#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/67/2016709.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016709_Fobs loop_ _publ_author_name 'Begum, Noor Shahina' 'Vasundhara, D. E.' 'Girija, C. R.' 'Nagendrappa, Gopalpur' _publ_section_title ; 5,7-syn-Bis(trimethylsilyl)-5-norbornene-2,3-endo-dicarboxylic acid: a rare co-existence of dimeric and catemeric synthons ; _journal_coeditor_code FA3150 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o423 _journal_page_last o425 _journal_volume 64 _journal_year 2008 _chemical_formula_sum 'C15 H26 O4 Si2' _chemical_formula_weight 326.54 _space_group_IT_number 14 _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 97.667(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.9370 _cell_length_b 6.8184 _cell_length_c 16.5770 _cell_measurement_reflns_used 21556 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 25.0 _cell_measurement_theta_min 1.21 _cell_volume 1897.3(4) _computing_cell_refinement 'SAINTPLUS (Bruker, 1998)' _computing_data_collection 'SMART (Bruker, 1998)' _computing_data_reduction SAINTPLUS _computing_molecular_graphics 'ORTEP-3 for Windows (Farrugia, 1997)' _computing_publication_material SHELXL-97 _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_measured_fraction_theta_full 1 _diffrn_measured_fraction_theta_max 1 _diffrn_measurement_device_type 'Bruker SMART CCD area detector' _diffrn_measurement_method '\f and \w' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0341 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 17324 _diffrn_reflns_theta_full 25 _diffrn_reflns_theta_max 25 _diffrn_reflns_theta_min 1.21 _exptl_absorpt_coefficient_mu 0.198 _exptl_absorpt_correction_type none _exptl_crystal_colour white _exptl_crystal_density_diffrn 1.143 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description rectangular _exptl_crystal_F_000 704.00 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.15 _refine_diff_density_max 1.162 _refine_diff_density_min -0.333 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 228 _refine_ls_number_reflns 3338 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.116 _refine_ls_R_factor_gt 0.0677 _refine_ls_shift/su_max 0.001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.1196P)^2^+0.2522P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_ref 0.1824 _reflns_d_resolution_high 0.8409 _reflns_number_gt 2641 _reflns_number_total 3338 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file fa3150IIsup2.hkl _[local]_cod_data_source_block II _[local]_cod_cif_authors_sg_H-M 'P 1 2~1~/c 1' #BEGIN Tags that were not found in dictionaries: _shelx_title ' gnvh2_ in P 21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 169.31 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_group _atom_site_disorder_assembly C1 C 0.72385(15) 0.0546(4) 0.80717(16) 0.0412(6) Uani 1 d . . . C2 C 0.63487(14) -0.0112(4) 0.79371(15) 0.0389(6) Uani 1 d . . . C3 C 0.62864(14) -0.1429(4) 0.86913(16) 0.0383(6) Uani 1 d . . . C4 C 0.71722(14) -0.1380(4) 0.91435(16) 0.0379(6) Uani 1 d . . . C5 C 0.73298(13) 0.0689(4) 0.94826(15) 0.0370(6) Uani 1 d . . . C6 C 0.73620(14) 0.1802(4) 0.88270(16) 0.0387(6) Uani 1 d . . . C7 C 0.76375(15) -0.1372(4) 0.84053(17) 0.0429(6) Uani 1 d . . . C8 C 0.9253(2) 0.0922(6) 0.8759(3) 0.0956(14) Uani 1 d . . . H8A H 0.9811 0.0792 0.8717 0.143 Uiso 1 calc R . . H8B H 0.9188 0.1396 0.9292 0.143 Uiso 1 calc R . . H8C H 0.9016 0.1832 0.8356 0.143 Uiso 1 calc R . . C9 C 0.9061(2) -0.3098(8) 0.9487(4) 0.1113(18) Uani 1 d . . . H9A H 0.9628 -0.328 0.9557 0.167 Uiso 1 calc R . . H9B H 0.8802 -0.4348 0.94 0.167 Uiso 1 calc R . . H9C H 0.8907 -0.2498 0.9966 0.167 Uiso 1 calc R . . C10 C 0.9091(3) -0.2585(11) 0.7670(4) 0.147(3) Uani 1 d . . . H10A H 0.8881 -0.1832 0.7201 0.221 Uiso 1 calc R . . H10B H 0.8901 -0.391 0.7608 0.221 Uiso 1 calc R . . H10C H 0.9663 -0.2581 0.7723 0.221 Uiso 1 calc R . . C11 C 0.6803(3) 0.3816(5) 1.0615(2) 0.0896(14) Uani 1 d . . . H11A H 0.6244 0.352 1.0537 0.134 Uiso 1 calc R . . H11B H 0.6922 0.4698 1.0196 0.134 Uiso 1 calc R . . H11C H 0.6944 0.442 1.1137 0.134 Uiso 1 calc R . . C12 C 0.7000(3) -0.0400(6) 1.1200(2) 0.0772(11) Uani 1 d . . . H12A H 0.7252 -0.1628 1.1111 0.116 Uiso 1 calc R . . H12B H 0.6434 -0.0526 1.1055 0.116 Uiso 1 calc R . . H12C H 0.7115 -0.0042 1.1764 0.116 Uiso 1 calc R . . C13 C 0.8441(3) 0.1998(8) 1.0969(3) 0.0976(14) Uani 1 d . . . H13A H 0.8474 0.2485 1.1516 0.146 Uiso 1 calc R . . H13B H 0.8656 0.2955 1.0634 0.146 Uiso 1 calc R . . H13C H 0.8739 0.0802 1.0967 0.146 Uiso 1 calc R . . C14 C 0.57027(14) -0.0795(4) 0.92443(16) 0.0409(6) Uani 1 d . . . C15 C 0.57271(15) 0.1469(4) 0.77608(16) 0.0416(6) Uani 1 d . . . O1 O 0.50192(11) 0.1119(3) 0.75801(15) 0.0628(6) Uani 1 d . . . O2 O 0.60012(12) 0.3253(3) 0.77698(14) 0.0547(6) Uani 1 d . . . O3 O 0.55174(13) 0.0884(3) 0.93425(14) 0.0594(6) Uani 1 d . . . O4 O 0.54348(14) -0.2273(3) 0.96336(16) 0.0671(7) Uani 1 d . . . Si2 Si 0.73810(5) 0.15205(11) 1.05643(4) 0.0469(3) Uani 1 d . . . Si1 Si 0.87633(5) -0.14913(13) 0.85926(6) 0.0574(3) Uani 1 d . . . H1 H 0.7401(15) 0.320(4) 0.8796(15) 0.029(6) Uiso 1 d . . . H2 H 0.6186(15) -0.276(4) 0.8527(16) 0.037(7) Uiso 1 d . . . H3 H 0.7257(15) -0.235(4) 0.9500(16) 0.035(7) Uiso 1 d . . . H4 H 0.555(2) 0.409(5) 0.762(2) 0.077(11) Uiso 1 d . . . H5 H 0.7468(16) -0.263(4) 0.8064(17) 0.047(7) Uiso 1 d . . . H6 H 0.6279(16) -0.092(4) 0.7481(17) 0.040(7) Uiso 1 d . . . H7 H 0.7404(16) 0.108(4) 0.7624(18) 0.040(7) Uiso 1 d . . . H13 H 0.518(2) -0.177(6) 1.002(3) 0.084(12) Uiso 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0324(13) 0.0563(16) 0.0363(14) 0.0027(12) 0.0098(11) 0.0005(11) C2 0.0331(13) 0.0479(14) 0.0353(13) -0.0033(11) 0.0030(10) 0.0009(11) C3 0.0304(13) 0.0407(14) 0.0443(14) -0.0018(11) 0.0063(11) 0.0000(10) C4 0.0315(13) 0.0445(14) 0.0375(13) 0.0039(11) 0.0042(10) 0.0031(10) C5 0.0284(12) 0.0461(14) 0.0365(13) -0.0011(11) 0.0043(10) 0.0023(10) C6 0.0298(12) 0.0459(15) 0.0410(14) 0.0017(11) 0.0073(10) -0.0026(10) C7 0.0314(13) 0.0552(16) 0.0432(14) -0.0061(12) 0.0093(11) 0.0047(11) C8 0.0441(19) 0.097(3) 0.149(4) -0.009(3) 0.027(2) -0.011(2) C9 0.060(2) 0.121(4) 0.145(5) 0.042(3) -0.015(3) 0.016(2) C10 0.064(3) 0.238(7) 0.147(5) -0.098(5) 0.041(3) 0.016(4) C11 0.142(4) 0.067(2) 0.058(2) -0.0113(17) 0.004(2) 0.027(2) C12 0.112(3) 0.076(2) 0.0462(18) 0.0049(16) 0.0218(19) -0.008(2) C13 0.073(3) 0.148(4) 0.067(2) -0.022(3) -0.007(2) -0.020(3) C14 0.0279(12) 0.0488(15) 0.0463(14) 0.0037(12) 0.0066(10) -0.0017(11) C15 0.0347(14) 0.0493(15) 0.0393(14) -0.0009(11) -0.0004(11) 0.0004(11) O1 0.0358(11) 0.0525(12) 0.0940(17) 0.0020(11) -0.0140(11) -0.0016(9) O2 0.0363(10) 0.0500(12) 0.0761(15) 0.0106(10) 0.0009(10) -0.0028(9) O3 0.0598(13) 0.0510(12) 0.0756(14) 0.0070(10) 0.0397(11) 0.0055(10) O4 0.0713(15) 0.0539(12) 0.0864(17) 0.0119(12) 0.0489(13) 0.0045(11) Si2 0.0529(5) 0.0525(5) 0.0346(4) -0.0027(3) 0.0037(3) -0.0002(3) Si1 0.0308(4) 0.0722(6) 0.0699(6) -0.0104(4) 0.0092(4) 0.0082(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 C1 C7 100.3(2) . . ? C6 C1 C2 107.9(2) . . ? C7 C1 C2 100.1(2) . . ? C6 C1 H7 115.5(17) . . ? C7 C1 H7 117.8(17) . . ? C2 C1 H7 113.4(17) . . ? C15 C2 C3 116.6(2) . . ? C15 C2 C1 117.3(2) . . ? C3 C2 C1 102.67(19) . . ? C15 C2 H6 104.8(16) . . ? C3 C2 H6 107.2(17) . . ? C1 C2 H6 107.6(17) . . ? C14 C3 C2 116.5(2) . . ? C14 C3 C4 111.4(2) . . ? C2 C3 C4 101.92(19) . . ? C14 C3 H2 110.0(16) . . ? C2 C3 H2 110.3(16) . . ? C4 C3 H2 106.0(15) . . ? C5 C4 C7 101.9(2) . . ? C5 C4 C3 107.5(2) . . ? C7 C4 C3 100.2(2) . . ? C5 C4 H3 116.2(17) . . ? C7 C4 H3 118.4(17) . . ? C3 C4 H3 111.0(16) . . ? C6 C5 C4 104.5(2) . . ? C6 C5 Si2 127.4(2) . . ? C4 C5 Si2 127.97(18) . . ? C5 C6 C1 109.7(2) . . ? C5 C6 H1 128.5(15) . . ? C1 C6 H1 121.5(15) . . ? C1 C7 C4 92.40(19) . . ? C1 C7 Si1 118.64(19) . . ? C4 C7 Si1 118.70(19) . . ? C1 C7 H5 115.1(15) . . ? C4 C7 H5 107.2(16) . . ? Si1 C7 H5 104.6(15) . . ? Si1 C8 H8A 109.5 . . ? Si1 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? Si1 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? Si1 C9 H9A 109.5 . . ? Si1 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? Si1 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? Si1 C10 H10A 109.5 . . ? Si1 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? Si1 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? Si2 C11 H11A 109.5 . . ? Si2 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? Si2 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? Si2 C12 H12A 109.5 . . ? Si2 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? Si2 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? Si2 C13 H13A 109.5 . . ? Si2 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? Si2 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? O3 C14 O4 123.5(3) . . ? O3 C14 C3 124.2(2) . . ? O4 C14 C3 112.3(2) . . ? O1 C15 O2 121.5(2) . . ? O1 C15 C2 123.1(2) . . ? O2 C15 C2 115.3(2) . . ? C15 O2 H4 106(2) . . ? C14 O4 H13 107(3) . . ? C12 Si2 C11 110.2(2) . . ? C12 Si2 C13 108.2(2) . . ? C11 Si2 C13 109.0(2) . . ? C12 Si2 C5 110.88(14) . . ? C11 Si2 C5 109.99(15) . . ? C13 Si2 C5 108.56(16) . . ? C8 Si1 C10 107.7(3) . . ? C8 Si1 C9 109.7(2) . . ? C10 Si1 C9 110.0(3) . . ? C8 Si1 C7 114.15(16) . . ? C10 Si1 C7 106.78(18) . . ? C9 Si1 C7 108.46(17) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C6 1.508(4) . ? C1 C7 1.541(4) . ? C1 C2 1.560(3) . ? C1 H7 0.90(3) . ? C2 C15 1.508(4) . ? C2 C3 1.554(4) . ? C2 H6 0.93(3) . ? C3 C14 1.499(4) . ? C3 C4 1.586(3) . ? C3 H2 0.95(3) . ? C4 C5 1.529(4) . ? C4 C7 1.541(4) . ? C4 H3 0.89(3) . ? C5 C6 1.333(4) . ? C5 Si2 1.872(3) . ? C6 H1 0.96(3) . ? C7 Si1 1.892(3) . ? C7 H5 1.04(3) . ? C8 Si1 1.847(4) . ? C8 H8A 0.96 . ? C8 H8B 0.96 . ? C8 H8C 0.96 . ? C9 Si1 1.859(5) . ? C9 H9A 0.96 . ? C9 H9B 0.96 . ? C9 H9C 0.96 . ? C10 Si1 1.852(5) . ? C10 H10A 0.96 . ? C10 H10B 0.96 . ? C10 H10C 0.96 . ? C11 Si2 1.854(4) . ? C11 H11A 0.96 . ? C11 H11B 0.96 . ? C11 H11C 0.96 . ? C12 Si2 1.851(3) . ? C12 H12A 0.96 . ? C12 H12B 0.96 . ? C12 H12C 0.96 . ? C13 Si2 1.859(4) . ? C13 H13A 0.96 . ? C13 H13B 0.96 . ? C13 H13C 0.96 . ? C14 O3 1.203(3) . ? C14 O4 1.310(3) . ? C15 O1 1.220(3) . ? C15 O2 1.301(3) . ? O2 H4 0.96(4) . ? O4 H13 0.89(4) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C6 C1 C2 C15 64.1(3) . . . . ? C7 C1 C2 C15 168.5(2) . . . . ? C6 C1 C2 C3 -65.2(3) . . . . ? C7 C1 C2 C3 39.2(2) . . . . ? C15 C2 C3 C14 -9.8(3) . . . . ? C1 C2 C3 C14 119.9(2) . . . . ? C15 C2 C3 C4 -131.2(2) . . . . ? C1 C2 C3 C4 -1.6(2) . . . . ? C14 C3 C4 C5 -55.4(3) . . . . ? C2 C3 C4 C5 69.5(2) . . . . ? C14 C3 C4 C7 -161.5(2) . . . . ? C2 C3 C4 C7 -36.5(2) . . . . ? C7 C4 C5 C6 34.4(2) . . . . ? C3 C4 C5 C6 -70.4(2) . . . . ? C7 C4 C5 Si2 -150.22(19) . . . . ? C3 C4 C5 Si2 105.0(2) . . . . ? C4 C5 C6 C1 -0.4(3) . . . . ? Si2 C5 C6 C1 -175.86(17) . . . . ? C7 C1 C6 C5 -33.5(3) . . . . ? C2 C1 C6 C5 70.8(3) . . . . ? C6 C1 C7 C4 49.7(2) . . . . ? C2 C1 C7 C4 -60.7(2) . . . . ? C6 C1 C7 Si1 -75.1(2) . . . . ? C2 C1 C7 Si1 174.51(18) . . . . ? C5 C4 C7 C1 -51.1(2) . . . . ? C3 C4 C7 C1 59.4(2) . . . . ? C5 C4 C7 Si1 73.6(2) . . . . ? C3 C4 C7 Si1 -175.90(17) . . . . ? C2 C3 C14 O3 -29.4(4) . . . . ? C4 C3 C14 O3 86.9(3) . . . . ? C2 C3 C14 O4 152.8(2) . . . . ? C4 C3 C14 O4 -90.9(3) . . . . ? C3 C2 C15 O1 -63.9(4) . . . . ? C1 C2 C15 O1 173.8(3) . . . . ? C3 C2 C15 O2 119.8(3) . . . . ? C1 C2 C15 O2 -2.5(3) . . . . ? C6 C5 Si2 C12 162.1(2) . . . . ? C4 C5 Si2 C12 -12.3(3) . . . . ? C6 C5 Si2 C11 40.0(3) . . . . ? C4 C5 Si2 C11 -134.4(3) . . . . ? C6 C5 Si2 C13 -79.2(3) . . . . ? C4 C5 Si2 C13 106.4(3) . . . . ? C1 C7 Si1 C8 23.9(3) . . . . ? C4 C7 Si1 C8 -86.8(3) . . . . ? C1 C7 Si1 C10 -95.0(3) . . . . ? C4 C7 Si1 C10 154.3(3) . . . . ? C1 C7 Si1 C9 146.5(3) . . . . ? C4 C7 Si1 C9 35.9(3) . . . . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9604.26 -0.54 0.54 o 2 0 0 3761.11 4953.77 79.60 o 3 0 0 28.37 59.04 3.70 o 4 0 0 64.32 78.61 3.59 o 5 0 0 15918.41 21246.95 337.49 o 6 0 0 16182.81 22985.55 392.21 o 7 0 0 5939.37 6709.19 109.11 o 8 0 0 5250.82 7528.44 122.34 o 9 0 0 592.46 616.52 13.92 o 10 0 0 367.31 409.80 11.03 o 11 0 0 1354.19 1544.06 29.59 o 12 0 0 1.29 3.68 4.28 o 13 0 0 1219.76 1597.97 31.62 o 14 0 0 87.02 83.10 6.51 o 15 0 0 108.58 121.62 7.54 o 16 0 0 434.51 458.20 15.61 o 17 0 0 179.56 189.84 9.59 o 18 0 0 35.76 54.20 6.60 o 19 0 0 0.66 2.88 5.21 o 1 1 0 533.74 645.00 8.00 o 2 1 0 4274.70 5875.82 58.69 o 3 1 0 5569.14 7225.81 72.08 o 4 1 0 356.76 482.38 5.89 o 5 1 0 1362.54 1554.78 16.62 o 6 1 0 281.21 298.26 4.79 o 7 1 0 0.79 2.04 1.62 o 8 1 0 4119.12 4815.38 52.49 o 9 1 0 40.70 45.10 2.49 o 10 1 0 730.44 871.55 13.07 o 11 1 0 1814.04 1991.35 26.02 o 12 1 0 7.00 5.67 3.25 o 13 1 0 722.39 741.22 12.62 o 14 1 0 261.97 272.40 7.25 o 15 1 0 44.37 72.73 4.54 o 16 1 0 435.30 435.92 9.91 o 17 1 0 31.74 45.52 4.47 o 18 1 0 303.49 307.56 8.67 o 19 1 0 26.89 29.70 4.35 o 0 2 0 2125.51 2280.13 66.48 o 1 2 0 983.61 1118.10 13.00 o 2 2 0 259.27 300.52 4.15 o 3 2 0 2287.76 2661.76 27.55 o 4 2 0 372.08 545.40 8.88 o 5 2 0 0.01 4.85 2.13 o 6 2 0 742.32 875.68 10.43 o 7 2 0 85.68 106.18 2.85 o 8 2 0 424.69 400.07 6.07 o 9 2 0 18.67 33.65 2.23 o 10 2 0 5.30 0.93 2.43 o 11 2 0 4.80 10.26 3.10 o 12 2 0 38.04 30.20 3.56 o 13 2 0 13.67 10.78 3.44 o 14 2 0 286.15 283.59 7.44 o 15 2 0 126.23 118.83 5.28 o 16 2 0 10.44 12.07 3.70 o 17 2 0 0.65 5.50 3.42 o 18 2 0 3.89 9.86 4.40 o 19 2 0 8.21 21.39 5.60 o 1 3 0 347.21 455.90 8.97 o 2 3 0 113.42 131.26 3.11 o 3 3 0 40.10 32.33 1.86 o 4 3 0 36.36 43.88 2.01 o 5 3 0 3082.78 3573.23 37.28 o 6 3 0 826.83 918.07 11.29 o 7 3 0 221.72 242.72 4.60 o 8 3 0 147.52 154.01 3.80 o 9 3 0 2.14 13.73 2.10 o 10 3 0 539.65 545.05 8.33 o 11 3 0 140.47 151.44 4.71 o 12 3 0 65.45 60.53 3.97 o 13 3 0 27.92 27.25 3.96 o 14 3 0 2.13 4.91 4.03 o 15 3 0 2.44 2.14 5.71 o 16 3 0 326.11 310.31 10.49 o 17 3 0 23.68 23.30 4.95 o 18 3 0 11.98 7.71 4.60 o 0 4 0 5511.61 6575.49 94.75 o 1 4 0 125.52 145.01 8.81 o 2 4 0 177.45 195.67 4.35 o 3 4 0 102.37 107.71 3.33 o 4 4 0 154.44 164.77 4.09 o 5 4 0 388.73 365.35 6.54 o 6 4 0 676.55 718.11 10.53 o 7 4 0 273.06 267.02 6.10 o 8 4 0 796.51 790.79 11.61 o 9 4 0 6.23 2.37 2.41 o 10 4 0 0.01 3.70 3.05 o 11 4 0 92.27 79.33 5.04 o 12 4 0 31.45 31.88 4.48 o 13 4 0 423.07 426.68 11.65 o 14 4 0 10.10 9.89 4.32 o 15 4 0 6.11 5.17 4.63 o 16 4 0 199.17 187.75 8.72 o 17 4 0 3.07 9.08 4.68 o 1 5 0 16.89 7.03 2.52 o 2 5 0 756.20 725.97 11.88 o 3 5 0 20.26 30.75 3.01 o 4 5 0 77.55 87.31 3.99 o 5 5 0 510.97 516.28 8.80 o 6 5 0 21.06 18.35 2.88 o 7 5 0 10.64 12.72 2.78 o 8 5 0 47.10 44.52 3.50 o 9 5 0 58.11 54.40 3.85 o 10 5 0 24.08 29.01 3.80 o 11 5 0 327.31 327.48 8.93 o 12 5 0 7.02 7.77 4.17 o 13 5 0 215.11 210.45 8.65 o 14 5 0 0.05 8.97 4.50 o 15 5 0 2.98 2.41 5.42 o 0 6 0 276.72 285.21 10.05 o 1 6 0 46.66 55.33 3.90 o 2 6 0 411.64 411.75 9.93 o 3 6 0 77.37 68.10 4.56 o 4 6 0 101.46 100.20 5.13 o 5 6 0 3.80 -3.09 3.09 o 6 6 0 85.89 101.54 5.75 o 7 6 0 15.89 18.03 3.89 o 8 6 0 503.41 531.29 12.19 o 9 6 0 35.80 41.54 4.99 o 10 6 0 1.30 0.26 4.38 o 11 6 0 3.38 -4.14 4.14 o 12 6 0 3.52 0.06 7.14 o 13 6 0 28.99 41.94 6.73 o 1 7 0 35.55 30.10 4.73 o 2 7 0 19.18 14.00 4.40 o 3 7 0 36.04 40.83 7.47 o 4 7 0 5.55 9.25 3.84 o 5 7 0 81.12 83.85 5.49 o 6 7 0 0.00 -3.58 3.59 o 7 7 0 67.27 81.89 5.69 o 8 7 0 53.87 61.59 5.27 o 9 7 0 3.15 5.87 5.69 o 10 7 0 18.76 26.38 6.26 o 0 8 0 9.05 16.33 17.38 o 1 8 0 2.09 1.16 4.19 o 2 8 0 1.75 6.07 4.63 o 3 8 0 0.32 -2.42 4.42 o -19 1 1 219.96 199.44 7.38 o -18 1 1 11.97 13.90 3.96 o -17 1 1 26.99 26.82 4.12 o -16 1 1 22.31 26.97 3.96 o -15 1 1 58.82 53.91 4.20 o -14 1 1 23.51 27.87 3.80 o -13 1 1 1597.99 1376.11 21.83 o -12 1 1 91.35 106.52 4.70 o -11 1 1 554.03 529.93 10.52 o -10 1 1 877.16 817.48 12.44 o -9 1 1 141.58 144.39 3.74 o -8 1 1 73.64 53.86 2.48 o -7 1 1 808.78 770.82 9.32 o -6 1 1 4929.47 4872.72 49.53 o -5 1 1 90.69 68.87 3.40 o -4 1 1 1938.12 1936.72 20.23 o -3 1 1 426.30 372.71 5.31 o -2 1 1 2921.90 2652.56 29.65 o -1 1 1 1373.34 1255.35 23.09 o 0 1 1 27164.89 23857.06 252.88 o 1 1 1 11187.50 9975.98 142.69 o 2 1 1 284.58 277.82 3.54 o 3 1 1 975.33 761.57 8.49 o 4 1 1 1268.62 1255.50 13.52 o 5 1 1 1624.20 1732.99 18.42 o 6 1 1 1570.59 1550.92 16.81 o 7 1 1 3466.34 3509.94 36.28 o 8 1 1 858.53 813.35 10.78 o 9 1 1 840.16 835.10 11.26 o 10 1 1 668.94 440.16 8.13 o 11 1 1 626.63 557.51 12.95 o 12 1 1 541.41 470.12 9.08 o 13 1 1 18.77 13.72 3.43 o 14 1 1 111.82 119.06 5.37 o 15 1 1 60.96 55.11 4.15 o 16 1 1 303.66 271.41 7.14 o 17 1 1 245.41 226.90 7.31 o 18 1 1 6.20 3.97 3.81 o 19 1 1 71.90 74.92 5.39 o -19 2 1 129.08 120.44 8.41 o -18 2 1 299.32 283.37 8.33 o -17 2 1 115.81 107.71 5.49 o -16 2 1 713.27 615.89 12.10 o -15 2 1 116.52 124.46 5.47 o -14 2 1 351.49 300.50 7.65 o -13 2 1 538.97 438.09 9.08 o -12 2 1 48.83 68.83 4.43 o -11 2 1 1803.10 1415.68 25.56 o -10 2 1 1958.90 1826.17 22.13 o -9 2 1 524.17 487.17 7.27 o -8 2 1 2015.99 2010.16 22.04 o -7 2 1 21.99 15.11 2.13 o -6 2 1 600.57 668.75 10.56 o -5 2 1 10152.47 10857.33 108.55 o -4 2 1 2952.07 2872.80 29.79 o -3 2 1 535.66 410.61 5.41 o -2 2 1 78.99 63.81 1.77 o -1 2 1 788.02 654.06 7.64 o 0 2 1 64.86 51.77 1.49 o 1 2 1 333.45 272.85 5.43 o 2 2 1 4381.55 4326.52 46.77 o 3 2 1 1002.42 850.04 9.73 o 4 2 1 3894.35 4022.08 41.12 o 5 2 1 507.39 490.12 6.46 o 6 2 1 191.63 138.24 3.63 o 7 2 1 1084.12 1016.28 12.05 o 8 2 1 633.32 520.98 6.90 o 9 2 1 14.64 12.11 2.23 o 10 2 1 714.81 669.78 9.92 o 11 2 1 479.43 381.39 7.88 o 12 2 1 1785.42 1632.48 20.93 o 13 2 1 208.89 165.90 5.60 o 14 2 1 91.91 93.75 6.23 o 15 2 1 54.35 47.55 4.08 o 16 2 1 264.23 213.20 7.68 o 17 2 1 397.66 351.82 10.13 o 18 2 1 153.98 139.62 7.93 o 19 2 1 15.89 11.45 5.15 o -18 3 1 26.08 28.72 5.23 o -17 3 1 83.79 63.23 5.36 o -16 3 1 11.67 11.12 4.82 o -15 3 1 19.17 15.63 3.98 o -14 3 1 26.51 26.50 4.05 o -13 3 1 758.74 645.14 12.73 o -12 3 1 15.18 17.56 3.35 o -11 3 1 167.24 167.50 5.31 o -10 3 1 4.85 2.36 2.47 o -9 3 1 0.26 1.20 2.07 o -8 3 1 479.93 427.41 6.68 o -7 3 1 813.90 780.67 10.13 o -6 3 1 2929.16 2991.20 31.74 o -5 3 1 280.01 213.89 4.19 o -4 3 1 695.52 630.90 8.18 o -3 3 1 256.60 284.42 5.00 o -2 3 1 57.09 49.75 3.71 o -1 3 1 183.52 159.23 4.88 o 0 3 1 3492.22 3367.40 42.97 o 1 3 1 187.91 193.51 8.55 o 2 3 1 2867.71 2798.61 31.37 o 3 3 1 462.79 357.95 5.79 o 4 3 1 459.47 428.59 6.68 o 5 3 1 216.88 198.43 3.84 o 6 3 1 11.28 12.74 1.81 o 7 3 1 593.85 490.16 7.12 o 8 3 1 1980.19 1862.81 20.98 o 9 3 1 167.06 163.87 6.13 o 10 3 1 2011.38 1750.34 21.62 o 11 3 1 14.74 15.93 3.51 o 12 3 1 49.41 53.38 4.86 o 13 3 1 0.37 0.57 3.67 o 14 3 1 1.22 4.93 4.03 o 15 3 1 295.55 255.74 9.29 o 16 3 1 298.18 263.99 9.83 o 17 3 1 136.33 146.15 7.92 o 18 3 1 16.54 17.52 4.80 o -17 4 1 23.53 15.64 5.11 o -16 4 1 7.48 9.03 4.82 o -15 4 1 173.72 144.65 7.51 o -14 4 1 1.28 4.76 4.49 o -13 4 1 128.84 126.85 6.59 o -12 4 1 4.12 0.06 3.74 o -11 4 1 218.65 215.68 6.14 o -10 4 1 8.64 9.82 3.23 o -9 4 1 372.88 326.34 6.68 o -8 4 1 536.07 471.01 8.15 o -7 4 1 4.54 6.51 2.41 o -6 4 1 2.23 0.49 2.04 o -5 4 1 92.34 79.49 3.12 o -4 4 1 140.40 133.68 3.76 o -3 4 1 445.46 376.08 5.92 o -2 4 1 74.78 51.04 2.37 o -1 4 1 0.09 1.35 3.36 o 0 4 1 1620.52 1525.25 17.97 o 1 4 1 95.39 85.29 4.63 o 2 4 1 68.29 59.17 2.70 o 3 4 1 297.45 263.94 5.26 o 4 4 1 98.44 95.52 3.27 o 5 4 1 186.54 144.12 3.97 o 6 4 1 105.40 95.93 3.50 o 7 4 1 296.79 288.09 5.95 o 8 4 1 38.00 41.71 3.32 o 9 4 1 35.31 38.61 3.60 o 10 4 1 37.49 36.32 3.83 o 11 4 1 33.00 28.97 4.31 o 12 4 1 119.78 105.19 7.03 o 13 4 1 102.09 92.59 6.00 o 14 4 1 5.50 12.52 4.45 o 15 4 1 46.77 53.28 5.53 o 16 4 1 4.99 13.35 4.55 o 17 4 1 1.10 0.07 4.30 o -15 5 1 7.47 10.07 6.95 o -14 5 1 12.22 10.72 5.97 o -13 5 1 2.95 2.36 4.12 o -12 5 1 4.02 7.39 4.22 o -11 5 1 14.19 17.23 3.72 o -10 5 1 14.06 18.09 3.47 o -9 5 1 21.48 20.28 3.62 o -8 5 1 0.21 -2.61 2.64 o -7 5 1 4.91 0.25 2.40 o -6 5 1 242.92 243.99 5.77 o -5 5 1 102.89 96.95 4.21 o -4 5 1 23.42 18.46 2.77 o -3 5 1 18.82 19.10 2.79 o -2 5 1 21.11 10.13 3.23 o -1 5 1 75.79 82.08 4.27 o 0 5 1 47.03 36.65 3.12 o 1 5 1 105.87 89.53 3.97 o 2 5 1 132.10 106.89 4.39 o 3 5 1 101.11 89.47 3.95 o 4 5 1 3.74 3.68 2.51 o 5 5 1 29.98 18.91 3.42 o 6 5 1 77.83 81.44 4.06 o 7 5 1 15.14 18.14 3.07 o 8 5 1 41.70 51.33 3.75 o 9 5 1 102.70 90.13 4.51 o 10 5 1 0.16 1.11 3.17 o 11 5 1 4.61 6.64 3.41 o 12 5 1 27.18 25.12 6.70 o 13 5 1 32.74 33.78 5.08 o 14 5 1 7.58 22.06 5.30 o 15 5 1 10.55 15.75 4.78 o -13 6 1 0.36 12.09 5.91 o -12 6 1 51.27 57.32 8.27 o -11 6 1 0.05 8.53 4.54 o -10 6 1 11.22 7.72 4.26 o -9 6 1 0.01 -2.31 3.66 o -8 6 1 37.28 35.71 4.27 o -7 6 1 135.49 158.11 6.47 o -6 6 1 76.43 74.64 4.82 o -5 6 1 8.27 15.94 4.59 o -4 6 1 28.78 30.50 3.95 o -3 6 1 41.18 34.45 3.56 o -2 6 1 447.02 443.06 9.29 o -1 6 1 21.79 20.54 3.30 o 0 6 1 47.41 46.42 4.25 o 1 6 1 214.09 213.35 9.09 o 2 6 1 161.65 152.24 6.12 o 3 6 1 24.94 23.42 3.56 o 4 6 1 66.40 58.18 4.46 o 5 6 1 187.14 178.56 6.61 o 6 6 1 55.73 58.72 5.33 o 7 6 1 4.74 5.86 4.45 o 8 6 1 64.28 73.24 5.20 o 9 6 1 0.58 -3.17 5.00 o 10 6 1 6.77 -0.68 4.26 o 11 6 1 105.19 95.85 6.63 o 12 6 1 46.62 47.44 6.78 o 13 6 1 10.06 11.89 6.12 o -10 7 1 29.05 52.75 8.19 o -9 7 1 1.77 3.68 4.61 o -8 7 1 82.78 74.55 5.97 o -7 7 1 19.61 13.90 4.08 o -6 7 1 0.41 2.43 3.70 o -5 7 1 140.91 144.05 7.61 o -4 7 1 0.41 -0.33 4.23 o -3 7 1 101.79 107.92 6.73 o -2 7 1 117.12 121.11 6.99 o -1 7 1 109.48 100.96 6.50 o 0 7 1 32.97 35.90 4.84 o 1 7 1 3.39 3.52 4.06 o 2 7 1 138.01 152.82 6.51 o 3 7 1 10.17 8.55 3.61 o 4 7 1 0.01 -2.74 4.16 o 5 7 1 26.02 19.78 4.10 o 6 7 1 31.66 28.12 4.39 o 7 7 1 6.60 11.74 4.15 o 8 7 1 226.68 254.52 9.44 o 9 7 1 47.55 50.41 5.91 o -3 8 1 31.32 27.45 5.29 o -2 8 1 8.96 14.48 4.92 o -1 8 1 0.83 3.51 4.43 o 0 8 1 52.20 67.63 6.98 o 1 8 1 1.84 3.96 4.32 o 2 8 1 0.03 -0.85 4.29 o -20 0 2 1.72 26.64 10.98 o -19 0 2 682.54 684.58 24.14 o -18 0 2 152.62 158.26 9.26 o -17 0 2 2.83 7.25 5.23 o -16 0 2 21.11 36.51 5.91 o -15 0 2 64.25 78.91 6.79 o -14 0 2 505.42 521.09 19.73 o -13 0 2 744.97 765.57 18.23 o -12 0 2 203.26 306.93 19.17 o -11 0 2 3198.87 4026.72 68.84 o -10 0 2 2060.48 2718.49 67.85 o -9 0 2 1742.62 2068.62 36.86 o -8 0 2 3447.65 4533.92 75.15 o -7 0 2 99.24 112.33 4.27 o -6 0 2 2281.90 3112.89 57.19 o -5 0 2 977.09 1862.56 27.76 o -4 0 2 1990.82 3432.60 62.43 o -3 0 2 13713.70 20648.39 289.73 o -2 0 2 2890.06 4434.29 77.43 o -1 0 2 13203.39 17742.29 355.07 o 0 0 2 250.98 283.99 11.75 o 1 0 2 8342.51 10774.15 236.53 o 2 0 2 3203.35 4210.27 60.54 o 3 0 2 10366.29 13522.96 189.88 o 4 0 2 5789.94 6678.88 94.52 o 5 0 2 9357.73 12053.21 169.75 o 6 0 2 106.02 85.40 3.27 o 7 0 2 12055.59 16056.62 256.54 o 8 0 2 199.13 259.99 7.72 o 9 0 2 0.25 0.73 3.09 o 10 0 2 2487.50 2640.11 46.47 o 11 0 2 594.89 594.69 16.30 o 12 0 2 554.25 686.10 16.40 o 13 0 2 846.69 790.58 18.67 o 14 0 2 37.28 31.11 5.28 o 15 0 2 474.79 451.77 13.79 o 16 0 2 1.81 6.61 5.02 o 17 0 2 355.66 367.75 13.11 o 18 0 2 132.94 130.74 11.12 o 19 0 2 28.09 36.76 6.68 o -19 1 2 11.22 18.27 4.08 o -18 1 2 31.53 41.76 4.41 o -17 1 2 245.69 233.61 7.41 o -16 1 2 319.59 323.98 8.39 o -15 1 2 115.57 119.18 5.42 o -14 1 2 32.42 39.16 3.99 o -13 1 2 9.46 15.91 3.45 o -12 1 2 108.38 106.57 4.63 o -11 1 2 403.01 382.18 7.77 o -10 1 2 264.06 269.27 5.40 o -9 1 2 1861.69 2233.45 25.89 o -8 1 2 1297.04 1501.92 16.79 o -7 1 2 5.68 13.41 1.49 o -6 1 2 95.57 89.23 2.81 o -5 1 2 1347.22 1736.52 19.20 o -4 1 2 21.06 16.33 1.46 o -3 1 2 9021.50 12511.09 133.76 o -2 1 2 290.35 411.86 5.78 o -1 1 2 3102.59 4444.24 47.28 o 0 1 2 10769.07 14032.75 148.06 o 1 1 2 4.22 7.43 1.06 o 2 1 2 6527.70 8185.22 90.45 o 3 1 2 1197.50 1405.84 14.91 o 4 1 2 7634.54 9281.08 92.57 o 5 1 2 76.72 90.43 2.24 o 6 1 2 27.51 27.36 1.64 o 7 1 2 1115.01 1237.62 14.02 o 8 1 2 1839.77 2155.34 23.24 o 9 1 2 128.49 140.53 3.71 o 10 1 2 24.55 16.07 2.78 o 11 1 2 77.08 65.59 3.74 o 12 1 2 668.82 704.21 11.85 o 13 1 2 58.32 69.99 4.23 o 14 1 2 2.19 2.42 3.06 o 15 1 2 48.85 60.60 4.31 o 16 1 2 21.02 28.15 3.93 o 17 1 2 5.46 -1.08 3.56 o 18 1 2 12.44 17.74 4.59 o 19 1 2 4.76 12.57 4.69 o -19 2 2 0.77 6.79 3.76 o -18 2 2 31.83 42.00 4.57 o -17 2 2 1.12 3.11 3.67 o -16 2 2 0.26 1.58 5.20 o -15 2 2 49.65 52.97 4.52 o -14 2 2 0.09 4.35 3.28 o -13 2 2 0.98 -1.97 3.63 o -12 2 2 278.18 272.25 6.75 o -11 2 2 1249.60 1330.71 18.68 o -10 2 2 24.18 25.64 2.74 o -9 2 2 62.19 64.77 2.63 o -8 2 2 20.74 18.96 2.04 o -7 2 2 236.06 333.08 5.26 o -6 2 2 18.28 28.68 1.88 o -5 2 2 461.18 560.31 7.24 o -4 2 2 1322.07 1400.56 15.34 o -3 2 2 11.47 16.23 1.40 o -2 2 2 121.04 108.47 2.29 o -1 2 2 0.40 2.68 1.07 o 0 2 2 371.43 402.37 8.17 o 1 2 2 517.72 624.12 7.92 o 2 2 2 15.62 19.48 1.41 o 3 2 2 40.25 27.77 1.40 o 4 2 2 6.07 9.97 1.36 o 5 2 2 241.38 297.77 6.72 o 6 2 2 693.92 883.19 10.55 o 7 2 2 0.52 2.22 1.65 o 8 2 2 312.52 293.87 4.99 o 9 2 2 6.76 6.55 1.95 o 10 2 2 469.73 445.69 11.95 o 11 2 2 0.33 -3.90 5.53 o 12 2 2 0.94 0.88 2.92 o 13 2 2 4.78 4.83 3.02 o 14 2 2 23.46 20.66 3.49 o 15 2 2 9.03 7.87 3.68 o 16 2 2 0.03 -1.15 3.86 o 17 2 2 5.53 11.86 4.36 o 18 2 2 39.64 32.76 5.62 o -18 3 2 7.58 19.56 5.32 o -17 3 2 8.93 13.96 8.28 o -16 3 2 230.08 205.90 7.58 o -15 3 2 299.06 304.39 8.90 o -14 3 2 0.00 0.96 3.18 o -13 3 2 132.68 147.38 5.48 o -12 3 2 3.26 4.64 3.12 o -11 3 2 159.02 147.58 4.69 o -10 3 2 1.04 1.87 2.48 o -9 3 2 552.69 612.33 8.78 o -8 3 2 70.08 71.17 2.84 o -7 3 2 31.88 27.16 2.15 o -6 3 2 153.50 143.58 3.43 o -5 3 2 478.69 588.84 7.93 o -4 3 2 486.17 599.37 7.87 o -3 3 2 178.96 152.74 3.23 o -2 3 2 1138.65 1268.29 14.27 o -1 3 2 463.18 547.46 7.04 o 0 3 2 154.65 167.45 3.68 o 1 3 2 179.23 205.21 3.99 o 2 3 2 37.64 43.25 2.10 o 3 3 2 15.83 25.79 1.87 o 4 3 2 74.58 75.28 2.60 o 5 3 2 8.94 4.61 1.50 o 6 3 2 71.87 63.18 2.55 o 7 3 2 1.67 3.65 1.76 o 8 3 2 806.12 812.47 11.39 o 9 3 2 23.93 35.20 2.49 o 10 3 2 69.93 64.97 4.45 o 11 3 2 140.39 125.88 6.10 o 12 3 2 12.74 17.29 4.17 o 13 3 2 112.37 120.92 6.46 o 14 3 2 8.54 12.20 5.78 o 15 3 2 19.32 34.15 5.16 o 16 3 2 0.52 7.63 4.68 o 17 3 2 54.23 56.86 7.58 o 18 3 2 8.11 13.35 4.73 o -17 4 2 0.00 5.53 4.72 o -16 4 2 89.64 90.45 6.60 o -15 4 2 0.90 6.02 5.27 o -14 4 2 1.35 -4.00 4.00 o -13 4 2 181.92 178.50 6.63 o -12 4 2 6.67 8.32 3.51 o -11 4 2 777.45 762.73 12.83 o -10 4 2 10.42 9.29 2.97 o -9 4 2 42.59 57.30 4.62 o -8 4 2 0.05 1.40 2.28 o -7 4 2 21.72 25.64 2.59 o -6 4 2 504.12 539.35 8.63 o -5 4 2 67.77 50.30 2.48 o -4 4 2 6.83 4.37 2.78 o -3 4 2 2701.80 2849.17 30.50 o -2 4 2 407.35 486.76 11.29 o -1 4 2 929.31 1017.27 13.25 o 0 4 2 0.06 -1.74 2.10 o 1 4 2 49.31 73.91 2.91 o 2 4 2 2238.71 2245.23 26.28 o 3 4 2 39.53 51.17 2.92 o 4 4 2 46.44 37.54 2.43 o 5 4 2 23.89 14.84 2.17 o 6 4 2 0.10 -0.51 2.25 o 7 4 2 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