#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/67/2016703.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016703_Fobs loop_ _publ_author_name 'Zhao, Wen-Na' 'Han, Lei' 'Luo, Cheng-Cai' _publ_section_title ; A novel tetranuclear copper(I) sulfanide complex with bis(diphenylphosphino)amine ; _journal_coeditor_code EM3015 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m280 _journal_page_last m282 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.0144 _cell_length_b 18.2738 _cell_length_c 17.1713 _exptl_crystal_F_000 2496.00 _reflns_d_resolution_high 0.8387 _[local]_cod_data_source_file em3015Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' H in P-1 Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 733.49 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 39978.98 40955.30 1038.82 o 4 0 0 28667.22 30802.17 801.60 o 6 0 0 45498.20 42889.09 1116.59 o 8 0 0 143833.55 144443.31 3671.81 o 10 0 0 70241.43 75211.82 1959.63 o 12 0 0 478.22 463.21 94.59 o 14 0 0 3934.87 3455.57 186.75 o 16 0 0 392.27 779.17 127.26 o 18 0 0 676.50 834.51 147.74 o 20 0 0 92.93 865.96 179.19 o 2 1 0 23449.03 23122.10 294.55 o 4 1 0 81585.23 77867.64 1005.80 o 6 1 0 9704.77 11515.34 265.01 o 8 1 0 1343.39 1413.16 61.72 o 10 1 0 450.23 611.00 53.74 o 12 1 0 5245.39 5273.36 152.96 o 14 1 0 10602.40 10184.27 254.27 o 16 1 0 560.55 654.47 82.31 o 18 1 0 730.71 829.31 114.95 o 20 1 0 7.26 -58.56 188.45 o 0 2 0 57698.36 60971.38 1085.48 o 2 2 0 14272.75 11276.66 148.44 o 4 2 0 888.75 1378.19 32.30 o 6 2 0 1138.52 989.86 73.97 o 8 2 0 53901.98 54811.64 1200.33 o 10 2 0 1326.23 1333.68 118.61 o 12 2 0 9329.51 9374.00 446.27 o 14 2 0 2561.20 2494.18 118.88 o 16 2 0 2028.82 2144.48 122.74 o 18 2 0 790.95 1035.93 407.99 o 20 2 0 652.33 673.33 197.60 o 2 3 0 114920.46 122590.66 1541.94 o 4 3 0 2246.19 2028.13 39.56 o 6 3 0 32589.19 31883.66 732.63 o 8 3 0 256.98 397.02 24.28 o 10 3 0 1678.62 1929.69 112.88 o 12 3 0 328.30 335.61 138.48 o 14 3 0 1725.80 1699.66 96.98 o 16 3 0 287.28 277.62 327.05 o 18 3 0 17.57 207.36 86.71 o 20 3 0 683.95 897.65 133.11 o 0 4 0 4003.63 3858.72 97.76 o 2 4 0 520.54 412.74 68.44 o 4 4 0 36474.83 31158.45 453.76 o 6 4 0 17684.26 17360.77 235.53 o 8 4 0 1339.89 1328.19 35.06 o 10 4 0 1519.20 921.89 160.78 o 12 4 0 2328.38 1853.98 88.14 o 14 4 0 4208.92 4468.76 153.38 o 16 4 0 786.40 919.16 296.58 o 18 4 0 614.07 795.71 112.51 o 2 5 0 4805.07 3519.84 111.59 o 4 5 0 9199.39 8829.36 128.05 o 6 5 0 4764.95 6091.15 97.16 o 8 5 0 2852.86 2865.32 58.41 o 10 5 0 2.79 56.64 62.17 o 12 5 0 2240.36 2157.58 173.34 o 14 5 0 117.97 24.61 355.33 o 16 5 0 589.66 922.94 141.52 o 18 5 0 12.19 -103.37 103.37 o 0 6 0 14.48 16.98 18.86 o 2 6 0 3351.36 3906.11 65.07 o 4 6 0 102424.56 96608.13 1227.39 o 6 6 0 4709.33 3980.25 72.94 o 8 6 0 1571.30 1386.26 78.01 o 10 6 0 1037.79 971.54 62.22 o 12 6 0 965.00 845.92 105.56 o 14 6 0 9994.70 10144.30 962.26 o 16 6 0 149.81 297.43 112.15 o 18 6 0 499.77 315.23 122.14 o 2 7 0 11403.50 13403.50 187.26 o 4 7 0 2017.62 2271.24 66.12 o 6 7 0 12193.04 13489.18 409.99 o 8 7 0 7375.15 6660.62 143.29 o 10 7 0 3427.49 3540.54 74.52 o 12 7 0 308.70 329.53 106.66 o 14 7 0 1753.83 1117.07 143.60 o 16 7 0 3475.17 3438.01 216.25 o 18 7 0 1175.84 1327.47 170.17 o 0 8 0 20665.95 21586.87 411.87 o 2 8 0 16213.11 16969.52 234.18 o 4 8 0 34806.40 36317.61 477.42 o 6 8 0 10968.75 10823.96 192.76 o 8 8 0 30538.09 30599.17 413.85 o 10 8 0 123.29 119.78 78.21 o 12 8 0 742.16 661.66 108.73 o 14 8 0 14.95 187.72 96.54 o 16 8 0 9788.37 10533.21 413.48 o 18 8 0 238.93 -47.30 137.50 o 2 9 0 28632.46 26866.99 406.33 o 4 9 0 5274.08 5608.04 96.66 o 6 9 0 15.77 49.16 64.65 o 8 9 0 175.42 294.19 31.80 o 10 9 0 12804.73 14250.72 378.43 o 12 9 0 3366.07 3332.94 190.89 o 14 9 0 1414.85 1348.92 146.77 o 16 9 0 1235.90 1436.45 167.98 o 18 9 0 662.93 396.17 160.66 o 0 10 0 80210.41 79411.08 1442.93 o 2 10 0 30239.85 31050.41 416.19 o 4 10 0 8682.06 9056.43 191.12 o 6 10 0 758.13 748.84 47.86 o 8 10 0 25789.58 27681.79 446.79 o 10 10 0 4343.08 4747.08 113.53 o 12 10 0 0.09 49.98 93.37 o 14 10 0 232.64 115.32 103.37 o 16 10 0 556.06 357.40 121.17 o 2 11 0 7215.99 6912.50 148.95 o 4 11 0 3360.86 3182.30 87.65 o 6 11 0 1557.39 1365.07 67.05 o 8 11 0 11.29 278.07 66.51 o 10 11 0 7970.52 8109.74 170.92 o 12 11 0 174.49 301.82 109.71 o 14 11 0 1389.18 1315.77 148.23 o 16 11 0 97.01 -82.40 82.40 o 0 12 0 1172.41 1173.42 61.81 o 2 12 0 4037.29 3659.45 106.21 o 4 12 0 2000.92 1807.16 122.03 o 6 12 0 1060.49 1042.94 76.95 o 8 12 0 104.59 25.17 38.14 o 10 12 0 952.04 904.00 192.36 o 12 12 0 806.88 805.50 114.10 o 14 12 0 24.75 -46.08 90.20 o 16 12 0 140.51 113.61 135.31 o 2 13 0 971.81 820.00 55.44 o 4 13 0 550.42 578.05 59.76 o 6 13 0 373.08 250.03 47.66 o 8 13 0 746.65 714.18 104.15 o 10 13 0 1012.08 802.67 77.88 o 12 13 0 1819.80 1954.76 158.71 o 14 13 0 436.19 235.02 119.46 o 16 13 0 19.55 -92.64 92.64 o 0 14 0 28.24 104.83 72.65 o 2 14 0 14056.30 13060.19 305.74 o 4 14 0 4615.53 4383.10 118.79 o 6 14 0 2160.91 1903.20 188.40 o 8 14 0 1165.32 831.93 93.40 o 10 14 0 1435.13 1445.38 163.95 o 12 14 0 4189.92 4427.34 240.87 o 14 14 0 9.17 209.66 118.97 o 2 15 0 134.03 318.19 65.51 o 4 15 0 1381.11 1024.89 264.88 o 6 15 0 969.83 1094.01 123.47 o 8 15 0 1.74 61.94 87.17 o 10 15 0 21.01 186.87 81.02 o 12 15 0 39.81 336.93 147.74 o 14 15 0 208.64 -134.09 134.09 o 0 16 0 1207.03 1017.85 118.97 o 2 16 0 1682.59 1731.28 237.34 o 4 16 0 10215.14 10945.59 277.94 o 6 16 0 4418.87 4324.79 463.33 o 8 16 0 569.83 574.22 118.39 o 10 16 0 48.65 425.64 92.89 o 12 16 0 1365.41 1158.03 161.15 o 2 17 0 360.02 588.32 90.69 o 4 17 0 58.33 285.42 72.97 o 6 17 0 1767.55 1742.16 104.44 o 8 17 0 2177.04 2382.86 117.60 o 10 17 0 42.59 529.60 239.65 o 12 17 0 8.05 243.06 137.01 o 0 18 0 311.13 241.85 102.15 o 2 18 0 8.27 41.91 100.81 o 4 18 0 1873.33 2025.15 110.97 o 6 18 0 62.02 -9.95 66.45 o 8 18 0 456.44 435.17 78.61 o 10 18 0 51.12 394.22 149.45 o 2 19 0 1168.88 788.69 117.75 o 4 19 0 53.51 -52.75 52.75 o 6 19 0 2412.13 2074.75 119.91 o 8 19 0 479.76 661.74 95.45 o 0 20 0 304.59 298.65 111.66 o 2 20 0 62.77 -83.53 341.68 o 4 20 0 47.47 -33.24 121.53 o 6 20 0 62.41 151.67 86.93 o 2 21 0 556.72 437.57 100.39 o 4 21 0 36.82 -226.00 226.00 o 1 1 1 120389.70 124715.28 2005.96 o 2 1 1 1.41 66.10 22.64 o 3 1 1 12872.23 14957.07 227.67 o 4 1 1 11.24 142.39 44.91 o 5 1 1 3317.31 2912.10 46.71 o 6 1 1 4586.90 5073.35 73.11 o 7 1 1 47076.28 45182.05 524.72 o 8 1 1 1311.59 1325.42 52.89 o 9 1 1 74455.10 73302.77 950.53 o 10 1 1 1109.83 1195.51 93.62 o 11 1 1 344.55 419.05 35.73 o 12 1 1 453.24 374.66 57.85 o 13 1 1 302.94 328.76 90.12 o 14 1 1 871.68 846.56 57.01 o 15 1 1 6263.25 6423.50 137.24 o 16 1 1 239.81 376.81 55.78 o 17 1 1 2785.63 2918.17 96.91 o 18 1 1 189.00 403.05 63.08 o 19 1 1 24.80 261.62 218.84 o 20 1 1 5.31 132.13 122.11 o 0 2 1 2010.40 2287.25 82.30 o 1 2 1 17523.63 17148.03 198.49 o 2 2 1 1369.16 1418.40 23.07 o 3 2 1 32242.96 35672.69 458.13 o 4 2 1 2488.68 2175.23 37.69 o 5 2 1 23408.99 24400.80 288.12 o 6 2 1 862.00 884.18 26.49 o 7 2 1 577.25 744.68 59.25 o 8 2 1 90.74 216.29 55.53 o 9 2 1 7355.33 7728.38 108.97 o 10 2 1 459.24 571.73 40.47 o 11 2 1 1942.43 1494.44 91.95 o 12 2 1 28.81 38.37 61.19 o 13 2 1 2470.88 2539.80 77.46 o 14 2 1 117.23 182.01 43.88 o 15 2 1 4721.30 4973.67 187.35 o 16 2 1 55.31 173.96 118.20 o 17 2 1 459.63 415.62 60.44 o 18 2 1 13.16 85.91 164.12 o 19 2 1 27.44 387.58 66.14 o 20 2 1 0.40 93.18 157.61 o 1 3 1 5782.56 6391.63 80.20 o 2 3 1 13059.96 12875.80 135.20 o 3 3 1 181.14 98.04 19.16 o 4 3 1 32.26 84.70 26.24 o 5 3 1 3482.07 2806.20 53.52 o 6 3 1 218.86 226.41 37.72 o 7 3 1 17829.87 17521.79 196.06 o 8 3 1 166.90 197.68 51.37 o 9 3 1 493.10 572.03 24.72 o 10 3 1 2355.49 2119.85 146.91 o 11 3 1 13867.19 13192.19 206.53 o 12 3 1 57.62 197.77 37.25 o 13 3 1 1448.03 1696.02 96.70 o 14 3 1 478.79 390.17 114.93 o 15 3 1 3.58 25.98 119.05 o 16 3 1 53.91 250.15 53.48 o 17 3 1 49.11 316.63 94.90 o 18 3 1 506.72 602.73 137.80 o 19 3 1 131.08 711.49 183.55 o 20 3 1 19.72 178.28 342.44 o 0 4 1 492.20 671.27 43.39 o 1 4 1 21376.88 22433.85 248.75 o 2 4 1 3654.79 4055.79 58.50 o 3 4 1 64286.57 62304.02 560.52 o 4 4 1 11024.66 12092.26 120.35 o 5 4 1 3190.45 2752.03 44.01 o 6 4 1 276.46 349.08 48.87 o 7 4 1 6065.92 5419.27 73.48 o 8 4 1 706.57 806.85 47.63 o 9 4 1 1306.81 1370.16 42.14 o 10 4 1 53.98 54.50 89.95 o 11 4 1 676.94 581.04 78.93 o 12 4 1 696.03 661.65 67.07 o 13 4 1 1645.11 1492.26 161.24 o 14 4 1 119.06 25.10 64.68 o 15 4 1 2168.69 2280.10 100.18 o 16 4 1 58.46 98.16 135.78 o 17 4 1 323.43 349.42 125.62 o 18 4 1 143.05 395.98 106.29 o 19 4 1 1001.37 1702.10 125.12 o 1 5 1 387.68 464.91 22.63 o 2 5 1 1354.82 1515.49 22.69 o 3 5 1 40591.61 36059.32 330.11 o 4 5 1 3390.19 3532.26 43.03 o 5 5 1 56398.98 52111.32 523.85 o 6 5 1 3049.85 3097.79 41.70 o 7 5 1 11351.10 11899.19 121.11 o 8 5 1 1240.13 1226.78 36.94 o 9 5 1 712.45 575.01 50.02 o 10 5 1 92.57 97.67 59.39 o 11 5 1 1156.60 997.67 61.19 o 12 5 1 243.99 86.13 59.33 o 13 5 1 6472.64 6631.33 132.98 o 14 5 1 36.50 167.64 108.24 o 15 5 1 2236.86 2714.24 128.26 o 16 5 1 186.42 403.26 56.78 o 17 5 1 669.28 963.67 78.81 o 18 5 1 38.16 -40.45 165.66 o 19 5 1 514.82 620.91 143.23 o 0 6 1 16070.95 17657.95 237.30 o 1 6 1 144.56 437.11 27.69 o 2 6 1 699.77 511.81 22.55 o 3 6 1 347.66 217.84 14.00 o 4 6 1 482.47 626.60 18.03 o 5 6 1 4028.38 3365.92 64.12 o 6 6 1 636.30 785.21 41.35 o 7 6 1 12979.72 13931.19 140.70 o 8 6 1 661.73 598.40 32.44 o 9 6 1 4639.56 4583.52 76.83 o 10 6 1 1.53 -2.69 30.16 o 11 6 1 106.03 155.53 45.60 o 12 6 1 183.17 353.50 101.52 o 13 6 1 1352.83 1375.65 99.06 o 14 6 1 1.42 -132.26 132.26 o 15 6 1 476.67 609.31 151.12 o 16 6 1 554.10 322.77 117.52 o 17 6 1 776.20 1059.63 142.01 o 18 6 1 5.78 -218.20 218.20 o 19 6 1 133.70 52.29 95.02 o 1 7 1 4277.72 4846.89 55.78 o 2 7 1 33.52 114.93 21.71 o 3 7 1 7450.55 7523.95 80.48 o 4 7 1 193.80 234.55 27.53 o 5 7 1 17619.30 16831.48 165.20 o 6 7 1 178.98 25.59 28.46 o 7 7 1 9539.39 9088.59 136.91 o 8 7 1 836.06 802.28 37.70 o 9 7 1 3111.33 3349.62 70.69 o 10 7 1 41.10 80.55 67.07 o 11 7 1 1289.79 1217.00 57.71 o 12 7 1 9.30 50.35 34.13 o 13 7 1 5551.25 5929.03 199.88 o 14 7 1 299.83 260.66 106.81 o 15 7 1 1121.32 1096.78 338.88 o 16 7 1 4.38 80.15 249.65 o 17 7 1 1442.02 1391.06 116.84 o 18 7 1 2.26 -87.42 120.19 o 19 7 1 361.78 462.82 103.74 o 0 8 1 8426.60 8236.48 124.18 o 1 8 1 65.18 57.01 24.66 o 2 8 1 2454.38 2520.95 45.49 o 3 8 1 831.02 842.21 24.17 o 4 8 1 4631.28 4590.96 56.42 o 5 8 1 3310.49 3941.94 58.93 o 6 8 1 841.94 749.76 46.21 o 7 8 1 1857.06 1607.62 41.00 o 8 8 1 728.54 761.91 53.31 o 9 8 1 10813.06 11050.82 120.68 o 10 8 1 593.16 726.84 63.34 o 11 8 1 3927.71 4240.26 215.33 o 12 8 1 356.58 354.97 72.63 o 13 8 1 130.71 200.82 144.33 o 14 8 1 67.45 90.49 279.88 o 15 8 1 4685.15 4745.81 182.66 o 16 8 1 0.33 106.45 81.71 o 17 8 1 884.12 1214.27 111.00 o 18 8 1 14.72 -25.85 83.75 o 1 9 1 24052.82 23543.21 225.49 o 2 9 1 107.76 225.89 44.09 o 3 9 1 826.05 847.69 32.19 o 4 9 1 125.84 106.13 30.67 o 5 9 1 16.11 64.45 31.28 o 6 9 1 7.47 17.15 45.82 o 7 9 1 25329.01 24743.19 241.04 o 8 9 1 36.36 -32.66 46.97 o 9 9 1 14365.90 14536.95 165.67 o 10 9 1 97.05 122.31 66.28 o 11 9 1 162.75 188.60 144.33 o 12 9 1 2.00 23.33 63.02 o 13 9 1 543.28 399.27 163.22 o 14 9 1 113.89 -117.63 117.63 o 15 9 1 6162.83 6162.61 204.45 o 16 9 1 64.33 -47.86 170.78 o 17 9 1 3326.25 2798.06 145.32 o 18 9 1 14.44 45.01 116.29 o 0 10 1 2741.42 2668.67 61.30 o 1 10 1 44575.96 43828.23 406.80 o 2 10 1 0.38 100.14 34.49 o 3 10 1 4157.53 3326.78 114.12 o 4 10 1 661.34 598.23 63.47 o 5 10 1 644.66 673.44 39.75 o 6 10 1 1029.97 890.00 51.73 o 7 10 1 1689.32 1426.06 71.99 o 8 10 1 10.47 -64.96 64.96 o 9 10 1 2039.80 2151.07 79.93 o 10 10 1 58.96 29.82 55.13 o 11 10 1 10251.95 10345.37 209.09 o 12 10 1 3.87 386.35 72.80 o 13 10 1 350.69 326.95 103.00 o 14 10 1 6.14 17.11 148.11 o 15 10 1 981.21 708.53 242.70 o 16 10 1 54.23 -53.55 77.49 o 17 10 1 199.03 360.92 256.84 o 1 11 1 18575.69 18875.16 265.71 o 2 11 1 366.13 437.20 50.31 o 3 11 1 529.96 483.86 64.95 o 4 11 1 512.78 421.50 48.13 o 5 11 1 2680.18 2278.53 53.10 o 6 11 1 351.04 331.85 46.51 o 7 11 1 2232.79 2009.38 77.41 o 8 11 1 32.10 -36.95 37.96 o 9 11 1 9795.54 10373.53 219.46 o 10 11 1 200.30 419.49 115.72 o 11 11 1 913.69 1152.21 84.23 o 12 11 1 18.16 -82.65 82.65 o 13 11 1 62.22 124.61 145.79 o 14 11 1 73.62 -87.28 87.28 o 15 11 1 18.11 0.67 71.31 o 16 11 1 17.12 116.72 84.12 o 17 11 1 74.80 -278.93 306.33 o 0 12 1 378.53 406.63 40.61 o 1 12 1 4907.23 4515.80 92.59 o 2 12 1 95.31 204.76 33.03 o 3 12 1 257.69 315.87 45.18 o 4 12 1 64.00 35.03 40.39 o 5 12 1 1042.96 806.06 52.19 o 6 12 1 359.98 440.28 70.23 o 7 12 1 40.62 52.16 29.17 o 8 12 1 105.09 101.95 31.96 o 9 12 1 2981.48 3007.05 66.82 o 10 12 1 4.96 69.04 53.81 o 11 12 1 488.40 422.54 141.59 o 12 12 1 57.87 229.44 73.28 o 13 12 1 4871.87 5554.70 188.74 o 14 12 1 87.54 -137.10 158.47 o 15 12 1 193.29 458.92 503.44 o 16 12 1 7.50 -109.34 109.34 o 1 13 1 1668.71 1318.33 80.90 o 2 13 1 63.05 97.26 79.75 o 3 13 1 6157.94 6140.95 97.91 o 4 13 1 103.96 163.18 68.70 o 5 13 1 35.25 164.94 59.79 o 6 13 1 380.49 373.51 54.42 o 7 13 1 4201.53 3619.33 73.65 o 8 13 1 473.50 493.49 63.72 o 9 13 1 47.14 45.65 88.91 o 10 13 1 25.20 -79.10 79.10 o 11 13 1 2113.70 1925.65 78.29 o 12 13 1 93.18 -97.50 105.81 o 13 13 1 1659.42 1426.98 178.46 o 14 13 1 391.31 800.05 679.58 o 15 13 1 23.82 -80.91 193.45 o 16 13 1 6.94 77.42 526.60 o 0 14 1 208.57 -27.20 108.37 o 1 14 1 570.36 573.90 51.89 o 2 14 1 142.62 50.57 67.11 o 3 14 1 745.70 579.90 57.84 o 4 14 1 8.65 -38.74 87.14 o 5 14 1 466.72 455.57 46.05 o 6 14 1 57.24 14.17 78.19 o 7 14 1 1161.52 1304.34 49.90 o 8 14 1 415.67 269.95 44.28 o 9 14 1 37.87 303.45 95.79 o 10 14 1 11.72 -93.29 93.29 o 11 14 1 144.22 -0.07 50.17 o 12 14 1 245.41 450.89 89.09 o 13 14 1 16.91 -11.98 79.75 o 14 14 1 5.08 46.69 87.91 o 15 14 1 2.49 -118.01 472.48 o 1 15 1 882.89 583.60 50.57 o 2 15 1 120.62 91.63 102.81 o 3 15 1 7745.30 7523.14 149.64 o 4 15 1 85.25 136.58 90.85 o 5 15 1 9237.90 8922.94 182.87 o 6 15 1 19.58 -0.91 57.39 o 7 15 1 4221.32 4092.94 84.82 o 8 15 1 61.76 139.48 40.30 o 9 15 1 661.76 710.95 100.03 o 10 15 1 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