#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016560_Fobs loop_ _publ_author_name 'Yamaguchi, Tomoka' 'Sunatsuki, Yukinari' 'Ishida, Hiroyuki' _publ_section_title ; Mononuclear nickel(II) and zinc(II) complexes with deprotonated forms of the tripodal hexadentate ligand 1,3-bis(2-hydroxybenzylidene)-2-(2-hydroxybenzylideneaminomethyl)-2-methylpropane-1,3-diamine ; _journal_coeditor_code JZ3116 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m156 _journal_page_last m160 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.969 _cell_angle_gamma 90.000 _cell_length_a 18.5304 _cell_length_b 13.4092 _cell_length_c 19.7923 _exptl_crystal_F_000 2248.00 _reflns_d_resolution_high 0.7111 _[local]_cod_data_source_file jz3116Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070913ya' _shelx_refln_list_code 4 _shelx_F_calc_maximum 621.60 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 191766.98 202388.72 2362.65 o 6 0 0 386386.03 416549.34 5588.61 o 8 0 0 73483.60 84995.26 899.37 o 10 0 0 36873.86 43944.96 454.25 o 12 0 0 33225.96 36133.45 389.12 o 14 0 0 16539.02 17068.84 214.54 o 16 0 0 13.72 0.94 31.12 o 18 0 0 4651.24 4956.73 141.42 o 20 0 0 13359.02 12738.16 251.59 o 22 0 0 16.55 47.27 48.93 o 24 0 0 505.89 529.15 78.54 o 26 0 0 2438.19 2555.27 136.75 o 3 1 0 5096.28 5559.25 39.45 o 5 1 0 11804.46 8574.52 77.93 o 7 1 0 20499.96 16532.65 131.36 o 9 1 0 1398.06 1254.91 31.76 o 11 1 0 3814.35 3328.68 48.68 o 13 1 0 7321.30 6462.28 77.53 o 15 1 0 84.20 116.54 34.42 o 17 1 0 165.75 109.67 31.63 o 19 1 0 3614.87 3456.25 69.94 o 21 1 0 1577.12 1677.76 61.49 o 23 1 0 63.74 19.02 35.67 o 25 1 0 475.93 489.24 57.72 o 0 2 0 3140.82 1491.40 39.11 o 2 2 0 2137.88 3251.81 35.02 o 4 2 0 119.70 197.41 23.22 o 6 2 0 15279.13 17140.01 122.18 o 8 2 0 1156.88 1127.94 28.31 o 10 2 0 1875.45 1951.82 37.42 o 12 2 0 4712.36 4719.95 62.15 o 14 2 0 3380.90 3524.04 65.32 o 16 2 0 1239.10 1314.36 48.07 o 18 2 0 6007.28 5702.00 84.81 o 20 2 0 3464.56 3551.26 73.68 o 22 2 0 190.61 210.10 43.88 o 24 2 0 1276.19 1514.71 68.48 o 1 3 0 44558.48 46523.23 394.25 o 3 3 0 163.35 170.62 21.85 o 5 3 0 1.93 4.73 12.59 o 7 3 0 8918.58 9169.72 73.56 o 9 3 0 9353.71 9994.11 84.97 o 11 3 0 18.94 76.05 23.04 o 13 3 0 2802.77 2869.24 55.56 o 15 3 0 8622.88 8779.71 92.33 o 17 3 0 47.12 48.19 28.64 o 19 3 0 8.08 30.88 32.16 o 21 3 0 539.86 612.82 48.04 o 23 3 0 177.83 120.53 43.57 o 25 3 0 83.78 108.20 51.26 o 0 4 0 8997.31 11850.45 188.80 o 2 4 0 13.47 57.84 12.74 o 4 4 0 93.49 56.30 13.59 o 6 4 0 7609.94 8394.11 68.78 o 8 4 0 10802.88 11320.58 99.67 o 10 4 0 1050.49 884.91 32.75 o 12 4 0 9906.07 9954.33 97.61 o 14 4 0 7485.06 7537.61 89.09 o 16 4 0 1403.55 1406.53 46.87 o 18 4 0 4239.92 3986.67 70.40 o 20 4 0 5021.26 4871.04 85.22 o 22 4 0 52.66 49.95 37.54 o 24 4 0 743.13 795.24 59.41 o 1 5 0 9878.41 6434.26 48.55 o 3 5 0 3475.89 3719.17 38.22 o 5 5 0 7689.56 5427.88 83.40 o 7 5 0 7093.58 4740.88 47.92 o 9 5 0 792.53 651.81 27.16 o 11 5 0 12530.26 12075.89 109.24 o 13 5 0 2472.56 2446.62 52.04 o 15 5 0 6242.84 5937.94 77.01 o 17 5 0 134.85 192.44 34.80 o 19 5 0 5373.67 5474.55 85.43 o 21 5 0 461.65 424.40 46.05 o 23 5 0 53.44 38.47 38.40 o 25 5 0 800.89 1088.79 67.62 o 0 6 0 46541.43 55338.83 546.25 o 2 6 0 1582.03 1838.45 24.88 o 4 6 0 13.08 19.33 13.23 o 6 6 0 4698.52 4700.05 57.32 o 8 6 0 10831.78 10887.97 108.52 o 10 6 0 1300.96 1511.30 38.74 o 12 6 0 3843.65 4057.56 66.10 o 14 6 0 769.12 844.28 38.71 o 16 6 0 58.81 75.75 27.81 o 18 6 0 1627.11 1641.38 52.16 o 20 6 0 4045.70 3753.84 74.87 o 22 6 0 16.14 -1.06 28.49 o 24 6 0 546.24 451.50 52.82 o 1 7 0 70.59 534.72 20.11 o 3 7 0 19219.06 20825.21 147.55 o 5 7 0 15608.21 19074.09 138.03 o 7 7 0 8268.82 7614.34 71.43 o 9 7 0 855.66 815.72 32.68 o 11 7 0 5174.00 5409.93 70.86 o 13 7 0 5499.78 5513.76 70.38 o 15 7 0 190.11 248.65 32.37 o 17 7 0 31.15 42.24 27.27 o 19 7 0 12.27 22.61 31.35 o 21 7 0 497.96 498.78 50.98 o 23 7 0 224.03 211.18 45.54 o 0 8 0 113.34 148.01 23.05 o 2 8 0 0.47 14.44 10.99 o 4 8 0 6758.70 7069.58 62.51 o 6 8 0 1036.35 1023.52 30.11 o 8 8 0 173.69 297.95 23.57 o 10 8 0 1254.18 1275.12 40.65 o 12 8 0 2862.92 2841.40 86.10 o 14 8 0 703.50 653.11 50.29 o 16 8 0 52.80 52.38 27.95 o 18 8 0 90.43 101.70 32.92 o 20 8 0 165.97 143.75 37.59 o 22 8 0 15.52 1.43 29.65 o 1 9 0 10131.47 10293.91 95.83 o 3 9 0 1392.22 1595.71 33.79 o 5 9 0 2493.55 2184.35 39.69 o 7 9 0 9794.78 9766.93 88.42 o 9 9 0 1223.12 1218.30 38.42 o 11 9 0 785.58 856.80 33.01 o 13 9 0 7253.80 7149.02 95.41 o 15 9 0 4330.24 4178.95 126.27 o 17 9 0 1314.92 1216.00 159.98 o 19 9 0 1207.17 1105.02 62.21 o 21 9 0 696.97 738.56 63.47 o 0 10 0 18026.21 19222.82 216.28 o 2 10 0 7249.18 7769.10 72.41 o 4 10 0 105.11 122.02 21.13 o 6 10 0 8933.65 9147.31 86.45 o 8 10 0 6168.34 6251.50 67.48 o 10 10 0 23.37 12.37 17.29 o 12 10 0 2543.15 2517.41 48.12 o 14 10 0 6907.78 7012.47 83.28 o 16 10 0 342.10 285.23 37.66 o 18 10 0 605.89 536.56 51.06 o 20 10 0 2001.01 1633.72 171.13 o 22 10 0 337.85 304.97 49.89 o 1 11 0 12212.77 11726.82 100.61 o 3 11 0 130.11 126.85 24.24 o 5 11 0 3802.00 3668.91 49.49 o 7 11 0 8021.20 7801.61 78.00 o 9 11 0 16.83 -0.57 15.57 o 11 11 0 333.00 421.81 30.37 o 13 11 0 1952.43 2006.15 45.60 o 15 11 0 269.19 302.14 30.35 o 17 11 0 3.20 4.38 22.38 o 19 11 0 3115.94 3427.18 67.83 o 21 11 0 1188.15 1122.70 172.37 o 0 12 0 8653.13 8306.37 114.32 o 2 12 0 1821.01 1843.46 44.01 o 4 12 0 1765.68 1708.21 38.35 o 6 12 0 7329.37 7456.97 77.18 o 8 12 0 1295.25 1442.13 38.96 o 10 12 0 1.12 6.49 18.33 o 12 12 0 1763.58 1829.50 43.73 o 14 12 0 2086.74 1986.00 51.35 o 16 12 0 76.16 76.32 27.19 o 18 12 0 4055.38 3992.23 83.69 o 20 12 0 3475.07 3335.19 73.17 o 1 13 0 10.21 41.12 14.31 o 3 13 0 758.50 780.59 56.41 o 5 13 0 73.42 98.32 24.02 o 7 13 0 224.62 227.90 27.41 o 9 13 0 347.97 367.42 30.57 o 11 13 0 1.83 -14.32 22.77 o 13 13 0 749.65 752.40 40.14 o 15 13 0 373.23 345.46 34.43 o 17 13 0 300.76 369.57 36.63 o 0 14 0 5789.20 5823.36 196.66 o 2 14 0 268.66 271.98 28.17 o 4 14 0 692.44 692.55 33.71 o 6 14 0 184.76 208.14 27.60 o 8 14 0 358.94 376.07 31.76 o 10 14 0 13.85 3.58 19.46 o 12 14 0 8.43 38.66 27.18 o 14 14 0 11.46 2.99 20.04 o 16 14 0 56.50 36.92 29.23 o 1 15 0 902.48 943.68 78.97 o 3 15 0 63.84 67.39 24.71 o 5 15 0 3320.03 3530.11 58.90 o 7 15 0 2128.52 2166.18 45.09 o 9 15 0 3.71 -0.58 18.31 o 11 15 0 310.07 342.19 32.87 o 13 15 0 1657.83 1833.27 81.51 o 15 15 0 189.19 236.61 33.08 o 0 16 0 4608.48 4330.55 406.85 o 2 16 0 2218.52 2297.76 64.91 o 4 16 0 189.79 173.17 27.47 o 6 16 0 4338.59 4384.57 63.46 o 8 16 0 1962.38 2069.17 50.60 o 10 16 0 207.27 192.58 32.92 o 12 16 0 2912.40 3098.31 70.00 o 1 17 0 2147.77 2553.82 66.69 o 3 17 0 40.92 69.04 28.10 o 5 17 0 25.43 33.44 23.15 o 7 17 0 1394.35 1724.36 46.04 o 9 17 0 77.45 81.00 30.06 o 11 17 0 438.88 556.52 49.34 o 0 18 0 2855.48 2889.60 163.11 o 2 18 0 47.27 71.23 22.82 o 4 18 0 45.40 76.94 32.43 o 6 18 0 837.60 858.63 40.31 o -25 1 1 77.83 100.96 49.56 o -23 1 1 6.55 38.31 38.25 o -21 1 1 5603.23 5583.13 90.00 o -19 1 1 22.07 47.21 33.51 o -17 1 1 4205.54 4176.23 68.33 o -15 1 1 16504.05 17734.79 160.66 o -13 1 1 1428.14 1171.38 42.26 o -11 1 1 10944.34 11557.70 99.13 o -9 1 1 24295.65 26800.59 193.82 o -7 1 1 13069.37 12706.68 93.20 o -5 1 1 78995.13 90188.10 676.78 o -3 1 1 8241.89 5748.75 41.38 o 3 1 1 5323.44 8180.80 56.24 o 5 1 1 6312.67 6394.37 66.57 o 7 1 1 22733.21 21839.90 146.04 o 9 1 1 3446.30 3096.36 43.18 o 11 1 1 3966.83 4106.69 55.29 o 13 1 1 2346.48 2176.46 50.27 o 15 1 1 34.63 56.53 30.03 o 17 1 1 1832.23 1930.47 54.22 o 19 1 1 3221.30 3145.89 70.49 o 21 1 1 38.94 58.10 35.43 o 23 1 1 31.54 33.80 36.22 o 25 1 1 28.86 21.90 42.84 o -24 2 1 382.43 385.80 52.81 o -22 2 1 3097.83 3196.74 76.58 o -20 2 1 2996.03 2908.04 67.90 o -18 2 1 919.75 856.16 45.84 o -16 2 1 3490.97 3675.63 65.66 o -14 2 1 7131.83 6907.79 86.18 o -12 2 1 481.27 599.16 33.12 o -10 2 1 16484.59 15588.63 123.43 o -8 2 1 49254.68 48924.07 350.54 o -6 2 1 2493.51 2331.47 34.21 o -4 2 1 800.31 90.80 19.85 o -2 2 1 53685.59 47173.32 308.75 o 0 2 1 16971.95 19940.39 115.54 o 2 2 1 265.93 2084.77 23.90 o 4 2 1 1852.61 4143.60 52.84 o 6 2 1 14990.51 14725.48 108.01 o 8 2 1 11554.45 14376.86 106.04 o 10 2 1 164.23 35.52 19.08 o 12 2 1 16446.63 17050.10 141.93 o 14 2 1 4404.89 4831.76 73.61 o 16 2 1 411.50 379.70 37.68 o 18 2 1 11983.59 11702.70 124.59 o 20 2 1 950.13 924.40 52.70 o 22 2 1 16.75 26.01 33.66 o 24 2 1 61.74 95.25 44.07 o -25 3 1 266.28 291.09 58.87 o -23 3 1 23.98 15.92 34.11 o -21 3 1 5694.70 5662.49 92.01 o -19 3 1 1664.04 1593.70 54.34 o -17 3 1 13.55 7.82 22.68 o -15 3 1 2491.58 2807.00 60.14 o -13 3 1 6383.06 6386.31 77.00 o -11 3 1 3524.22 4069.89 53.67 o -9 3 1 28967.54 31698.59 232.60 o -7 3 1 9709.85 8775.83 71.45 o -5 3 1 529.94 1763.77 27.56 o -3 3 1 322.35 105.85 22.09 o -1 3 1 84009.21 89981.23 652.03 o 1 3 1 778.97 2425.20 27.95 o 3 3 1 106.42 356.07 27.93 o 5 3 1 22662.78 24661.13 169.46 o 7 3 1 1792.12 915.68 30.61 o 9 3 1 14611.13 19481.72 144.64 o 11 3 1 11389.54 11777.64 104.35 o 13 3 1 6033.22 5572.25 68.68 o 15 3 1 163.82 339.39 39.23 o 17 3 1 10727.78 10510.83 114.32 o 19 3 1 10420.42 9810.69 114.72 o 21 3 1 419.93 297.40 47.00 o 23 3 1 820.32 880.20 60.04 o 25 3 1 3736.21 4341.30 100.97 o -24 4 1 17.85 20.43 37.85 o -22 4 1 17.22 24.59 32.95 o -20 4 1 4271.61 4016.00 83.50 o -18 4 1 566.58 600.61 41.90 o -16 4 1 331.37 410.43 36.12 o -14 4 1 483.72 442.38 38.51 o -12 4 1 2147.88 2241.62 47.21 o -10 4 1 4245.34 3582.55 47.94 o -8 4 1 12487.18 10357.75 87.59 o -6 4 1 183.74 220.63 17.26 o -4 4 1 3014.08 5701.88 52.35 o -2 4 1 8125.86 5957.30 57.13 o 0 4 1 103.21 293.35 15.97 o 2 4 1 9280.57 13426.14 99.70 o 4 4 1 1054.42 2347.27 50.34 o 6 4 1 19697.80 20079.05 143.35 o 8 4 1 197.25 105.27 18.25 o 10 4 1 2764.59 2383.58 45.30 o 12 4 1 18981.82 18996.61 159.71 o 14 4 1 353.24 358.53 33.44 o 16 4 1 844.99 860.78 42.06 o 18 4 1 2776.97 2873.70 62.92 o 20 4 1 3408.52 3156.49 69.64 o 22 4 1 391.88 489.51 49.78 o 24 4 1 354.02 322.14 53.81 o -25 5 1 56.94 34.46 40.54 o -23 5 1 220.22 169.52 45.21 o -21 5 1 338.90 304.61 44.61 o -19 5 1 2.08 7.97 24.21 o -17 5 1 26.04 28.51 27.58 o -15 5 1 5444.11 5636.00 75.27 o -13 5 1 609.92 594.46 40.01 o -11 5 1 2418.98 2619.98 50.04 o -9 5 1 375.97 650.39 27.10 o -7 5 1 3.76 -5.31 13.72 o -5 5 1 2941.30 3510.99 68.85 o -3 5 1 2796.87 2229.32 30.23 o -1 5 1 127.59 150.60 13.89 o 1 5 1 1551.37 1001.81 19.57 o 3 5 1 3011.21 2394.09 29.82 o 5 5 1 305.98 360.68 19.91 o 7 5 1 757.46 1106.01 25.43 o 9 5 1 643.22 781.46 27.77 o 11 5 1 393.61 406.66 30.02 o 13 5 1 3897.36 3886.15 63.67 o 15 5 1 1220.20 1266.20 45.89 o 17 5 1 417.24 475.86 38.42 o 19 5 1 13.54 14.28 30.03 o 21 5 1 0.31 -7.43 28.52 o 23 5 1 0.76 13.74 36.95 o 25 5 1 74.52 52.69 43.01 o -24 6 1 24.80 18.04 41.68 o -22 6 1 14.26 34.62 37.08 o -20 6 1 1276.02 1255.95 55.67 o -18 6 1 593.43 639.59 43.93 o -16 6 1 854.15 853.99 41.70 o -14 6 1 876.88 836.27 42.57 o -12 6 1 1660.41 1746.46 47.35 o -10 6 1 2167.80 2233.38 43.38 o -8 6 1 494.91 377.78 29.96 o -6 6 1 8066.53 9052.52 87.17 o -4 6 1 1555.37 1680.71 25.97 o -2 6 1 2908.67 3053.39 31.38 o 0 6 1 802.55 876.52 20.51 o 2 6 1 1245.86 1412.30 22.32 o 4 6 1 7294.77 6941.97 56.67 o 6 6 1 2358.00 2828.51 42.49 o 8 6 1 7.07 2.61 16.67 o 10 6 1 3464.88 3224.54 50.41 o 12 6 1 2115.93 2028.37 46.47 o 14 6 1 208.23 177.11 32.28 o 16 6 1 12.15 3.43 20.53 o 18 6 1 1134.38 1099.38 49.22 o 20 6 1 22.30 33.01 30.68 o 22 6 1 188.19 191.85 42.35 o 24 6 1 21.07 43.98 39.42 o -23 7 1 279.44 235.20 47.98 o -21 7 1 1567.87 1518.93 58.48 o -19 7 1 1005.78 1100.93 50.49 o -17 7 1 171.26 192.14 35.99 o -15 7 1 4103.53 4244.08 66.35 o -13 7 1 2636.34 2578.76 54.95 o -11 7 1 615.86 727.59 38.72 o -9 7 1 15312.34 15436.06 227.82 o -7 7 1 4205.25 3415.42 43.87 o -5 7 1 2380.16 3370.55 39.72 o -3 7 1 3395.90 3613.89 40.03 o -1 7 1 12642.28 12563.96 89.89 o 1 7 1 94.19 21.22 11.86 o 3 7 1 5209.85 5897.12 53.69 o 5 7 1 11204.81 10584.34 82.10 o 7 7 1 208.27 128.67 20.20 o 9 7 1 4181.81 4711.59 88.70 o 11 7 1 7073.86 7196.82 109.73 o 13 7 1 408.83 433.20 34.33 o 15 7 1 2320.75 2291.60 50.51 o 17 7 1 698.35 744.21 41.42 o 19 7 1 905.92 897.99 46.38 o 21 7 1 80.33 89.51 40.23 o 23 7 1 210.57 151.86 43.03 o -22 8 1 1060.05 1147.44 57.10 o -20 8 1 634.60 604.81 47.19 o -18 8 1 11.72 -6.64 25.56 o -16 8 1 23.61 39.31 27.01 o -14 8 1 11203.78 11031.71 118.51 o -12 8 1 2025.93 2331.36 58.09 o -10 8 1 29.90 2.02 17.53 o -8 8 1 16450.49 15786.03 127.80 o -6 8 1 23689.08 25021.10 188.48 o -4 8 1 78.97 34.49 16.79 o -2 8 1 29144.73 27719.37 196.38 o 0 8 1 30516.57 31274.21 217.44 o 2 8 1 415.25 884.13 23.70 o 4 8 1 44.81 161.74 19.53 o 6 8 1 20107.01 19789.58 150.64 o 8 8 1 108.23 161.69 22.49 o 10 8 1 192.15 148.41 31.27 o 12 8 1 1829.14 1701.76 47.32 o 14 8 1 1418.36 1524.19 46.69 o 16 8 1 566.10 590.54 37.80 o 18 8 1 1099.50 1132.13 48.67 o 20 8 1 1592.59 1545.71 58.36 o 22 8 1 51.55 71.78 37.36 o -21 9 1 3576.98 3502.65 100.16 o -19 9 1 284.99 310.51 48.34 o -17 9 1 368.56 224.96 48.37 o -15 9 1 6190.05 5855.35 116.74 o -13 9 1 828.22 668.17 86.58 o -11 9 1 915.23 821.19 32.70 o -9 9 1 5661.71 5749.56 67.85 o -7 9 1 16079.66 16219.66 141.74 o -5 9 1 824.42 558.36 27.90 o -3 9 1 16665.21 18198.68 145.77 o -1 9 1 38933.41 40181.99 293.59 o 1 9 1 125.87 44.09 18.17 o 3 9 1 6884.52 8025.18 71.11 o 5 9 1 4743.32 4711.21 59.08 o 7 9 1 15.04 20.59 20.04 o 9 9 1 3429.55 4080.19 55.57 o 11 9 1 814.34 700.84 33.33 o 13 9 1 95.05 83.22 28.25 o 15 9 1 3.91 2.00 23.25 o 17 9 1 884.58 746.12 62.56 o 19 9 1 1087.35 1092.03 62.01 o 21 9 1 113.77 147.83 52.53 o -22 10 1 20.77 81.07 42.72 o -20 10 1 647.74 593.74 56.93 o -18 10 1 254.58 276.43 39.83 o -16 10 1 223.95 174.52 34.17 o -14 10 1 279.82 251.25 24.92 o -12 10 1 160.86 121.10 25.91 o -10 10 1 473.69 565.05 30.79 o -8 10 1 935.93 942.74 32.45 o -6 10 1 4544.09 4735.15 58.06 o -4 10 1 183.15 247.04 25.83 o -2 10 1 7422.34 6942.42 64.50 o 0 10 1 2251.25 2063.43 36.41 o 2 10 1 109.86 57.12 18.82 o 4 10 1 257.13 256.28 23.32 o 6 10 1 797.88 794.32 36.00 o 8 10 1 88.73 156.38 26.52 o 10 10 1 95.38 84.42 22.83 o 12 10 1 3867.25 3631.60 78.64 o 14 10 1 91.79 46.69 16.82 o 16 10 1 44.89 15.64 28.02 o 18 10 1 592.37 618.78 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