#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/67/2016720.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016720_Fobs loop_ _publ_author_name 'Sarangarajan, Thanjavur R.' 'Krishnamoorthy, Belli S.' 'Panchanatheswaran, Krishnaswamy' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Three-dimensional frameworks built from piperazine-2,5-dione and simple metal salts (M = Co, Ni, Cu and Ag) ; _journal_coeditor_code GG3165 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m286 _journal_page_last m291 _journal_volume 64 _journal_year 2008 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6276 _cell_length_b 14.7180 _cell_length_c 5.2468 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.7672 _[local]_cod_data_source_file gg3165IVsup5.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' 242' _shelx_refln_list_code 4 _shelx_F_calc_maximum 233.50 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12107.45 11951.94 432.73 o 4 0 0 21767.69 22649.98 376.66 o 6 0 0 19997.85 20515.49 350.49 o 8 0 0 1075.67 1242.21 56.33 o 10 0 0 1379.94 1452.53 40.67 o 12 0 0 1782.05 1723.16 95.54 o 2 1 0 17358.31 17289.71 350.03 o 4 1 0 22833.72 23873.02 382.25 o 6 1 0 2113.80 2195.07 29.73 o 8 1 0 7667.62 7836.68 118.84 o 10 1 0 1388.09 1451.90 25.69 o 12 1 0 341.58 335.23 23.70 o 2 2 0 1026.17 1037.43 24.78 o 4 2 0 5685.11 5592.31 73.69 o 6 2 0 3961.63 3616.36 63.10 o 8 2 0 254.30 234.92 6.13 o 10 2 0 1662.58 1713.08 31.19 o 12 2 0 3756.66 3800.02 147.99 o 2 3 0 14264.81 13569.57 180.33 o 4 3 0 17555.06 17506.71 278.96 o 6 3 0 1365.67 1427.04 22.11 o 8 3 0 5409.49 5453.77 74.94 o 10 3 0 1108.66 1165.72 25.87 o 12 3 0 65.73 74.00 13.71 o 0 4 0 54523.64 62814.32 1986.05 o 2 4 0 7.13 21.68 8.35 o 4 4 0 6591.53 6671.52 85.93 o 6 4 0 4734.08 4762.97 60.62 o 8 4 0 148.18 149.87 4.93 o 10 4 0 1167.99 1183.23 25.21 o 12 4 0 1866.84 1682.79 81.48 o 2 5 0 9352.50 8612.13 144.99 o 4 5 0 18281.23 18363.86 245.97 o 6 5 0 404.88 425.54 8.52 o 8 5 0 4568.43 4508.28 68.62 o 10 5 0 1467.20 1463.47 33.91 o 2 6 0 4567.21 4444.87 77.74 o 4 6 0 9236.78 9021.75 147.37 o 6 6 0 12137.53 12209.71 168.84 o 8 6 0 1282.21 1326.63 33.21 o 10 6 0 1081.27 1100.88 38.06 o 2 7 0 16220.41 16403.68 270.32 o 4 7 0 11940.62 11750.17 248.64 o 6 7 0 4177.17 4391.44 60.54 o 8 7 0 9016.15 9425.34 159.34 o 10 7 0 821.14 822.65 30.43 o 0 8 0 20924.61 20653.75 643.72 o 2 8 0 17.08 28.39 4.03 o 4 8 0 5110.48 5008.19 71.71 o 6 8 0 4110.99 4121.15 62.49 o 8 8 0 50.60 57.58 4.86 o 10 8 0 1884.25 2008.01 65.59 o 2 9 0 4399.60 4212.02 66.16 o 4 9 0 10913.59 11164.09 153.29 o 6 9 0 0.72 15.11 7.24 o 8 9 0 2234.86 2213.36 44.66 o 10 9 0 1528.34 1580.10 57.77 o 0 10 0 22242.53 23047.87 740.54 o 2 10 0 518.30 544.82 11.86 o 4 10 0 2815.49 2844.00 53.61 o 6 10 0 3644.40 3814.57 67.00 o 8 10 0 268.23 259.04 9.20 o 10 10 0 540.25 537.63 25.42 o 2 11 0 5689.69 5603.30 90.81 o 4 11 0 6385.21 6468.70 97.88 o 6 11 0 830.80 823.20 22.51 o 8 11 0 3451.50 3504.68 69.82 o 10 11 0 513.62 435.59 29.44 o 0 12 0 18144.09 18683.63 520.60 o 2 12 0 804.39 838.25 20.21 o 4 12 0 2717.95 2688.99 46.30 o 6 12 0 5205.96 5508.09 91.22 o 8 12 0 690.95 689.05 34.20 o 2 13 0 4891.78 5102.94 99.85 o 4 13 0 5135.56 5333.74 95.20 o 6 13 0 1260.38 1290.13 28.20 o 8 13 0 4847.62 5229.73 159.80 o 0 14 0 12759.80 12811.82 326.03 o 2 14 0 271.62 244.76 11.16 o 4 14 0 3020.82 3097.77 59.20 o 6 14 0 3331.06 3253.01 74.37 o 8 14 0 10.55 13.97 7.91 o 2 15 0 3442.66 3523.90 108.29 o 4 15 0 5826.25 5920.76 128.23 o 6 15 0 10.66 11.18 7.15 o 0 16 0 4982.93 5123.46 222.73 o 2 16 0 179.33 209.85 15.81 o 4 16 0 514.33 485.32 31.75 o 6 16 0 1626.69 1624.02 59.34 o 2 17 0 1674.95 1703.92 61.57 o 4 17 0 1774.85 1699.61 64.84 o 0 18 0 7506.09 7919.26 402.63 o 2 18 0 300.91 312.95 18.10 o 4 18 0 1604.65 1663.48 105.87 o 1 0 1 10891.29 10966.73 178.59 o 2 0 1 4876.71 4798.74 86.38 o 3 0 1 573.01 593.71 36.12 o 4 0 1 1303.05 1315.02 40.05 o 5 0 1 10906.84 10582.73 161.26 o 6 0 1 310.93 295.78 6.12 o 7 0 1 6556.69 6550.07 92.84 o 8 0 1 66.05 70.99 4.28 o 9 0 1 862.35 930.68 32.14 o 10 0 1 36.84 36.01 4.42 o 11 0 1 5443.73 5606.86 121.29 o 12 0 1 17.05 11.14 7.43 o 0 1 1 1133.60 1057.66 22.39 o 1 1 1 3182.46 3038.46 46.21 o 2 1 1 554.96 510.01 12.90 o 3 1 1 35789.86 35711.18 2232.15 o 4 1 1 47.28 55.04 1.69 o 5 1 1 4080.57 4094.19 36.72 o 6 1 1 372.54 393.35 5.03 o 7 1 1 3882.65 3828.76 35.75 o 8 1 1 305.48 320.76 5.40 o 9 1 1 7844.52 8082.95 77.19 o 10 1 1 85.40 81.81 3.50 o 11 1 1 80.83 90.97 4.92 o 12 1 1 0.36 11.15 5.90 o 1 2 1 24509.66 25299.41 361.55 o 2 2 1 1472.01 1415.48 14.34 o 3 2 1 53.50 54.29 1.55 o 4 2 1 56.18 68.40 2.15 o 5 2 1 8696.05 8338.42 100.99 o 6 2 1 13.29 15.36 1.40 o 7 2 1 7225.90 7463.21 78.28 o 8 2 1 7.56 11.67 1.56 o 9 2 1 198.42 217.18 5.40 o 10 2 1 88.23 73.16 3.20 o 11 2 1 2631.40 2661.87 53.22 o 12 2 1 54.17 46.74 7.11 o 0 3 1 3058.49 2918.39 50.59 o 1 3 1 203.28 222.69 3.89 o 2 3 1 1657.40 1592.70 17.98 o 3 3 1 6845.24 5849.66 72.13 o 4 3 1 6.85 11.21 1.55 o 5 3 1 1069.22 1029.74 10.96 o 6 3 1 64.21 68.47 2.95 o 7 3 1 1725.39 1694.48 17.67 o 8 3 1 72.60 71.30 2.57 o 9 3 1 4944.21 5000.38 50.16 o 10 3 1 428.25 431.77 8.54 o 11 3 1 55.52 48.08 4.44 o 12 3 1 4.40 3.13 6.29 o 1 4 1 11167.24 10590.16 110.20 o 2 4 1 207.48 193.67 3.88 o 3 4 1 27.41 47.64 2.12 o 4 4 1 185.55 199.06 3.18 o 5 4 1 5281.08 4901.38 42.80 o 6 4 1 4.40 5.98 1.45 o 7 4 1 6285.85 6321.41 65.64 o 8 4 1 27.79 24.01 2.07 o 9 4 1 30.61 29.71 2.65 o 10 4 1 3.95 3.29 3.16 o 11 4 1 2612.48 2563.63 56.14 o 12 4 1 33.62 25.44 5.81 o 0 5 1 268.48 269.33 5.01 o 1 5 1 2694.03 2618.32 32.80 o 2 5 1 784.45 794.09 11.29 o 3 5 1 24424.20 24440.15 239.12 o 4 5 1 654.19 677.10 8.38 o 5 5 1 2560.57 2544.29 26.12 o 6 5 1 131.71 137.19 3.06 o 7 5 1 3479.17 3484.25 35.52 o 8 5 1 779.21 779.66 10.85 o 9 5 1 6441.28 6674.05 71.25 o 10 5 1 11.62 8.27 3.21 o 11 5 1 43.26 31.67 5.36 o 1 6 1 12255.01 11919.43 138.75 o 2 6 1 353.37 345.71 5.65 o 3 6 1 810.77 838.06 14.55 o 4 6 1 254.01 234.82 3.97 o 5 6 1 9769.13 9744.79 95.14 o 6 6 1 157.47 151.19 3.40 o 7 6 1 4852.61 4910.17 54.33 o 8 6 1 39.63 36.78 2.41 o 9 6 1 1067.36 1076.36 17.13 o 10 6 1 2.96 5.98 2.98 o 11 6 1 4277.95 4389.01 120.65 o 0 7 1 672.82 680.16 14.55 o 1 7 1 1563.22 1508.86 20.69 o 2 7 1 2.76 5.58 1.86 o 3 7 1 19845.96 19600.09 200.70 o 4 7 1 380.38 416.57 6.32 o 5 7 1 3190.31 3262.32 37.83 o 6 7 1 320.64 325.31 5.80 o 7 7 1 2082.48 2094.54 25.61 o 8 7 1 12.13 14.72 2.28 o 9 7 1 6182.35 6295.47 86.47 o 10 7 1 558.19 541.51 15.62 o 11 7 1 165.29 176.95 11.80 o 1 8 1 12308.45 12384.57 145.75 o 2 8 1 31.30 33.01 1.97 o 3 8 1 10.64 11.60 2.22 o 4 8 1 1.05 1.52 1.69 o 5 8 1 6234.73 6186.55 60.81 o 6 8 1 83.69 86.10 3.24 o 7 8 1 5266.30 5358.41 60.85 o 8 8 1 13.83 13.28 2.64 o 9 8 1 104.52 95.21 4.75 o 10 8 1 28.76 26.67 4.64 o 11 8 1 2230.42 2154.83 112.50 o 0 9 1 693.75 701.18 16.76 o 1 9 1 510.28 488.34 7.91 o 2 9 1 48.38 48.08 2.90 o 3 9 1 6609.62 6369.52 72.34 o 4 9 1 304.39 322.91 6.19 o 5 9 1 304.58 318.39 8.43 o 6 9 1 35.03 33.76 2.06 o 7 9 1 2303.83 2262.76 28.72 o 8 9 1 94.78 90.17 3.60 o 9 9 1 3479.32 3397.66 58.52 o 10 9 1 16.85 17.82 4.59 o 1 10 1 4657.76 4509.00 60.59 o 2 10 1 108.71 113.62 3.95 o 3 10 1 1.86 1.40 2.04 o 4 10 1 256.51 249.90 5.20 o 5 10 1 2824.60 2741.93 32.30 o 6 10 1 29.97 29.89 2.93 o 7 10 1 3375.53 3489.70 44.74 o 8 10 1 84.77 75.85 4.03 o 9 10 1 33.05 19.12 6.23 o 10 10 1 12.07 18.88 5.65 o 0 11 1 325.42 333.91 11.14 o 1 11 1 774.64 800.48 12.52 o 2 11 1 69.64 85.37 3.94 o 3 11 1 9082.44 9202.16 107.40 o 4 11 1 1.67 4.21 1.82 o 5 11 1 1512.33 1548.50 20.61 o 6 11 1 74.80 67.09 3.41 o 7 11 1 1162.29 1180.08 19.10 o 8 11 1 82.65 69.15 5.36 o 9 11 1 3975.30 3908.05 110.85 o 10 11 1 16.60 24.21 10.00 o 1 12 1 6257.67 6292.31 80.59 o 2 12 1 37.79 34.33 2.98 o 3 12 1 341.16 348.47 7.79 o 4 12 1 21.94 14.20 2.09 o 5 12 1 5360.23 5541.04 64.02 o 6 12 1 142.85 130.66 4.83 o 7 12 1 2500.53 2486.70 41.11 o 8 12 1 49.21 47.29 4.29 o 9 12 1 721.85 667.43 35.48 o 0 13 1 4.00 1.60 3.35 o 1 13 1 1388.76 1398.89 22.59 o 2 13 1 5.98 13.95 2.99 o 3 13 1 9456.76 9516.09 117.59 o 4 13 1 39.26 52.77 3.57 o 5 13 1 1090.16 1098.24 18.16 o 6 13 1 70.21 74.61 4.56 o 7 13 1 1553.59 1536.27 45.67 o 8 13 1 2.67 2.61 5.37 o 9 13 1 3391.65 3257.31 115.33 o 1 14 1 4675.21 4865.24 70.04 o 2 14 1 319.87 298.25 8.83 o 3 14 1 4.89 4.89 3.95 o 4 14 1 193.95 166.20 5.88 o 5 14 1 3005.08 3041.87 45.09 o 6 14 1 45.97 37.35 4.51 o 7 14 1 2990.57 3087.96 70.02 o 8 14 1 18.25 8.67 7.32 o 0 15 1 1.64 11.18 6.44 o 1 15 1 315.06 352.79 28.77 o 2 15 1 7.07 15.30 3.98 o 3 15 1 3247.46 3202.19 53.08 o 4 15 1 66.43 75.56 5.54 o 5 15 1 122.24 129.52 9.40 o 6 15 1 1.12 2.66 4.63 o 7 15 1 1257.70 1237.38 39.17 o 1 16 1 2810.41 2807.21 59.76 o 2 16 1 40.16 23.03 4.80 o 3 16 1 44.51 41.90 5.37 o 4 16 1 14.28 16.82 4.63 o 5 16 1 1943.10 1949.67 49.44 o 6 16 1 59.13 48.13 6.96 o 0 17 1 6.01 11.20 8.15 o 1 17 1 410.55 413.64 19.20 o 2 17 1 3.52 0.00 5.06 o 3 17 1 3903.43 3926.03 89.25 o 4 17 1 16.09 23.82 5.90 o 5 17 1 690.53 676.37 28.02 o 1 18 1 1982.19 2041.59 51.69 o 2 18 1 1.60 9.38 5.63 o 3 18 1 61.42 51.23 8.75 o 0 0 2 20040.50 19333.05 417.13 o 1 0 2 951.16 961.76 16.50 o 2 0 2 3659.02 3749.34 73.56 o 3 0 2 3322.67 3308.05 64.60 o 4 0 2 4530.56 4398.55 69.54 o 5 0 2 321.33 343.03 5.75 o 6 0 2 14995.53 15052.56 177.74 o 7 0 2 238.48 247.13 5.34 o 8 0 2 32.04 41.00 6.05 o 9 0 2 196.00 160.34 19.14 o 10 0 2 1816.26 1905.57 39.08 o 11 0 2 196.48 179.50 11.28 o 12 0 2 2436.70 2400.10 108.32 o 1 1 2 568.92 589.66 7.86 o 2 1 2 26658.25 27338.98 314.54 o 3 1 2 527.27 572.88 7.04 o 4 1 2 4303.20 4055.32 42.64 o 5 1 2 550.79 571.44 7.43 o 6 1 2 1230.40 1232.88 13.75 o 7 1 2 14.25 15.32 1.79 o 8 1 2 4392.10 4354.90 115.84 o 9 1 2 184.64 169.37 8.16 o 10 1 2 2265.85 2268.90 32.74 o 11 1 2 209.74 185.85 8.73 o 0 2 2 23123.76 22821.48 364.64 o 1 2 2 629.03 638.73 7.60 o 2 2 2 4736.81 4676.79 59.90 o 3 2 2 246.81 268.20 4.34 o 4 2 2 3585.70 3412.34 108.14 o 5 2 2 140.48 136.29 2.64 o 6 2 2 12655.75 12621.07 365.84 o 7 2 2 272.87 276.23 6.17 o 8 2 2 15.66 42.85 5.97 o 9 2 2 75.43 62.34 2.65 o 10 2 2 1086.62 1091.74 20.43 o 11 2 2 27.25 17.46 4.93 o 1 3 2 189.91 199.02 3.54 o 2 3 2 24527.26 24958.08 284.76 o 3 3 2 335.77 362.27 5.73 o 4 3 2 7327.69 7094.33 80.57 o 5 3 2 178.75 197.40 3.17 o 6 3 2 1.34 18.93 5.01 o 7 3 2 142.31 140.60 2.81 o 8 3 2 2035.03 2022.99 22.99 o 9 3 2 459.26 443.91 7.99 o 10 3 2 2277.22 2317.18 35.59 o 11 3 2 39.68 31.81 4.20 o 0 4 2 11552.27 10665.28 154.63 o 1 4 2 231.36 248.96 4.11 o 2 4 2 2003.91 1881.04 22.27 o 3 4 2 402.58 441.40 6.38 o 4 4 2 3022.95 3011.99 31.38 o 5 4 2 68.61 76.95 2.13 o 6 4 2 10268.67 9967.89 139.09 o 7 4 2 0.23 2.18 1.66 o 8 4 2 1.00 5.38 1.62 o 9 4 2 29.05 26.19 3.87 o 10 4 2 1450.05 1469.88 24.67 o 11 4 2 55.28 50.84 5.39 o 1 5 2 347.88 316.55 5.29 o 2 5 2 18003.31 18157.48 231.19 o 3 5 2 840.57 852.95 15.06 o 4 5 2 2571.66 2315.29 60.23 o 5 5 2 567.77 577.96 7.76 o 6 5 2 1656.58 1644.75 51.14 o 7 5 2 7.92 5.34 1.88 o 8 5 2 4412.31 4381.97 143.23 o 9 5 2 412.54 372.63 19.39 o 10 5 2 1944.13 1910.95 35.69 o 11 5 2 190.74 167.97 8.38 o 0 6 2 18085.75 17901.09 326.00 o 1 6 2 1607.80 1619.63 36.89 o 2 6 2 3701.96 3678.21 44.04 o 3 6 2 3152.21 3268.17 35.56 o 4 6 2 3464.80 3374.10 43.25 o 5 6 2 158.21 163.06 3.35 o 6 6 2 12138.67 12350.07 134.37 o 7 6 2 408.24 415.46 6.97 o 8 6 2 64.61 67.77 3.40 o 9 6 2 75.04 73.50 3.51 o 10 6 2 1293.29 1293.37 39.20 o 11 6 2 25.02 33.58 5.86 o 1 7 2 307.78 324.40 6.41 o 2 7 2 16959.68 17062.95 187.09 o 3 7 2 1.12 1.69 1.78 o 4 7 2 5040.53 5081.41 57.15 o 5 7 2 131.18 140.73 3.78 o 6 7 2 180.66 178.95 4.63 o 7 7 2 148.95 152.12 4.78 o 8 7 2 2725.90 2748.65 37.18 o 9 7 2 2.02 1.95 3.11 o 10 7 2 2010.04 1995.53 60.56 o 11 7 2 155.10 145.98 10.60 o 0 8 2 12774.80 12605.01 310.21 o 1 8 2 138.33 133.60 3.74 o 2 8 2 2754.87 2716.85 36.47 o 3 8 2 196.17 185.97 3.83 o 4 8 2 2139.04 2061.82 26.30 o 5 8 2 19.32 20.77 1.90 o 6 8 2 8615.27 8619.77 106.93 o 7 8 2 156.17 160.58 5.50 o 8 8 2 40.01 37.95 3.32 o 9 8 2 10.27 11.31 2.94 o 10 8 2 844.36 815.05 30.92 o 1 9 2 375.72 378.25 6.44 o 2 9 2 11505.25 11555.21 153.03 o 3 9 2 14.10 13.81 1.94 o 4 9 2 3479.93 3522.03 40.41 o 5 9 2 35.16 33.42 2.66 o 6 9 2 209.21 210.08 5.36 o 7 9 2 20.63 16.47 2.82 o 8 9 2 2232.10 2274.93 53.98 o 9 9 2 4.69 3.74 3.98 o 10 9 2 1624.33 1507.97 53.73 o 0 10 2 4603.64 4481.44 168.38 o 1 10 2 74.64 69.86 3.02 o 2 10 2 663.00 664.25 11.27 o 3 10 2 251.58 250.24 5.94 o 4 10 2 1796.69 1868.27 23.68 o 5 10 2 40.78 33.90 2.32 o 6 10 2 5793.13 6044.97 69.21 o 7 10 2 0.38 -0.01 2.62 o 8 10 2 6.69 4.33 3.79 o 9 10 2 8.54 5.28 4.29 o 10 10 2 1334.77 1318.04 65.36 o 1 11 2 31.63 26.59 2.58 o 2 11 2 7362.54 7391.01 90.74 o 3 11 2 15.78 12.11 2.46 o 4 11 2 1966.86 1971.61 25.55 o 5 11 2 0.37 1.00 2.19 o 6 11 2 420.99 424.34 9.76 o 7 11 2 0.37 0.18 3.12 o 8 11 2 2383.38 2406.32 55.10 o 9 11 2 4.94 15.54 7.70 o 0 12 2 10616.28 10462.88 267.73 o 1 12 2 691.16 698.16 12.60 o 2 12 2 2450.49 2487.06 35.89 o 3 12 2 1664.04 1718.81 26.29 o 4 12 2 1542.23 1513.29 23.72 o 5 12 2 116.46 100.85 4.22 o 6 12 2 7062.35 7193.98 96.24 o 7 12 2 222.80 238.24 9.81 o 8 12 2 153.02 151.70 8.65 o 9 12 2 15.00 5.65 9.40 o 1 13 2 519.39 525.77 11.34 o 2 13 2 7432.63 7530.24 91.91 o 3 13 2 44.54 45.41 4.29 o 4 13 2 3008.80 3041.32 53.73 o 5 13 2 297.10 285.40 10.10 o 6 13 2 89.30 85.80 10.01 o 7 13 2 69.78 53.65 5.43 o 8 13 2 1740.89 1729.10 51.16 o 0 14 2 4074.25 4079.46 98.54 o 1 14 2 0.93 0.62 3.69 o 2 14 2 727.73 736.80 15.25 o 3 14 2 2.14 3.68 4.56 o 4 14 2 1030.41 1076.25 21.12 o 5 14 2 1.04 3.22 4.26 o 6 14 2 4186.24 4285.92 93.28 o 7 14 2 30.12 22.76 5.96 o 1 15 2 74.62 78.31 7.23 o 2 15 2 4175.58 4145.28 69.38 o 3 15 2 1.89 -1.79 4.36 o 4 15 2 1434.51 1483.57 43.65 o 5 15 2 25.86 32.50 6.29 o 6 15 2 214.34 189.51 10.57 o 0 16 2 2875.57 2798.57 84.55 o 1 16 2 14.88 8.28 4.83 o 2 16 2 426.57 419.58 13.83 o 3 16 2 2.89 3.94 4.43 o 4 16 2 890.29 919.68 29.08 o 5 16 2 31.32 28.64 6.18 o 1 17 2 17.76 18.08 3.91 o 2 17 2 3245.85 3297.88 73.82 o 3 17 2 0.73 3.21 5.32 o 4 17 2 1472.36 1438.56 44.26 o 0 18 2 4385.64 4296.17 180.04 o 1 18 2 56.23 38.21 10.51 o 2 18 2 1045.72 1026.60 43.03 o 1 0 3 9593.65 9326.87 163.83 o 2 0 3 176.59 184.88 5.57 o 3 0 3 188.28 194.43 5.56 o 4 0 3 0.71 0.00 2.50 o 5 0 3 8426.31 8362.07 134.83 o 6 0 3 450.00 465.19 14.20 o 7 0 3 4539.61 4651.04 84.88 o 8 0 3 1715.12 1750.29 38.97 o 9 0 3 609.49 641.43 24.76 o 10 0 3 20.86 9.33 7.05 o 11 0 3 1538.46 1541.51 70.45 o 0 1 3 917.84 910.28 24.60 o 1 1 3 3168.10 3154.42 35.94 o 2 1 3 684.31 715.51 9.52 o 3 1 3 10931.42 11087.55 129.53 o 4 1 3 400.68 403.99 6.85 o 5 1 3 703.08 691.21 10.81 o 6 1 3 606.85 615.79 11.09 o 7 1 3 691.52 705.34 12.75 o 8 1 3 91.24 97.56 4.52 o 9 1 3 4540.85 4590.38 122.24 o 10 1 3 98.63 92.21 6.69 o 11 1 3 181.58 179.98 11.73 o 1 2 3 4113.42 3800.07 42.59 o 2 2 3 20.03 19.49 1.86 o 3 2 3 290.42 306.91 5.14 o 4 2 3 711.14 738.06 11.06 o 5 2 3 6345.63 6316.03 79.27 o 6 2 3 734.16 761.95 11.87 o 7 2 3 4602.74 4752.73 59.71 o 8 2 3 77.41 71.60 3.88 o 9 2 3 404.63 394.41 11.83 o 10 2 3 113.26 98.65 6.67 o 11 2 3 2426.97 2364.44 103.34 o 0 3 3 722.08 777.01 15.99 o 1 3 3 4471.09 4453.92 46.95 o 2 3 3 2.08 4.18 1.97 o 3 3 3 12241.67 12417.01 132.08 o 4 3 3 13.47 8.02 2.04 o 5 3 3 121.51 108.86 3.53 o 6 3 3 50.15 50.80 2.88 o 7 3 3 2245.19 2290.92 32.19 o 8 3 3 0.72 6.11 2.94 o 9 3 3 5038.21 5136.84 92.93 o 10 3 3 2.55 15.29 5.38 o 11 3 3 24.43 12.67 8.06 o 1 4 3 8348.52 8364.09 107.33 o 2 4 3 1.44 5.58 1.68 o 3 4 3 79.77 93.39 4.43 o 4 4 3 93.04 104.04 3.58 o 5 4 3 8282.91 8358.57 98.31 o 6 4 3 138.22 136.13 3.97 o 7 4 3 4246.16 4298.17 65.63 o 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68.46 o 5 11 4 348.61 329.47 12.72 o 6 11 4 40.77 41.69 4.68 o 7 11 4 4.20 11.28 9.77 o 0 12 4 4554.35 4394.05 285.57 o 1 12 4 275.59 280.72 9.50 o 2 12 4 153.29 139.35 7.60 o 3 12 4 292.25 300.67 11.50 o 4 12 4 1267.96 1350.42 34.19 o 5 12 4 109.06 108.08 7.36 o 6 12 4 2137.91 2028.01 59.83 o 1 13 4 121.69 101.06 7.73 o 2 13 4 1603.75 1590.24 62.50 o 3 13 4 70.67 58.41 5.92 o 4 13 4 1505.76 1445.75 39.08 o 5 13 4 493.65 481.03 20.70 o 0 14 4 3627.40 3630.21 145.56 o 1 14 4 212.01 202.39 12.48 o 2 14 4 362.90 388.28 20.31 o 3 14 4 125.07 103.91 13.49 o 4 14 4 397.89 330.06 21.76 o 1 15 4 381.04 365.97 16.94 o 2 15 4 2495.81 2402.95 87.34 o 1 0 5 3260.53 3406.66 54.29 o 2 0 5 32.87 38.31 3.36 o 3 0 5 351.11 362.80 7.85 o 4 0 5 172.66 186.29 14.91 o 5 0 5 1683.53 1710.97 51.51 o 6 0 5 86.17 82.89 9.36 o 7 0 5 1473.63 1452.00 99.90 o 8 0 5 179.32 165.43 22.04 o 0 1 5 325.00 337.78 8.58 o 1 1 5 126.80 140.99 3.74 o 2 1 5 351.53 369.64 7.20 o 3 1 5 3578.84 3613.69 41.31 o 4 1 5 88.55 89.67 3.34 o 5 1 5 440.47 456.63 24.20 o 6 1 5 485.22 466.86 23.99 o 7 1 5 1370.87 1455.20 64.69 o 8 1 5 112.43 109.56 12.90 o 1 2 5 5139.93 5353.38 62.55 o 2 2 5 552.72 560.78 8.91 o 3 2 5 233.15 227.27 5.30 o 4 2 5 236.78 243.12 8.05 o 5 2 5 2360.49 2389.92 50.64 o 6 2 5 39.10 40.00 5.03 o 7 2 5 1827.42 1640.05 123.21 o 8 2 5 417.79 399.27 23.58 o 0 3 5 62.65 49.75 3.96 o 1 3 5 1037.06 1076.82 16.31 o 2 3 5 20.46 29.75 2.39 o 3 3 5 9424.15 9519.82 135.37 o 4 3 5 23.81 23.15 3.32 o 5 3 5 1729.67 1745.22 35.67 o 6 3 5 136.89 130.29 7.30 o 7 3 5 1415.85 1373.62 55.55 o 8 3 5 20.59 8.77 11.47 o 1 4 5 4410.36 4461.74 58.83 o 2 4 5 126.96 124.08 4.29 o 3 4 5 509.05 513.59 10.02 o 4 4 5 262.92 264.96 6.80 o 5 4 5 2765.07 2773.39 51.23 o 6 4 5 75.33 74.54 7.01 o 7 4 5 1566.84 1462.65 45.46 o 8 4 5 154.30 143.27 22.91 o 0 5 5 811.03 802.09 20.95 o 1 5 5 116.51 127.00 3.99 o 2 5 5 434.78 424.12 9.00 o 3 5 5 3013.50 2998.39 47.13 o 4 5 5 230.39 233.99 9.48 o 5 5 5 209.83 197.57 10.21 o 6 5 5 583.39 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205.57 191.53 10.33 o 2 11 5 190.46 169.41 10.85 o 3 11 5 2662.77 2719.67 89.73 o 4 11 5 18.11 15.05 5.07 o 1 12 5 2732.97 2790.64 78.74 o 2 12 5 258.55 251.40 15.01 o 3 12 5 24.13 22.48 10.06 o 0 13 5 99.96 73.63 11.96 o 0 0 6 2314.33 2377.29 79.25 o 1 0 6 288.22 258.07 29.67 o 2 0 6 117.34 125.60 8.18 o 3 0 6 297.32 290.73 19.71 o 4 0 6 843.61 823.03 155.21 o 5 0 6 29.07 22.18 16.64 o 1 1 6 200.94 199.17 6.54 o 2 1 6 1894.26 1930.93 43.68 o 3 1 6 32.71 30.62 9.63 o 4 1 6 1858.63 1655.64 149.48 o 5 1 6 220.98 194.57 15.73 o 0 2 6 4295.23 4173.46 133.81 o 1 2 6 258.78 272.91 12.60 o 2 2 6 669.37 655.77 25.92 o 3 2 6 565.38 567.92 26.13 o 4 2 6 593.54 578.31 63.65 o 5 2 6 111.41 103.53 11.81 o 1 3 6 1145.48 1108.54 29.99 o 2 3 6 2857.42 2730.01 62.98 o 3 3 6 16.93 15.22 6.02 o 4 3 6 1943.51 1841.90 112.37 o 5 3 6 563.52 554.77 33.41 o 0 4 6 5042.98 5380.13 182.09 o 1 4 6 423.27 402.84 16.63 o 2 4 6 620.07 592.14 16.51 o 3 4 6 615.92 649.40 44.93 o 4 4 6 1082.83 1178.74 124.52 o 5 4 6 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