#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/65/2016554.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016554_Fobs loop_ _publ_author_name 'Orozco, Fab\'ian' 'Insuasty, Braulio' 'Low, John N.' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Hydrogen-bonded sheet structures in neutral, anionic and hydrated 6-amino-2-(morpholin-4-yl)-5-nitrosopyrimidines ; _journal_coeditor_code GG3151 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o220 _journal_page_last o225 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-I 2ya' _symmetry_space_group_name_H-M 'I 1 2/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.045 _cell_angle_gamma 90.000 _cell_length_a 9.4410 _cell_length_b 16.3470 _cell_length_c 18.7990 _exptl_crystal_F_000 1328.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file gg3151IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50 R = 0.05' _shelx_refln_list_code 4 _shelx_F_calc_maximum 259.75 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33669.23 31650.53 221.12 o 4 0 0 457.97 413.47 21.97 o 6 0 0 239.08 376.49 22.62 o 8 0 0 244.90 285.34 35.77 o 10 0 0 135.97 236.22 27.71 o 12 0 0 793.49 837.55 46.20 o 3 1 0 5677.84 5469.07 32.65 o 5 1 0 3582.42 3502.31 30.88 o 7 1 0 611.78 577.13 20.43 o 9 1 0 7380.99 7461.53 57.58 o 11 1 0 122.19 150.30 32.49 o 2 2 0 51.74 85.21 5.66 o 4 2 0 970.82 1120.58 13.90 o 6 2 0 325.47 329.78 14.01 o 8 2 0 8.34 -4.51 18.40 o 10 2 0 33.70 57.90 18.82 o 12 2 0 8.20 2.50 35.36 o 1 3 0 61081.64 51790.72 279.54 o 3 3 0 12309.79 11768.22 44.89 o 5 3 0 3597.26 3404.02 22.35 o 7 3 0 194.92 170.18 10.77 o 9 3 0 347.59 382.75 20.03 o 11 3 0 28.54 41.97 27.98 o 0 4 0 22688.05 22041.28 166.94 o 2 4 0 610.70 663.52 8.84 o 4 4 0 6569.54 6721.04 30.69 o 6 4 0 2709.56 2806.10 24.40 o 8 4 0 595.27 530.10 16.68 o 10 4 0 823.75 782.36 25.31 o 12 4 0 19.89 -18.38 40.15 o 1 5 0 1047.89 1212.60 11.47 o 3 5 0 2022.14 2139.21 14.28 o 5 5 0 369.70 369.94 9.79 o 7 5 0 1104.90 1028.09 23.21 o 9 5 0 4685.32 4773.15 46.67 o 11 5 0 0.90 38.51 28.94 o 0 6 0 2897.35 2964.14 26.89 o 2 6 0 4.28 0.87 8.96 o 4 6 0 1993.12 2178.33 16.30 o 6 6 0 130.89 129.55 15.20 o 8 6 0 41.02 14.10 17.37 o 10 6 0 288.42 380.24 34.35 o 1 7 0 453.02 520.18 10.03 o 3 7 0 3.42 0.37 7.88 o 5 7 0 1208.10 1143.93 16.16 o 7 7 0 675.53 677.59 15.35 o 9 7 0 136.16 180.15 24.26 o 11 7 0 1.75 -18.33 33.99 o 0 8 0 5131.90 5146.59 42.02 o 2 8 0 659.20 669.93 10.51 o 4 8 0 0.53 23.17 8.60 o 6 8 0 26.57 8.55 13.89 o 8 8 0 254.76 275.46 19.29 o 10 8 0 895.95 829.84 36.16 o 1 9 0 717.11 615.96 11.76 o 3 9 0 0.10 46.77 12.00 o 5 9 0 88.75 128.12 11.58 o 7 9 0 337.93 334.28 17.66 o 9 9 0 410.76 389.78 31.78 o 11 9 0 494.09 574.53 56.43 o 0 10 0 412.33 426.02 17.00 o 2 10 0 184.22 226.68 11.55 o 4 10 0 25.43 25.67 13.32 o 6 10 0 786.43 885.22 20.18 o 8 10 0 12.96 -4.30 26.04 o 10 10 0 4.22 46.39 32.60 o 1 11 0 489.40 500.45 14.39 o 3 11 0 87.40 107.49 16.01 o 5 11 0 691.54 635.47 19.75 o 7 11 0 29.40 19.04 28.21 o 9 11 0 4.14 -23.74 25.73 o 0 12 0 128.82 71.62 20.89 o 2 12 0 43.29 35.96 13.71 o 4 12 0 961.96 941.55 19.88 o 6 12 0 0.03 2.94 23.47 o 8 12 0 398.50 364.62 32.50 o 10 12 0 233.99 364.07 79.99 o 1 13 0 1128.82 1011.58 20.10 o 3 13 0 7.50 20.64 15.18 o 5 13 0 179.91 188.72 27.54 o 7 13 0 53.58 54.01 32.93 o 9 13 0 3.13 20.03 28.05 o 0 14 0 880.17 822.92 53.99 o 2 14 0 0.02 1.66 21.60 o 4 14 0 112.94 31.86 38.04 o 6 14 0 29.14 13.07 25.12 o 8 14 0 6.24 -2.83 46.66 o 1 15 0 28.71 14.34 21.79 o 3 15 0 4.21 15.47 24.33 o 5 15 0 159.58 124.63 33.69 o 7 15 0 38.80 34.45 33.17 o 0 16 0 1156.40 1161.48 40.77 o 2 16 0 32.80 33.98 27.71 o 4 16 0 150.37 31.64 30.96 o 6 16 0 463.61 472.28 36.54 o 8 16 0 44.63 84.21 87.87 o 1 17 0 194.55 286.45 29.99 o 3 17 0 24.90 45.52 33.32 o 5 17 0 133.97 181.10 36.15 o 7 17 0 40.30 -2.11 35.06 o 0 18 0 995.11 952.89 90.14 o 2 18 0 951.27 1017.96 39.49 o 4 18 0 40.39 98.27 33.99 o 6 18 0 8.62 -50.06 50.06 o 1 19 0 152.76 113.76 36.99 o 3 19 0 198.00 210.99 33.71 o 5 19 0 9.05 14.77 33.47 o 0 20 0 1787.35 1696.28 80.29 o 2 20 0 21.96 60.50 50.00 o 4 20 0 45.19 3.71 32.63 o 1 21 0 575.63 319.50 48.62 o -12 1 1 1242.09 1430.44 38.73 o -10 1 1 38.18 25.94 18.10 o -8 1 1 13.69 14.66 19.75 o -6 1 1 154.42 125.39 9.00 o -4 1 1 690.54 507.40 10.67 o -2 1 1 6596.95 6540.89 29.77 o 2 1 1 1208.74 976.48 9.37 o 4 1 1 633.26 633.69 10.91 o 6 1 1 4310.32 4309.73 33.33 o 8 1 1 9904.36 9994.74 65.17 o 10 1 1 0.74 30.22 18.03 o 12 1 1 121.32 72.91 39.24 o -11 2 1 158.63 179.05 28.54 o -9 2 1 1509.85 1535.24 28.09 o -7 2 1 6894.41 6960.99 44.19 o -5 2 1 7352.56 7635.54 43.26 o -3 2 1 11747.72 11461.78 50.79 o -1 2 1 1933.16 2263.28 11.40 o 1 2 1 0.26 -4.61 4.61 o 3 2 1 2984.64 3040.24 18.53 o 5 2 1 23.12 55.16 11.92 o 7 2 1 321.69 382.33 26.63 o 9 2 1 0.60 30.10 18.79 o 11 2 1 1036.72 1107.22 29.50 o -12 3 1 5.52 -9.66 34.13 o -10 3 1 49.73 31.86 27.64 o -8 3 1 311.42 395.11 15.62 o -6 3 1 76.14 39.78 11.22 o -4 3 1 324.45 452.71 8.27 o -2 3 1 3618.81 3492.51 17.13 o 0 3 1 109.08 77.08 5.80 o 2 3 1 22814.09 21502.45 84.98 o 4 3 1 1044.65 995.67 10.43 o 6 3 1 4.01 15.61 10.45 o 8 3 1 369.75 365.81 20.94 o 10 3 1 270.62 282.18 19.75 o 12 3 1 54.53 27.75 38.11 o -11 4 1 465.13 481.27 39.01 o -9 4 1 2867.03 2750.38 32.75 o -7 4 1 1854.76 1888.57 22.12 o -5 4 1 807.90 768.38 10.43 o -3 4 1 17.48 81.16 19.02 o -1 4 1 16728.77 16643.44 68.06 o 1 4 1 7805.17 8233.21 38.54 o 3 4 1 20443.41 19185.04 69.93 o 5 4 1 4585.49 4496.54 25.33 o 7 4 1 550.14 543.78 15.37 o 9 4 1 1664.29 1685.65 29.20 o 11 4 1 77.85 122.80 32.20 o -10 5 1 66.21 36.71 20.75 o -8 5 1 413.98 383.10 19.88 o -6 5 1 43.97 23.59 10.31 o -4 5 1 6770.13 7267.63 32.42 o -2 5 1 701.14 689.01 10.33 o 0 5 1 4610.43 4989.88 25.84 o 2 5 1 5436.46 5114.09 24.89 o 4 5 1 1.71 8.62 7.21 o 6 5 1 1822.52 1701.11 19.19 o 8 5 1 0.00 -7.12 15.30 o 10 5 1 679.69 775.65 29.73 o -11 6 1 262.36 212.56 33.36 o -9 6 1 0.73 3.37 22.26 o -7 6 1 1450.69 1430.94 19.81 o -5 6 1 3073.80 3062.83 20.22 o -3 6 1 9669.20 10231.78 43.72 o -1 6 1 6629.06 6551.08 31.49 o 1 6 1 3407.61 3320.14 21.22 o 3 6 1 3686.05 3885.74 20.97 o 5 6 1 168.38 254.06 9.19 o 7 6 1 99.21 97.40 17.72 o 9 6 1 338.73 374.89 19.76 o 11 6 1 308.21 320.34 36.44 o -10 7 1 2085.27 2126.24 43.68 o -8 7 1 5.96 -4.90 18.34 o -6 7 1 962.38 979.75 15.09 o -4 7 1 13805.92 14509.72 64.43 o -2 7 1 4762.15 4965.37 27.10 o 0 7 1 487.95 473.08 11.06 o 2 7 1 3.15 28.80 9.86 o 4 7 1 636.27 696.02 10.38 o 6 7 1 635.98 694.59 12.26 o 8 7 1 3786.27 3803.62 42.23 o 10 7 1 86.03 75.30 37.99 o -11 8 1 98.24 6.45 79.15 o -9 8 1 1043.07 981.44 33.71 o -7 8 1 1058.38 944.71 26.05 o -5 8 1 1655.48 1621.80 19.62 o -3 8 1 3875.00 3821.35 24.50 o -1 8 1 71.17 32.05 10.60 o 1 8 1 226.50 198.84 9.16 o 3 8 1 95.37 89.77 10.73 o 5 8 1 606.51 585.47 13.70 o 7 8 1 363.92 330.14 14.50 o 9 8 1 68.59 85.41 28.58 o 11 8 1 195.72 279.93 52.77 o -10 9 1 832.06 827.32 37.99 o -8 9 1 1.33 0.07 21.39 o -6 9 1 32.32 2.52 15.32 o -4 9 1 497.86 513.33 13.70 o -2 9 1 1809.25 1923.70 17.56 o 0 9 1 18.67 13.25 10.81 o 2 9 1 4399.02 4318.33 26.67 o 4 9 1 109.13 116.82 11.80 o 6 9 1 93.69 87.40 14.57 o 8 9 1 245.63 185.12 34.17 o 10 9 1 2.10 -1.89 29.38 o -9 10 1 164.77 134.19 24.31 o -7 10 1 1163.52 1145.14 31.28 o -5 10 1 397.41 425.89 14.15 o -3 10 1 352.29 384.34 16.26 o -1 10 1 292.71 272.30 13.28 o 1 10 1 22.86 37.72 11.31 o 3 10 1 3763.40 4033.80 37.14 o 5 10 1 872.78 860.80 18.69 o 7 10 1 957.31 936.41 30.79 o 9 10 1 1147.81 1223.52 43.38 o -10 11 1 11.35 71.44 37.31 o -8 11 1 828.99 835.48 40.40 o -6 11 1 15.65 18.64 18.89 o -4 11 1 1971.94 1800.75 22.29 o -2 11 1 658.64 681.98 14.96 o 0 11 1 223.64 266.75 15.08 o 2 11 1 738.18 672.87 15.07 o 4 11 1 1036.92 1122.92 18.15 o 6 11 1 1047.09 1061.61 34.31 o 8 11 1 0.51 -9.77 24.91 o 10 11 1 4.40 -12.67 37.93 o -9 12 1 27.76 121.76 58.17 o -7 12 1 24.49 25.62 26.58 o -5 12 1 25.51 85.13 23.65 o -3 12 1 259.51 275.66 14.88 o -1 12 1 6.89 6.01 13.71 o 1 12 1 756.98 753.15 19.62 o 3 12 1 12.98 16.62 15.63 o 5 12 1 58.10 61.22 19.37 o 7 12 1 1.19 34.78 29.87 o 9 12 1 186.64 163.66 31.97 o -8 13 1 61.54 56.20 29.58 o -6 13 1 1310.63 1353.45 42.72 o -4 13 1 320.62 277.44 26.96 o -2 13 1 0.77 0.81 19.32 o 0 13 1 370.12 343.13 20.51 o 2 13 1 2186.73 2263.15 28.57 o 4 13 1 122.75 119.74 16.35 o 6 13 1 24.00 4.07 28.49 o 8 13 1 111.77 127.91 40.83 o -9 14 1 29.93 -8.89 34.58 o -7 14 1 890.89 821.31 37.66 o -5 14 1 16.31 4.48 25.96 o -3 14 1 26.32 22.66 25.40 o -1 14 1 0.08 7.69 20.13 o 1 14 1 147.33 153.76 18.39 o 3 14 1 99.82 124.82 20.15 o 5 14 1 2.10 43.38 38.25 o 7 14 1 544.88 582.43 39.76 o 9 14 1 273.01 439.14 76.42 o -8 15 1 25.56 -37.81 44.20 o -6 15 1 38.64 88.75 28.21 o -4 15 1 4.14 85.54 28.58 o -2 15 1 2.75 29.16 27.33 o 0 15 1 334.94 306.35 29.59 o 2 15 1 3569.41 3722.58 45.83 o 4 15 1 120.60 75.35 26.82 o 6 15 1 0.04 -6.29 32.24 o 8 15 1 63.71 36.16 32.99 o -7 16 1 189.91 130.77 41.89 o -5 16 1 202.60 262.22 30.00 o -3 16 1 21.44 12.00 29.18 o -1 16 1 690.53 678.50 25.62 o 1 16 1 466.89 515.88 26.75 o 3 16 1 1341.33 1271.66 35.86 o 5 16 1 270.55 214.22 31.84 o 7 16 1 56.74 14.54 54.78 o -6 17 1 18.57 -15.80 36.93 o -4 17 1 0.38 6.96 26.30 o -2 17 1 3.10 -5.89 27.06 o 0 17 1 126.70 142.14 25.53 o 2 17 1 244.21 240.69 38.73 o 4 17 1 386.20 388.82 32.66 o 6 17 1 843.18 946.26 39.69 o -5 18 1 32.53 14.49 38.81 o -3 18 1 2.25 17.61 33.34 o -1 18 1 64.33 17.59 32.47 o 1 18 1 4.19 7.79 33.63 o 3 18 1 94.62 103.54 52.21 o 5 18 1 70.29 119.20 43.74 o -4 19 1 0.32 11.02 33.92 o -2 19 1 208.03 207.27 45.39 o 0 19 1 2.71 50.81 41.78 o 2 19 1 362.31 468.49 52.43 o 4 19 1 5.59 -42.75 42.75 o -3 20 1 92.92 84.73 34.13 o -1 20 1 556.44 693.37 49.47 o 1 20 1 12.65 -13.11 43.18 o 3 20 1 73.86 68.44 52.73 o 0 21 1 247.59 416.06 61.85 o -12 0 2 95.15 56.67 37.68 o -10 0 2 207.19 264.13 28.36 o -8 0 2 18.52 -67.49 78.29 o -6 0 2 1143.74 1084.77 20.77 o -4 0 2 18097.33 16962.88 100.77 o -2 0 2 52973.22 46457.55 290.24 o 2 0 2 9151.68 7706.50 41.65 o 4 0 2 16603.65 17058.98 111.38 o 6 0 2 295.90 272.30 20.91 o 8 0 2 4027.03 3869.11 52.91 o 10 0 2 2253.30 2231.81 45.14 o 12 0 2 121.47 125.11 41.82 o -11 1 2 15.53 61.45 21.71 o -9 1 2 601.35 654.57 24.88 o -7 1 2 691.87 658.37 23.75 o -5 1 2 195.56 186.38 9.63 o -3 1 2 79.36 99.76 8.98 o -1 1 2 15387.66 14948.81 69.56 o 1 1 2 5360.05 5012.39 20.31 o 3 1 2 576.95 599.67 10.54 o 5 1 2 1307.03 1215.32 16.96 o 7 1 2 338.24 354.89 17.90 o 9 1 2 3045.48 3058.08 36.75 o 11 1 2 72.45 53.55 22.84 o -12 2 2 45.99 19.59 34.97 o -10 2 2 124.31 66.62 25.73 o -8 2 2 295.33 334.14 18.67 o -6 2 2 3761.40 3718.48 28.00 o -4 2 2 15171.59 15447.20 64.14 o -2 2 2 10274.87 9445.74 44.18 o 0 2 2 149.76 239.74 6.44 o 2 2 2 50.47 120.80 7.46 o 4 2 2 4570.54 4887.25 30.39 o 6 2 2 49.20 59.62 7.10 o 8 2 2 747.84 707.24 21.49 o 10 2 2 20.35 13.92 17.49 o 12 2 2 0.02 -25.00 28.62 o -11 3 2 0.33 7.44 27.27 o -9 3 2 236.58 244.23 16.90 o -7 3 2 40.37 39.56 8.97 o -5 3 2 5061.16 5352.45 32.66 o -3 3 2 185.59 210.08 9.33 o 1 3 2 26952.71 25013.83 107.66 o 3 3 2 4313.02 4542.02 21.54 o 5 3 2 75.17 49.78 8.52 o 7 3 2 918.83 910.78 16.20 o 9 3 2 392.18 391.19 22.10 o 11 3 2 1337.90 1451.29 33.64 o -12 4 2 81.25 29.75 35.54 o -10 4 2 1544.22 1555.30 30.27 o -8 4 2 28.12 34.19 17.42 o -6 4 2 3340.13 3347.56 23.03 o -4 4 2 911.82 793.42 9.67 o -2 4 2 4066.43 4040.55 20.92 o 0 4 2 19011.09 19100.45 75.26 o 2 4 2 444.11 587.74 9.10 o 4 4 2 15109.46 15777.06 60.79 o 6 4 2 1078.02 1041.20 14.69 o 8 4 2 6352.29 6213.10 50.34 o 10 4 2 40.76 6.53 19.22 o 12 4 2 2.27 35.74 39.13 o -11 5 2 850.88 956.12 38.95 o -9 5 2 49.14 63.42 27.48 o -7 5 2 43.12 64.07 12.95 o -5 5 2 295.97 410.48 10.23 o -3 5 2 3.34 7.47 7.52 o -1 5 2 234.96 227.67 8.58 o 1 5 2 23996.33 24021.53 102.87 o 3 5 2 2695.94 2831.48 15.45 o 5 5 2 1826.85 1695.38 15.28 o 7 5 2 547.08 566.11 16.09 o 9 5 2 570.37 482.83 24.19 o 11 5 2 512.38 519.45 38.55 o -10 6 2 2.05 80.74 23.36 o -8 6 2 2609.46 2540.28 32.85 o -6 6 2 6.20 21.13 12.25 o -4 6 2 4741.90 4991.77 27.16 o -2 6 2 811.26 715.10 10.05 o 0 6 2 2440.83 2396.51 18.00 o 2 6 2 8424.36 8660.89 40.03 o 4 6 2 839.89 828.47 9.86 o 6 6 2 551.01 594.14 16.39 o 8 6 2 450.67 523.63 21.14 o 10 6 2 308.81 376.46 31.85 o -11 7 2 45.14 78.02 38.36 o -9 7 2 0.28 6.02 27.18 o -7 7 2 106.00 149.47 13.77 o -5 7 2 2640.36 2595.30 22.38 o -3 7 2 2400.04 2538.55 17.32 o -1 7 2 4760.40 4815.22 25.45 o 1 7 2 59.11 42.30 9.66 o 3 7 2 854.46 766.49 11.29 o 5 7 2 7422.02 7868.67 40.85 o 7 7 2 458.88 436.40 14.58 o 9 7 2 13.67 52.65 29.84 o 11 7 2 41.45 32.40 32.84 o -10 8 2 1171.12 1263.87 47.57 o -8 8 2 984.23 1012.85 28.22 o -6 8 2 1157.66 993.57 17.02 o -4 8 2 701.95 769.67 15.13 o -2 8 2 149.38 183.58 9.92 o 0 8 2 1564.83 1576.49 15.63 o 2 8 2 165.82 155.31 10.16 o 4 8 2 243.10 280.58 10.62 o 6 8 2 104.79 118.46 10.02 o 8 8 2 506.66 497.84 25.11 o 10 8 2 5.78 -5.49 31.72 o -11 9 2 531.66 629.65 63.04 o -9 9 2 265.40 224.73 24.06 o -7 9 2 459.82 366.87 23.12 o -5 9 2 1978.29 1995.55 21.65 o -3 9 2 401.71 451.09 12.10 o -1 9 2 61.50 100.61 8.87 o 1 9 2 107.43 96.90 10.43 o 3 9 2 810.69 795.34 14.53 o 5 9 2 2357.75 2185.78 21.43 o 7 9 2 113.77 143.50 18.56 o 9 9 2 270.49 230.47 29.21 o 11 9 2 272.93 465.02 57.99 o -10 10 2 0.79 -15.62 33.75 o -8 10 2 350.90 343.30 30.99 o -6 10 2 69.71 68.07 17.12 o -4 10 2 140.90 164.96 13.60 o -2 10 2 784.40 651.54 15.19 o 0 10 2 1886.47 1812.66 20.51 o 2 10 2 248.96 261.68 13.75 o 4 10 2 47.67 25.63 14.40 o 6 10 2 135.22 110.34 18.67 o 8 10 2 1.54 -6.17 29.01 o 10 10 2 592.83 615.41 35.87 o -9 11 2 239.47 268.93 43.01 o -7 11 2 850.10 841.87 30.63 o -5 11 2 2999.57 2875.09 36.60 o -3 11 2 2588.19 2648.69 29.92 o -1 11 2 230.87 228.40 11.76 o 1 11 2 1632.48 1618.04 21.44 o 3 11 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36.62 o -5 15 2 336.39 330.30 51.01 o -3 15 2 584.74 566.94 28.62 o -1 15 2 782.58 721.93 28.75 o 1 15 2 103.40 155.92 33.10 o 3 15 2 88.94 52.95 32.41 o 5 15 2 119.36 115.67 30.04 o 7 15 2 258.67 426.06 47.84 o -8 16 2 66.16 116.44 45.51 o -6 16 2 17.52 14.60 31.02 o -4 16 2 1.99 12.55 25.99 o -2 16 2 416.94 378.61 28.53 o 0 16 2 104.46 59.58 22.78 o 2 16 2 1479.33 1578.44 39.50 o 4 16 2 178.28 95.46 59.25 o 6 16 2 5.76 92.99 32.28 o 8 16 2 238.36 261.41 56.29 o -7 17 2 32.73 13.05 48.79 o -5 17 2 29.21 12.11 33.69 o -3 17 2 401.33 387.17 33.11 o -1 17 2 737.51 826.06 30.69 o 1 17 2 207.52 183.32 26.83 o 3 17 2 163.90 94.12 28.92 o 5 17 2 178.31 208.22 46.92 o 7 17 2 10.73 33.66 31.95 o -6 18 2 13.02 55.86 36.16 o -4 18 2 683.56 732.16 39.27 o -2 18 2 80.72 122.68 29.58 o 0 18 2 2.41 70.58 32.82 o 2 18 2 28.32 -8.21 29.46 o 4 18 2 118.34 78.00 33.94 o 6 18 2 265.32 191.23 38.29 o -5 19 2 102.17 74.33 47.51 o -3 19 2 2167.35 2249.44 49.06 o -1 19 2 1092.21 1174.74 42.90 o 1 19 2 304.64 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