#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016533.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016533_Fobs loop_ _publ_author_name 'Zhylenko, Iryna S.' 'Solntsev, Pavlo V.' 'Rusanov, Eduard B.' 'Chernega, Alexander N.' 'Domasevitch, Konstantin V.' _publ_section_title ; Hydrate frameworks involving the pyridazino[4,5-d]pyridazine unit as a multiple hydrogen-bond acceptor ; _journal_coeditor_code BM3049 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o237 _journal_page_last o241 _journal_volume 64 _journal_year 2008 _space_group_IT_number 63 _symmetry_space_group_name_Hall '-C 2c 2' _symmetry_space_group_name_H-M 'C m c m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8804 _cell_length_b 6.6540 _cell_length_c 18.3908 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7400 _[local]_cod_data_source_file bm3049Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xtal4a in Cmcm' _shelx_refln_list_code 4 _shelx_F_calc_maximum 84.94 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x, y, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y, -z-1/2' 'x, -y, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z-1/2' 'x+1/2, -y+1/2, z-1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10.92 12.82 1.98 o 4 0 0 2699.02 2693.05 5.29 o 6 0 0 1190.03 1206.07 16.31 o 10 0 0 306.33 322.14 1.90 o 12 0 0 426.02 438.13 8.86 o 5 1 0 1004.81 1087.01 6.57 o 7 1 0 700.28 706.52 2.39 o 9 1 0 52.90 52.22 3.20 o 11 1 0 1000.18 1020.83 5.07 o 13 1 0 126.70 137.13 7.69 o 2 2 0 905.86 902.45 10.47 o 4 2 0 1357.30 1349.42 12.10 o 6 2 0 107.18 118.79 1.19 o 8 2 0 4927.72 4509.88 43.79 o 10 2 0 190.45 207.18 1.33 o 12 2 0 267.10 284.77 12.61 o 1 3 0 1674.37 1970.43 7.55 o 3 3 0 755.53 771.68 9.00 o 5 3 0 2.59 4.03 1.35 o 7 3 0 227.71 239.82 4.66 o 9 3 0 240.32 233.93 1.84 o 11 3 0 282.93 289.33 9.36 o 2 4 0 28.17 37.66 1.66 o 4 4 0 1156.65 1169.02 19.20 o 6 4 0 43.44 38.43 1.19 o 8 4 0 1606.59 1600.93 18.60 o 10 4 0 0.62 3.46 1.06 o 1 5 0 0.49 4.45 1.63 o 3 5 0 3.51 2.53 1.57 o 5 5 0 2.68 4.99 1.56 o 7 5 0 16.79 19.51 1.97 o 9 5 0 234.44 220.35 4.21 o 11 5 0 15.19 21.35 1.58 o 2 6 0 11.14 13.34 1.76 o 4 6 0 878.39 925.57 14.25 o 6 6 0 83.36 87.10 2.26 o 8 6 0 313.38 321.59 10.02 o 1 7 0 0.00 0.34 2.56 o 3 7 0 164.42 165.19 5.44 o 5 7 0 48.41 44.92 1.77 o 7 7 0 26.36 23.24 1.34 o 0 8 0 0.28 0.00 1.91 o 2 8 0 8.73 9.61 1.60 o 4 8 0 232.50 208.75 2.99 o 6 8 0 55.75 54.31 2.67 o 1 1 1 51.43 55.56 1.37 o 3 1 1 2930.10 2789.44 14.50 o 5 1 1 380.59 383.45 1.86 o 7 1 1 12.56 13.00 0.99 o 9 1 1 32.24 31.58 1.05 o 11 1 1 38.89 42.11 1.43 o 13 1 1 5.18 6.64 1.26 o 2 2 1 100.71 99.32 1.17 o 4 2 1 4.94 11.44 0.79 o 6 2 1 541.39 515.19 4.02 o 8 2 1 290.96 284.67 3.39 o 10 2 1 61.59 63.19 0.78 o 12 2 1 11.05 12.27 1.50 o 1 3 1 253.58 277.26 2.09 o 3 3 1 1490.93 1513.89 13.14 o 5 3 1 24.59 26.58 0.73 o 7 3 1 270.50 282.95 3.47 o 9 3 1 50.78 44.52 1.39 o 11 3 1 124.78 123.16 1.12 o 0 4 1 1282.69 1367.64 4.18 o 2 4 1 200.10 189.77 1.19 o 4 4 1 207.10 240.43 3.14 o 6 4 1 164.98 160.88 1.24 o 8 4 1 183.06 174.98 1.62 o 10 4 1 93.86 96.94 1.42 o 1 5 1 148.15 181.40 3.13 o 3 5 1 327.37 337.34 1.67 o 5 5 1 14.74 15.90 1.17 o 7 5 1 133.59 129.52 2.01 o 9 5 1 2.63 5.32 1.36 o 11 5 1 73.99 72.45 1.46 o 0 6 1 619.94 597.22 4.45 o 2 6 1 11.25 12.71 1.17 o 4 6 1 3.16 5.06 0.96 o 6 6 1 47.70 52.85 0.89 o 8 6 1 144.04 146.48 2.53 o 1 7 1 0.05 0.54 1.27 o 3 7 1 74.57 73.89 2.07 o 5 7 1 32.14 34.57 1.06 o 7 7 1 4.16 3.64 0.96 o 0 8 1 53.49 53.98 1.74 o 2 8 1 3.14 3.99 1.39 o 4 8 1 2.31 3.20 1.15 o 6 8 1 0.02 1.71 1.15 o 2 0 2 3265.06 3105.41 44.87 o 4 0 2 3337.33 3347.33 9.85 o 6 0 2 883.97 770.06 5.88 o 8 0 2 1930.21 1709.74 10.55 o 10 0 2 29.61 31.36 1.07 o 12 0 2 108.55 129.66 3.40 o 1 1 2 2229.48 2198.08 22.35 o 3 1 2 161.13 187.05 1.26 o 5 1 2 369.67 342.74 2.55 o 7 1 2 57.36 55.86 0.80 o 9 1 2 634.61 591.51 2.62 o 11 1 2 60.26 60.54 1.26 o 13 1 2 29.33 36.80 1.05 o 2 2 2 122.82 127.54 1.37 o 4 2 2 3668.96 3627.48 39.38 o 6 2 2 151.72 126.57 1.18 o 8 2 2 2042.63 1901.96 9.08 o 10 2 2 16.97 19.14 1.20 o 12 2 2 120.02 133.52 2.88 o 1 3 2 90.57 129.27 7.80 o 3 3 2 326.86 291.35 2.14 o 5 3 2 1.41 2.88 0.72 o 7 3 2 18.61 18.34 0.74 o 9 3 2 265.17 266.21 2.79 o 11 3 2 56.74 56.67 1.26 o 2 4 2 213.18 193.08 1.25 o 4 4 2 859.69 872.79 4.53 o 6 4 2 32.93 33.99 0.85 o 8 4 2 911.82 874.38 7.71 o 10 4 2 43.93 51.68 1.11 o 1 5 2 430.14 452.35 3.77 o 3 5 2 3.00 5.39 0.90 o 5 5 2 133.42 142.35 1.88 o 7 5 2 97.60 100.91 1.14 o 9 5 2 113.60 121.44 2.22 o 11 5 2 14.46 12.92 1.01 o 0 6 2 643.78 650.71 3.51 o 2 6 2 151.91 146.94 1.19 o 4 6 2 118.17 124.01 1.15 o 6 6 2 11.19 13.05 0.97 o 8 6 2 235.29 225.33 2.91 o 1 7 2 49.45 54.05 1.41 o 3 7 2 0.43 1.76 0.91 o 5 7 2 30.63 33.16 0.99 o 7 7 2 15.56 12.54 1.09 o 0 8 2 177.95 168.48 3.39 o 2 8 2 1.03 2.75 1.49 o 4 8 2 103.52 103.62 2.27 o 6 8 2 0.10 1.72 1.00 o 1 1 3 1225.74 1152.90 5.03 o 3 1 3 6.76 12.41 0.83 o 5 1 3 10.82 7.94 0.74 o 7 1 3 92.41 95.66 1.02 o 9 1 3 4.73 9.15 1.41 o 11 1 3 20.93 24.96 1.08 o 13 1 3 0.05 4.05 1.05 o 0 2 3 2682.45 2723.10 5.93 o 2 2 3 160.10 162.26 1.39 o 4 2 3 198.25 202.67 2.44 o 6 2 3 19.20 25.27 0.73 o 8 2 3 292.92 279.44 2.04 o 10 2 3 13.51 16.96 1.03 o 12 2 3 0.27 2.59 0.82 o 1 3 3 109.74 137.50 1.21 o 3 3 3 1398.23 1449.94 16.48 o 5 3 3 240.36 257.03 1.58 o 7 3 3 95.30 96.01 0.95 o 9 3 3 3.71 3.33 0.75 o 11 3 3 151.48 169.48 2.20 o 2 4 3 166.50 161.82 1.44 o 4 4 3 12.09 8.50 0.99 o 6 4 3 176.67 190.97 1.73 o 8 4 3 806.74 778.66 6.55 o 10 4 3 5.74 8.73 0.81 o 1 5 3 78.10 85.74 1.12 o 3 5 3 682.82 720.08 4.85 o 5 5 3 166.22 169.73 1.12 o 7 5 3 101.65 102.67 1.82 o 9 5 3 30.31 34.26 1.42 o 0 6 3 1239.27 1280.66 14.97 o 2 6 3 3.84 3.29 0.85 o 4 6 3 18.93 20.81 0.83 o 6 6 3 9.63 9.87 0.92 o 8 6 3 488.30 445.29 5.77 o 1 7 3 207.77 197.29 1.39 o 3 7 3 66.34 63.24 0.98 o 5 7 3 14.22 13.46 0.89 o 7 7 3 99.42 91.43 2.34 o 0 8 3 453.93 406.11 3.13 o 2 8 3 0.64 2.11 1.11 o 4 8 3 1.01 2.35 1.03 o 0 0 4 1654.24 1558.38 6.26 o 2 0 4 991.37 945.67 18.60 o 6 0 4 2142.49 2068.55 7.24 o 8 0 4 0.37 3.66 0.98 o 10 0 4 1.88 3.74 1.03 o 12 0 4 29.75 43.20 2.00 o 1 1 4 287.68 299.92 2.38 o 5 1 4 1907.09 2069.83 8.76 o 7 1 4 30.48 42.29 0.75 o 9 1 4 724.34 713.34 5.72 o 11 1 4 262.01 287.84 2.00 o 13 1 4 73.10 88.84 2.81 o 0 2 4 1057.46 984.15 3.83 o 2 2 4 3321.11 3151.47 29.61 o 4 2 4 813.73 902.30 4.83 o 6 2 4 1849.75 1826.09 8.70 o 8 2 4 0.61 5.21 0.75 o 10 2 4 36.32 37.89 1.18 o 12 2 4 36.64 45.90 2.42 o 1 3 4 1836.34 1780.07 5.65 o 3 3 4 2107.95 2196.11 16.28 o 5 3 4 1240.78 1294.48 10.58 o 7 3 4 68.10 60.36 0.80 o 9 3 4 309.74 318.49 3.23 o 11 3 4 83.15 87.91 2.03 o 0 4 4 219.80 216.66 4.01 o 2 4 4 736.03 727.57 4.89 o 4 4 4 214.39 237.89 2.25 o 6 4 4 151.14 147.49 1.96 o 8 4 4 47.95 55.43 0.88 o 10 4 4 84.85 81.27 2.45 o 1 5 4 91.29 103.89 1.14 o 3 5 4 4.18 4.96 0.87 o 5 5 4 104.95 110.52 1.17 o 7 5 4 50.83 47.70 0.93 o 9 5 4 15.33 15.39 0.89 o 0 6 4 611.09 616.07 13.32 o 2 6 4 45.55 44.68 0.98 o 4 6 4 59.61 61.31 0.91 o 6 6 4 7.48 8.36 0.85 o 8 6 4 91.32 87.51 2.88 o 1 7 4 92.61 88.71 1.21 o 3 7 4 11.67 13.28 0.97 o 5 7 4 25.26 33.33 0.91 o 7 7 4 49.04 50.44 1.10 o 0 8 4 100.01 94.89 2.05 o 2 8 4 28.96 30.35 1.16 o 4 8 4 0.03 0.67 1.06 o 1 1 5 947.70 936.43 7.23 o 3 1 5 17.33 21.62 0.91 o 5 1 5 32.09 33.89 0.72 o 7 1 5 90.85 93.88 1.18 o 9 1 5 42.08 39.48 1.42 o 11 1 5 0.69 2.57 0.86 o 0 2 5 0.68 6.11 1.68 o 2 2 5 373.82 378.14 2.76 o 4 2 5 759.43 720.45 6.51 o 6 2 5 184.96 187.13 2.62 o 8 2 5 74.30 56.82 1.19 o 10 2 5 75.34 71.67 1.49 o 12 2 5 11.16 15.98 0.83 o 1 3 5 59.97 69.21 1.18 o 3 3 5 636.43 643.14 3.93 o 5 3 5 3.05 4.95 0.91 o 7 3 5 23.98 22.81 0.99 o 9 3 5 392.04 393.91 5.07 o 11 3 5 4.14 6.78 0.80 o 0 4 5 1.52 6.38 1.24 o 2 4 5 89.86 84.29 1.02 o 4 4 5 34.91 33.91 0.82 o 6 4 5 472.94 489.62 3.08 o 8 4 5 155.39 132.49 1.29 o 10 4 5 23.78 20.88 0.94 o 1 5 5 222.44 242.48 1.38 o 3 5 5 103.89 117.47 1.10 o 5 5 5 9.36 10.00 0.84 o 7 5 5 19.08 19.58 0.98 o 9 5 5 290.81 285.61 5.53 o 0 6 5 659.21 627.53 10.53 o 2 6 5 6.61 9.92 0.94 o 4 6 5 52.91 50.82 1.10 o 6 6 5 21.92 24.16 0.93 o 8 6 5 317.85 303.47 6.08 o 1 7 5 118.51 120.34 1.76 o 3 7 5 40.22 36.99 0.95 o 5 7 5 0.07 2.07 0.91 o 7 7 5 77.45 70.71 2.00 o 0 8 5 608.44 552.30 9.09 o 2 8 5 17.40 16.30 1.23 o 4 8 5 0.56 0.73 1.11 o 0 0 6 278.54 283.54 2.65 o 4 0 6 143.21 119.88 1.66 o 6 0 6 157.01 165.34 1.44 o 8 0 6 256.33 203.39 7.11 o 10 0 6 359.32 338.14 5.21 o 12 0 6 185.43 219.74 7.52 o 1 1 6 1865.70 1864.93 10.43 o 3 1 6 589.94 620.37 4.33 o 5 1 6 1245.34 1372.99 10.49 o 7 1 6 102.22 85.79 1.11 o 9 1 6 31.58 25.43 0.75 o 11 1 6 119.49 121.93 1.70 o 0 2 6 95.10 116.76 2.88 o 2 2 6 652.60 651.45 4.04 o 4 2 6 471.88 516.72 5.79 o 6 2 6 5.39 5.50 0.90 o 8 2 6 135.64 98.48 1.05 o 10 2 6 110.02 108.65 1.26 o 12 2 6 143.52 167.31 4.19 o 1 3 6 110.75 129.70 2.31 o 3 3 6 226.25 239.03 1.18 o 5 3 6 245.76 278.47 2.76 o 7 3 6 49.41 51.81 0.84 o 9 3 6 9.26 8.74 0.75 o 11 3 6 94.39 97.90 2.42 o 0 4 6 397.61 381.99 2.36 o 2 4 6 37.82 39.70 1.03 o 4 4 6 313.55 333.24 2.40 o 6 4 6 101.14 103.69 1.14 o 8 4 6 72.45 65.92 0.89 o 10 4 6 1.05 2.15 0.98 o 1 5 6 0.97 0.45 1.01 o 3 5 6 530.10 522.96 2.66 o 5 5 6 110.90 123.85 1.15 o 7 5 6 60.29 54.80 1.01 o 9 5 6 22.74 28.44 0.94 o 0 6 6 250.21 237.76 5.89 o 2 6 6 5.67 10.18 0.95 o 4 6 6 100.30 106.22 0.98 o 6 6 6 108.26 113.59 1.65 o 8 6 6 13.13 13.07 1.04 o 1 7 6 17.99 15.77 1.51 o 3 7 6 67.49 69.90 1.12 o 5 7 6 1.81 3.43 0.90 o 7 7 6 30.14 32.61 1.02 o 0 8 6 1.18 4.80 2.28 o 2 8 6 8.97 9.96 1.38 o 4 8 6 28.47 28.89 1.17 o 1 1 7 1342.71 1376.53 7.09 o 3 1 7 161.30 168.46 1.67 o 5 1 7 177.92 184.36 1.19 o 7 1 7 121.07 104.08 1.08 o 9 1 7 20.50 20.56 0.94 o 11 1 7 1.02 2.66 0.92 o 0 2 7 74.42 74.15 1.71 o 2 2 7 1270.13 1279.40 7.46 o 4 2 7 75.50 61.99 0.91 o 6 2 7 86.50 89.78 0.86 o 8 2 7 6.06 3.68 0.72 o 10 2 7 111.38 104.35 1.44 o 12 2 7 7.08 11.76 0.84 o 1 3 7 344.53 355.23 2.19 o 3 3 7 13.57 22.92 0.78 o 5 3 7 248.29 248.15 3.28 o 7 3 7 151.01 117.64 1.74 o 9 3 7 24.89 22.99 1.12 o 11 3 7 0.81 2.97 1.00 o 0 4 7 534.07 509.07 14.00 o 2 4 7 202.20 194.02 1.91 o 4 4 7 153.22 160.75 1.01 o 6 4 7 4.23 4.57 0.92 o 8 4 7 60.01 55.25 1.09 o 10 4 7 104.39 97.77 2.09 o 1 5 7 153.76 150.89 2.67 o 3 5 7 27.02 30.88 1.11 o 5 5 7 167.99 170.39 2.04 o 7 5 7 66.71 64.00 0.88 o 9 5 7 46.01 49.62 2.24 o 0 6 7 91.19 90.32 2.21 o 2 6 7 175.57 164.73 2.02 o 4 6 7 68.15 65.57 0.98 o 6 6 7 46.84 47.80 0.99 o 8 6 7 43.40 34.90 1.03 o 1 7 7 125.45 113.00 1.87 o 3 7 7 104.94 104.36 1.27 o 5 7 7 138.02 138.34 1.82 o 7 7 7 21.19 21.34 1.03 o 0 8 7 61.50 60.29 2.72 o 2 8 7 21.88 19.31 2.69 o 4 8 7 128.00 111.95 3.86 o 0 0 8 929.16 1068.88 55.22 o 2 0 8 1981.44 2110.40 21.36 o 4 0 8 1843.64 1797.94 39.40 o 6 0 8 694.64 739.66 5.57 o 8 0 8 215.27 155.10 11.24 o 10 0 8 109.68 102.07 1.19 o 12 0 8 143.64 153.36 4.46 o 1 1 8 3861.24 4106.17 9.01 o 3 1 8 44.52 60.87 1.12 o 5 1 8 64.93 42.99 0.80 o 7 1 8 742.56 632.30 5.62 o 9 1 8 580.32 520.23 3.07 o 11 1 8 19.57 17.39 0.84 o 0 2 8 1817.27 2007.22 9.12 o 2 2 8 184.43 205.50 1.74 o 4 2 8 260.67 266.44 2.01 o 6 2 8 99.72 109.52 1.21 o 8 2 8 270.83 207.38 1.24 o 10 2 8 64.23 59.73 1.07 o 12 2 8 74.13 82.44 2.10 o 1 3 8 401.06 455.11 7.81 o 3 3 8 93.87 83.41 0.90 o 5 3 8 0.89 4.79 0.88 o 7 3 8 240.42 228.26 2.01 o 9 3 8 181.38 172.10 2.09 o 11 3 8 22.92 20.17 1.16 o 0 4 8 466.93 530.26 7.45 o 2 4 8 88.13 89.68 1.23 o 4 4 8 111.10 117.12 1.07 o 6 4 8 14.36 19.50 0.90 o 8 4 8 116.85 90.57 1.03 o 10 4 8 34.29 39.46 1.08 o 1 5 8 362.03 365.64 7.90 o 3 5 8 0.90 2.72 0.86 o 5 5 8 21.53 22.38 0.93 o 7 5 8 118.57 126.51 1.54 o 9 5 8 51.00 49.71 1.41 o 0 6 8 37.91 47.03 2.07 o 2 6 8 45.47 47.33 1.09 o 4 6 8 17.80 20.38 0.95 o 6 6 8 2.42 4.79 0.96 o 8 6 8 17.17 16.29 1.02 o 1 7 8 5.75 10.61 1.43 o 3 7 8 0.71 2.23 1.08 o 5 7 8 3.65 4.85 1.06 o 7 7 8 3.46 4.63 0.98 o 0 8 8 11.44 15.48 2.64 o 2 8 8 1.02 3.34 1.28 o 4 8 8 20.76 21.21 1.49 o 1 1 9 48.69 47.56 0.99 o 3 1 9 179.80 186.16 1.85 o 5 1 9 0.10 1.98 0.78 o 7 1 9 0.00 3.35 0.75 o 9 1 9 20.47 23.28 0.75 o 11 1 9 0.00 1.00 0.82 o 0 2 9 688.94 733.34 7.91 o 2 2 9 24.57 32.92 0.92 o 4 2 9 145.60 151.63 2.22 o 6 2 9 63.30 64.66 1.38 o 8 2 9 5.93 4.87 1.08 o 10 2 9 50.63 55.44 0.84 o 12 2 9 90.58 93.05 3.31 o 1 3 9 155.04 137.24 1.31 o 3 3 9 1.07 2.09 0.84 o 5 3 9 214.00 230.44 3.30 o 7 3 9 24.38 24.20 1.05 o 9 3 9 24.67 27.80 1.02 o 11 3 9 8.14 11.96 1.00 o 0 4 9 18.59 22.60 2.63 o 2 4 9 353.81 349.42 3.35 o 4 4 9 98.52 102.58 0.98 o 6 4 9 1.18 1.51 0.87 o 8 4 9 1.63 4.97 0.94 o 10 4 9 62.48 63.89 1.74 o 1 5 9 20.25 21.09 2.88 o 3 5 9 87.80 84.09 1.04 o 5 5 9 238.53 236.61 3.28 o 7 5 9 0.80 2.04 0.85 o 9 5 9 3.97 4.83 1.21 o 0 6 9 22.32 25.99 1.99 o 2 6 9 10.31 13.94 1.22 o 4 6 9 509.05 514.43 6.41 o 6 6 9 4.04 1.50 0.94 o 8 6 9 0.11 1.96 0.97 o 1 7 9 30.60 30.56 1.71 o 3 7 9 90.32 86.10 1.27 o 5 7 9 92.04 95.95 3.16 o 0 8 9 0.36 4.25 2.28 o 2 8 9 1.40 5.28 1.90 o 2 0 10 2036.42 2181.70 8.55 o 4 0 10 0.45 2.12 1.11 o 6 0 10 1.24 2.99 1.19 o 8 0 10 347.93 272.55 2.11 o 10 0 10 661.29 659.85 4.45 o 12 0 10 80.97 84.23 5.42 o 1 1 10 2997.55 2985.96 32.13 o 3 1 10 10.64 11.68 0.76 o 5 1 10 777.48 723.17 7.14 o 7 1 10 928.03 856.07 6.36 o 9 1 10 126.19 102.62 0.84 o 11 1 10 1.57 1.62 0.89 o 0 2 10 865.31 1052.65 5.18 o 2 2 10 2183.13 2221.96 7.07 o 4 2 10 5.83 7.11 0.82 o 6 2 10 118.01 116.51 1.28 o 8 2 10 152.43 114.22 0.95 o 10 2 10 364.18 355.68 2.79 o 1 3 10 1240.88 1247.33 10.94 o 3 3 10 331.07 328.78 2.52 o 5 3 10 592.04 562.12 5.76 o 7 3 10 242.60 225.58 2.55 o 9 3 10 202.13 185.43 2.18 o 11 3 10 4.65 9.25 1.09 o 0 4 10 120.08 138.78 1.60 o 2 4 10 184.56 174.80 1.36 o 4 4 10 206.30 202.00 1.85 o 6 4 10 142.57 133.32 1.75 o 8 4 10 88.02 88.75 2.33 o 10 4 10 13.63 14.98 1.33 o 1 5 10 0.80 2.95 1.53 o 3 5 10 112.80 119.32 1.23 o 5 5 10 40.66 39.18 1.75 o 7 5 10 9.31 14.66 0.86 o 9 5 10 128.04 120.29 2.60 o 0 6 10 19.33 20.50 2.28 o 2 6 10 1.87 2.44 1.00 o 4 6 10 320.10 318.38 1.47 o 6 6 10 70.65 70.72 1.38 o 8 6 10 43.46 39.77 1.22 o 1 7 10 0.00 4.12 3.01 o 3 7 10 98.58 105.96 2.55 o 5 7 10 17.49 19.99 1.24 o 0 8 10 0.64 5.72 2.32 o 2 8 10 2.30 4.89 1.48 o 1 1 11 54.32 53.83 1.15 o 3 1 11 418.16 416.69 1.59 o 5 1 11 46.99 43.46 0.94 o 7 1 11 100.97 98.09 0.91 o 9 1 11 2.62 4.90 0.82 o 11 1 11 17.22 18.34 1.40 o 0 2 11 876.17 887.71 9.06 o 2 2 11 38.68 40.21 0.94 o 4 2 11 829.69 788.70 4.76 o 6 2 11 112.63 104.47 1.12 o 8 2 11 27.74 22.00 0.82 o 10 2 11 128.24 136.13 3.10 o 1 3 11 905.38 872.24 2.23 o 3 3 11 350.97 335.26 3.37 o 5 3 11 0.69 1.02 0.75 o 7 3 11 686.44 686.17 4.26 o 9 3 11 0.10 0.00 0.87 o 11 3 11 62.22 58.01 2.34 o 0 4 11 97.02 94.17 7.74 o 2 4 11 269.07 245.05 4.02 o 4 4 11 1688.95 1675.24 17.03 o 6 4 11 38.07 34.47 0.86 o 8 4 11 7.54 5.48 0.84 o 10 4 11 170.19 163.44 5.03 o 1 5 11 458.73 444.68 4.83 o 3 5 11 194.69 191.18 1.57 o 5 5 11 19.65 21.26 0.92 o 7 5 11 407.39 398.41 5.93 o 9 5 11 3.96 5.24 0.91 o 0 6 11 82.87 74.01 2.17 o 2 6 11 0.75 1.43 1.55 o 4 6 11 585.11 573.40 10.38 o 6 6 11 20.90 23.99 1.31 o 1 7 11 30.41 28.61 1.74 o 3 7 11 94.17 87.40 1.52 o 5 7 11 67.34 67.88 3.05 o 0 8 11 0.00 0.00 2.77 o 0 0 12 0.15 1.40 1.44 o 2 0 12 220.22 248.47 2.10 o 4 0 12 4809.98 4580.15 62.08 o 6 0 12 299.22 280.76 3.07 o 8 0 12 104.26 88.64 2.02 o 10 0 12 26.46 27.62 1.54 o 1 1 12 97.44 78.02 0.93 o 3 1 12 945.81 973.97 3.66 o 5 1 12 557.85 514.23 3.12 o 7 1 12 387.63 400.88 1.53 o 9 1 12 66.92 52.85 1.39 o 11 1 12 79.57 86.52 2.22 o 0 2 12 728.47 741.98 9.31 o 2 2 12 0.90 3.86 0.86 o 4 2 12 3930.29 3773.90 35.53 o 6 2 12 78.29 66.78 1.07 o 8 2 12 210.41 202.75 1.37 o 10 2 12 14.61 16.96 1.06 o 1 3 12 64.43 52.81 1.87 o 3 3 12 73.13 81.23 1.09 o 5 3 12 147.72 146.63 0.98 o 7 3 12 134.57 140.55 1.15 o 9 3 12 28.23 26.31 1.08 o 0 4 12 505.57 513.46 9.13 o 2 4 12 56.64 56.92 1.25 o 4 4 12 1119.44 1115.01 10.10 o 6 4 12 17.08 18.36 1.08 o 8 4 12 167.01 153.63 2.97 o 10 4 12 4.39 5.63 1.12 o 1 5 12 79.13 76.92 4.26 o 3 5 12 51.13 57.47 1.92 o 5 5 12 166.17 172.33 2.76 o 7 5 12 4.03 5.44 0.86 o 9 5 12 23.78 26.37 1.32 o 0 6 12 257.78 249.12 2.85 o 2 6 12 65.33 61.67 2.78 o 4 6 12 128.56 129.68 2.64 o 6 6 12 2.32 1.09 1.05 o 1 7 12 41.40 40.31 1.96 o 3 7 12 2.13 5.65 1.18 o 5 7 12 16.98 17.40 1.30 o 1 1 13 104.25 104.50 0.96 o 3 1 13 47.97 50.55 1.16 o 5 1 13 40.06 36.83 0.97 o 7 1 13 22.72 24.31 0.94 o 9 1 13 1.45 2.40 0.90 o 11 1 13 0.56 3.08 0.95 o 0 2 13 58.08 49.61 1.79 o 2 2 13 57.92 56.98 0.93 o 4 2 13 107.20 99.07 0.95 o 6 2 13 1.28 1.97 0.78 o 8 2 13 7.49 9.32 0.86 o 10 2 13 7.27 6.43 0.88 o 1 3 13 32.78 36.98 1.22 o 3 3 13 7.42 8.18 0.86 o 5 3 13 0.09 1.06 0.96 o 7 3 13 22.90 20.01 0.86 o 9 3 13 1.16 1.23 0.94 o 0 4 13 41.39 46.05 4.09 o 2 4 13 7.54 7.11 1.33 o 4 4 13 27.33 28.35 0.95 o 6 4 13 8.19 12.03 0.84 o 8 4 13 0.22 1.76 0.85 o 1 5 13 16.03 16.99 1.69 o 3 5 13 5.68 10.86 2.11 o 5 5 13 0.18 0.00 1.17 o 7 5 13 17.50 16.19 0.96 o 0 6 13 2.40 2.57 2.03 o 2 6 13 7.30 6.64 1.18 o 4 6 13 48.53 56.26 1.64 o 6 6 13 0.08 2.70 1.11 o 1 7 13 29.88 26.86 3.12 o 3 7 13 1.24 1.41 2.09 o 0 0 14 1013.24 1044.12 4.78 o 2 0 14 198.41 174.24 1.71 o 4 0 14 7214.16 6705.93 10.29 o 6 0 14 73.87 67.24 2.25 o 8 0 14 358.38 362.69 3.78 o 10 0 14 174.07 173.97 2.90 o 1 1 14 763.62 736.07 3.73 o 3 1 14 285.86 262.52 1.44 o 5 1 14 89.27 86.16 1.05 o 7 1 14 893.74 869.04 2.87 o 9 1 14 12.34 15.89 1.52 o 0 2 14 309.51 326.24 5.39 o 2 2 14 3.70 5.32 0.88 o 4 2 14 3855.92 3731.07 15.32 o 6 2 14 91.32 88.79 1.26 o 8 2 14 210.72 219.50 2.27 o 10 2 14 51.36 53.83 1.92 o 1 3 14 23.87 28.45 1.09 o 3 3 14 222.13 209.90 1.60 o 5 3 14 226.39 221.19 2.65 o 7 3 14 168.13 169.02 1.98 o 9 3 14 9.16 9.03 0.87 o 0 4 14 521.61 506.52 3.07 o 2 4 14 12.03 14.58 1.21 o 4 4 14 1220.21 1267.90 10.62 o 6 4 14 2.79 1.37 0.87 o 8 4 14 160.00 176.47 5.08 o 1 5 14 0.21 0.25 1.85 o 3 5 14 1.34 4.12 1.50 o 5 5 14 53.97 55.17 1.15 o 7 5 14 5.19 7.63 0.96 o 0 6 14 448.89 445.45 3.13 o 2 6 14 5.74 8.17 1.06 o 4 6 14 238.59 240.68 4.19 o 6 6 14 5.20 10.15 1.17 o 1 7 14 41.43 41.44 1.80 o 3 7 14 0.79 2.65 1.18 o 1 1 15 221.96 206.21 1.62 o 3 1 15 14.39 17.64 0.80 o 5 1 15 8.27 10.16 0.80 o 7 1 15 112.17 115.75 0.94 o 9 1 15 0.70 2.29 1.31 o 0 2 15 113.79 105.57 1.36 o 2 2 15 149.30 147.94 1.34 o 4 2 15 576.95 548.76 2.20 o 6 2 15 28.09 32.83 0.88 o 8 2 15 2.22 4.83 0.89 o 10 2 15 104.88 95.77 2.94 o 1 3 15 226.31 201.61 1.36 o 3 3 15 350.69 344.71 2.20 o 5 3 15 11.32 11.13 0.84 o 7 3 15 275.86 276.78 2.94 o 9 3 15 9.23 11.32 1.01 o 0 4 15 347.82 318.63 2.75 o 2 4 15 13.99 15.29 1.12 o 4 4 15 446.11 436.64 2.72 o 6 4 15 67.76 70.73 1.37 o 8 4 15 14.67 15.38 0.95 o 1 5 15 92.12 93.48 1.66 o 3 5 15 179.10 171.72 1.79 o 5 5 15 25.85 21.06 1.78 o 7 5 15 130.24 141.75 3.25 o 0 6 15 7.50 2.42 2.12 o 2 6 15 22.42 27.95 1.77 o 4 6 15 262.49 248.75 2.54 o 1 7 15 28.14 28.48 1.67 o 0 0 16 1212.74 1108.64 4.82 o 2 0 16 500.87 499.91 1.77 o 4 0 16 302.78 323.08 3.96 o 6 0 16 0.44 0.85 1.24 o 8 0 16 223.37 228.57 9.97 o 10 0 16 165.63 154.89 1.67 o 1 1 16 176.72 161.08 13.47 o 3 1 16 3.04 6.58 0.79 o 5 1 16 242.59 252.07 2.01 o 7 1 16 55.36 63.76 0.89 o 9 1 16 2.21 4.19 1.10 o 0 2 16 1081.84 978.45 10.08 o 2 2 16 80.44 81.59 0.98 o 4 2 16 684.06 709.53 1.99 o 6 2 16 0.01 1.89 0.85 o 8 2 16 205.35 219.77 3.31 o 1 3 16 0.52 2.84 1.02 o 3 3 16 6.98 10.06 0.90 o 5 3 16 87.54 90.37 1.79 o 7 3 16 4.59 2.58 0.88 o 9 3 16 16.65 18.78 0.94 o 0 4 16 122.21 103.38 2.23 o 2 4 16 21.42 24.20 1.19 o 4 4 16 562.75 573.40 5.46 o 6 4 16 53.76 58.37 1.05 o 8 4 16 72.10 73.36 1.63 o 1 5 16 3.65 4.26 1.33 o 3 5 16 194.64 202.79 1.99 o 5 5 16 90.04 95.36 1.22 o 7 5 16 19.19 18.04 1.37 o 0 6 16 0.06 0.00 2.42 o 2 6 16 8.05 8.64 1.08 o 4 6 16 255.94 236.20 1.49 o 1 1 17 20.69 23.48 1.04 o 3 1 17 1.78 1.73 0.80 o 5 1 17 12.65 15.73 0.80 o 7 1 17 1.70 3.62 0.79 o 9 1 17 2.61 4.34 1.57 o 0 2 17 36.42 49.01 1.61 o 2 2 17 11.34 15.53 0.91 o 4 2 17 33.66 33.28 1.03 o 6 2 17 10.91 16.10 0.91 o 8 2 17 3.03 2.52 0.92 o 1 3 17 19.20 19.56 1.02 o 3 3 17 11.71 19.45 1.08 o 5 3 17 12.27 16.07 0.84 o 7 3 17 6.52 7.33 0.87 o 0 4 17 122.27 136.68 2.55 o 2 4 17 13.39 13.62 1.20 o 4 4 17 309.75 313.83 2.15 o 6 4 17 39.30 46.42 1.63 o 1 5 17 34.52 33.89 1.49 o 3 5 17 4.32 2.33 1.78 o 5 5 17 34.29 36.47 1.26 o 0 6 17 0.28 4.31 2.54 o 2 6 17 0.03 1.01 1.14 o 0 0 18 221.19 194.55 2.70 o 2 0 18 165.94 140.20 1.33 o 4 0 18 0.26 1.45 1.11 o 6 0 18 101.04 108.75 1.58 o 8 0 18 56.94 71.46 2.67 o 1 1 18 284.38 223.99 2.01 o 3 1 18 33.65 42.53 1.13 o 5 1 18 88.13 85.32 1.15 o 7 1 18 119.49 129.95 1.27 o 9 1 18 145.87 147.90 3.89 o 0 2 18 65.86 42.29 1.49 o 2 2 18 280.68 258.76 1.35 o 4 2 18 12.62 13.82 0.83 o 6 2 18 146.27 153.04 2.83 o 8 2 18 39.54 48.79 1.29 o 1 3 18 280.50 261.60 2.73 o 3 3 18 63.53 65.41 1.12 o 5 3 18 77.53 76.88 1.64 o 7 3 18 81.51 88.98 2.52 o 0 4 18 74.22 65.50 2.18 o 2 4 18 67.42 68.74 2.71 o 4 4 18 6.35 7.73 1.08 o 6 4 18 46.89 45.93 1.08 o 1 5 18 13.67 14.38 1.51 o 3 5 18 1.92 1.16 1.73 o 5 5 18 7.16 5.32 1.17 o 0 6 18 55.58 55.89 2.74 o 2 6 18 2.44 3.68 2.21 o 1 1 19 2.59 5.59 0.97 o 3 1 19 14.34 15.22 0.82 o 5 1 19 1.43 5.10 0.83 o 7 1 19 0.55 2.28 0.97 o 0 2 19 86.47 85.99 1.71 o 2 2 19 3.18 5.66 0.86 o 4 2 19 20.21 25.13 0.89 o 6 2 19 11.62 12.54 0.86 o 8 2 19 1.90 4.33 0.93 o 1 3 19 36.08 33.41 1.13 o 3 3 19 1.05 2.39 0.93 o 5 3 19 61.82 71.71 2.26 o 7 3 19 13.28 13.57 0.93 o 0 4 19 18.58 15.16 2.06 o 2 4 19 55.78 61.01 1.58 o 4 4 19 24.11 27.96 1.55 o 6 4 19 0.86 2.74 0.98 o 1 5 19 15.45 16.16 1.65 o 3 5 19 30.60 35.18 1.28 o 0 0 20 22.49 26.16 2.68 o 2 0 20 39.22 36.64 1.19 o 4 0 20 71.62 86.69 1.57 o 6 0 20 213.06 232.32 3.96 o 1 1 20 63.57 62.87 1.18 o 3 1 20 30.92 30.92 0.87 o 5 1 20 14.31 18.85 0.85 o 7 1 20 13.80 17.09 1.10 o 0 2 20 31.09 27.30 1.59 o 2 2 20 1.82 2.85 0.89 o 4 2 20 28.60 34.57 0.87 o 6 2 20 47.51 53.52 1.17 o 1 3 20 23.54 24.68 1.30 o 3 3 20 28.59 32.15 1.53 o 5 3 20 24.30 25.65 1.00 o 0 4 20 102.74 94.99 2.69 o 2 4 20 13.67 16.59 2.68 o 4 4 20 64.34 75.47 1.79 o 1 5 20 76.13 73.55 1.74 o 1 1 21 7.27 8.58 1.16 o 3 1 21 77.91 86.42 1.45 o 5 1 21 11.94 13.44 0.92 o 0 2 21 71.45 79.38 1.69 o 2 2 21 10.70 11.44 0.99 o 4 2 21 26.26 32.89 0.99 o 6 2 21 106.36 102.70 2.05 o 1 3 21 0.01 1.83 1.25 o 3 3 21 135.17 143.39 3.16 o 5 3 21 12.30 13.05 1.01 o 0 4 21 0.15 0.00 2.23 o 2 4 21 0.16 2.37 1.40 o 0 0 22 365.92 379.08 3.74 o 2 0 22 39.16 32.60 2.13 o 4 0 22 188.04 222.58 10.32 o 6 0 22 170.05 148.40 5.19 o 1 1 22 0.08 1.55 1.12 o 3 1 22 457.19 474.39 4.92 o 5 1 22 199.98 194.58 5.94 o 0 2 22 79.69 73.45 1.75 o 2 2 22 2.88 2.56 1.02 o 4 2 22 190.77 216.61 4.70 o 1 3 22 2.07 5.69 1.40 o 3 3 22 91.45 97.02 3.20 o 0 4 22 1.14 5.61 2.65 o 1 1 23 0.08 0.18 1.08 o 3 1 23 13.68 20.17 2.66 o 0 2 23 101.06 104.98 3.59 o 2 2 23 0.01 1.21 1.14 o 4 2 23 1.20 1.98 1.06 o 1 3 23 44.25 42.22 1.66 o 0 0 24 35.44 35.93 2.13 o 2 0 24 11.82 9.33 2.51 o 1 1 24 41.23 37.65 1.30 o 3 1 24 107.80 99.24 2.55 o 0 2 24 14.82 17.95 1.85 o