#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:14:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180835 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/66/2016614.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016614_Fobs loop_ _publ_author_name 'Harrison, William T. A.' _publ_section_title ; Two scandium--biuret complexes: [Sc(C~2~H~5~N~3~O~2~)(H~2~O)~5~]Cl~3~·H~2~O and [Sc(C~2~H~5~N~3~O~2~)~4~](NO~3~)~3~ ; _journal_coeditor_code SK3214 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m205 _journal_page_last m208 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.247 _cell_angle_gamma 90.000 _cell_length_a 15.2430 _cell_length_b 7.5653 _cell_length_c 14.1276 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.7695 _cod_data_source_file sk3214Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wh513 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 205.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1032.99 955.16 15.47 o 4 0 0 10934.11 11033.24 177.25 o 5 0 0 15283.35 14986.70 210.08 o 6 0 0 10181.34 10031.61 138.01 o 7 0 0 10215.19 9600.62 99.84 o 8 0 0 790.10 783.17 12.60 o 9 0 0 678.51 727.98 16.75 o 10 0 0 185.45 216.82 6.57 o 11 0 0 2413.93 2619.15 37.63 o 12 0 0 31.41 39.12 4.26 o 13 0 0 1832.63 1852.29 44.34 o 14 0 0 451.68 476.79 16.77 o 15 0 0 106.70 123.14 10.85 o 16 0 0 91.93 83.60 10.33 o 17 0 0 1725.99 1707.08 74.02 o 2 1 0 1180.21 1173.84 41.80 o 3 1 0 58.31 56.06 1.70 o 4 1 0 3527.33 3436.60 36.42 o 5 1 0 6713.96 6607.43 68.58 o 6 1 0 2108.09 2111.43 21.84 o 7 1 0 926.62 899.43 9.89 o 8 1 0 439.81 455.83 6.15 o 9 1 0 317.23 311.23 5.06 o 10 1 0 1355.27 1400.50 15.11 o 11 1 0 464.71 453.60 6.92 o 12 1 0 75.06 87.03 3.53 o 13 1 0 0.26 1.07 2.96 o 14 1 0 1522.85 1554.11 34.82 o 15 1 0 33.13 38.23 5.94 o 16 1 0 107.62 101.13 7.99 o 17 1 0 33.86 27.56 7.00 o 0 2 0 7295.90 7069.76 83.25 o 1 2 0 370.38 370.45 5.35 o 2 2 0 42351.45 43419.84 1048.55 o 3 2 0 425.80 405.30 5.83 o 4 2 0 7572.25 7285.58 78.28 o 5 2 0 527.51 426.63 5.94 o 6 2 0 5013.76 4910.31 48.72 o 7 2 0 73.28 68.80 2.43 o 8 2 0 1413.18 1392.11 14.05 o 9 2 0 9450.28 9570.27 92.36 o 10 2 0 185.26 185.35 4.67 o 11 2 0 1387.07 1388.77 19.53 o 12 2 0 573.15 590.30 10.92 o 13 2 0 758.08 752.70 16.00 o 14 2 0 549.23 541.16 17.15 o 15 2 0 1018.77 1063.62 40.42 o 16 2 0 2.13 -5.65 6.68 o 17 2 0 9.70 6.82 8.18 o 1 3 0 1726.07 1639.76 15.07 o 2 3 0 7317.50 7062.30 73.54 o 3 3 0 12690.03 13107.22 173.90 o 4 3 0 93.25 75.90 2.82 o 5 3 0 2.90 2.15 1.46 o 6 3 0 278.31 237.23 4.15 o 7 3 0 286.62 307.67 5.08 o 8 3 0 231.05 241.82 4.62 o 9 3 0 39.16 42.14 3.40 o 10 3 0 1599.71 1671.94 32.63 o 11 3 0 566.44 580.36 11.26 o 12 3 0 5.70 9.14 3.01 o 13 3 0 644.72 617.86 17.58 o 14 3 0 477.19 444.68 15.94 o 15 3 0 21.06 7.24 7.23 o 16 3 0 6.59 9.12 7.66 o 0 4 0 5773.00 5806.74 68.94 o 1 4 0 820.41 888.93 9.50 o 2 4 0 28569.91 28229.13 320.80 o 3 4 0 34.28 53.23 2.13 o 4 4 0 4549.25 4496.66 50.77 o 5 4 0 37.89 30.46 2.99 o 6 4 0 1827.83 1824.47 22.32 o 7 4 0 1123.11 1151.09 15.28 o 8 4 0 678.24 638.44 9.89 o 9 4 0 1988.98 2065.58 29.79 o 10 4 0 1.28 -0.30 2.56 o 11 4 0 310.82 293.89 7.52 o 12 4 0 35.12 33.18 5.25 o 13 4 0 152.43 165.68 11.10 o 14 4 0 114.96 108.72 11.83 o 15 4 0 1041.54 1042.58 38.11 o 16 4 0 19.74 15.40 10.69 o 1 5 0 3040.33 2998.23 28.62 o 2 5 0 2906.95 2888.23 30.13 o 3 5 0 36.39 13.71 1.95 o 4 5 0 125.16 127.05 3.60 o 5 5 0 4803.63 4961.48 62.45 o 6 5 0 145.16 145.20 3.72 o 7 5 0 1689.42 1741.02 26.79 o 8 5 0 2321.49 2424.45 39.63 o 9 5 0 7.58 9.58 3.06 o 10 5 0 55.06 56.06 5.70 o 11 5 0 19.27 16.79 5.14 o 12 5 0 5720.08 5915.14 171.71 o 13 5 0 66.91 64.17 7.46 o 14 5 0 8.16 9.34 9.45 o 15 5 0 283.13 212.44 20.77 o 0 6 0 8665.79 8797.46 146.74 o 1 6 0 106.16 112.06 3.32 o 2 6 0 403.22 390.63 6.16 o 3 6 0 95.23 106.78 3.49 o 4 6 0 2085.23 2073.44 25.12 o 5 6 0 8.14 11.17 2.58 o 6 6 0 682.55 704.90 11.59 o 7 6 0 1476.63 1475.21 20.35 o 8 6 0 488.10 495.45 9.92 o 9 6 0 39.54 35.57 4.25 o 10 6 0 369.19 375.01 12.43 o 11 6 0 717.50 750.16 25.51 o 12 6 0 25.10 28.67 18.61 o 13 6 0 14.19 9.67 6.82 o 1 7 0 2048.49 2156.65 34.35 o 2 7 0 75.83 65.42 3.63 o 3 7 0 1680.13 1687.48 29.09 o 4 7 0 153.94 153.51 4.73 o 5 7 0 179.60 198.71 5.61 o 6 7 0 58.14 49.47 4.03 o 7 7 0 62.64 62.19 8.03 o 8 7 0 532.24 540.58 13.51 o 9 7 0 30.41 18.92 4.69 o 10 7 0 785.96 776.14 25.35 o 11 7 0 309.69 281.83 11.89 o 12 7 0 78.93 67.18 9.08 o 0 8 0 3692.44 3827.28 111.24 o 1 8 0 115.85 121.45 4.87 o 2 8 0 160.81 154.10 6.50 o 3 8 0 62.16 55.52 4.89 o 4 8 0 581.00 591.50 19.22 o 5 8 0 199.78 195.68 7.87 o 6 8 0 930.22 980.94 24.11 o 7 8 0 333.26 320.28 11.89 o 8 8 0 353.96 346.02 11.63 o 9 8 0 31.84 35.94 8.86 o 10 8 0 87.43 74.49 11.39 o 1 9 0 338.84 335.42 34.35 o 2 9 0 1.76 16.99 7.99 o 3 9 0 1373.20 1439.80 56.00 o 4 9 0 192.00 180.34 14.18 o 5 9 0 77.01 70.47 10.17 o 6 9 0 673.85 643.92 28.57 o 7 9 0 427.00 404.83 24.98 o -17 1 1 2847.74 2991.80 91.83 o -16 1 1 142.03 148.94 8.87 o -15 1 1 150.75 146.52 11.83 o -14 1 1 300.87 303.71 9.09 o -13 1 1 5208.95 5425.51 89.39 o -12 1 1 1.05 0.57 1.91 o -11 1 1 1317.76 1375.03 14.41 o -10 1 1 4164.53 4036.42 43.11 o -9 1 1 277.90 283.72 4.99 o -8 1 1 22.89 22.60 2.08 o -7 1 1 759.37 799.38 7.83 o -6 1 1 4069.13 3942.39 38.26 o -5 1 1 850.32 901.37 8.80 o -4 1 1 2807.43 2992.32 32.78 o -3 1 1 6380.16 6242.84 62.37 o -2 1 1 777.55 694.18 40.30 o 0 1 1 32.80 14.94 1.94 o 1 1 1 8573.26 8351.23 241.06 o 2 1 1 4991.57 4712.68 46.94 o 3 1 1 2610.98 2549.92 24.60 o 4 1 1 247.37 234.32 3.80 o 5 1 1 1587.54 1555.49 15.71 o 6 1 1 4761.51 4375.72 40.37 o 7 1 1 1928.24 1839.78 19.08 o 8 1 1 10450.88 10214.84 100.63 o 9 1 1 4699.73 4708.96 49.25 o 10 1 1 3372.14 3468.96 39.12 o 11 1 1 16.71 23.58 3.26 o 12 1 1 569.85 569.22 10.21 o 13 1 1 634.04 659.99 13.90 o 14 1 1 2953.36 3132.02 70.20 o 15 1 1 367.45 372.01 15.66 o 16 1 1 26.58 21.16 5.84 o -17 2 1 156.09 163.41 20.99 o -16 2 1 360.24 374.40 17.42 o -15 2 1 142.70 160.21 12.45 o -14 2 1 201.46 190.22 8.58 o -13 2 1 1714.10 1803.30 33.14 o -12 2 1 11.19 15.06 2.92 o -11 2 1 202.97 197.76 4.89 o -10 2 1 237.65 264.07 6.12 o -9 2 1 728.91 676.24 8.00 o -8 2 1 1245.36 1311.25 15.48 o -7 2 1 3230.01 3481.34 39.78 o -6 2 1 366.56 447.61 6.86 o -5 2 1 327.46 369.81 5.28 o -4 2 1 4.83 8.55 1.43 o -3 2 1 553.92 644.78 7.64 o -2 2 1 6909.34 6649.89 64.94 o -1 2 1 7868.66 7935.82 65.20 o 0 2 1 1719.37 1776.24 21.49 o 1 2 1 18792.47 18468.74 211.80 o 2 2 1 3990.00 3965.58 36.46 o 3 2 1 108.68 92.36 2.48 o 4 2 1 12567.94 12302.75 131.34 o 5 2 1 2191.94 2312.56 26.54 o 6 2 1 3252.73 3046.19 31.06 o 7 2 1 18.27 12.11 1.90 o 8 2 1 959.86 877.62 13.15 o 9 2 1 7.35 4.01 2.00 o 10 2 1 86.21 91.36 3.43 o 11 2 1 1720.53 1714.80 25.07 o 12 2 1 504.10 489.62 10.13 o 13 2 1 583.39 592.61 15.27 o 14 2 1 27.34 23.24 7.73 o 15 2 1 87.20 94.16 9.26 o 16 2 1 137.89 121.26 12.97 o -17 3 1 1.65 -1.96 6.97 o -16 3 1 0.58 -1.57 5.43 o -15 3 1 3952.40 4135.78 158.13 o -14 3 1 10.26 9.21 6.71 o -13 3 1 2.65 5.11 3.73 o -12 3 1 2292.91 2322.81 40.82 o -11 3 1 2396.87 2410.94 39.49 o -10 3 1 95.79 78.56 3.48 o -9 3 1 59.60 53.47 3.27 o -8 3 1 3648.21 3664.21 38.64 o -7 3 1 523.95 547.07 9.10 o -6 3 1 6256.81 6291.65 67.46 o -5 3 1 1720.18 1869.34 25.04 o -4 3 1 12594.10 12833.34 160.18 o -3 3 1 52.62 37.87 1.73 o -2 3 1 503.56 571.11 6.79 o -1 3 1 7660.66 7163.04 81.31 o 0 3 1 7307.89 7258.26 67.87 o 1 3 1 269.54 276.47 3.55 o 2 3 1 1568.25 1645.80 16.33 o 3 3 1 4353.97 4021.11 45.54 o 4 3 1 1916.85 1702.59 16.35 o 5 3 1 4.17 3.38 1.77 o 6 3 1 3908.38 3901.63 46.62 o 7 3 1 1354.64 1335.00 16.23 o 8 3 1 2987.90 3005.47 36.99 o 9 3 1 553.18 556.78 10.28 o 10 3 1 2752.23 2851.83 44.50 o 11 3 1 2898.01 2957.90 51.96 o 12 3 1 3376.94 3518.64 84.90 o 13 3 1 191.21 180.79 12.49 o 14 3 1 191.80 171.87 10.90 o 15 3 1 306.28 299.38 15.57 o 16 3 1 1006.11 1029.57 52.25 o -16 4 1 7.19 13.00 8.18 o -15 4 1 570.69 551.30 22.80 o -14 4 1 256.23 273.77 11.64 o -13 4 1 235.78 206.46 8.35 o -12 4 1 608.82 628.31 13.81 o -11 4 1 1362.01 1367.09 25.77 o -10 4 1 82.13 86.90 4.69 o -9 4 1 9.73 21.88 2.57 o -8 4 1 487.60 505.80 9.63 o -7 4 1 8.45 5.61 1.90 o -6 4 1 83.30 89.75 3.47 o -5 4 1 1849.07 1879.72 130.51 o -4 4 1 4062.36 4278.20 47.55 o -3 4 1 62.92 63.81 2.24 o -2 4 1 872.61 862.57 12.45 o -1 4 1 1839.02 1770.61 18.13 o 0 4 1 1708.30 1678.53 18.77 o 1 4 1 602.65 544.01 6.46 o 2 4 1 7033.85 7207.56 59.23 o 3 4 1 127.67 99.62 3.71 o 4 4 1 9.12 7.35 1.93 o 5 4 1 19.19 33.94 2.31 o 6 4 1 404.26 374.48 6.03 o 7 4 1 71.71 77.53 2.96 o 8 4 1 55.60 51.61 3.05 o 9 4 1 86.99 91.28 3.77 o 10 4 1 19.03 17.07 3.18 o 11 4 1 197.48 208.25 7.58 o 12 4 1 15.59 12.93 5.47 o 13 4 1 844.91 811.69 26.00 o 14 4 1 325.82 310.54 13.45 o 15 4 1 15.81 16.93 10.16 o -15 5 1 662.94 625.61 49.73 o -14 5 1 216.77 189.16 10.82 o -13 5 1 888.77 898.94 30.10 o -12 5 1 91.03 80.98 7.05 o -11 5 1 755.12 751.52 21.47 o -10 5 1 540.56 560.42 11.06 o -9 5 1 95.89 87.57 4.58 o -8 5 1 13.25 15.75 3.51 o -7 5 1 54.67 59.60 4.26 o -6 5 1 0.36 -1.63 1.90 o -5 5 1 2.55 3.90 1.99 o -4 5 1 10.37 14.83 2.14 o -3 5 1 1061.81 1048.52 12.89 o -2 5 1 539.69 539.98 7.38 o -1 5 1 298.31 360.78 5.18 o 0 5 1 1666.79 1589.96 19.76 o 1 5 1 60.27 45.85 2.33 o 2 5 1 52.71 38.43 2.29 o 3 5 1 148.70 141.86 3.74 o 4 5 1 1711.45 1638.91 22.01 o 5 5 1 743.99 728.53 10.08 o 6 5 1 1830.04 1884.43 29.07 o 7 5 1 396.91 395.75 10.23 o 8 5 1 2733.33 2874.68 46.33 o 9 5 1 24.16 32.73 3.96 o 10 5 1 1063.08 1081.39 24.05 o 11 5 1 794.45 857.74 24.79 o 12 5 1 866.17 878.38 26.77 o 13 5 1 294.57 245.79 12.82 o 14 5 1 115.13 90.99 13.14 o -14 6 1 67.35 55.69 10.92 o -13 6 1 2.83 -2.52 7.11 o -12 6 1 201.12 214.43 12.08 o -11 6 1 2309.84 2274.21 52.72 o -10 6 1 238.93 218.16 7.88 o -9 6 1 1119.45 1136.58 24.75 o -8 6 1 19.46 21.15 3.26 o -7 6 1 333.14 348.82 10.34 o -6 6 1 1303.27 1321.40 20.77 o -5 6 1 1865.00 1925.58 25.66 o -4 6 1 673.25 676.62 10.56 o -3 6 1 181.47 199.78 4.67 o -2 6 1 603.36 626.45 8.99 o -1 6 1 1324.16 1376.65 19.55 o 0 6 1 230.54 228.80 4.70 o 1 6 1 346.14 341.97 6.32 o 2 6 1 3540.20 3645.92 42.51 o 3 6 1 132.31 129.14 4.96 o 4 6 1 26.70 18.17 2.52 o 5 6 1 364.64 357.38 6.59 o 6 6 1 2123.15 2182.13 29.36 o 7 6 1 488.75 509.86 11.49 o 8 6 1 396.87 385.11 9.24 o 9 6 1 1718.29 1706.38 39.62 o 10 6 1 0.36 -0.77 5.30 o 11 6 1 6.58 11.76 6.42 o 12 6 1 58.48 65.58 11.69 o 13 6 1 453.18 446.30 33.66 o -12 7 1 68.13 68.85 8.35 o -11 7 1 64.15 61.79 6.81 o -10 7 1 503.81 479.66 15.82 o -9 7 1 80.09 49.83 5.87 o -8 7 1 781.50 840.53 19.85 o -7 7 1 526.03 503.03 12.66 o -6 7 1 1186.93 1161.23 19.03 o -5 7 1 361.51 349.03 7.04 o -4 7 1 419.63 415.47 8.32 o -3 7 1 45.15 45.38 3.10 o -2 7 1 97.01 90.03 4.17 o -1 7 1 29.55 30.88 3.11 o 0 7 1 0.34 -2.28 2.28 o 1 7 1 545.35 559.20 11.44 o 2 7 1 4082.63 4249.89 71.71 o 3 7 1 735.14 733.43 12.02 o 4 7 1 165.99 154.94 4.84 o 5 7 1 469.29 475.31 9.25 o 6 7 1 1386.56 1349.06 27.82 o 7 7 1 926.77 938.63 21.30 o 8 7 1 1099.39 1109.41 25.90 o 9 7 1 1842.25 1889.51 46.62 o 10 7 1 512.01 513.70 16.54 o 11 7 1 424.15 382.00 14.76 o -10 8 1 139.32 146.15 12.16 o -9 8 1 716.16 702.37 22.58 o -8 8 1 33.24 22.64 6.94 o -7 8 1 1169.26 1183.45 32.46 o -6 8 1 108.18 92.84 6.93 o -5 8 1 49.01 38.96 5.77 o -4 8 1 258.68 244.74 7.57 o -3 8 1 1368.58 1435.32 26.73 o -2 8 1 1359.11 1386.53 29.87 o -1 8 1 148.90 145.13 7.17 o 0 8 1 3394.76 3491.18 77.60 o 1 8 1 204.20 175.90 5.11 o 2 8 1 153.69 142.22 5.63 o 3 8 1 206.76 190.37 7.31 o 4 8 1 1352.99 1396.80 33.71 o 5 8 1 121.65 132.81 7.43 o 6 8 1 335.99 333.24 11.64 o 7 8 1 189.55 171.05 11.17 o 8 8 1 558.00 554.23 29.37 o 9 8 1 13.19 22.13 8.30 o -7 9 1 168.01 170.04 18.37 o -6 9 1 587.41 583.86 50.65 o -5 9 1 157.72 106.14 17.22 o -4 9 1 72.36 66.64 7.32 o -3 9 1 28.21 44.32 8.56 o -2 9 1 28.95 26.01 6.74 o -1 9 1 6.89 15.75 8.64 o 0 9 1 943.36 927.42 27.04 o 1 9 1 385.68 358.35 17.17 o 2 9 1 54.11 45.13 7.13 o 3 9 1 0.02 -8.14 8.14 o 4 9 1 244.89 245.49 16.66 o 5 9 1 181.33 139.77 28.84 o 6 9 1 130.56 105.18 10.06 o -18 0 2 193.33 186.84 13.67 o -17 0 2 945.63 893.59 42.56 o -16 0 2 6515.74 6508.17 249.57 o -15 0 2 828.36 862.68 23.07 o -14 0 2 273.34 297.06 10.18 o -13 0 2 1524.60 1641.73 39.45 o -12 0 2 3301.36 3466.84 60.58 o -11 0 2 2328.27 2283.56 53.04 o -10 0 2 1539.11 1732.93 26.59 o -9 0 2 15168.58 15740.53 264.46 o -8 0 2 81.11 47.15 5.37 o -7 0 2 5210.41 5015.02 58.03 o -6 0 2 16482.91 17091.49 236.00 o -5 0 2 28086.14 28302.13 472.23 o -4 0 2 3437.81 3536.97 78.83 o -3 0 2 6316.69 6207.10 94.73 o 1 0 2 6386.37 6806.22 179.33 o 2 0 2 3852.32 3504.27 49.20 o 3 0 2 12198.47 12078.66 197.03 o 4 0 2 1083.01 1081.62 18.74 o 5 0 2 6088.76 6540.09 88.14 o 6 0 2 7.56 -0.80 2.34 o 7 0 2 55.62 35.47 3.28 o 8 0 2 2822.87 2922.20 41.09 o 9 0 2 0.81 0.37 2.84 o 10 0 2 3431.39 3393.22 61.62 o 11 0 2 3811.38 4003.41 97.63 o 12 0 2 18.20 18.11 4.15 o 13 0 2 29.53 35.43 13.09 o 14 0 2 3533.16 3671.18 135.19 o 15 0 2 393.34 371.99 30.01 o 16 0 2 3862.48 4081.46 162.09 o -18 1 2 441.08 429.48 22.38 o -17 1 2 0.02 2.68 4.51 o -16 1 2 23.96 21.44 5.00 o -15 1 2 106.66 100.70 4.97 o -14 1 2 147.20 151.48 5.10 o -13 1 2 1002.69 1061.83 19.18 o -12 1 2 191.23 201.55 6.96 o -11 1 2 3346.46 3476.47 32.50 o -10 1 2 139.81 124.81 3.81 o -9 1 2 293.31 272.63 5.60 o -8 1 2 69.39 78.33 2.06 o -7 1 2 1243.14 1464.65 14.04 o -6 1 2 7677.57 7834.34 107.54 o -5 1 2 3890.57 3913.32 42.31 o -4 1 2 877.47 1018.22 12.74 o -3 1 2 1223.37 1218.68 16.08 o -2 1 2 3726.71 3392.27 180.24 o -1 1 2 2.99 -0.83 0.83 o 0 1 2 6.16 11.43 0.85 o 1 1 2 1538.77 1468.58 14.63 o 2 1 2 3140.73 2982.72 28.60 o 3 1 2 11.46 22.28 1.46 o 4 1 2 643.26 597.04 6.75 o 5 1 2 460.71 537.52 6.45 o 6 1 2 1770.70 1762.48 21.33 o 7 1 2 22.44 18.08 1.89 o 8 1 2 785.16 799.58 9.78 o 9 1 2 351.57 377.39 7.88 o 10 1 2 972.56 944.78 13.34 o 11 1 2 1447.37 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