 -4 8 46.31 47.20 2.41 o 1 -4 8 39.95 39.89 2.19 o 2 -4 8 97.03 99.07 6.06 o 3 -4 8 213.23 206.53 10.48 o -4 -3 8 109.49 118.23 7.06 o -3 -3 8 52.89 56.44 4.34 o -2 -3 8 38.82 42.21 3.60 o -1 -3 8 87.68 87.83 3.58 o 0 -3 8 568.25 558.46 16.49 o 1 -3 8 110.96 108.31 4.11 o 2 -3 8 88.15 87.36 5.30 o 3 -3 8 40.40 41.24 3.65 o 4 -3 8 65.78 76.37 5.43 o -4 -2 8 37.39 40.02 3.79 o -3 -2 8 62.35 62.46 4.34 o -2 -2 8 163.85 160.48 8.07 o -1 -2 8 142.29 136.18 5.07 o 0 -2 8 74.76 76.60 3.35 o 1 -2 8 60.76 60.48 2.77 o 2 -2 8 132.75 129.86 7.39 o 3 -2 8 88.09 98.39 6.04 o 4 -2 8 28.43 29.96 2.46 o -3 -1 8 114.17 108.49 6.36 o -2 -1 8 188.45 188.59 6.49 o -1 -1 8 111.37 115.26 6.52 o 1 -1 8 167.20 162.79 8.76 o 2 -1 8 217.61 219.73 10.82 o 3 -1 8 36.47 38.17 3.57 o 4 -1 8 53.76 57.30 3.21 o -4 0 8 71.35 63.86 4.81 o -3 0 8 322.81 324.79 13.32 o -2 0 8 335.96 339.60 15.53 o -1 0 8 411.15 422.65 18.34 o 0 0 8 129.98 139.51 7.34 o 1 0 8 227.06 259.04 11.82 o 2 0 8 125.80 122.04 7.37 o 3 0 8 86.11 73.12 5.35 o 4 0 8 109.96 102.14 4.50 o -3 1 8 110.97 109.09 6.13 o -2 1 8 685.14 678.52 28.01 o -1 1 8 169.78 169.00 8.92 o 0 1 8 286.58 283.58 13.73 o 1 1 8 240.78 255.30 12.37 o 2 1 8 299.73 281.68 13.54 o 3 1 8 21.93 22.85 3.26 o -4 2 8 94.91 83.14 5.32 o -3 2 8 108.14 110.59 6.40 o -2 2 8 330.60 340.10 15.66 o -1 2 8 217.22 227.49 10.99 o 0 2 8 165.25 155.24 8.86 o 1 2 8 64.87 72.68 5.35 o 2 2 8 122.55 134.13 7.87 o -4 3 8 45.50 45.50 3.93 o -3 3 8 127.63 118.68 6.81 o -2 3 8 76.43 72.73 5.07 o -1 3 8 182.83 181.21 9.74 o 0 3 8 70.09 68.27 5.16 o 1 3 8 100.89 94.22 6.41 o 2 3 8 71.17 94.80 6.25 o -3 4 8 76.43 71.86 4.99 o -2 4 8 93.23 93.49 5.98 o -1 4 8 14.10 21.09 2.73 o 0 4 8 30.12 29.93 3.64 o 1 4 8 38.10 41.20 4.20 o -1 5 8 44.55 43.19 4.19 o 1 -6 9 24.36 25.18 2.70 o -2 -5 9 35.65 33.75 3.76 o -1 -5 9 21.38 22.02 2.91 o 0 -5 9 27.71 31.96 3.26 o 1 -5 9 32.07 36.80 3.35 o 2 -5 9 33.90 40.01 3.65 o -3 -4 9 19.69 21.68 2.90 o -2 -4 9 24.65 28.15 3.14 o -1 -4 9 21.42 20.95 2.83 o 0 -4 9 208.38 219.00 7.36 o 1 -4 9 50.28 49.73 3.89 o 2 -4 9 23.79 26.42 3.05 o 3 -4 9 6.58 10.40 2.33 o -3 -3 9 190.76 187.54 9.74 o -2 -3 9 148.62 145.14 7.90 o -1 -3 9 58.69 64.14 4.19 o 0 -3 9 198.56 201.33 6.55 o 1 -3 9 537.72 528.34 16.01 o 2 -3 9 64.31 64.45 4.67 o 3 -3 9 61.86 59.40 4.65 o -4 -2 9 47.92 48.22 4.24 o -2 -2 9 179.07 163.34 8.47 o -1 -2 9 331.43 336.83 10.69 o 0 -2 9 224.13 214.14 7.35 o 1 -2 9 663.26 649.78 19.06 o 2 -2 9 148.44 165.11 9.16 o 3 -2 9 42.73 52.91 4.44 o -4 -1 9 71.90 81.73 5.67 o -2 -1 9 278.81 281.78 12.93 o -1 -1 9 78.67 89.10 5.67 o 0 -1 9 140.76 145.74 8.07 o 1 -1 9 278.82 256.81 13.27 o 2 -1 9 353.82 311.97 15.28 o 3 -1 9 40.94 38.32 3.87 o -4 0 9 57.65 50.88 4.48 o -3 0 9 68.91 67.26 5.05 o -2 0 9 157.63 155.28 8.56 o -1 0 9 218.82 224.75 11.19 o 0 0 9 206.64 214.71 10.94 o 1 0 9 46.24 43.90 4.24 o 2 0 9 51.48 53.45 4.67 o 3 0 9 58.74 54.38 4.81 o -3 1 9 138.21 158.79 8.47 o -1 1 9 273.74 261.39 12.60 o 0 1 9 93.72 95.65 6.07 o 1 1 9 161.84 156.05 8.91 o 2 1 9 5.59 4.58 2.08 o 3 1 9 79.34 70.55 5.51 o -4 2 9 172.14 179.84 9.48 o -3 2 9 197.67 179.20 9.41 o -2 2 9 133.38 144.22 7.98 o -1 2 9 195.89 188.41 9.69 o 0 2 9 388.52 369.84 18.14 o 1 2 9 83.59 83.47 6.12 o 2 2 9 28.52 23.81 3.65 o -3 3 9 115.08 120.11 7.35 o -2 3 9 222.79 214.02 11.20 o -1 3 9 85.57 78.53 5.52 o 0 3 9 165.00 145.38 8.65 o 1 3 9 95.00 95.39 6.73 o 2 3 9 88.48 83.53 6.42 o -2 4 9 59.58 62.66 4.86 o -1 4 9 111.91 115.30 7.37 o 0 4 9 130.94 142.40 8.94 o 1 4 9 46.94 43.06 4.54 o -1 -5 10 95.18 98.89 6.39 o 0 -5 10 48.80 52.37 4.16 o 1 -5 10 68.90 79.73 5.33 o 2 -5 10 40.51 42.74 4.05 o -2 -4 10 26.33 27.94 3.23 o -1 -4 10 65.32 75.06 5.14 o 0 -4 10 362.35 384.58 12.05 o 1 -4 10 68.31 69.84 4.93 o 2 -4 10 24.77 26.11 3.33 o -3 -3 10 79.19 76.76 5.49 o -2 -3 10 73.51 67.97 4.90 o -1 -3 10 71.87 74.10 3.48 o 0 -3 10 58.15 58.32 3.04 o 1 -3 10 142.85 143.19 8.27 o 2 -3 10 44.51 55.49 4.61 o 3 -3 10 35.21 38.97 4.11 o -3 -2 10 33.22 30.48 3.41 o -2 -2 10 75.76 72.62 4.95 o -1 -2 10 63.16 61.85 5.25 o 0 -2 10 116.78 109.77 4.55 o 1 -2 10 28.60 24.09 2.03 o 2 -2 10 113.52 109.61 6.81 o 3 -2 10 19.39 22.02 3.38 o -4 -1 10 103.12 104.72 6.65 o -3 -1 10 64.21 67.40 4.95 o -2 -1 10 27.87 29.30 2.26 o -1 -1 10 325.92 321.62 14.72 o 0 -1 10 94.97 103.95 6.48 o 1 -1 10 37.09 37.32 3.80 o 2 -1 10 7.70 11.11 2.62 o 3 -1 10 220.03 210.45 11.32 o -4 0 10 32.48 35.84 3.76 o -3 0 10 163.09 168.33 9.16 o -2 0 10 187.07 157.12 8.89 o -1 0 10 83.27 79.53 5.37 o 0 0 10 300.66 289.71 14.40 o 1 0 10 164.04 169.69 9.36 o 2 0 10 121.05 124.16 7.65 o 3 0 10 35.75 36.52 4.16 o -3 1 10 97.37 104.67 6.59 o -2 1 10 117.02 129.25 7.66 o -1 1 10 404.13 375.27 18.18 o 0 1 10 93.95 99.60 6.49 o 1 1 10 73.13 74.44 5.71 o 2 1 10 84.56 82.39 6.12 o 3 1 10 118.69 104.86 7.15 o -3 2 10 97.01 90.75 6.42 o -2 2 10 84.04 71.97 5.49 o -1 2 10 172.92 171.76 10.16 o 0 2 10 117.82 125.58 7.81 o 1 2 10 106.98 114.85 7.68 o 2 2 10 29.01 26.96 3.97 o -2 3 10 56.89 63.10 4.99 o -1 3 10 125.47 139.64 8.64 o 1 3 10 59.54 61.30 5.32 o 0 -5 11 41.11 43.23 4.02 o 1 -5 11 16.07 13.48 2.77 o -2 -4 11 38.43 42.04 4.03 o -1 -4 11 36.77 43.23 3.98 o 0 -4 11 11.41 13.06 1.82 o 1 -4 11 53.13 52.75 4.59 o 2 -4 11 71.38 77.52 5.70 o -3 -3 11 36.06 34.70 3.87 o -2 -3 11 102.39 95.59 6.22 o -1 -3 11 113.23 105.63 4.55 o 0 -3 11 109.98 109.09 4.65 o 1 -3 11 228.66 212.03 10.86 o 2 -3 11 60.06 66.51 5.57 o -3 -2 11 47.44 47.76 4.39 o -2 -2 11 240.30 204.49 10.58 o -1 -2 11 46.72 45.59 2.95 o 0 -2 11 110.94 96.69 7.86 o 1 -2 11 60.89 56.33 4.85 o 2 -2 11 491.72 459.48 20.86 o -3 -1 11 53.29 47.48 4.54 o -2 -1 11 82.17 88.87 5.70 o -1 -1 11 244.06 232.55 11.93 o 0 -1 11 83.74 88.75 6.05 o 1 -1 11 30.59 29.17 3.77 o 2 -1 11 36.63 34.77 4.19 o 3 -1 11 133.72 132.01 8.54 o -3 0 11 41.02 48.93 4.36 o -2 0 11 62.79 66.60 5.20 o -1 0 11 69.20 70.87 5.43 o 0 0 11 66.09 74.17 5.32 o 1 0 11 91.67 93.69 6.64 o 2 0 11 36.53 32.15 4.13 o -3 1 11 62.94 61.67 5.23 o -2 1 11 69.89 67.96 5.44 o 0 1 11 73.61 71.51 5.56 o 1 1 11 69.16 89.87 6.19 o 2 1 11 26.72 26.90 3.99 o -3 2 11 121.89 137.08 8.43 o -2 2 11 142.44 138.26 8.68 o -1 2 11 46.01 38.56 4.21 o 0 2 11 159.27 159.03 9.12 o 1 2 11 92.11 96.76 6.84 o -1 3 11 131.91 138.08 8.96 o 0 3 11 25.53 28.40 4.12 o -1 -4 12 98.03 102.46 6.63 o 0 -4 12 26.72 31.25 2.57 o 1 -4 12 35.34 40.19 4.28 o -2 -3 12 25.61 26.20 3.50 o -1 -3 12 35.59 34.49 3.65 o 0 -3 12 81.34 75.58 3.87 o 1 -3 12 46.47 42.28 4.40 o 2 -3 12 18.25 19.03 3.41 o -2 -2 12 49.36 47.31 4.23 o -1 -2 12 99.74 98.60 4.53 o 0 -2 12 30.65 32.11 2.48 o 1 -2 12 31.20 29.97 3.82 o 2 -2 12 2.08 3.33 2.33 o -3 -1 12 104.95 97.99 6.74 o -2 -1 12 46.81 45.82 3.11 o 0 -1 12 211.20 195.45 10.80 o 1 -1 12 107.37 120.20 7.56 o 2 -1 12 13.14 13.20 3.12 o -2 0 12 180.09 185.62 10.26 o -1 0 12 51.63 55.36 4.91 o 0 0 12 121.76 131.77 7.80 o 1 0 12 83.96 85.66 6.24 o 2 0 12 86.12 80.15 6.38 o -2 1 12 72.57 68.10 5.49 o -1 1 12 84.45 88.04 6.32 o 0 1 12 120.42 119.78 7.89 o 1 1 12 93.11 91.32 6.76 o -1 2 12 52.39 50.33 5.06 o 0 2 12 33.25 33.13 4.31 o -1 -3 13 29.12 24.21 3.27 o 0 -3 13 15.83 13.47 1.89 o 1 -3 13 110.23 106.83 7.30 o -1 -2 13 127.94 119.79 6.75 o 0 -2 13 23.61 23.78 2.46 o 1 -2 13 19.50 19.82 3.56 o -2 -1 13 46.41 47.75 3.22 o -1 -1 13 40.84 42.59 4.19 o 0 -1 13 82.33 80.77 6.06 o 1 -1 13 45.46 44.05 4.71 o -2 0 13 39.91 40.06 4.40 o -1 0 13 70.41 80.97 6.07 o 0 0 13 20.74 22.62 3.63 o 1 0 13 29.78 31.22 4.09 o -1 1 13 67.42 70.62 5.85 o 0 1 13 42.71 43.11 4.51 o