#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016516.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016516_Fobs loop_ _publ_author_name 'Wong, Jessica H.' 'Olmstead, Marilyn M.' 'Fettinger, James C.' 'Gervay-Hague, Jacquelyn' _publ_section_title ; Vinyl sulfones ; _journal_coeditor_code SK3201 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o132 _journal_page_last o136 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.769 _cell_angle_beta 89.938 _cell_angle_gamma 63.533 _cell_length_a 8.9333 _cell_length_b 10.0143 _cell_length_c 22.0588 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file sk3201Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JF1259FF in P-1 FINAL 26.10.2006 MERGE-I TWIN' _shelx_refln_list_code 4 _shelx_F_calc_maximum 202.88 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 199.37 164.75 5.96 o 2 0 0 330.30 332.81 10.69 o 3 0 0 1386.97 1359.72 58.98 o 4 0 0 1169.84 1212.97 33.59 o 5 0 0 224.79 231.81 8.42 o 6 0 0 622.42 616.11 21.83 o 7 0 0 1684.67 1671.00 45.55 o 8 0 0 143.53 167.11 7.58 o 9 0 0 220.07 207.22 10.43 o 10 0 0 265.78 266.20 21.25 o -9 1 0 303.24 326.58 17.10 o -8 1 0 45.78 46.15 5.95 o -7 1 0 420.54 474.19 15.83 o -6 1 0 428.99 437.71 14.50 o -5 1 0 202.86 227.18 8.42 o -4 1 0 99.68 114.73 4.84 o -3 1 0 780.37 738.66 21.69 o -2 1 0 10926.87 11862.94 267.14 o -1 1 0 5391.83 5750.98 153.95 o 0 1 0 8970.41 9483.83 242.38 o 1 1 0 200.11 172.48 5.09 o 2 1 0 1996.46 2000.72 69.07 o 3 1 0 648.68 649.13 29.05 o 4 1 0 912.32 1155.93 32.28 o 5 1 0 992.13 1047.82 29.79 o 6 1 0 51.36 65.88 3.74 o 7 1 0 2181.49 2228.80 58.51 o 8 1 0 16.16 18.83 3.83 o 9 1 0 254.68 234.27 9.57 o 10 1 0 289.42 297.27 16.85 o -9 2 0 131.17 126.80 10.15 o -8 2 0 178.45 170.26 11.00 o -7 2 0 35.10 43.66 5.62 o -6 2 0 2019.28 2050.96 62.01 o -5 2 0 67.04 92.47 4.86 o -4 2 0 193.92 195.59 7.37 o -3 2 0 3513.58 3710.86 91.44 o -2 2 0 9009.77 9880.34 227.07 o -1 2 0 5357.56 5493.11 147.13 o 0 2 0 7267.61 7424.64 222.64 o 1 2 0 5275.77 5462.38 129.09 o 2 2 0 318.66 340.79 12.84 o 3 2 0 647.68 641.43 16.53 o 4 2 0 526.07 519.63 16.97 o 5 2 0 16.00 29.23 2.15 o 6 2 0 754.76 767.01 22.88 o 7 2 0 1258.77 1308.17 36.61 o 8 2 0 602.91 624.61 19.72 o 9 2 0 101.27 82.96 6.31 o 10 2 0 83.21 91.20 11.86 o 11 2 0 73.06 96.17 18.09 o -8 3 0 375.03 406.59 20.30 o -7 3 0 28.13 25.54 6.60 o -6 3 0 127.38 112.89 6.80 o -5 3 0 488.99 489.60 26.77 o -4 3 0 138.29 133.67 5.71 o -3 3 0 54.35 42.99 3.53 o -2 3 0 1803.20 1807.03 47.55 o -1 3 0 1042.98 950.99 80.47 o 0 3 0 248.94 270.95 9.21 o 1 3 0 5250.04 5239.79 123.74 o 2 3 0 11397.46 12347.69 267.59 o 3 3 0 1450.48 1353.38 31.98 o 4 3 0 913.31 1091.92 26.57 o 5 3 0 15.84 30.18 4.06 o 6 3 0 3163.71 3135.66 68.11 o 7 3 0 57.75 69.35 3.98 o 8 3 0 431.00 429.93 14.44 o 9 3 0 243.53 270.68 12.36 o 10 3 0 31.67 33.89 7.77 o 11 3 0 63.91 96.42 11.40 o -8 4 0 547.74 575.05 31.85 o -7 4 0 318.91 331.32 17.29 o -6 4 0 17.29 19.66 5.78 o -5 4 0 324.95 340.07 13.93 o -4 4 0 770.00 780.14 55.40 o -3 4 0 370.22 350.00 11.84 o -2 4 0 341.23 310.27 27.98 o -1 4 0 511.40 547.78 41.86 o 0 4 0 2207.13 2213.50 95.86 o 1 4 0 1010.94 845.76 25.23 o 2 4 0 8991.52 9819.12 217.92 o 3 4 0 726.52 717.23 31.07 o 4 4 0 1254.43 1193.91 28.60 o 5 4 0 1044.31 1021.98 25.13 o 6 4 0 728.69 724.79 18.84 o 7 4 0 61.90 69.29 3.45 o 8 4 0 1926.78 1907.81 60.05 o 9 4 0 544.62 547.39 26.99 o 10 4 0 178.01 191.94 13.19 o 11 4 0 81.08 54.80 12.45 o -7 5 0 309.47 325.70 17.57 o -6 5 0 71.16 74.45 11.04 o -5 5 0 109.18 106.91 9.53 o -4 5 0 533.85 487.97 27.69 o -3 5 0 17.49 23.38 8.41 o -2 5 0 339.27 332.49 13.04 o -1 5 0 1609.11 1644.60 99.82 o 0 5 0 4816.40 4978.04 233.70 o 1 5 0 544.24 570.76 17.45 o 2 5 0 1774.19 1814.15 48.28 o 3 5 0 3382.84 3631.07 89.55 o 4 5 0 106.92 115.11 4.14 o 5 5 0 238.60 234.22 7.28 o 6 5 0 54.22 67.99 3.21 o 7 5 0 1323.38 1280.05 42.28 o 8 5 0 405.57 402.57 21.13 o 9 5 0 547.69 539.77 26.69 o 10 5 0 1029.37 1056.69 46.84 o 11 5 0 35.27 41.03 8.64 o -6 6 0 76.38 57.94 9.72 o -5 6 0 74.48 73.66 7.62 o -4 6 0 558.62 602.56 26.67 o -3 6 0 782.41 773.44 26.90 o -2 6 0 840.31 850.87 28.96 o -1 6 0 440.35 460.20 14.90 o 0 6 0 4856.54 5112.41 130.01 o 1 6 0 1727.02 1824.07 55.18 o 2 6 0 342.10 306.12 10.45 o 3 6 0 58.13 50.61 3.11 o 4 6 0 188.23 187.27 7.34 o 5 6 0 204.87 238.64 14.15 o 6 6 0 607.79 568.61 15.43 o 7 6 0 2187.33 2060.52 53.02 o 8 6 0 627.54 606.74 21.89 o 9 6 0 257.92 255.96 11.51 o 10 6 0 168.65 189.95 13.14 o 11 6 0 32.97 31.24 8.39 o -5 7 0 86.78 59.56 11.04 o -4 7 0 91.84 86.62 8.29 o -3 7 0 762.57 745.97 31.76 o -2 7 0 441.80 486.97 18.51 o -1 7 0 2078.81 2197.58 86.79 o 0 7 0 177.36 199.26 9.60 o 1 7 0 416.77 415.92 18.01 o 2 7 0 362.60 377.83 12.64 o 3 7 0 363.50 343.90 13.76 o 4 7 0 134.24 131.23 10.75 o 5 7 0 69.11 93.51 4.07 o 6 7 0 451.09 428.85 16.73 o 7 7 0 1598.39 1511.88 52.44 o 8 7 0 16.80 20.11 4.32 o 9 7 0 108.64 93.89 6.85 o 10 7 0 31.14 26.79 7.39 o 11 7 0 75.58 82.83 12.28 o -4 8 0 813.03 837.77 35.71 o -3 8 0 25.96 10.65 10.43 o -2 8 0 336.37 336.61 17.46 o -1 8 0 209.69 220.69 18.06 o 0 8 0 2502.91 2576.90 100.79 o 1 8 0 2006.43 2068.17 54.71 o 2 8 0 888.95 939.89 31.26 o 3 8 0 16.28 12.01 3.16 o 4 8 0 736.34 758.28 44.68 o 5 8 0 487.61 469.47 13.71 o 6 8 0 2008.76 1899.20 49.53 o 7 8 0 448.92 439.34 16.90 o 8 8 0 152.12 160.85 8.42 o 9 8 0 241.35 212.17 10.31 o 10 8 0 89.31 76.24 15.07 o 11 8 0 68.11 79.41 10.63 o -3 9 0 20.97 15.01 7.02 o -2 9 0 20.71 25.44 7.02 o -1 9 0 330.64 329.30 17.19 o 0 9 0 157.52 148.54 14.29 o 1 9 0 196.04 184.88 11.84 o 2 9 0 441.48 453.25 15.26 o 3 9 0 810.75 793.35 27.37 o 4 9 0 496.86 482.19 15.45 o 5 9 0 347.33 338.92 11.61 o 6 9 0 122.58 116.27 5.75 o 7 9 0 33.33 36.71 5.13 o 8 9 0 45.54 51.64 5.61 o 9 9 0 210.05 171.84 9.18 o 10 9 0 271.80 241.13 11.76 o 11 9 0 77.07 65.67 10.07 o -2 10 0 120.06 125.01 10.42 o -1 10 0 206.48 208.72 13.42 o 0 10 0 820.51 824.45 35.12 o 1 10 0 352.26 379.05 18.91 o 2 10 0 350.36 371.37 15.46 o 3 10 0 748.90 748.27 25.25 o 4 10 0 595.47 625.63 19.15 o 5 10 0 105.55 100.90 5.39 o 6 10 0 16.50 19.69 4.74 o 7 10 0 28.98 23.21 8.07 o 8 10 0 166.03 151.91 8.59 o 9 10 0 317.78 320.48 15.63 o 10 10 0 253.37 235.88 11.87 o 0 11 0 74.20 65.11 11.09 o 1 11 0 219.54 286.22 16.21 o 2 11 0 21.08 14.88 7.44 o 3 11 0 27.80 31.45 9.72 o 4 11 0 88.70 97.10 11.62 o 5 11 0 72.05 63.91 5.27 o 6 11 0 72.15 85.59 6.64 o 7 11 0 300.01 286.29 14.49 o 8 11 0 400.23 378.91 15.73 o 9 11 0 130.78 132.59 8.56 o 2 12 0 122.83 127.04 10.84 o 3 12 0 20.32 16.39 11.62 o 4 12 0 780.06 829.46 36.27 o 5 12 0 92.33 83.97 15.95 o 6 12 0 81.74 59.51 17.14 o 7 12 0 288.99 290.48 13.29 o 8 12 0 577.97 557.40 21.34 o -8 -12 1 86.56 69.67 11.89 o -7 -12 1 27.64 38.52 12.54 o -6 -12 1 412.85 431.72 17.34 o -5 -12 1 147.55 123.40 13.52 o -4 -12 1 64.81 65.03 18.26 o -3 -12 1 20.46 16.43 11.72 o -2 -12 1 214.89 215.10 19.89 o -9 -11 1 264.97 259.84 12.56 o -8 -11 1 4.15 10.48 5.26 o -7 -11 1 7.89 3.96 4.83 o -6 -11 1 23.41 14.47 5.49 o -5 -11 1 141.00 127.07 6.43 o -4 -11 1 79.11 82.61 10.89 o -3 -11 1 464.03 458.17 22.57 o -2 -11 1 250.29 177.56 16.73 o -1 -11 1 236.49 276.95 22.75 o 0 -11 1 393.86 418.76 21.35 o -10 -10 1 85.14 83.84 7.89 o -9 -10 1 196.10 180.72 14.12 o -8 -10 1 65.39 61.82 6.46 o -7 -10 1 110.59 98.90 6.82 o -6 -10 1 13.94 22.46 4.09 o -5 -10 1 112.19 115.06 5.94 o -4 -10 1 70.78 81.88 5.07 o -3 -10 1 428.97 442.28 26.30 o -2 -10 1 1621.78 1612.61 99.28 o -1 -10 1 90.82 109.33 9.41 o 0 -10 1 100.32 121.38 10.10 o 1 -10 1 221.03 185.01 12.66 o 2 -10 1 210.05 207.17 13.55 o -11 -9 1 41.98 23.24 12.64 o -10 -9 1 44.04 53.43 6.56 o -9 -9 1 51.05 44.65 5.89 o -8 -9 1 272.80 271.37 11.93 o -7 -9 1 34.74 45.16 5.49 o -6 -9 1 18.55 24.08 3.76 o -5 -9 1 8.98 12.84 3.70 o -4 -9 1 174.42 152.21 5.82 o -3 -9 1 249.48 250.28 9.25 o -2 -9 1 143.79 145.98 8.12 o -1 -9 1 157.65 165.01 8.95 o 0 -9 1 103.15 99.85 12.33 o 1 -9 1 97.41 117.54 9.36 o 2 -9 1 268.79 325.22 17.39 o 3 -9 1 19.98 28.86 7.57 o -11 -8 1 147.51 139.69 11.77 o -10 -8 1 193.42 159.89 12.03 o -9 -8 1 80.57 77.42 6.59 o -8 -8 1 950.86 895.58 30.58 o -7 -8 1 84.82 82.32 5.99 o -6 -8 1 156.35 163.81 10.23 o -5 -8 1 1325.66 1364.70 37.10 o -4 -8 1 417.43 384.13 12.71 o -3 -8 1 195.22 186.79 10.99 o -2 -8 1 692.92 673.83 20.90 o -1 -8 1 1049.06 994.56 29.68 o 0 -8 1 216.72 210.41 10.06 o 1 -8 1 148.81 158.88 9.51 o 2 -8 1 1659.26 1797.45 66.86 o 3 -8 1 432.43 447.72 26.28 o 4 -8 1 68.54 53.88 8.54 o -11 -7 1 202.49 202.70 14.27 o -10 -7 1 43.60 57.78 8.40 o -9 -7 1 187.40 161.76 8.95 o -8 -7 1 1146.27 1091.30 35.86 o -7 -7 1 67.69 67.42 6.86 o -6 -7 1 572.47 553.97 21.73 o -5 -7 1 459.33 485.91 13.55 o -4 -7 1 436.31 453.58 12.74 o -3 -7 1 566.12 517.91 14.07 o -2 -7 1 665.06 620.45 19.21 o -1 -7 1 2104.01 2172.05 94.20 o 0 -7 1 189.22 192.81 8.90 o 1 -7 1 1085.72 1116.52 56.72 o 2 -7 1 135.60 138.30 7.85 o 3 -7 1 402.18 409.73 19.83 o 4 -7 1 83.59 65.61 8.82 o 5 -7 1 141.43 120.88 9.70 o -11 -6 1 94.87 109.88 12.08 o -10 -6 1 371.05 337.79 19.16 o -9 -6 1 992.74 924.71 41.55 o -8 -6 1 236.79 229.35 11.35 o -7 -6 1 36.45 70.04 9.87 o -6 -6 1 340.73 340.67 10.07 o -5 -6 1 573.38 559.77 15.12 o -4 -6 1 524.11 511.30 13.99 o -3 -6 1 147.08 178.20 7.58 o -2 -6 1 277.26 277.43 11.33 o -1 -6 1 1278.41 1368.64 51.00 o 0 -6 1 301.21 306.81 10.73 o 1 -6 1 2120.39 2245.95 88.81 o 2 -6 1 667.05 671.66 23.77 o 3 -6 1 267.66 278.34 23.36 o 4 -6 1 73.11 76.60 7.50 o 5 -6 1 132.02 134.92 9.67 o 6 -6 1 420.32 442.16 21.75 o -11 -5 1 109.54 105.49 10.69 o -10 -5 1 118.87 157.18 17.89 o -9 -5 1 400.43 371.09 19.92 o -8 -5 1 250.26 247.72 14.52 o -7 -5 1 99.87 86.75 3.91 o -6 -5 1 191.32 180.89 6.06 o -5 -5 1 1154.74 1097.03 30.39 o -4 -5 1 357.60 347.37 11.64 o -3 -5 1 2588.17 2758.61 67.80 o -2 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172.87 158.82 6.60 o -6 -3 1 412.92 494.22 15.69 o -5 -3 1 242.57 227.65 7.00 o -4 -3 1 12.73 21.89 2.21 o -3 -3 1 566.50 611.03 15.88 o -2 -3 1 98.49 90.16 3.67 o -1 -3 1 88.59 71.76 3.21 o 0 -3 1 77.49 62.92 5.28 o 1 -3 1 1776.46 1914.88 159.09 o 2 -3 1 3462.06 3585.95 125.10 o 3 -3 1 147.28 176.84 6.68 o 4 -3 1 425.09 463.15 14.97 o 5 -3 1 1333.88 1408.40 44.65 o 6 -3 1 19.84 23.82 7.88 o 7 -3 1 105.71 106.28 8.54 o 8 -3 1 3.92 2.76 6.91 o -10 -2 1 362.08 353.95 19.71 o -9 -2 1 483.30 467.92 15.83 o -8 -2 1 1316.00 1300.44 36.75 o -7 -2 1 59.77 74.09 4.26 o -6 -2 1 899.22 943.03 28.39 o -5 -2 1 507.51 520.76 16.19 o -4 -2 1 369.75 347.08 9.74 o -3 -2 1 2884.19 3193.82 76.21 o -2 -2 1 41161.00 42101.93 806.79 o -1 -2 1 9928.45 9676.30 451.11 o 0 -2 1 26.45 4.24 2.07 o 1 -2 1 93.63 101.12 7.78 o 2 -2 1 3621.41 3589.05 88.34 o 3 -2 1 2494.93 2679.90 67.81 o 4 -2 1 560.32 542.25 16.95 o 5 -2 1 474.55 501.12 16.09 o 6 -2 1 167.11 163.64 8.33 o 7 -2 1 35.80 48.08 5.89 o 8 -2 1 61.15 58.74 7.96 o 9 -2 1 278.16 296.57 18.09 o -10 -1 1 192.85 226.38 18.86 o -9 -1 1 38.47 64.21 5.72 o -8 -1 1 64.70 72.92 5.34 o -7 -1 1 443.77 467.75 15.38 o -6 -1 1 14.47 19.84 2.70 o -5 -1 1 0.61 7.28 1.87 o -4 -1 1 112.51 104.23 4.29 o -3 -1 1 27.64 33.22 1.94 o -2 -1 1 6278.06 6480.85 338.01 o -1 -1 1 5598.86 5366.29 110.51 o 0 -1 1 66.28 25.67 1.90 o 1 -1 1 9988.51 10326.38 260.61 o 2 -1 1 105.96 100.31 6.69 o 3 -1 1 476.35 548.83 16.79 o 4 -1 1 340.78 341.75 11.31 o 5 -1 1 560.36 586.30 18.18 o 6 -1 1 591.52 611.37 19.18 o 7 -1 1 87.71 87.84 6.61 o 8 -1 1 283.84 307.18 13.36 o 9 -1 1 189.98 190.34 15.32 o -10 0 1 250.23 319.54 24.07 o -9 0 1 86.74 101.84 9.24 o -8 0 1 578.23 551.90 18.03 o -7 0 1 559.69 603.09 19.08 o -6 0 1 747.63 790.41 23.62 o -5 0 1 520.18 462.32 14.76 o -4 0 1 512.35 505.67 15.71 o -3 0 1 567.85 570.87 17.16 o -2 0 1 15295.10 15831.80 334.36 o -1 0 1 157.12 131.73 4.66 o 0 0 1 1.14 0.00 0.75 o 1 0 1 5573.79 5444.24 124.77 o 2 0 1 40754.91 43480.44 2191.57 o 3 0 1 555.81 604.70 18.24 o 4 0 1 319.37 330.44 10.97 o 5 0 1 1127.49 1140.49 32.06 o 6 0 1 327.04 352.17 12.10 o 7 0 1 67.19 71.13 4.55 o 8 0 1 1011.62 1008.14 33.93 o 9 0 1 54.64 56.91 6.71 o 10 0 1 79.87 105.70 12.93 o -9 1 1 204.29 235.39 13.71 o -8 1 1 45.55 57.81 6.30 o -7 1 1 373.61 341.27 12.15 o -6 1 1 252.38 254.87 9.50 o -5 1 1 1940.97 2129.44 55.85 o -4 1 1 1021.80 1018.43 29.00 o -3 1 1 2283.49 2343.60 85.99 o -2 1 1 1266.93 1094.40 34.64 o -1 1 1 506.13 563.97 19.35 o 0 1 1 2.10 3.20 1.60 o 1 1 1 152.12 131.44 5.49 o 2 1 1 6376.01 6619.62 132.35 o 3 1 1 2912.71 3264.97 84.14 o 4 1 1 13.20 20.68 2.24 o 5 1 1 549.23 546.83 16.98 o 6 1 1 178.80 174.97 6.96 o 7 1 1 36.94 68.97 8.82 o 8 1 1 1117.50 1174.62 33.78 o 9 1 1 83.03 90.69 8.95 o 10 1 1 47.22 85.71 11.16 o -9 2 1 486.26 508.55 24.17 o -8 2 1 126.88 144.93 10.16 o -7 2 1 40.09 39.75 5.48 o -6 2 1 419.67 385.13 13.18 o -5 2 1 1143.18 1249.00 35.07 o -4 2 1 673.94 733.86 21.81 o -3 2 1 1500.47 1440.90 39.18 o -2 2 1 708.33 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10.15 o 0 6 26 5.62 9.58 7.25 o 1 6 26 85.43 95.87 10.25 o 2 6 26 53.91 57.33 8.93 o 3 6 26 72.02 90.82 10.92 o 4 6 26 20.87 23.57 7.89 o 1 7 26 84.65 103.13 10.57 o 2 7 26 4.72 0.39 6.57 o 3 7 26 220.47 207.49 13.89 o -2 -2 27 243.10 283.85 22.90 o -1 -2 27 41.50 32.14 12.64 o -3 -1 27 32.41 24.54 7.88 o -2 -1 27 132.83 152.23 15.75 o -1 -1 27 1.29 2.04 10.99 o 0 -1 27 1.83 13.57 13.78 o -3 0 27 324.29 350.42 19.41 o -2 0 27 15.67 7.08 7.23 o -1 0 27 230.35 220.20 19.21 o 0 0 27 1.05 14.25 12.20 o 1 0 27 1.22 10.16 11.47 o 2 0 27 240.02 352.45 28.69 o -3 1 27 1.15 6.52 7.70 o -2 1 27 11.50 8.42 7.66 o -1 1 27 512.97 503.67 25.25 o 0 1 27 2.40 0.00 9.48 o 2 1 27 135.68 154.47 24.99 o -3 2 27 29.53 32.67 8.68 o -2 2 27 520.37 562.39 49.69 o -1 2 27 291.75 292.51 26.69 o 0 2 27 3.92 0.00 9.82 o 1 2 27 515.82 493.52 45.07 o 2 2 27 14.66 5.88 9.48 o 3 2 27 33.96 22.61 7.27 o -3 3 27 28.26 30.38 8.43 o -2 3 27 1282.62 1482.36 60.39 o -1 3 27 11.79 7.04 8.08 o 0 3 27 19.58 20.90 10.16 o 1 3 27 294.92 301.75 47.70 o 2 3 27 12.21 1.30 6.71 o 3 3 27 331.06 347.74 25.53 o -2 4 27 46.65 42.20 11.13 o -1 4 27 1.00 9.28 8.41 o 0 4 27 29.43 39.64 11.81 o 1 4 27 12.30 9.80 7.30 o 2 4 27 524.52 495.89 24.71 o 3 4 27 1.22 13.73 7.72 o -1 5 27 413.12 440.85 30.15 o 0 5 27 30.99 18.80 7.30 o 1 5 27 1.07 4.00 6.95 o 2 5 27 1264.43 1310.84 54.20 o 3 5 27 29.59 18.13 8.04 o 1 6 27 422.22 434.95 41.38 o 2 6 27 43.62 31.54 12.23 o 3 6 27 30.25 37.43 8.70 o -2 0 28 45.74 17.15 7.99 o -1 0 28 45.70 54.36 14.25 o -2 1 28 9.71 4.31 7.68 o -1 1 28 118.44 104.89 24.29 o -2 2 28 11.96 8.42 7.82 o -1 2 28 432.48 473.84 24.54 o 0 2 28 28.53 16.09 12.01 o 2 2 28 48.89 29.42 11.09 o -1 3 28 304.84 358.39 30.83 o 0 3 28 48.28 31.56 14.00 o 1 3 28 427.84 410.35 70.45 o 2 3 28 9.09 16.00 10.99 o 0 4 28 306.93 327.37 18.40 o 1 4 28 287.09 247.02 28.78 o 2 4 28 11.72 6.66 7.84 o