#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:13:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180833 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/64/2016484.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016484_Fobs loop_ _publ_author_name 'Smith, Graham' 'Wermuth, Urs D.' 'White, Jonathan M.' _publ_section_title ; One-dimensional hydrogen-bonded structures in the 1:1 proton-transfer compounds of 4,5-dichlorophthalic acid with 8-hydroxyquinoline, 8-aminoquinoline and quinoline-2-carboxylic acid (quinaldic acid) ; _journal_coeditor_code GD3186 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o180 _journal_page_last o183 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8915 _cell_length_b 7.2887 _cell_length_c 30.8009 _exptl_crystal_F_000 776.00 _reflns_d_resolution_high 0.8043 _cod_data_source_file gd3186Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jmwgs119 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 256.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1221.14 1194.98 24.85 o 4 0 0 139.45 140.07 4.97 o 6 0 0 447.54 447.70 11.16 o 8 0 0 457.04 483.69 6.83 o 1 1 0 75.66 84.80 4.07 o 2 1 0 1496.23 1699.99 7.88 o 3 1 0 662.18 687.88 5.82 o 4 1 0 353.61 342.09 12.92 o 5 1 0 257.86 230.61 7.55 o 6 1 0 982.81 936.20 9.86 o 7 1 0 54.06 58.80 1.91 o 8 1 0 18.40 22.82 2.25 o 0 2 0 34877.92 38444.39 259.74 o 1 2 0 4120.00 4257.03 20.13 o 2 2 0 704.31 792.13 8.44 o 3 2 0 16.15 19.82 2.84 o 4 2 0 26.53 16.08 3.61 o 5 2 0 827.26 744.26 13.41 o 6 2 0 174.73 159.59 2.72 o 7 2 0 1747.17 1751.25 31.46 o 8 2 0 31.48 28.80 2.38 o 2 3 0 2145.20 2405.31 16.22 o 3 3 0 13.74 13.68 4.25 o 4 3 0 2242.68 2218.16 21.62 o 5 3 0 86.18 83.20 7.70 o 6 3 0 77.72 86.60 3.01 o 7 3 0 343.19 361.05 6.13 o 2 4 0 13207.99 15075.67 501.93 o 3 4 0 280.66 324.35 5.01 o 4 4 0 185.23 159.44 21.91 o 5 4 0 1290.22 1300.82 44.21 o 6 4 0 163.01 172.70 3.84 o 7 4 0 101.05 112.74 3.24 o 1 5 0 97.81 95.94 1.58 o 2 5 0 183.67 196.52 3.67 o 3 5 0 99.06 101.31 6.99 o 4 5 0 6.08 5.28 2.67 o 5 5 0 14.00 15.73 4.96 o 6 5 0 0.25 1.58 4.26 o 7 5 0 314.50 388.10 5.72 o 0 6 0 2055.06 1938.25 53.00 o 1 6 0 45.34 48.19 1.59 o 2 6 0 5775.12 6011.15 253.05 o 3 6 0 2004.99 1951.29 78.67 o 4 6 0 14.46 22.85 3.38 o 5 6 0 83.44 92.73 9.10 o 6 6 0 141.42 147.32 4.05 o 1 7 0 6.41 6.77 1.71 o 2 7 0 391.48 418.44 8.21 o 3 7 0 11.10 13.24 1.87 o 4 7 0 91.61 97.54 3.19 o 5 7 0 156.11 142.48 3.77 o 0 8 0 248.25 213.12 4.95 o 1 8 0 0.01 5.84 3.71 o 2 8 0 7.38 8.58 2.46 o 3 8 0 316.42 390.99 5.17 o 1 0 1 4757.86 4251.04 13.44 o 2 0 1 1.63 4.05 1.09 o 3 0 1 1751.36 1887.41 8.66 o 4 0 1 12.60 14.18 2.58 o 5 0 1 31.55 31.05 4.21 o 6 0 1 1818.51 1997.37 73.73 o 7 0 1 1032.33 987.72 15.93 o 8 0 1 286.88 327.20 4.05 o -8 1 1 46.61 48.22 1.93 o -7 1 1 614.09 605.05 15.45 o -6 1 1 398.71 415.68 12.97 o -5 1 1 1728.62 1644.03 19.11 o -4 1 1 541.13 546.28 27.29 o -3 1 1 2036.33 2083.61 32.63 o -2 1 1 141.31 169.17 1.39 o -1 1 1 1966.88 2043.84 14.12 o 0 1 1 711.56 763.53 3.49 o 2 1 1 132.51 157.58 1.34 o 3 1 1 1891.93 1937.57 23.36 o 4 1 1 542.96 522.63 14.69 o 5 1 1 1632.34 1547.26 18.50 o 6 1 1 337.19 347.56 9.66 o 7 1 1 721.45 708.42 10.28 o -8 2 1 30.75 30.90 1.73 o -7 2 1 133.49 142.30 5.91 o -6 2 1 1232.62 1194.00 26.07 o -5 2 1 537.16 511.74 11.32 o -4 2 1 135.22 131.24 5.42 o -3 2 1 738.43 757.79 10.10 o -2 2 1 398.62 469.96 6.59 o -1 2 1 65591.49 63240.09 447.52 o 0 2 1 10560.55 10688.40 126.25 o 2 2 1 442.50 527.15 6.93 o 3 2 1 731.41 743.58 9.95 o 4 2 1 150.67 150.73 5.56 o 5 2 1 556.47 514.35 11.38 o 6 2 1 1201.65 1155.75 21.04 o 7 2 1 100.19 107.70 3.73 o -7 3 1 65.29 69.75 4.29 o -6 3 1 650.20 681.33 7.30 o -5 3 1 274.08 240.59 22.28 o -4 3 1 525.16 493.87 10.53 o -3 3 1 153.88 173.99 5.64 o -2 3 1 39.43 36.00 3.34 o 0 3 1 43.97 50.29 2.39 o 2 3 1 27.21 23.61 3.35 o 3 3 1 169.27 189.93 5.77 o 4 3 1 619.27 602.22 11.60 o 5 3 1 263.04 241.72 15.31 o 6 3 1 719.63 747.76 7.55 o 7 3 1 60.87 59.42 1.95 o -7 4 1 166.46 199.75 5.53 o -6 4 1 72.75 78.42 2.93 o -5 4 1 83.22 85.94 6.14 o -4 4 1 238.65 266.39 8.25 o -2 4 1 1212.81 1420.70 9.95 o 2 4 1 1224.56 1407.77 9.72 o 4 4 1 241.46 251.15 8.12 o 5 4 1 77.74 81.46 3.40 o 6 4 1 67.69 72.76 2.86 o 7 4 1 132.02 172.27 5.75 o -6 5 1 127.38 136.73 3.46 o -5 5 1 115.43 131.75 5.35 o -4 5 1 114.23 132.38 4.10 o -3 5 1 1449.33 1373.75 70.88 o -2 5 1 20.84 21.24 1.76 o -1 5 1 220.00 208.99 3.73 o 0 5 1 100.70 104.28 1.96 o 1 5 1 223.91 220.83 2.23 o 2 5 1 23.75 23.28 3.34 o 3 5 1 1390.70 1338.03 59.53 o 4 5 1 140.95 137.68 4.35 o 5 5 1 112.44 115.55 5.52 o 6 5 1 116.27 125.56 5.21 o 7 5 1 183.71 203.74 4.41 o -6 6 1 18.54 20.17 2.79 o -5 6 1 31.33 27.84 4.58 o -4 6 1 1064.40 1158.61 10.83 o -3 6 1 2105.53 2110.44 88.98 o -2 6 1 501.49 510.15 10.21 o -1 6 1 130.51 115.79 1.92 o 0 6 1 326.70 311.61 3.34 o 1 6 1 145.10 133.23 2.08 o 2 6 1 539.15 521.78 9.34 o 3 6 1 2089.92 2146.94 84.88 o 4 6 1 1083.46 1187.85 10.76 o 5 6 1 32.54 25.45 3.49 o 6 6 1 23.76 27.95 2.78 o -5 7 1 96.56 90.01 3.11 o -4 7 1 79.40 80.59 2.93 o -3 7 1 383.26 394.07 16.63 o -2 7 1 78.63 77.60 5.95 o -1 7 1 6.29 7.99 2.33 o 0 7 1 5.57 5.53 1.38 o 1 7 1 1.66 1.18 0.77 o 2 7 1 88.93 87.17 5.55 o 3 7 1 384.03 393.94 33.55 o 4 7 1 98.80 101.53 3.14 o 5 7 1 103.13 98.43 3.25 o -4 8 1 427.92 270.80 4.02 o -3 8 1 1957.82 2048.95 11.66 o 0 8 1 0.85 2.66 2.62 o 1 0 2 4912.71 4122.67 61.49 o 2 0 2 8075.00 7909.22 199.91 o 3 0 2 55.78 74.68 1.94 o 4 0 2 2041.00 2191.35 12.70 o 5 0 2 26.43 25.30 4.38 o 6 0 2 1.06 2.91 1.32 o 7 0 2 1137.05 1070.22 8.05 o 8 0 2 125.33 126.07 2.68 o -8 1 2 70.95 67.54 2.05 o -7 1 2 328.05 329.26 4.04 o -6 1 2 162.34 154.97 4.18 o -5 1 2 2190.50 2032.84 21.24 o -4 1 2 703.15 715.62 32.21 o -3 1 2 119.53 131.99 2.86 o -2 1 2 999.94 1062.80 6.44 o -1 1 2 1018.30 1136.01 8.35 o 0 1 2 421.42 506.05 2.96 o 2 1 2 1141.94 1184.41 15.68 o 3 1 2 79.36 88.75 2.45 o 4 1 2 696.59 687.64 18.31 o 5 1 2 2369.39 2217.63 22.17 o 6 1 2 112.61 106.09 2.47 o 7 1 2 311.28 309.58 4.80 o -8 2 2 345.20 330.14 3.39 o -7 2 2 398.12 460.61 9.29 o -6 2 2 279.43 286.12 4.25 o -5 2 2 208.46 182.06 7.51 o -4 2 2 295.61 327.92 8.17 o -3 2 2 515.00 556.10 8.77 o -2 2 2 1719.61 1942.93 14.72 o -1 2 2 1660.39 1897.38 64.66 o 0 2 2 3469.85 3746.15 50.85 o 1 2 2 1575.30 1699.26 34.63 o 2 2 2 1493.69 1602.42 63.29 o 3 2 2 464.07 483.47 8.16 o 4 2 2 314.20 328.95 10.63 o 5 2 2 192.38 175.83 7.02 o 6 2 2 284.66 284.69 4.82 o 7 2 2 485.83 472.25 5.22 o -7 3 2 214.50 216.03 5.04 o -6 3 2 748.45 730.04 7.59 o -5 3 2 325.10 294.58 13.31 o -4 3 2 2825.81 2819.36 24.46 o -3 3 2 92.26 100.42 4.46 o -2 3 2 1226.39 1366.35 12.28 o 0 3 2 24.70 21.57 2.13 o 2 3 2 1300.77 1479.74 12.82 o 3 3 2 82.56 96.68 4.55 o 4 3 2 2579.30 2659.45 23.68 o 5 3 2 365.81 344.18 15.27 o 6 3 2 859.88 841.47 11.79 o 7 3 2 201.79 207.18 3.13 o -7 4 2 228.18 255.13 5.93 o -6 4 2 20.55 24.85 3.40 o -5 4 2 1368.89 1366.13 16.58 o -4 4 2 663.55 701.95 12.86 o -2 4 2 5371.08 6102.45 101.93 o 1 4 2 886.55 942.98 10.89 o 2 4 2 5827.63 6894.65 60.96 o 3 4 2 244.57 220.22 6.95 o 4 4 2 607.83 678.43 12.67 o 5 4 2 1384.21 1251.09 15.78 o 6 4 2 14.79 15.48 4.97 o 7 4 2 231.96 293.49 7.12 o -7 5 2 32.75 33.84 2.57 o -6 5 2 113.41 108.41 3.60 o -5 5 2 269.83 321.35 5.74 o -4 5 2 661.64 757.25 9.04 o -3 5 2 496.02 475.93 6.88 o -2 5 2 455.96 470.62 9.98 o -1 5 2 151.30 153.59 1.93 o 0 5 2 121.10 128.07 2.70 o 1 5 2 158.75 158.19 2.19 o 2 5 2 448.92 467.55 4.67 o 3 5 2 494.96 447.02 10.60 o 4 5 2 651.77 781.30 8.76 o 5 5 2 284.33 302.24 8.15 o 6 5 2 108.17 110.96 4.80 o 7 5 2 21.69 26.41 2.66 o -6 6 2 102.27 88.80 3.09 o -5 6 2 3.32 5.71 2.25 o -4 6 2 548.24 620.14 8.11 o -3 6 2 393.24 390.13 20.95 o -2 6 2 1033.01 1035.31 41.29 o -1 6 2 28.84 27.89 1.31 o 0 6 2 1147.15 1075.08 7.18 o 1 6 2 33.12 32.20 1.45 o 2 6 2 1265.93 1324.10 45.51 o 3 6 2 404.59 418.90 16.58 o 4 6 2 536.20 617.78 7.75 o 5 6 2 6.51 9.23 3.76 o 6 6 2 85.67 81.79 3.26 o -5 7 2 126.49 144.89 2.82 o -4 7 2 70.83 72.59 2.91 o -3 7 2 258.42 259.71 16.24 o -2 7 2 52.72 46.62 2.23 o -1 7 2 27.30 25.58 1.65 o 0 7 2 0.31 0.52 0.72 o 1 7 2 28.63 27.81 1.65 o 2 7 2 39.44 37.95 2.31 o 3 7 2 285.96 300.60 25.83 o 4 7 2 96.19 102.29 3.13 o 5 7 2 124.12 123.18 3.57 o -3 8 2 621.01 663.98 6.68 o -2 8 2 151.11 152.91 3.84 o 0 8 2 25.19 21.57 2.47 o 4 8 2 280.33 198.32 3.54 o 1 0 3 2997.74 2625.31 180.07 o 2 0 3 5888.84 5670.23 93.07 o 3 0 3 496.99 610.75 7.09 o 4 0 3 186.10 160.77 3.70 o 5 0 3 30.36 35.96 3.96 o 6 0 3 142.89 149.13 4.01 o 7 0 3 477.26 484.01 4.53 o 8 0 3 252.13 271.21 3.66 o -8 1 3 145.56 149.44 6.38 o -7 1 3 95.94 92.34 4.21 o -6 1 3 1277.40 1231.09 24.52 o -5 1 3 752.80 702.25 12.85 o -4 1 3 5.99 7.35 3.04 o -3 1 3 6406.16 6852.37 25.84 o -2 1 3 242.38 270.44 2.53 o -1 1 3 1323.12 1314.93 8.74 o 0 1 3 133.91 159.07 2.01 o 1 1 3 1361.50 1364.36 21.53 o 2 1 3 260.61 285.43 4.11 o 3 1 3 6618.61 6949.56 29.33 o 4 1 3 13.12 10.85 2.28 o 5 1 3 716.13 690.86 12.51 o 6 1 3 1263.12 1223.18 11.33 o 7 1 3 63.84 60.73 1.93 o -8 2 3 250.88 230.90 4.44 o -7 2 3 631.61 672.02 21.81 o -6 2 3 150.14 150.85 2.48 o -5 2 3 103.16 88.63 6.92 o -4 2 3 318.52 344.05 8.36 o -3 2 3 3233.31 3566.39 22.44 o -2 2 3 283.28 412.62 6.00 o -1 2 3 2824.46 3273.06 12.70 o 0 2 3 97.45 82.91 1.90 o 1 2 3 3477.16 4147.88 154.57 o 2 2 3 300.42 399.22 6.21 o 3 2 3 3049.05 3342.41 21.35 o 4 2 3 377.31 366.98 8.15 o 5 2 3 121.90 106.13 6.67 o 6 2 3 150.39 149.56 2.56 o 7 2 3 557.72 581.19 15.32 o 8 2 3 222.44 205.66 3.84 o -8 3 3 4.75 2.79 2.18 o -7 3 3 86.88 95.92 2.88 o -6 3 3 353.41 395.53 5.68 o -5 3 3 263.92 233.69 8.56 o -4 3 3 1992.12 2034.85 20.88 o -3 3 3 317.85 330.21 7.38 o -2 3 3 24.83 28.99 3.33 o 0 3 3 1055.74 1186.42 13.10 o 2 3 3 32.34 35.53 3.29 o 3 3 3 307.22 328.56 7.47 o 4 3 3 1908.03 1954.30 20.37 o 5 3 3 224.74 206.95 8.01 o 6 3 3 331.81 360.28 7.57 o 7 3 3 94.18 102.58 4.68 o -7 4 3 127.93 128.17 9.68 o -6 4 3 4.36 6.72 2.74 o -5 4 3 263.87 294.90 5.76 o -4 4 3 45.34 37.59 8.17 o -2 4 3 1117.58 1269.23 18.84 o 1 4 3 944.01 1011.15 11.40 o 2 4 3 997.36 1154.47 6.26 o 3 4 3 213.35 199.30 6.65 o 4 4 3 32.94 37.21 7.26 o 5 4 3 296.70 278.45 7.47 o 6 4 3 2.60 4.15 4.63 o -6 5 3 267.05 265.09 5.59 o -5 5 3 1140.91 1234.46 10.97 o -4 5 3 559.87 630.69 24.15 o -3 5 3 434.30 398.32 6.39 o -2 5 3 183.97 180.48 4.59 o -1 5 3 190.60 194.88 2.27 o 0 5 3 0.45 4.33 1.39 o 1 5 3 226.85 248.82 4.18 o 2 5 3 159.06 171.12 2.93 o 3 5 3 396.31 362.10 9.54 o 5 5 3 1212.75 1166.99 15.32 o 7 5 3 3.34 2.41 2.78 o -5 6 3 86.62 92.13 4.93 o -4 6 3 754.61 806.95 9.20 o -3 6 3 679.02 687.07 31.35 o -2 6 3 5.95 7.98 1.80 o -1 6 3 468.50 451.39 6.72 o 0 6 3 366.33 372.37 8.11 o 1 6 3 443.65 452.92 10.02 o 2 6 3 1.35 5.75 1.74 o 3 6 3 714.86 760.33 32.82 o 4 6 3 781.62 875.99 9.04 o 5 6 3 73.32 68.36 3.79 o 6 6 3 124.08 113.25 3.62 o -5 7 3 129.04 104.64 3.04 o -4 7 3 83.65 90.00 3.14 o -3 7 3 508.57 505.92 25.15 o -2 7 3 184.88 184.11 8.15 o -1 7 3 443.11 431.71 17.89 o 0 7 3 2.73 2.36 1.69 o 1 7 3 422.22 407.67 13.61 o 2 7 3 163.95 166.28 13.69 o 3 7 3 514.43 533.71 42.33 o 4 7 3 75.02 84.36 2.88 o 5 7 3 126.88 116.50 3.38 o -3 8 3 134.55 136.36 3.26 o -2 8 3 60.78 69.59 3.42 o 0 8 3 161.02 140.67 4.84 o 0 0 4 2721.16 2496.03 13.28 o 1 0 4 1659.95 1489.91 115.03 o 2 0 4 7920.65 7398.37 185.95 o 3 0 4 1359.47 1621.11 7.37 o 4 0 4 701.92 856.49 8.10 o 5 0 4 1004.39 989.02 10.17 o 6 0 4 3065.01 2947.59 83.24 o 7 0 4 8.07 8.88 2.12 o 8 0 4 35.93 36.09 2.86 o -8 1 4 52.96 41.78 1.97 o -7 1 4 207.24 208.48 8.89 o -6 1 4 253.90 258.21 9.18 o -5 1 4 1969.44 1827.72 20.59 o -4 1 4 1993.28 2043.92 53.34 o -3 1 4 197.83 209.86 3.58 o -2 1 4 3671.59 3875.37 118.60 o -1 1 4 6.15 10.42 1.42 o 0 1 4 3040.27 3068.52 18.47 o 1 1 4 9.62 12.14 0.99 o 2 1 4 3548.02 3516.26 68.34 o 3 1 4 247.40 252.85 4.76 o 4 1 4 2020.51 1997.37 61.97 o 5 1 4 1851.70 1749.80 19.84 o 6 1 4 314.89 316.38 4.14 o 7 1 4 158.28 161.60 3.52 o 8 1 4 57.21 47.62 2.53 o -8 2 4 185.19 173.60 4.00 o -7 2 4 3.23 4.31 2.17 o -6 2 4 877.52 885.32 18.48 o -5 2 4 6.69 5.25 6.74 o -4 2 4 596.49 641.44 11.26 o -3 2 4 464.44 445.14 8.14 o -2 2 4 710.32 832.82 6.64 o -1 2 4 2673.88 2866.58 17.08 o 0 2 4 160.85 157.78 3.30 o 1 2 4 2515.00 2649.61 67.46 o 2 2 4 815.75 906.68 26.39 o 3 2 4 461.76 437.07 7.89 o 4 2 4 569.54 610.39 10.84 o 5 2 4 8.92 18.15 6.69 o 6 2 4 871.31 857.74 19.07 o 7 2 4 3.79 5.12 1.94 o 8 2 4 211.22 193.57 3.70 o -7 3 4 1035.51 1093.78 11.10 o -6 3 4 306.11 313.72 7.97 o -5 3 4 512.33 523.97 12.12 o -4 3 4 1085.31 1065.55 15.33 o -3 3 4 216.70 219.36 6.18 o -2 3 4 4537.35 5130.33 24.85 o 0 3 4 125.10 122.14 3.40 o 1 3 4 233.81 233.94 5.09 o 2 3 4 4484.09 5220.59 25.08 o 3 3 4 176.29 189.30 5.96 o 4 3 4 1299.42 1128.22 15.42 o 5 3 4 559.62 500.19 11.67 o 6 3 4 278.92 260.82 11.95 o 7 3 4 1005.54 1065.55 13.02 o -7 4 4 89.71 92.67 3.63 o -6 4 4 123.70 133.54 3.38 o -5 4 4 135.88 135.15 5.72 o -4 4 4 216.38 230.70 7.79 o -2 4 4 2352.49 2597.53 12.43 o 1 4 4 326.51 347.28 6.99 o 2 4 4 2140.44 2607.86 9.39 o 3 4 4 645.93 569.62 10.78 o 4 4 4 251.15 218.52 7.69 o 5 4 4 148.20 121.91 5.42 o 7 4 4 94.40 100.19 4.27 o -6 5 4 15.16 15.96 2.17 o -5 5 4 101.14 91.24 4.43 o -4 5 4 150.16 162.17 8.77 o -3 5 4 225.98 206.40 4.75 o -2 5 4 578.98 547.67 13.75 o -1 5 4 11.89 12.16 1.20 o 0 5 4 1107.75 1103.22 6.68 o 1 5 4 10.97 12.56 1.27 o 2 5 4 611.79 615.54 9.46 o 3 5 4 196.01 174.91 8.14 o 5 5 4 75.23 72.84 4.35 o -6 6 4 58.72 53.49 2.41 o -5 6 4 36.44 35.28 1.75 o -4 6 4 378.93 392.33 6.83 o -3 6 4 385.03 389.24 6.85 o -2 6 4 40.48 35.98 2.17 o -1 6 4 334.10 333.53 8.84 o 0 6 4 1163.23 1082.03 9.97 o 1 6 4 422.16 441.96 10.10 o 2 6 4 98.91 98.02 3.05 o 3 6 4 356.03 394.92 6.55 o 4 6 4 350.50 412.70 6.27 o 5 6 4 36.89 28.46 3.35 o 6 6 4 43.84 41.84 2.45 o -5 7 4 84.50 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