#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016772.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016772_Fobs loop_ _publ_author_name 'G\'omez, Sandra L.' 'Raysth, Walter' 'Palma, Alirio' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Three aryl-substituted tetrahydro-1,4-epoxy-1-benzazepines: hydrogen-bonded structures in two or three dimensions ; _journal_coeditor_code LN3112 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o519 _journal_page_last o523 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.6174 _cell_length_b 11.5580 _cell_length_c 13.4650 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7690 _[local]_cod_data_source_file ln3112IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' WAL84C' _shelx_refln_list_code 4 _shelx_F_calc_maximum 125.64 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1085.28 1057.34 16.54 o 4 0 0 1414.41 1492.00 24.48 o 6 0 0 4.60 3.79 24.24 o 8 0 0 14.95 27.16 19.18 o 10 0 0 628.21 626.02 40.71 o 12 0 0 126.42 103.46 43.59 o 1 1 0 422.51 424.90 12.09 o 2 1 0 805.14 796.60 15.33 o 3 1 0 5.69 -11.01 11.00 o 4 1 0 25.63 22.84 7.66 o 5 1 0 10.72 19.64 7.66 o 6 1 0 3298.87 3625.09 35.94 o 7 1 0 0.89 21.06 9.76 o 8 1 0 50.82 41.48 11.06 o 9 1 0 96.82 94.22 10.70 o 10 1 0 52.57 24.22 30.13 o 11 1 0 0.98 -22.03 26.25 o 12 1 0 28.67 48.92 52.53 o 0 2 0 3562.61 3164.62 56.68 o 1 2 0 14531.81 13305.15 151.92 o 2 2 0 15785.47 14167.50 140.86 o 3 2 0 1112.52 1164.01 15.16 o 4 2 0 951.32 919.58 12.97 o 5 2 0 112.38 133.86 8.23 o 6 2 0 248.31 243.49 10.99 o 7 2 0 96.72 83.24 11.12 o 8 2 0 265.58 289.75 15.95 o 9 2 0 3.29 15.72 22.12 o 10 2 0 127.04 78.23 15.49 o 11 2 0 1561.09 1616.63 44.38 o 12 2 0 82.65 49.62 43.40 o 1 3 0 577.79 665.90 32.93 o 2 3 0 7832.37 7619.42 81.72 o 3 3 0 13.89 12.74 6.36 o 4 3 0 159.36 150.43 8.34 o 5 3 0 40.06 4.20 8.39 o 6 3 0 200.21 176.56 10.40 o 7 3 0 179.21 205.71 12.26 o 8 3 0 1393.64 1370.93 21.99 o 9 3 0 415.03 351.35 13.04 o 10 3 0 28.36 3.19 11.50 o 11 3 0 56.09 97.70 31.77 o 12 3 0 0.15 -5.96 38.56 o 0 4 0 17.10 26.03 11.91 o 1 4 0 456.88 422.45 10.70 o 2 4 0 2771.69 2724.65 31.85 o 3 4 0 1009.36 1140.64 18.82 o 4 4 0 819.18 936.93 16.81 o 5 4 0 934.62 911.18 14.36 o 6 4 0 8.43 29.49 9.01 o 7 4 0 248.81 253.26 13.03 o 8 4 0 10.20 -21.61 14.41 o 9 4 0 1581.79 1495.96 21.53 o 10 4 0 105.17 94.20 15.69 o 11 4 0 1.35 50.38 34.71 o 12 4 0 29.41 45.11 40.08 o 1 5 0 50.75 30.95 8.18 o 2 5 0 1368.12 1474.05 22.61 o 3 5 0 8119.89 8245.46 84.67 o 4 5 0 4008.51 4031.12 46.17 o 5 5 0 34.72 32.10 13.32 o 6 5 0 563.56 536.52 12.73 o 7 5 0 34.78 21.34 15.31 o 8 5 0 265.20 246.24 12.36 o 9 5 0 19.58 17.16 10.02 o 10 5 0 114.80 158.99 19.33 o 11 5 0 21.27 92.62 36.85 o 0 6 0 206.06 255.59 16.62 o 1 6 0 743.51 707.95 18.48 o 2 6 0 5543.98 5608.98 65.66 o 3 6 0 16.62 10.41 11.46 o 4 6 0 89.31 127.87 13.09 o 5 6 0 331.37 401.13 15.60 o 6 6 0 13.33 -2.26 14.68 o 7 6 0 63.89 41.16 21.23 o 8 6 0 16.02 -6.11 11.68 o 9 6 0 13.21 9.14 15.47 o 10 6 0 97.97 90.95 48.09 o 11 6 0 99.27 182.32 39.09 o 1 7 0 287.09 240.04 12.35 o 2 7 0 867.23 904.13 15.57 o 3 7 0 116.82 139.04 15.50 o 4 7 0 266.91 277.60 18.02 o 5 7 0 1516.00 1490.01 28.79 o 6 7 0 236.79 263.88 16.62 o 7 7 0 329.63 308.59 18.30 o 8 7 0 182.12 163.58 14.37 o 9 7 0 108.22 127.53 17.72 o 10 7 0 269.36 265.91 33.31 o 11 7 0 23.27 61.78 55.45 o 0 8 0 2328.52 2272.62 88.68 o 1 8 0 73.71 83.21 15.65 o 2 8 0 885.36 917.67 16.52 o 3 8 0 107.28 119.53 17.55 o 4 8 0 2030.91 1963.48 34.60 o 5 8 0 0.10 21.58 15.43 o 6 8 0 441.60 383.72 18.12 o 7 8 0 16.44 -6.79 17.82 o 8 8 0 7.77 23.67 18.63 o 9 8 0 0.06 20.10 17.84 o 10 8 0 42.32 22.04 36.26 o 1 9 0 147.30 127.40 15.78 o 2 9 0 150.47 144.94 14.08 o 3 9 0 64.83 111.27 17.86 o 4 9 0 220.56 236.22 20.95 o 5 9 0 42.05 58.49 15.78 o 6 9 0 191.01 171.53 16.22 o 7 9 0 234.85 199.67 25.08 o 8 9 0 20.53 28.02 20.42 o 9 9 0 34.15 64.18 23.27 o 10 9 0 275.66 332.85 41.10 o 0 10 0 119.43 147.81 49.18 o 1 10 0 56.27 124.20 24.16 o 2 10 0 294.22 305.85 15.15 o 3 10 0 7.99 13.05 15.30 o 4 10 0 9.67 -14.90 14.87 o 5 10 0 300.51 304.42 19.21 o 6 10 0 329.06 306.96 19.12 o 7 10 0 782.14 746.75 34.68 o 8 10 0 0.63 -17.59 27.85 o 9 10 0 77.35 33.74 33.57 o 1 11 0 566.99 505.43 22.46 o 2 11 0 7.93 -3.50 14.75 o 3 11 0 516.18 543.94 26.12 o 4 11 0 171.43 135.62 20.92 o 5 11 0 10.06 13.34 17.49 o 6 11 0 475.45 402.95 32.52 o 7 11 0 2.91 -8.14 24.71 o 8 11 0 3.15 -18.19 27.78 o 0 12 0 86.42 109.68 56.37 o 1 12 0 0.88 39.50 17.28 o 2 12 0 2.89 7.05 14.03 o 3 12 0 1.23 40.14 19.16 o 4 12 0 1.39 10.79 18.94 o 5 12 0 261.18 292.92 50.23 o 6 12 0 62.69 39.72 27.70 o 7 12 0 2.12 12.97 32.48 o 1 13 0 172.73 212.34 18.27 o 2 13 0 343.77 354.05 35.58 o 3 13 0 219.82 236.97 23.69 o 4 13 0 15.01 71.93 35.94 o 5 13 0 8.11 25.74 34.89 o 6 13 0 35.19 18.53 28.89 o 0 14 0 44.98 99.52 29.16 o 1 14 0 6.29 53.85 17.79 o 2 14 0 593.95 685.95 43.48 o 3 14 0 15.24 -8.45 26.99 o 4 14 0 5.83 9.82 28.68 o 2 0 1 3407.60 3285.63 37.26 o 3 0 1 202.59 153.87 15.29 o 4 0 1 70.24 76.64 8.96 o 5 0 1 908.03 854.14 14.08 o 6 0 1 188.37 183.21 10.07 o 7 0 1 1102.86 1140.97 18.57 o 8 0 1 11.46 34.56 13.47 o 9 0 1 479.52 430.95 16.77 o 10 0 1 10.43 40.27 23.89 o 11 0 1 34.66 67.50 21.12 o 12 0 1 139.45 206.57 51.90 o -11 1 1 134.50 105.56 24.73 o -10 1 1 550.15 526.73 19.38 o -9 1 1 111.56 86.32 13.15 o -8 1 1 395.51 393.57 13.18 o -7 1 1 354.01 354.11 16.20 o -6 1 1 39.59 20.14 8.70 o -5 1 1 945.18 1013.69 13.83 o -4 1 1 273.60 294.28 8.12 o -3 1 1 289.04 292.57 10.97 o -2 1 1 7058.84 6986.07 86.01 o 1 1 1 2505.42 1383.51 36.72 o 2 1 1 7000.58 6957.05 94.25 o 3 1 1 277.26 296.33 15.34 o 4 1 1 292.54 326.14 10.68 o 5 1 1 962.17 1024.27 18.91 o 6 1 1 33.81 31.16 9.72 o 7 1 1 343.63 349.47 15.18 o 8 1 1 391.39 403.59 16.95 o 9 1 1 112.99 103.32 13.87 o 10 1 1 542.99 504.99 20.18 o 11 1 1 129.71 111.82 32.79 o 12 1 1 128.01 173.57 33.32 o -12 2 1 20.63 -26.93 36.86 o -11 2 1 110.70 133.82 27.61 o -10 2 1 16.02 9.53 14.69 o -9 2 1 496.91 472.97 15.13 o -8 2 1 109.46 120.05 11.26 o -7 2 1 790.88 760.09 15.44 o -6 2 1 335.12 351.77 11.44 o -5 2 1 403.13 412.64 10.11 o -4 2 1 305.02 274.41 8.47 o -3 2 1 791.00 806.60 13.99 o -2 2 1 11765.72 11834.80 187.07 o -1 2 1 1343.83 1240.29 15.53 o 0 2 1 133.18 135.63 16.37 o 1 2 1 1309.46 1213.62 16.98 o 2 2 1 11639.05 11577.35 125.72 o 3 2 1 777.93 791.52 11.35 o 4 2 1 289.39 255.08 9.44 o 5 2 1 406.55 440.72 13.71 o 6 2 1 323.26 337.07 11.79 o 7 2 1 784.59 792.50 13.54 o 8 2 1 114.29 145.93 22.56 o 9 2 1 508.24 505.88 18.15 o 10 2 1 16.34 17.96 16.00 o 11 2 1 111.79 171.26 43.60 o 12 2 1 20.67 -18.08 57.43 o -12 3 1 173.69 172.08 60.71 o -11 3 1 239.30 281.77 78.51 o -10 3 1 105.87 101.69 25.00 o -9 3 1 291.73 281.71 13.45 o -8 3 1 63.76 62.51 10.35 o -7 3 1 1.89 -8.69 9.60 o -6 3 1 81.35 78.94 9.31 o -5 3 1 314.38 307.81 9.32 o -4 3 1 2018.08 2134.46 23.26 o -3 3 1 883.96 833.48 15.28 o -2 3 1 2013.60 1881.12 44.62 o -1 3 1 14738.56 13826.22 169.11 o 0 3 1 259.64 279.32 18.90 o 1 3 1 14671.55 14331.07 161.38 o 2 3 1 2038.07 1900.66 25.19 o 3 3 1 910.74 882.77 12.19 o 4 3 1 1983.08 2144.90 25.26 o 5 3 1 332.03 319.59 9.45 o 6 3 1 85.07 95.47 11.00 o 7 3 1 2.41 12.24 11.58 o 8 3 1 66.73 68.99 15.70 o 9 3 1 288.33 290.11 16.13 o 10 3 1 103.23 99.87 22.36 o 11 3 1 245.17 230.12 27.26 o 12 3 1 176.82 200.62 40.67 o -12 4 1 1.36 -59.54 60.55 o -11 4 1 0.23 -8.15 33.69 o -10 4 1 61.24 89.77 15.95 o -9 4 1 238.86 224.53 14.01 o -8 4 1 37.22 31.89 10.31 o -7 4 1 180.36 178.75 10.39 o -6 4 1 21.61 14.38 10.29 o -5 4 1 190.62 210.76 9.98 o -4 4 1 789.48 817.40 17.14 o -3 4 1 391.39 462.58 16.51 o -2 4 1 52.16 37.74 9.96 o -1 4 1 866.93 840.63 14.07 o 0 4 1 400.16 365.12 12.16 o 1 4 1 845.08 851.81 18.37 o 2 4 1 53.17 32.03 11.11 o 3 4 1 398.64 464.76 9.86 o 4 4 1 804.75 803.44 12.58 o 5 4 1 193.17 206.83 8.85 o 6 4 1 20.51 34.59 11.20 o 7 4 1 177.79 185.66 12.08 o 8 4 1 36.34 41.52 14.21 o 9 4 1 240.74 239.74 15.67 o 10 4 1 59.17 89.17 39.35 o 11 4 1 0.17 2.97 24.36 o 12 4 1 1.53 -11.74 61.25 o -11 5 1 53.17 2.31 36.56 o -10 5 1 167.30 170.62 20.87 o -9 5 1 147.69 128.41 12.56 o -8 5 1 14.38 28.67 13.89 o -7 5 1 23.70 35.57 10.39 o -6 5 1 109.49 103.96 14.60 o -5 5 1 267.90 296.02 18.47 o -4 5 1 115.97 133.49 17.67 o -3 5 1 4729.89 4827.32 56.86 o -2 5 1 671.66 726.19 14.74 o -1 5 1 1659.47 1555.35 20.08 o 0 5 1 4170.71 4090.61 44.13 o 1 5 1 1681.43 1592.16 29.39 o 2 5 1 660.89 712.35 20.63 o 3 5 1 4692.74 4691.06 60.87 o 4 5 1 115.33 119.15 11.12 o 5 5 1 253.90 269.81 12.77 o 6 5 1 113.53 95.17 11.85 o 7 5 1 23.51 22.36 11.37 o 8 5 1 16.10 17.97 15.08 o 9 5 1 146.85 151.43 12.20 o 10 5 1 166.77 172.91 24.53 o 11 5 1 50.91 77.43 53.53 o -11 6 1 51.03 102.73 55.39 o -10 6 1 206.56 207.13 30.42 o -9 6 1 121.29 136.36 13.96 o -8 6 1 31.21 5.36 13.18 o -7 6 1 494.23 463.66 17.40 o -6 6 1 473.80 496.45 19.39 o -5 6 1 5.91 5.32 14.31 o -4 6 1 151.25 213.66 16.84 o -3 6 1 2815.91 2840.92 40.02 o -2 6 1 70.24 76.48 15.33 o -1 6 1 55.71 42.94 11.14 o 0 6 1 693.24 627.53 15.30 o 1 6 1 52.34 51.30 9.97 o 2 6 1 68.13 103.60 15.53 o 3 6 1 2814.40 2824.28 35.72 o 4 6 1 161.88 183.52 13.94 o 5 6 1 8.21 9.95 11.61 o 6 6 1 474.01 507.57 15.69 o 7 6 1 490.70 456.71 15.99 o 8 6 1 34.10 -9.20 12.65 o 9 6 1 115.76 128.83 14.31 o 10 6 1 205.69 214.03 25.84 o 11 6 1 48.58 97.85 41.22 o -11 7 1 145.57 108.64 41.06 o -10 7 1 104.90 97.84 36.72 o -9 7 1 122.02 130.89 17.79 o -8 7 1 330.24 328.95 18.85 o -7 7 1 98.97 70.35 13.97 o -6 7 1 150.24 118.55 15.50 o -5 7 1 1139.30 1203.36 29.74 o -4 7 1 268.18 300.99 17.96 o -3 7 1 14.17 8.33 15.34 o -2 7 1 57.65 62.35 9.72 o -1 7 1 374.93 370.68 17.65 o 0 7 1 428.60 455.14 18.96 o 1 7 1 370.90 377.41 18.82 o 2 7 1 60.53 84.69 21.65 o 3 7 1 14.94 17.18 15.00 o 4 7 1 281.57 340.89 15.91 o 5 7 1 1135.35 1188.52 24.38 o 6 7 1 146.80 147.25 16.34 o 7 7 1 94.31 72.29 11.77 o 8 7 1 335.25 305.15 20.95 o 9 7 1 118.02 106.30 18.47 o 10 7 1 99.42 76.70 34.01 o 11 7 1 149.78 102.49 59.96 o -10 8 1 12.26 -49.83 33.22 o -9 8 1 135.34 164.73 40.26 o -8 8 1 325.47 315.37 20.85 o -7 8 1 69.73 58.67 15.08 o -6 8 1 103.03 82.52 18.00 o -5 8 1 2090.63 2034.85 36.48 o -4 8 1 284.71 312.00 19.09 o -3 8 1 101.46 116.95 17.85 o -2 8 1 23.61 36.60 10.17 o -1 8 1 118.46 129.53 13.89 o 0 8 1 1691.71 1680.96 29.53 o 1 8 1 115.13 100.82 13.69 o 2 8 1 25.04 41.67 17.83 o 3 8 1 101.53 89.97 18.18 o 4 8 1 288.37 268.84 24.06 o 5 8 1 2088.52 2011.53 35.19 o 6 8 1 101.33 109.61 12.61 o 7 8 1 61.22 25.34 12.25 o 8 8 1 327.30 286.50 28.49 o 9 8 1 143.27 129.61 20.35 o 10 8 1 13.77 38.68 35.62 o -9 9 1 28.60 36.23 31.42 o -8 9 1 36.84 22.01 22.16 o -7 9 1 125.23 121.08 16.96 o -6 9 1 116.59 116.66 17.86 o -5 9 1 89.49 57.11 16.13 o -4 9 1 106.35 100.27 18.35 o -3 9 1 67.52 89.15 17.83 o -2 9 1 191.28 194.80 13.93 o -1 9 1 806.48 780.74 23.03 o 0 9 1 885.09 807.95 29.13 o 1 9 1 827.89 807.01 22.25 o 2 9 1 189.08 170.36 18.67 o 3 9 1 65.69 71.11 23.11 o 4 9 1 110.11 115.21 16.56 o 5 9 1 86.92 82.57 22.94 o 6 9 1 108.26 133.92 15.09 o 7 9 1 120.24 117.86 32.98 o 8 9 1 39.18 49.02 19.43 o 9 9 1 29.25 44.15 57.90 o -9 10 1 17.85 -6.26 25.85 o -8 10 1 3.10 2.43 27.47 o -7 10 1 140.30 131.50 23.56 o -6 10 1 708.60 642.90 26.56 o -5 10 1 78.38 70.30 17.62 o -4 10 1 63.38 41.82 17.98 o -3 10 1 462.06 495.67 22.29 o -2 10 1 566.60 563.02 15.20 o -1 10 1 805.86 817.04 23.40 o 0 10 1 140.77 160.59 19.90 o 1 10 1 824.06 864.43 23.62 o 2 10 1 561.74 554.47 26.53 o 3 10 1 462.19 463.34 20.57 o 4 10 1 57.06 38.52 15.77 o 5 10 1 75.33 75.81 17.07 o 6 10 1 710.09 659.74 23.47 o 7 10 1 144.73 137.58 27.14 o 8 10 1 3.39 16.61 39.93 o 9 10 1 17.11 52.21 41.13 o -8 11 1 45.26 27.53 29.95 o -7 11 1 126.60 113.30 36.37 o -6 11 1 3.87 -7.82 34.78 o -5 11 1 10.05 48.64 34.55 o -4 11 1 118.57 149.98 36.48 o -3 11 1 367.37 383.55 36.50 o -2 11 1 78.35 99.34 14.57 o -1 11 1 363.62 368.09 21.47 o 0 11 1 1557.56 1432.07 30.61 o 1 11 1 366.58 365.70 28.50 o 2 11 1 83.50 99.12 13.91 o 3 11 1 370.15 381.55 20.63 o 4 11 1 118.77 93.76 18.94 o 5 11 1 11.56 -8.13 25.09 o 6 11 1 4.09 25.35 24.41 o 7 11 1 127.22 191.67 61.03 o 8 11 1 44.66 46.47 26.23 o -7 12 1 52.57 10.02 38.93 o -6 12 1 0.20 30.34 27.22 o -5 12 1 157.70 82.81 54.77 o -4 12 1 208.23 236.87 28.22 o -3 12 1 166.26 165.47 20.83 o -2 12 1 309.75 302.07 27.49 o -1 12 1 72.92 101.85 16.16 o 0 12 1 13.67 1.33 22.44 o 1 12 1 71.53 68.84 21.73 o 2 12 1 316.55 315.27 22.88 o 3 12 1 171.20 170.31 20.42 o 4 12 1 210.25 237.43 27.43 o 5 12 1 157.22 90.79 27.04 o 6 12 1 0.41 30.72 35.69 o 7 12 1 54.59 105.94 69.59 o -6 13 1 7.90 25.83 43.21 o -5 13 1 34.26 0.99 37.22 o -4 13 1 40.42 7.24 31.89 o -3 13 1 61.95 77.11 56.17 o -2 13 1 11.75 29.53 17.25 o -1 13 1 154.14 139.30 20.49 o 0 13 1 72.38 71.69 23.82 o 1 13 1 153.02 160.63 19.75 o 2 13 1 13.24 -8.97 30.23 o 3 13 1 66.78 110.80 27.58 o 4 13 1 43.02 25.45 32.17 o 5 13 1 32.17 59.11 31.12 o 6 13 1 8.90 41.37 40.17 o -4 14 1 113.70 150.94 39.66 o -3 14 1 163.91 106.02 30.70 o -2 14 1 116.57 101.65 31.30 o -1 14 1 0.79 18.95 18.72 o 0 14 1 13.91 65.54 22.70 o 1 14 1 0.73 27.11 34.53 o 2 14 1 120.46 129.68 28.80 o 3 14 1 165.61 110.21 38.51 o 4 14 1 109.96 127.50 30.38 o 0 0 2 54.21 486.84 44.09 o 1 0 2 110.32 43.36 9.61 o 2 0 2 6104.35 6116.76 78.92 o 3 0 2 5000.09 5162.52 57.54 o 4 0 2 13.02 5.11 11.36 o 5 0 2 548.15 598.27 13.97 o 6 0 2 137.78 149.85 13.44 o 7 0 2 253.02 252.15 15.59 o 8 0 2 1.98 4.28 19.27 o 9 0 2 34.77 25.71 14.16 o 10 0 2 11.04 27.84 19.75 o 11 0 2 19.94 23.84 51.26 o 12 0 2 69.90 140.31 51.32 o -12 1 2 244.38 165.89 53.64 o -11 1 2 5.46 7.08 23.22 o -10 1 2 22.73 3.29 15.47 o -9 1 2 104.41 136.52 14.52 o -8 1 2 22.64 33.75 21.10 o -7 1 2 3.53 13.30 13.31 o 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13.83 o 4 2 2 491.10 482.70 12.63 o 5 2 2 485.70 459.00 13.88 o 6 2 2 488.73 507.20 15.42 o 7 2 2 127.20 115.99 16.16 o 8 2 2 217.50 207.43 15.68 o 9 2 2 347.11 302.30 16.67 o 10 2 2 153.19 141.27 18.74 o 11 2 2 200.69 224.22 46.21 o 12 2 2 84.14 22.84 44.64 o -12 3 2 60.30 51.09 39.61 o -11 3 2 88.18 111.34 36.75 o -10 3 2 280.63 275.67 18.89 o -9 3 2 342.01 348.93 12.63 o -8 3 2 396.77 390.64 11.77 o -7 3 2 262.62 266.98 10.54 o -6 3 2 504.52 498.10 14.23 o -5 3 2 1165.11 1187.20 18.36 o -4 3 2 1149.69 1185.70 18.17 o -3 3 2 87.52 84.46 9.92 o -2 3 2 717.81 725.18 14.08 o -1 3 2 247.42 221.07 12.24 o 0 3 2 367.84 335.26 19.74 o 1 3 2 251.98 228.44 13.15 o 2 3 2 699.51 715.90 13.81 o 3 3 2 95.99 92.64 11.32 o 4 3 2 1163.99 1197.93 17.56 o 5 3 2 1182.27 1247.96 18.24 o 6 3 2 496.01 496.53 12.96 o 7 3 2 271.33 259.67 20.51 o 8 3 2 404.85 385.23 15.49 o 9 3 2 326.51 330.19 18.67 o 10 3 2 275.61 286.10 21.41 o 11 3 2 88.01 87.72 25.59 o 12 3 2 57.81 125.05 49.54 o -11 4 2 164.96 158.30 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