#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016555.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016555_Fobs loop_ _publ_author_name 'Orozco, Fab\'ian' 'Insuasty, Braulio' 'Low, John N.' 'Cobo, Justo' 'Glidewell, Christopher' _publ_section_title ; Hydrogen-bonded sheet structures in neutral, anionic and hydrated 6-amino-2-(morpholin-4-yl)-5-nitrosopyrimidines ; _journal_coeditor_code GG3151 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o220 _journal_page_last o225 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.794 _cell_angle_gamma 90.000 _cell_length_a 16.4210 _cell_length_b 7.3671 _cell_length_c 17.2050 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file gg3151IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 53 R = 0.06' _shelx_refln_list_code 4 _shelx_F_calc_maximum 232.48 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3342.48 3235.31 28.76 o 6 0 0 11.26 8.36 5.69 o 8 0 0 12688.22 13467.54 126.61 o 10 0 0 1876.61 2073.80 30.38 o 12 0 0 6.83 34.76 18.88 o 14 0 0 29.69 23.28 21.75 o 16 0 0 116.42 106.87 32.68 o 18 0 0 72.09 15.35 37.27 o 20 0 0 0.16 -20.74 54.23 o 1 1 0 43.44 -2.58 2.58 o 2 1 0 6302.21 6226.93 41.42 o 3 1 0 1.44 2.27 2.66 o 4 1 0 17.17 30.53 3.47 o 5 1 0 408.48 410.01 6.87 o 6 1 0 3813.44 3662.08 26.38 o 7 1 0 516.07 546.33 8.64 o 8 1 0 3072.85 3146.92 25.14 o 9 1 0 82.99 84.47 7.48 o 10 1 0 28.70 29.26 8.07 o 11 1 0 0.99 8.84 8.33 o 12 1 0 191.28 176.40 14.61 o 13 1 0 65.29 24.62 7.71 o 14 1 0 203.37 176.86 17.34 o 15 1 0 16.45 1.77 21.53 o 16 1 0 0.08 -12.65 21.23 o 17 1 0 82.92 49.61 31.50 o 18 1 0 39.97 40.79 33.82 o 19 1 0 52.18 42.06 37.66 o 20 1 0 28.98 -4.29 43.95 o 0 2 0 50914.66 49862.79 365.02 o 1 2 0 54046.88 53314.41 292.40 o 2 2 0 52623.68 52845.70 315.29 o 3 2 0 6606.95 6307.59 46.13 o 4 2 0 474.46 481.33 8.98 o 5 2 0 231.79 281.25 8.95 o 6 2 0 532.85 552.64 10.20 o 7 2 0 4608.63 4768.87 37.13 o 8 2 0 144.29 141.46 7.31 o 9 2 0 2499.83 2461.85 23.31 o 10 2 0 2135.99 2302.56 25.54 o 11 2 0 1439.91 1474.25 22.91 o 12 2 0 667.30 723.51 18.95 o 13 2 0 172.03 158.68 14.90 o 14 2 0 12.04 -1.38 16.59 o 15 2 0 561.88 541.19 27.39 o 16 2 0 0.01 -24.59 24.59 o 17 2 0 7.05 15.20 29.84 o 18 2 0 0.23 -6.97 29.68 o 19 2 0 57.20 -0.19 40.35 o 20 2 0 70.87 0.09 73.69 o 1 3 0 145.33 202.21 8.02 o 2 3 0 4671.43 4950.68 32.98 o 3 3 0 1956.66 1948.31 17.27 o 4 3 0 0.06 10.30 6.31 o 5 3 0 880.28 953.88 13.08 o 6 3 0 1317.78 1437.88 17.87 o 7 3 0 1497.34 1516.91 19.10 o 8 3 0 116.04 119.16 10.36 o 9 3 0 1343.75 1345.15 23.95 o 10 3 0 550.16 549.11 18.63 o 11 3 0 0.27 16.50 14.30 o 12 3 0 99.73 79.71 14.91 o 13 3 0 14.48 24.25 19.06 o 14 3 0 253.34 275.42 27.03 o 15 3 0 8.73 56.43 21.08 o 16 3 0 324.59 390.77 31.46 o 17 3 0 51.02 78.79 33.87 o 18 3 0 115.76 83.94 37.73 o 19 3 0 0.00 14.24 42.03 o 0 4 0 1501.50 1418.69 20.04 o 1 4 0 1.36 4.95 4.67 o 2 4 0 4621.44 4963.55 33.56 o 3 4 0 4607.56 5005.25 36.30 o 4 4 0 0.86 14.29 6.43 o 5 4 0 4137.80 4292.57 38.89 o 6 4 0 300.81 285.26 10.33 o 7 4 0 9.97 16.16 9.54 o 8 4 0 8.13 35.67 10.85 o 9 4 0 31.03 34.76 12.92 o 10 4 0 25.46 35.73 14.40 o 11 4 0 1138.88 1215.41 27.94 o 12 4 0 830.16 861.79 26.32 o 13 4 0 250.96 286.06 24.10 o 14 4 0 679.73 682.89 32.17 o 15 4 0 73.04 55.64 27.66 o 16 4 0 61.34 17.66 30.59 o 17 4 0 142.90 87.15 41.60 o 18 4 0 24.70 21.22 41.13 o 1 5 0 9.60 14.16 7.26 o 2 5 0 150.46 131.10 8.08 o 3 5 0 1.27 -4.37 6.94 o 4 5 0 3470.35 3793.09 33.74 o 5 5 0 83.89 77.58 11.88 o 6 5 0 669.76 667.29 17.03 o 7 5 0 0.40 5.93 11.91 o 8 5 0 50.81 43.32 13.56 o 9 5 0 118.40 148.29 17.70 o 10 5 0 800.37 839.64 25.44 o 11 5 0 38.72 35.83 17.53 o 12 5 0 172.13 221.10 26.11 o 13 5 0 175.68 155.38 28.47 o 14 5 0 3.40 4.58 26.52 o 15 5 0 13.37 -1.62 28.49 o 16 5 0 19.38 36.17 69.12 o 17 5 0 31.59 32.76 45.96 o 0 6 0 83.09 33.45 15.88 o 1 6 0 22.28 9.74 10.22 o 2 6 0 1189.56 1289.78 19.87 o 3 6 0 272.58 298.09 11.82 o 4 6 0 0.40 -9.78 9.78 o 5 6 0 40.80 39.73 12.98 o 6 6 0 177.29 143.66 15.11 o 7 6 0 496.50 543.75 20.84 o 8 6 0 129.73 141.22 18.93 o 9 6 0 10.43 23.53 17.18 o 10 6 0 2.58 -1.33 20.06 o 11 6 0 4.96 3.64 26.49 o 12 6 0 57.50 39.41 26.54 o 13 6 0 29.54 11.65 28.45 o 14 6 0 379.21 362.60 35.21 o 15 6 0 44.08 25.32 33.70 o 16 6 0 48.82 2.25 72.67 o 1 7 0 50.09 29.28 16.95 o 2 7 0 368.30 396.71 21.23 o 3 7 0 53.85 48.25 17.08 o 4 7 0 227.46 238.99 21.48 o 5 7 0 22.32 43.81 18.57 o 6 7 0 217.42 230.79 27.30 o 7 7 0 623.96 697.06 29.01 o 8 7 0 623.65 725.48 31.36 o 9 7 0 251.99 260.00 28.49 o 10 7 0 123.85 48.85 27.21 o 11 7 0 22.69 -30.21 30.21 o 12 7 0 323.46 396.87 35.73 o 13 7 0 47.61 51.29 38.85 o 14 7 0 0.00 -1.62 60.75 o 0 8 0 120.69 37.75 46.00 o 1 8 0 12.18 -11.69 32.03 o 2 8 0 126.24 187.43 31.72 o 3 8 0 0.26 17.90 26.57 o 4 8 0 3.05 55.90 40.96 o 5 8 0 25.02 69.35 42.74 o 6 8 0 1.26 -37.35 37.35 o 7 8 0 3.56 -3.38 46.75 o 8 8 0 202.21 149.07 47.95 o 9 8 0 118.60 76.59 42.41 o 10 8 0 27.87 41.58 41.94 o 11 8 0 7.39 67.72 59.42 o 1 9 0 41.18 116.42 47.17 o 2 9 0 1.71 70.85 48.30 o 3 9 0 22.05 45.10 59.70 o 4 9 0 2.92 92.97 52.57 o 5 9 0 0.06 27.89 51.54 o 6 9 0 22.21 -21.06 59.90 o 7 9 0 77.22 52.84 57.19 o -19 0 1 269.91 268.02 52.96 o -17 0 1 423.36 347.59 43.42 o -15 0 1 80.95 56.78 27.91 o -13 0 1 6.22 24.85 13.74 o -11 0 1 1913.18 1895.23 33.68 o -9 0 1 2043.30 2142.62 26.42 o -7 0 1 5850.24 6288.50 62.12 o -5 0 1 223.66 236.20 6.30 o -3 0 1 6.84 -2.62 4.16 o 3 0 1 578.59 392.43 7.11 o 5 0 1 4795.09 4408.42 40.62 o 7 0 1 1351.12 1402.04 19.38 o 9 0 1 974.92 905.31 16.60 o 11 0 1 335.49 335.19 17.14 o 13 0 1 18.35 0.35 18.97 o 15 0 1 743.92 716.14 37.85 o 17 0 1 537.26 505.16 45.31 o 19 0 1 107.42 108.68 55.22 o -20 1 1 198.29 134.93 39.30 o -19 1 1 18.32 24.54 34.15 o -18 1 1 184.37 149.84 30.98 o -17 1 1 41.27 54.94 24.33 o -16 1 1 44.39 20.87 23.42 o -15 1 1 11.03 11.99 18.50 o -14 1 1 2.92 1.88 15.67 o -13 1 1 164.33 132.82 13.91 o -12 1 1 104.79 93.13 14.72 o -11 1 1 195.60 174.24 10.74 o -10 1 1 765.65 770.26 12.17 o -9 1 1 114.34 96.87 5.58 o -8 1 1 936.08 939.24 11.18 o -7 1 1 804.06 848.75 10.00 o -6 1 1 802.54 847.20 11.06 o -5 1 1 112.58 146.62 4.95 o -4 1 1 1618.90 1456.23 12.06 o -3 1 1 19758.34 18931.39 108.30 o -2 1 1 2975.36 2800.41 20.99 o -1 1 1 126.00 139.22 3.13 o 0 1 1 268.84 287.13 3.80 o 1 1 1 3726.40 3699.39 22.93 o 2 1 1 263.71 162.61 3.82 o 3 1 1 2.89 7.16 3.10 o 4 1 1 48.51 56.75 4.32 o 5 1 1 927.22 757.35 9.15 o 6 1 1 4276.88 4444.80 30.93 o 7 1 1 248.80 227.35 7.73 o 8 1 1 488.81 449.68 8.55 o 9 1 1 493.11 475.21 9.62 o 10 1 1 111.31 149.31 9.96 o 11 1 1 233.56 254.50 10.38 o 12 1 1 50.56 41.13 10.45 o 13 1 1 13.38 7.05 11.98 o 14 1 1 56.31 65.85 17.72 o 15 1 1 32.37 29.90 19.46 o 16 1 1 235.77 291.20 30.36 o 17 1 1 112.52 79.27 30.61 o 18 1 1 1.20 61.44 34.37 o 19 1 1 0.24 1.42 38.39 o 20 1 1 20.36 53.66 42.28 o -20 2 1 150.41 143.09 42.73 o -19 2 1 125.87 96.05 35.82 o -18 2 1 96.43 21.49 32.37 o -17 2 1 10.53 19.00 25.91 o -16 2 1 41.87 42.25 24.61 o -15 2 1 185.62 169.55 21.59 o -14 2 1 3.31 15.29 14.90 o -13 2 1 2.62 28.79 11.12 o -12 2 1 106.09 48.83 14.41 o -11 2 1 24.09 20.36 7.71 o -10 2 1 50.31 51.60 9.10 o -9 2 1 1639.11 1601.07 17.10 o -8 2 1 279.84 270.92 6.95 o -7 2 1 388.02 450.34 9.08 o -6 2 1 0.30 10.66 5.81 o -5 2 1 1478.58 1478.58 17.07 o -4 2 1 2599.13 2480.11 21.93 o -3 2 1 40.91 48.73 4.50 o -2 2 1 11420.69 11052.92 65.91 o -1 2 1 7253.18 7415.17 41.44 o 0 2 1 7723.06 8081.99 46.37 o 1 2 1 5288.80 5305.42 35.01 o 2 2 1 17980.52 17786.97 103.02 o 3 2 1 5248.73 5171.62 37.28 o 4 2 1 614.61 611.14 10.03 o 5 2 1 3651.53 3733.66 30.26 o 6 2 1 49.87 62.15 9.39 o 7 2 1 0.60 9.67 5.14 o 8 2 1 1930.22 2002.45 21.07 o 9 2 1 154.51 130.75 9.29 o 10 2 1 15.94 19.11 8.89 o 11 2 1 5.77 -2.60 10.05 o 12 2 1 140.84 157.28 13.77 o 13 2 1 20.87 20.95 18.84 o 14 2 1 49.26 30.79 18.94 o 15 2 1 934.20 903.21 29.77 o 16 2 1 42.84 34.32 28.47 o 17 2 1 152.04 147.95 31.64 o 18 2 1 11.90 -4.33 31.34 o 19 2 1 38.58 -28.09 35.39 o -19 3 1 191.13 200.76 52.52 o -18 3 1 43.53 62.01 35.95 o -17 3 1 18.31 50.42 32.38 o -16 3 1 172.32 138.90 26.33 o -15 3 1 47.95 9.70 20.58 o -14 3 1 26.70 26.95 21.54 o -13 3 1 119.30 83.16 15.15 o -12 3 1 323.61 331.14 18.53 o -11 3 1 108.55 119.07 13.31 o -10 3 1 588.14 559.61 16.57 o -9 3 1 202.01 204.57 11.97 o -8 3 1 13.17 14.17 8.97 o -7 3 1 4.44 -7.46 7.46 o -6 3 1 89.51 99.62 7.98 o -5 3 1 0.20 -5.04 6.34 o -4 3 1 191.83 197.59 8.30 o -3 3 1 39.19 21.02 4.97 o -2 3 1 646.00 687.40 8.79 o -1 3 1 58.42 52.66 6.67 o 0 3 1 2072.26 2296.95 18.13 o 1 3 1 733.06 742.88 10.20 o 2 3 1 33.13 24.35 5.18 o 3 3 1 0.01 -0.62 5.07 o 4 3 1 1693.86 1825.43 18.82 o 5 3 1 2185.69 2270.65 21.75 o 6 3 1 1226.67 1219.91 16.56 o 7 3 1 2146.55 2117.63 24.48 o 8 3 1 2392.35 2545.73 32.39 o 9 3 1 7.05 11.07 11.07 o 10 3 1 751.49 783.65 22.04 o 11 3 1 164.92 144.61 17.41 o 12 3 1 3.80 21.21 14.82 o 13 3 1 291.35 245.23 23.21 o 14 3 1 667.71 593.19 27.38 o 15 3 1 250.97 155.37 29.07 o 16 3 1 0.04 -25.27 25.27 o 17 3 1 8.75 29.63 34.40 o 18 3 1 70.65 91.31 48.37 o 19 3 1 17.03 11.67 42.40 o -18 4 1 34.43 9.74 39.49 o -17 4 1 0.03 -6.03 33.57 o -16 4 1 473.49 536.27 37.65 o -15 4 1 129.48 170.17 28.25 o -14 4 1 268.46 324.96 39.51 o -13 4 1 87.46 89.17 18.38 o -12 4 1 38.42 17.49 15.59 o -11 4 1 230.85 236.27 17.85 o -10 4 1 5.26 15.56 12.88 o -9 4 1 20.41 23.72 12.64 o -8 4 1 24.73 23.42 10.10 o -7 4 1 257.14 291.83 12.41 o -6 4 1 164.73 176.88 10.96 o -5 4 1 24.70 17.64 7.59 o -4 4 1 0.67 1.10 5.54 o -3 4 1 3120.62 3326.68 27.26 o -2 4 1 2216.23 2407.45 20.41 o -1 4 1 1477.46 1489.14 15.21 o 0 4 1 1405.31 1407.78 15.07 o 1 4 1 763.65 712.34 10.40 o 2 4 1 2557.23 2710.59 23.78 o 3 4 1 2961.32 3088.78 26.31 o 4 4 1 7938.47 8447.60 62.47 o 5 4 1 1165.78 1151.28 17.51 o 6 4 1 527.84 459.65 12.19 o 7 4 1 198.86 172.27 12.06 o 8 4 1 210.37 191.53 12.89 o 9 4 1 4.05 3.58 12.83 o 10 4 1 608.23 693.14 26.09 o 11 4 1 359.21 357.63 19.87 o 12 4 1 362.78 410.46 25.22 o 13 4 1 478.70 509.03 24.50 o 14 4 1 42.11 14.77 30.59 o 15 4 1 8.22 -12.78 25.59 o 16 4 1 113.43 76.87 31.79 o 17 4 1 216.60 174.85 36.22 o 18 4 1 18.73 17.83 42.21 o -17 5 1 30.70 -24.64 41.06 o -16 5 1 0.08 -16.34 36.07 o -15 5 1 444.86 552.26 36.97 o -14 5 1 234.38 269.32 39.78 o -13 5 1 7.80 27.38 22.28 o -12 5 1 167.76 104.12 23.20 o -11 5 1 673.61 727.63 26.25 o -10 5 1 127.48 137.17 17.32 o -9 5 1 114.93 123.99 15.28 o -8 5 1 233.23 253.41 15.01 o -7 5 1 352.74 366.13 17.63 o -6 5 1 60.47 77.40 14.76 o -5 5 1 547.80 550.63 14.43 o -4 5 1 61.95 48.50 8.43 o -3 5 1 75.72 54.68 7.47 o -2 5 1 22.07 18.67 7.18 o -1 5 1 477.29 520.78 11.01 o 0 5 1 446.44 549.92 11.27 o 1 5 1 11.33 5.22 7.32 o 2 5 1 41.41 42.96 8.35 o 3 5 1 981.65 994.60 14.68 o 4 5 1 0.71 -7.57 7.57 o 5 5 1 1.71 25.00 10.35 o 6 5 1 25.95 31.65 11.22 o 7 5 1 5.12 7.68 10.76 o 8 5 1 771.25 792.80 20.73 o 9 5 1 129.13 108.80 17.24 o 10 5 1 167.25 184.28 21.84 o 11 5 1 2.18 -6.53 18.22 o 12 5 1 632.96 645.13 28.68 o 13 5 1 443.42 488.21 27.61 o 14 5 1 156.53 212.39 27.82 o 15 5 1 7.34 -31.33 31.34 o 16 5 1 15.09 96.16 40.87 o 17 5 1 39.85 3.60 47.45 o -16 6 1 8.32 35.71 46.05 o -15 6 1 285.31 219.36 44.46 o -14 6 1 14.64 6.48 30.08 o -13 6 1 41.41 74.17 27.57 o -12 6 1 199.63 178.97 26.88 o -11 6 1 1.95 19.27 22.20 o -10 6 1 0.00 -6.21 19.92 o -9 6 1 10.80 -18.72 18.72 o -8 6 1 146.93 159.80 19.54 o -7 6 1 196.79 221.82 17.58 o -6 6 1 410.66 421.93 17.46 o -5 6 1 1.75 13.78 13.46 o -4 6 1 174.21 159.98 13.98 o -3 6 1 1441.55 1603.76 25.96 o -2 6 1 124.72 109.33 10.85 o -1 6 1 29.55 18.57 9.81 o 0 6 1 63.16 58.83 10.91 o 1 6 1 8.47 4.85 10.04 o 2 6 1 15.73 31.82 9.88 o 3 6 1 282.68 276.75 11.54 o 4 6 1 283.73 285.93 12.98 o 5 6 1 1460.86 1487.49 26.27 o 6 6 1 1018.37 1100.63 23.46 o 7 6 1 18.43 -2.34 16.42 o 8 6 1 7.13 8.88 17.82 o 9 6 1 1.77 23.33 19.53 o 10 6 1 54.67 38.22 21.01 o 11 6 1 84.39 99.44 22.76 o 12 6 1 25.74 31.43 23.96 o 13 6 1 526.12 578.87 34.79 o 14 6 1 483.98 585.94 42.09 o 15 6 1 3.52 -2.41 36.98 o -14 7 1 87.79 78.18 52.80 o -13 7 1 233.84 278.71 40.14 o -12 7 1 74.25 96.42 30.22 o -11 7 1 2.07 -2.71 27.16 o -10 7 1 10.11 -25.10 25.10 o -9 7 1 246.19 238.66 30.88 o -8 7 1 627.18 743.70 31.63 o -7 7 1 25.20 14.28 23.29 o -6 7 1 0.01 14.38 24.03 o -5 7 1 141.94 105.40 24.64 o -4 7 1 316.78 297.36 21.68 o -3 7 1 118.09 96.93 22.20 o -2 7 1 30.14 32.77 15.87 o -1 7 1 230.73 220.00 20.61 o 0 7 1 56.53 50.08 15.78 o 1 7 1 5.71 31.67 15.82 o 2 7 1 10.80 19.46 14.74 o 3 7 1 18.74 3.19 16.02 o 4 7 1 324.34 323.65 18.32 o 5 7 1 130.04 97.33 20.12 o 6 7 1 18.85 -10.31 17.71 o 7 7 1 103.38 64.25 21.04 o 8 7 1 0.10 17.59 21.51 o 9 7 1 12.73 -16.75 22.55 o 10 7 1 69.40 18.86 27.23 o 11 7 1 186.88 155.88 36.44 o 12 7 1 84.62 53.11 41.53 o 13 7 1 94.09 0.60 44.75 o -11 8 1 11.85 81.47 42.31 o -10 8 1 39.94 10.82 42.95 o -9 8 1 16.13 -19.10 39.56 o -8 8 1 1.25 6.98 39.32 o -7 8 1 0.39 -37.08 37.08 o -6 8 1 98.78 55.63 71.94 o -5 8 1 231.31 106.40 44.46 o -4 8 1 20.87 35.05 28.97 o -3 8 1 0.60 9.23 28.31 o -2 8 1 61.61 98.18 29.42 o -1 8 1 211.59 241.72 29.96 o 0 8 1 287.87 301.31 29.48 o 1 8 1 5.62 15.28 32.32 o 2 8 1 0.68 -26.95 27.48 o 3 8 1 66.55 24.29 25.80 o 4 8 1 81.41 92.36 33.04 o 5 8 1 21.61 -1.60 34.05 o 6 8 1 419.33 415.09 56.17 o 7 8 1 223.73 183.72 37.34 o 8 8 1 135.15 126.94 37.13 o 9 8 1 1.48 18.88 48.09 o 10 8 1 107.90 36.16 64.31 o 11 8 1 0.13 9.53 62.82 o -7 9 1 109.95 98.36 57.54 o -6 9 1 31.17 32.57 54.37 o -5 9 1 22.34 -27.84 52.71 o -4 9 1 36.42 34.69 54.09 o -3 9 1 56.19 13.38 59.80 o -2 9 1 97.66 56.29 44.94 o -1 9 1 54.51 85.50 45.79 o 0 9 1 38.04 51.46 45.35 o 1 9 1 95.85 258.11 54.58 o 2 9 1 11.92 20.02 45.48 o 3 9 1 9.83 87.63 67.38 o 4 9 1 6.74 -1.16 51.96 o 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