#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016477.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016477_Fobs loop_ _publ_author_name 'Brito, Iv\'an' 'Mundaca, Aldo' 'C\'ardenas, Alejandro' 'L\'opez-Rodr\'iguez, Mat\'ias' _publ_section_title ; 3,3'-Dinitro-2,2'-dithiodipyridine ; _journal_coeditor_code FA3134 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o117 _journal_page_last o118 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.339 _cell_angle_gamma 90.000 _cell_length_a 3.8320 _cell_length_b 21.4002 _cell_length_c 7.8301 _exptl_crystal_F_000 316.00 _reflns_d_resolution_high 0.7746 _[local]_cod_data_source_file fa3134Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_F_calc_maximum 99.46 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 204.63 217.22 6.27 o 3 0 0 105.84 108.10 7.11 o 4 0 0 99.72 112.50 8.72 o 1 1 0 1515.71 1604.27 52.47 o 2 1 0 62.86 68.29 3.38 o 3 1 0 47.96 56.08 1.98 o 4 1 0 1.54 5.77 2.06 o 1 2 0 8391.35 7804.01 240.45 o 2 2 0 145.38 156.27 3.68 o 3 2 0 171.42 167.00 3.91 o 4 2 0 126.70 131.96 6.30 o 1 3 0 3625.25 3560.81 138.56 o 2 3 0 293.04 288.51 6.62 o 3 3 0 87.50 97.36 3.91 o 4 3 0 2.18 8.45 1.29 o 1 4 0 579.26 558.36 13.61 o 2 4 0 35.50 38.93 1.16 o 3 4 0 4.11 9.76 1.30 o 4 4 0 42.94 43.88 4.03 o 1 5 0 435.28 496.47 10.53 o 2 5 0 1837.51 1795.06 45.82 o 3 5 0 65.25 58.38 2.66 o 4 5 0 34.39 33.77 2.78 o 1 6 0 2986.15 2978.11 38.56 o 2 6 0 4.21 11.93 2.13 o 3 6 0 22.57 25.24 4.03 o 4 6 0 14.51 18.76 2.54 o 1 7 0 1173.31 1151.28 20.97 o 2 7 0 162.25 147.35 3.15 o 3 7 0 134.14 144.04 5.91 o 4 7 0 1.27 8.50 2.54 o 1 8 0 754.90 812.37 12.46 o 2 8 0 137.31 134.25 2.93 o 3 8 0 22.12 18.45 1.82 o 4 8 0 4.88 9.76 4.78 o 1 9 0 1269.22 1305.84 31.01 o 2 9 0 109.20 101.32 2.42 o 3 9 0 54.29 52.32 2.43 o 4 9 0 5.54 12.98 5.98 o 1 10 0 222.62 220.15 9.83 o 2 10 0 95.92 89.18 2.51 o 3 10 0 80.30 86.10 7.13 o 4 10 0 46.48 57.32 6.18 o 1 11 0 265.70 283.70 18.30 o 2 11 0 211.58 198.06 4.49 o 3 11 0 6.96 9.44 2.77 o 4 11 0 0.36 13.61 6.75 o 1 12 0 675.00 636.88 20.03 o 2 12 0 69.31 67.75 3.65 o 3 12 0 17.72 18.32 1.82 o 4 12 0 93.40 83.92 14.34 o 1 13 0 10.25 7.82 1.43 o 2 13 0 68.27 76.43 6.10 o 3 13 0 9.29 9.15 1.76 o 4 13 0 0.09 -2.95 5.11 o 1 14 0 145.06 132.13 9.33 o 2 14 0 13.54 14.25 1.58 o 3 14 0 144.60 143.43 9.01 o 4 14 0 17.03 19.56 5.64 o 1 15 0 39.14 37.99 2.97 o 2 15 0 30.14 32.81 4.30 o 3 15 0 3.26 1.62 1.97 o 0 16 0 759.90 824.08 36.62 o 1 16 0 4.03 8.93 7.53 o 2 16 0 8.07 7.48 1.71 o 3 16 0 27.03 27.08 5.77 o 1 17 0 27.13 35.34 2.48 o 2 17 0 163.80 166.04 7.34 o 3 17 0 39.90 44.05 5.95 o 0 18 0 1.45 -1.48 2.00 o 1 18 0 97.89 97.80 5.63 o 2 18 0 15.32 20.31 3.53 o 3 18 0 23.28 15.22 2.96 o 1 19 0 337.41 343.28 11.85 o 2 19 0 179.64 177.35 9.58 o 3 19 0 71.73 70.50 11.97 o 0 20 0 7.38 16.02 2.93 o 1 20 0 60.39 58.17 3.88 o 2 20 0 3.21 3.04 1.68 o 3 20 0 0.40 -1.34 4.01 o 1 21 0 179.74 169.37 9.29 o 2 21 0 225.49 199.62 12.40 o 3 21 0 10.50 3.56 2.73 o 0 22 0 431.98 407.05 42.21 o 1 22 0 125.94 115.09 15.36 o 2 22 0 0.84 0.43 2.47 o 1 23 0 8.87 4.22 2.50 o 2 23 0 28.04 33.97 6.02 o 0 24 0 412.05 363.35 26.43 o 1 24 0 121.09 115.90 16.05 o 2 24 0 0.01 3.42 2.10 o 1 25 0 3.88 3.50 5.38 o 0 26 0 21.13 25.91 7.13 o 1 26 0 103.97 98.71 11.09 o -4 1 1 220.10 214.42 9.08 o -3 1 1 68.96 75.02 3.22 o -2 1 1 10.74 10.62 0.77 o 0 1 1 3177.00 2896.12 89.72 o 1 1 1 10.01 7.26 0.58 o 2 1 1 220.02 221.01 4.51 o 3 1 1 714.80 683.98 17.33 o 4 1 1 89.21 78.08 9.71 o -4 2 1 2.70 6.96 1.24 o -3 2 1 521.66 522.12 13.86 o -2 2 1 10.03 17.99 3.28 o 1 2 1 190.05 198.49 5.66 o 2 2 1 384.82 387.08 8.53 o 3 2 1 7.02 17.87 2.13 o 4 2 1 3.85 10.48 3.47 o -4 3 1 44.15 52.21 2.95 o -3 3 1 227.19 231.55 9.86 o -2 3 1 1.29 8.58 1.99 o -1 3 1 9891.64 9423.68 288.99 o 1 3 1 645.16 621.27 9.53 o 2 3 1 280.99 268.05 8.03 o 3 3 1 69.75 70.19 2.79 o 4 3 1 306.62 290.47 25.67 o -4 4 1 53.48 62.28 3.70 o -3 4 1 217.74 204.61 9.60 o -2 4 1 3469.76 3464.55 62.99 o -1 4 1 3645.52 3712.21 83.54 o 1 4 1 1613.93 1561.17 20.88 o 2 4 1 106.85 106.35 4.34 o 3 4 1 71.23 67.83 3.26 o 4 4 1 9.15 17.10 3.40 o -4 5 1 3.93 6.81 1.07 o -3 5 1 10.35 18.09 4.53 o -2 5 1 429.98 447.86 9.60 o -1 5 1 6.94 4.73 1.89 o 0 5 1 2396.62 2309.50 76.03 o 1 5 1 0.79 0.73 0.65 o 2 5 1 14.41 16.92 3.05 o 3 5 1 14.63 20.63 5.13 o 4 5 1 4.01 12.61 3.06 o -4 6 1 11.21 10.85 1.47 o -3 6 1 536.33 511.46 19.56 o -2 6 1 4656.96 4582.63 82.84 o -1 6 1 56.99 60.03 2.00 o 1 6 1 309.19 284.81 5.73 o 2 6 1 598.78 575.01 12.71 o 3 6 1 87.84 90.58 9.51 o 4 6 1 78.79 74.47 7.91 o -4 7 1 10.72 13.44 1.88 o -3 7 1 136.34 135.30 4.97 o -2 7 1 138.72 151.54 4.17 o -1 7 1 254.30 284.82 5.51 o 0 7 1 177.96 183.97 5.20 o 1 7 1 94.93 94.08 2.88 o 2 7 1 292.95 287.10 6.55 o 3 7 1 7.53 11.58 4.23 o 4 7 1 172.81 141.30 13.01 o -4 8 1 48.56 50.35 3.35 o -3 8 1 631.34 584.05 18.86 o -2 8 1 151.95 181.12 5.56 o -1 8 1 1146.01 1181.00 27.81 o 0 8 1 233.51 221.67 9.46 o 1 8 1 722.40 714.34 18.77 o 2 8 1 163.42 154.43 3.67 o 3 8 1 41.74 47.50 3.30 o 4 8 1 24.68 32.67 6.71 o -4 9 1 50.63 61.23 3.81 o -3 9 1 86.09 90.02 5.53 o -2 9 1 382.45 365.32 6.86 o -1 9 1 55.08 49.94 1.74 o 0 9 1 281.72 268.73 15.57 o 1 9 1 6.00 2.83 1.11 o 2 9 1 17.74 18.88 1.45 o 3 9 1 546.69 530.18 25.28 o 4 9 1 11.16 12.49 6.34 o -4 10 1 18.65 19.83 10.82 o -3 10 1 0.02 3.87 2.08 o -2 10 1 122.49 109.62 3.86 o -1 10 1 203.48 220.71 4.68 o 1 10 1 67.06 67.56 3.83 o 2 10 1 31.95 27.25 2.18 o 3 10 1 6.36 15.95 7.05 o 4 10 1 9.02 14.98 5.20 o -4 11 1 92.29 106.64 9.33 o -3 11 1 105.54 96.61 7.80 o -2 11 1 26.24 25.38 2.24 o -1 11 1 451.46 412.11 7.82 o 1 11 1 0.47 1.50 1.22 o 2 11 1 295.06 284.68 8.01 o 3 11 1 33.15 46.71 5.70 o 4 11 1 30.36 19.87 6.97 o -4 12 1 6.62 7.80 8.68 o -3 12 1 5.02 8.51 1.50 o -2 12 1 21.65 21.86 1.34 o -1 12 1 202.53 198.99 5.15 o 0 12 1 14.37 20.79 3.41 o 1 12 1 341.15 324.73 13.35 o 2 12 1 0.71 6.44 1.43 o 3 12 1 14.72 19.00 4.95 o 4 12 1 1.98 -0.29 5.62 o -4 13 1 19.60 39.23 10.29 o -3 13 1 31.09 37.28 2.65 o -2 13 1 210.58 198.28 8.33 o -1 13 1 1793.81 1852.79 39.12 o 0 13 1 276.02 282.20 13.72 o 1 13 1 182.12 176.81 6.80 o 2 13 1 183.22 191.18 8.36 o 3 13 1 106.48 102.42 6.60 o -4 14 1 39.11 44.56 6.85 o -3 14 1 34.47 41.59 2.81 o -2 14 1 167.79 175.99 7.48 o -1 14 1 8.36 9.14 1.54 o 0 14 1 2.52 4.06 1.60 o 1 14 1 91.54 104.95 5.97 o 2 14 1 21.54 20.52 1.62 o 3 14 1 4.86 8.83 1.88 o -4 15 1 45.06 50.30 5.94 o -3 15 1 81.06 78.34 7.14 o -2 15 1 284.89 276.30 8.25 o -1 15 1 223.56 190.77 7.71 o 0 15 1 582.13 596.96 15.36 o 1 15 1 3.05 4.08 1.66 o 2 15 1 0.09 0.23 0.67 o 3 15 1 220.42 198.31 10.29 o -3 16 1 213.29 192.66 15.13 o -2 16 1 365.23 342.00 11.22 o -1 16 1 4.35 7.14 2.79 o 0 16 1 33.37 48.75 3.34 o 1 16 1 243.43 282.50 8.56 o 2 16 1 129.86 122.68 7.13 o 3 16 1 0.66 10.05 3.39 o -3 17 1 0.54 12.74 14.05 o -2 17 1 125.79 112.02 5.27 o -1 17 1 18.59 16.24 2.68 o 0 17 1 66.57 72.36 3.68 o 1 17 1 12.93 16.43 2.06 o 2 17 1 27.09 28.01 2.14 o 3 17 1 1.30 6.23 3.89 o -3 18 1 162.98 166.03 15.71 o -2 18 1 223.80 203.25 11.98 o -1 18 1 61.08 57.53 3.63 o 0 18 1 177.29 195.29 10.83 o 1 18 1 102.50 103.91 4.30 o 2 18 1 124.39 115.63 7.93 o 3 18 1 11.54 13.72 4.16 o -3 19 1 21.20 27.46 6.50 o -2 19 1 38.91 29.40 3.83 o -1 19 1 46.71 43.51 3.50 o 0 19 1 38.24 53.86 7.55 o 1 19 1 7.56 12.99 1.85 o 2 19 1 1.91 5.79 3.52 o 3 19 1 4.87 2.75 4.26 o -3 20 1 25.35 24.34 6.88 o -2 20 1 51.79 50.73 12.37 o -1 20 1 174.69 155.62 7.05 o 0 20 1 4.97 11.56 3.83 o 1 20 1 343.82 332.52 14.03 o 2 20 1 80.75 83.28 7.09 o 3 20 1 0.35 13.83 11.14 o -3 21 1 4.89 5.28 8.97 o -2 21 1 0.97 3.38 2.31 o -1 21 1 169.88 170.69 16.00 o 0 21 1 8.34 18.72 4.85 o 1 21 1 1.77 3.80 5.29 o 2 21 1 25.78 27.67 3.89 o -2 22 1 114.73 125.50 9.48 o -1 22 1 0.03 2.28 2.11 o 0 22 1 0.01 0.70 3.32 o 1 22 1 63.73 67.80 5.37 o 2 22 1 171.75 146.29 22.84 o -2 23 1 22.38 29.19 3.95 o -1 23 1 3.25 7.16 3.61 o 0 23 1 274.21 264.97 14.14 o 1 23 1 17.36 17.98 2.63 o 2 23 1 56.73 44.54 7.55 o -2 24 1 5.12 4.77 4.52 o -1 24 1 3.53 10.55 3.05 o 0 24 1 26.89 25.77 2.95 o 1 24 1 23.49 23.92 3.19 o 2 24 1 5.29 13.61 4.43 o -2 25 1 0.86 4.52 2.26 o -1 25 1 203.82 193.90 17.40 o 0 25 1 68.09 58.64 6.73 o 1 25 1 34.84 41.16 9.18 o -1 26 1 17.97 16.87 3.32 o 0 26 1 7.14 9.08 3.93 o 1 26 1 10.17 9.53 2.84 o 0 27 1 69.62 82.31 9.60 o -4 0 2 308.43 297.44 21.78 o -3 0 2 19.81 20.13 1.61 o -2 0 2 257.39 250.08 14.12 o 0 0 2 2399.12 2385.33 76.43 o 1 0 2 96.31 124.17 4.21 o 2 0 2 223.80 209.34 17.01 o 3 0 2 586.77 545.38 24.56 o 4 0 2 5.82 0.72 3.04 o -4 1 2 15.95 20.35 1.54 o -3 1 2 88.90 90.72 3.14 o -2 1 2 163.98 164.06 3.17 o -1 1 2 63.46 65.37 2.90 o 1 1 2 521.59 520.01 15.22 o 2 1 2 826.22 807.14 17.67 o 3 1 2 0.29 12.36 3.27 o 4 1 2 4.33 12.15 3.30 o -4 2 2 79.96 85.59 4.32 o -3 2 2 50.31 57.66 2.53 o -2 2 2 33.00 26.37 0.78 o -1 2 2 1410.78 1333.69 30.95 o 0 2 2 24.91 31.79 6.81 o 1 2 2 0.11 6.25 1.79 o 2 2 2 241.13 260.70 7.29 o 3 2 2 129.61 121.38 4.61 o 4 2 2 51.71 56.89 11.77 o -4 3 2 16.26 21.91 2.01 o -3 3 2 141.29 145.99 7.54 o -2 3 2 58.26 62.65 1.63 o -1 3 2 6.77 4.80 0.81 o 0 3 2 346.60 347.02 17.87 o 1 3 2 2031.64 2059.61 38.37 o 2 3 2 512.06 507.64 17.07 o 3 3 2 3.86 2.95 1.29 o 4 3 2 0.45 12.73 5.18 o -4 4 2 7.95 9.39 2.40 o -3 4 2 0.21 4.67 1.63 o -2 4 2 28.19 26.84 1.29 o -1 4 2 31.78 32.21 1.37 o 0 4 2 353.90 345.03 7.37 o 1 4 2 457.91 517.57 10.39 o 2 4 2 369.02 354.56 9.18 o 3 4 2 3.80 8.66 3.11 o 4 4 2 36.86 42.33 5.95 o -4 5 2 59.46 52.80 3.35 o -3 5 2 4.40 4.64 1.33 o -2 5 2 369.18 358.26 7.28 o -1 5 2 501.82 476.80 7.76 o 0 5 2 328.20 350.19 6.12 o 1 5 2 2118.32 2161.53 32.39 o 2 5 2 21.45 21.40 1.45 o 3 5 2 78.20 83.18 4.79 o 4 5 2 11.44 14.16 5.27 o -4 6 2 3.71 5.44 1.54 o -3 6 2 9.70 12.99 1.46 o -2 6 2 204.46 212.06 4.10 o -1 6 2 487.70 508.77 8.15 o 0 6 2 106.07 118.76 2.46 o 1 6 2 166.30 195.42 3.85 o 2 6 2 0.68 1.44 1.07 o 3 6 2 193.80 170.19 10.48 o 4 6 2 7.02 4.09 3.53 o -4 7 2 30.96 39.57 2.79 o -3 7 2 656.35 627.57 19.89 o -2 7 2 423.86 413.20 9.24 o -1 7 2 1.18 0.26 0.85 o 0 7 2 2670.32 2703.50 32.24 o 1 7 2 405.44 386.89 7.96 o 2 7 2 345.90 325.42 7.37 o 3 7 2 0.00 2.77 2.51 o 4 7 2 52.77 63.26 9.59 o -4 8 2 0.52 9.77 3.87 o -3 8 2 149.41 149.65 6.20 o -2 8 2 2.01 1.98 1.01 o -1 8 2 5.56 8.64 1.26 o 0 8 2 43.56 46.81 1.36 o 1 8 2 201.13 203.17 5.20 o 2 8 2 21.71 23.63 1.13 o 3 8 2 39.11 46.17 2.77 o 4 8 2 9.43 23.69 4.79 o -4 9 2 199.96 206.85 9.71 o -3 9 2 726.53 714.31 25.81 o -2 9 2 252.60 256.47 7.59 o -1 9 2 49.58 47.65 1.78 o 0 9 2 633.61 650.55 11.06 o 1 9 2 940.40 953.91 28.31 o 2 9 2 430.60 422.40 9.41 o 3 9 2 115.53 119.38 7.41 o 4 9 2 59.31 92.77 18.71 o -4 10 2 212.72 181.11 11.37 o -3 10 2 21.83 20.46 2.81 o -2 10 2 130.72 138.27 5.79 o -1 10 2 1060.64 1016.15 28.15 o 0 10 2 1.51 2.17 0.87 o 1 10 2 80.67 88.43 2.99 o 2 10 2 357.80 363.83 10.82 o 3 10 2 427.00 414.25 21.07 o -4 11 2 46.07 50.51 8.46 o -3 11 2 43.51 39.62 2.48 o -2 11 2 225.80 224.73 7.71 o -1 11 2 47.66 42.58 1.83 o 0 11 2 0.58 1.11 1.01 o 1 11 2 210.52 214.42 5.32 o 2 11 2 19.76 27.73 2.32 o 3 11 2 1.22 7.16 2.55 o -4 12 2 243.74 227.93 14.49 o -3 12 2 62.85 68.59 4.99 o -2 12 2 111.95 106.65 4.20 o -1 12 2 312.25 296.59 10.47 o 0 12 2 306.29 314.52 7.97 o 1 12 2 6.67 6.11 1.79 o 2 12 2 1638.58 1619.34 43.36 o 3 12 2 210.10 204.90 10.91 o -4 13 2 49.46 42.46 6.11 o -3 13 2 38.22 39.04 2.69 o -2 13 2 42.99 45.85 5.40 o -1 13 2 63.05 63.70 2.31 o 0 13 2 34.06 33.13 2.25 o 1 13 2 149.36 150.09 3.55 o 2 13 2 101.84 106.95 5.57 o 3 13 2 5.15 8.06 2.96 o -4 14 2 0.33 8.70 2.49 o -3 14 2 114.89 110.20 9.22 o -2 14 2 404.60 395.86 11.28 o -1 14 2 443.79 429.24 10.21 o 0 14 2 53.50 57.78 3.33 o 1 14 2 430.96 447.81 15.83 o 2 14 2 15.53 15.43 1.40 o 3 14 2 209.07 188.21 17.08 o -4 15 2 56.39 49.53 7.74 o -3 15 2 203.58 189.82 8.94 o -2 15 2 40.63 47.62 4.29 o -1 15 2 2.43 4.39 1.75 o 0 15 2 103.15 105.60 5.59 o 1 15 2 641.32 663.90 29.73 o 2 15 2 3.47 5.45 1.30 o 3 15 2 0.58 1.52 4.27 o -4 16 2 11.21 18.52 4.11 o -3 16 2 11.15 13.75 2.13 o -2 16 2 32.40 44.40 2.69 o -1 16 2 203.60 189.72 6.00 o 0 16 2 191.69 188.18 5.71 o 1 16 2 1.38 0.28 1.55 o 2 16 2 23.98 31.35 3.09 o 3 16 2 15.61 17.04 3.63 o -3 17 2 148.75 143.85 9.03 o -2 17 2 358.69 359.21 15.51 o -1 17 2 15.68 16.65 1.80 o 0 17 2 804.24 837.05 22.37 o 1 17 2 65.17 75.27 5.09 o 2 17 2 96.33 96.02 5.00 o 3 17 2 2.36 10.08 3.60 o -3 18 2 36.94 32.68 4.29 o -2 18 2 0.28 5.52 1.76 o -1 18 2 99.51 101.01 5.57 o 0 18 2 18.39 18.20 2.72 o 1 18 2 357.99 353.96 13.97 o 2 18 2 2.35 -0.24 1.92 o 3 18 2 4.92 15.98 5.47 o -3 19 2 158.34 168.89 15.62 o -2 19 2 39.47 42.80 3.23 o -1 19 2 1.66 2.39 1.41 o 0 19 2 101.85 103.69 4.35 o 1 19 2 646.61 645.95 21.91 o 2 19 2 121.47 121.33 6.83 o -3 20 2 10.81 5.70 9.49 o -2 20 2 5.93 6.57 4.46 o -1 20 2 123.31 135.91 5.43 o 0 20 2 33.02 28.48 4.46 o 1 20 2 4.53 7.62 2.86 o 2 20 2 195.11 200.53 14.53 o -3 21 2 40.80 43.68 8.54 o -2 21 2 30.19 32.55 4.10 o -1 21 2 0.40 -0.45 2.00 o 0 21 2 20.83 25.74 2.69 o 1 21 2 109.49 105.97 8.87 o 2 21 2 77.26 59.61 7.42 o -2 22 2 98.35 95.78 9.05 o -1 22 2 46.75 50.06 11.46 o 0 22 2 85.94 90.91 7.90 o 1 22 2 0.77 -2.80 2.80 o 2 22 2 104.93 82.15 9.53 o -2 23 2 16.60 5.33 3.31 o -1 23 2 1.85 -0.37 5.81 o 0 23 2 15.48 20.62 4.01 o 1 23 2 8.26 8.29 3.37 o 2 23 2 6.93 2.61 4.87 o -2 24 2 55.01 53.29 5.20 o -1 24 2 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