#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:14:35 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180836 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/67/2016791.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016791_Fobs loop_ _publ_author_name 'Blerk, Charmaine van' 'Kruger, Gert J.' _publ_section_title ; Hydrogen-bonding motifs and thermotropic polymorphism in redetermined halide salts of hexamethylenediamine ; _journal_coeditor_code BM3056 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o537 _journal_page_last o542 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.423 _cell_angle_gamma 90.000 _cell_length_a 4.8884 _cell_length_b 12.8756 _cell_length_c 9.7488 _exptl_crystal_F_000 348.00 _reflns_d_resolution_high 0.7460 _cod_data_source_file bm3056IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 7cvb53_a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 179.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8474.51 9624.07 246.05 o 2 0 0 22298.14 23812.78 580.39 o 3 0 0 4023.72 4051.57 81.42 o 4 0 0 735.11 828.51 21.29 o 5 0 0 77.09 99.31 4.28 o 6 0 0 74.24 99.91 7.02 o 1 1 0 1521.06 1633.53 20.55 o 2 1 0 8154.02 8268.89 97.42 o 3 1 0 4878.02 5048.69 59.72 o 4 1 0 4984.03 5132.87 88.96 o 5 1 0 1848.10 1887.66 38.83 o 6 1 0 888.93 892.92 23.94 o 0 2 0 12732.78 13743.96 392.14 o 1 2 0 28692.45 30187.53 696.05 o 2 2 0 8022.32 8402.15 104.99 o 3 2 0 2977.08 3193.43 37.90 o 4 2 0 593.80 602.15 9.19 o 5 2 0 1.16 4.58 1.49 o 6 2 0 13.03 14.46 3.56 o 1 3 0 1031.60 1069.59 14.65 o 2 3 0 1896.44 1980.95 26.56 o 3 3 0 2740.30 2814.58 41.15 o 4 3 0 1520.75 1552.62 21.34 o 5 3 0 912.08 981.77 20.87 o 6 3 0 268.05 271.18 8.95 o 0 4 0 8275.44 8591.14 314.01 o 1 4 0 1342.04 1346.08 43.39 o 2 4 0 1662.53 1725.95 21.79 o 3 4 0 489.51 504.43 8.46 o 4 4 0 22.06 24.46 1.25 o 5 4 0 5.85 6.71 1.42 o 6 4 0 23.32 19.13 2.94 o 1 5 0 67.55 71.14 4.59 o 2 5 0 45.35 42.71 2.14 o 3 5 0 77.02 88.83 1.88 o 4 5 0 42.16 43.68 2.16 o 5 5 0 11.43 10.90 1.44 o 6 5 0 7.26 3.14 3.44 o 0 6 0 2135.85 1977.13 50.28 o 1 6 0 50.70 50.23 2.28 o 2 6 0 567.92 588.14 13.28 o 3 6 0 151.83 143.68 3.59 o 4 6 0 17.90 12.10 1.99 o 5 6 0 40.74 42.75 2.30 o 6 6 0 1.42 0.15 2.53 o 1 7 0 95.34 83.58 2.14 o 2 7 0 690.54 687.75 13.32 o 3 7 0 298.63 289.95 6.26 o 4 7 0 626.39 616.52 12.33 o 5 7 0 132.49 133.44 4.13 o 0 8 0 5785.42 5866.38 148.12 o 1 8 0 2843.13 2702.58 50.08 o 2 8 0 2671.35 2575.28 46.29 o 3 8 0 604.59 607.82 11.96 o 4 8 0 290.99 292.01 6.64 o 5 8 0 5.20 3.57 1.51 o 1 9 0 240.38 251.89 5.40 o 2 9 0 1174.26 1167.49 21.45 o 3 9 0 1037.54 1009.53 19.27 o 4 9 0 921.23 882.02 17.29 o 5 9 0 503.36 491.08 10.26 o 0 10 0 4457.82 4357.77 117.45 o 1 10 0 3586.18 3566.77 65.95 o 2 10 0 1982.69 1991.31 36.05 o 3 10 0 893.86 878.46 17.00 o 4 10 0 114.41 112.76 3.66 o 5 10 0 17.57 20.35 2.08 o 1 11 0 295.55 307.01 6.60 o 2 11 0 537.56 532.13 10.68 o 3 11 0 906.92 900.63 17.53 o 4 11 0 589.79 586.33 13.57 o 5 11 0 339.99 327.45 8.89 o 0 12 0 1555.88 1574.31 34.18 o 1 12 0 1658.35 1643.92 30.84 o 2 12 0 739.16 746.46 14.63 o 3 12 0 298.56 305.40 7.02 o 4 12 0 61.56 60.72 3.39 o 1 13 0 72.98 72.47 2.93 o 2 13 0 192.19 182.48 4.74 o 3 13 0 273.70 264.16 7.13 o 4 13 0 157.99 147.92 5.20 o 0 14 0 223.23 216.81 7.84 o 1 14 0 247.90 234.39 5.20 o 2 14 0 99.06 84.98 5.71 o 3 14 0 37.31 33.66 2.65 o 1 15 0 12.80 10.05 1.87 o 2 15 0 7.95 3.44 2.39 o 3 15 0 32.76 27.22 3.25 o 0 16 0 1.80 5.05 2.69 o 1 16 0 0.93 -2.52 2.87 o 2 16 0 3.29 5.78 2.78 o 1 17 0 0.78 3.44 4.24 o -6 1 1 7.67 10.16 2.64 o -5 1 1 84.91 82.13 3.21 o -4 1 1 293.38 286.40 4.71 o -3 1 1 809.51 863.75 11.88 o -2 1 1 1646.60 1615.96 26.02 o -1 1 1 3474.78 3535.36 74.42 o 0 1 1 1004.62 1010.71 16.82 o 1 1 1 2050.42 2093.54 32.21 o 2 1 1 396.11 424.95 5.59 o 3 1 1 1.00 3.90 0.55 o 4 1 1 11.21 9.62 1.33 o 5 1 1 117.16 112.01 3.29 o 6 1 1 4.32 1.95 2.52 o -6 2 1 199.95 193.98 10.07 o -5 2 1 396.94 416.20 9.62 o -4 2 1 584.87 594.22 8.49 o -3 2 1 147.96 139.21 2.09 o -2 2 1 291.46 325.22 5.05 o -1 2 1 3271.72 3305.66 60.05 o 0 2 1 104.27 150.85 4.00 o 1 2 1 9964.07 10460.21 199.79 o 2 2 1 3151.85 3147.49 45.88 o 3 2 1 3624.17 3670.87 53.59 o 4 2 1 1591.46 1618.18 23.65 o 5 2 1 531.25 537.37 12.02 o 6 2 1 190.37 186.61 10.07 o -6 3 1 35.50 32.63 4.48 o -5 3 1 617.69 652.48 14.34 o -4 3 1 1361.30 1410.05 18.27 o -3 3 1 6153.40 6203.63 83.08 o -2 3 1 8700.41 8798.81 128.10 o -1 3 1 12739.29 12164.56 562.13 o 0 3 1 20989.42 21773.50 328.42 o 1 3 1 2882.22 2971.15 47.93 o 2 3 1 4128.51 4198.53 67.31 o 3 3 1 15.04 28.99 2.07 o 4 3 1 16.27 19.30 1.04 o 5 3 1 160.70 165.02 3.76 o 6 3 1 238.60 250.28 13.33 o -6 4 1 509.28 526.17 15.13 o -5 4 1 872.95 885.34 19.78 o -4 4 1 1294.29 1297.72 17.97 o -3 4 1 586.38 633.02 8.36 o -2 4 1 97.69 118.90 3.31 o -1 4 1 1229.96 1265.49 20.65 o 0 4 1 5796.43 5724.82 85.31 o 1 4 1 9386.42 9519.71 153.98 o 2 4 1 11229.35 11290.59 178.13 o 3 4 1 6036.83 6000.85 87.17 o 4 4 1 3921.96 3950.90 63.89 o 5 4 1 1199.59 1217.31 22.60 o 6 4 1 406.15 439.49 19.50 o -6 5 1 64.53 81.90 5.01 o -5 5 1 537.57 525.87 12.44 o -4 5 1 2197.96 2254.87 30.97 o -3 5 1 6047.79 6254.02 91.44 o -2 5 1 11302.01 11034.28 177.31 o -1 5 1 17750.91 17717.70 343.40 o 0 5 1 13101.95 13271.10 179.56 o 1 5 1 8619.42 8761.73 141.40 o 2 5 1 2157.51 2093.50 42.41 o 3 5 1 192.36 211.18 4.36 o 4 5 1 29.96 47.10 2.25 o 5 5 1 360.91 376.58 7.98 o 6 5 1 202.31 214.88 7.98 o -6 6 1 391.97 399.46 14.17 o -5 6 1 892.18 868.52 15.68 o -4 6 1 957.27 973.95 16.59 o -3 6 1 653.12 648.63 11.14 o -2 6 1 171.86 196.59 3.79 o -1 6 1 1952.50 1963.83 26.79 o 0 6 1 1406.68 1395.34 19.08 o 1 6 1 9873.96 9961.92 160.67 o 2 6 1 6275.05 6209.52 114.66 o 3 6 1 6000.44 5892.17 106.69 o 4 6 1 2690.79 2687.99 49.44 o 5 6 1 1047.41 1052.27 18.09 o 6 6 1 287.45 291.22 8.09 o -5 7 1 285.10 296.26 6.20 o -4 7 1 917.62 927.14 15.90 o -3 7 1 3229.42 3193.63 58.72 o -2 7 1 5730.89 5497.66 100.11 o -1 7 1 6733.21 6467.37 97.67 o 0 7 1 8504.31 8502.03 124.85 o 1 7 1 2749.65 2655.10 43.17 o 2 7 1 1630.01 1644.66 29.69 o 3 7 1 26.30 41.25 2.54 o 4 7 1 34.11 34.89 2.48 o 5 7 1 150.91 156.44 4.01 o -5 8 1 241.81 240.47 5.45 o -4 8 1 507.07 499.54 10.42 o -3 8 1 280.34 303.90 7.76 o -2 8 1 9.99 10.82 1.24 o -1 8 1 8.00 12.64 1.46 o 0 8 1 1798.00 1778.09 26.44 o 1 8 1 1410.20 1368.46 22.60 o 2 8 1 2809.18 2771.19 45.31 o 3 8 1 1544.54 1544.44 28.81 o 4 8 1 916.33 883.38 17.24 o 5 8 1 339.68 322.55 8.93 o -5 9 1 3.19 1.31 1.63 o -4 9 1 235.76 238.40 5.16 o -3 9 1 281.52 282.40 6.30 o -2 9 1 1001.38 975.60 18.72 o -1 9 1 1463.43 1452.83 26.29 o 0 9 1 663.18 645.85 12.42 o 1 9 1 1113.92 1136.47 18.92 o 2 9 1 17.08 19.05 1.19 o 3 9 1 70.14 68.26 2.60 o 4 9 1 54.10 55.71 2.64 o 5 9 1 27.65 27.38 3.08 o -5 10 1 60.44 60.27 3.56 o -4 10 1 5.12 3.34 1.59 o -3 10 1 166.00 166.89 4.37 o -2 10 1 0.50 -1.03 1.03 o -1 10 1 17.48 16.95 1.23 o 0 10 1 46.48 45.44 1.90 o 1 10 1 51.69 54.62 2.44 o 2 10 1 108.08 104.50 3.07 o 3 10 1 74.85 69.64 2.99 o 4 10 1 28.28 28.31 2.06 o 5 10 1 14.71 12.78 2.28 o -5 11 1 13.72 14.80 2.36 o -4 11 1 17.62 17.15 1.96 o -3 11 1 26.26 33.07 2.13 o -2 11 1 16.26 19.26 1.50 o -1 11 1 31.37 41.38 2.02 o 0 11 1 11.67 17.43 1.34 o 1 11 1 6.10 8.04 1.04 o 2 11 1 16.16 19.78 1.66 o 3 11 1 0.71 -0.74 1.42 o 4 11 1 6.99 6.43 1.71 o 5 11 1 0.01 -0.06 3.04 o -4 12 1 0.04 -0.74 2.72 o -3 12 1 9.01 8.64 1.63 o -2 12 1 7.20 6.22 1.35 o -1 12 1 77.99 87.96 3.62 o 0 12 1 43.34 52.58 2.05 o 1 12 1 235.05 251.13 4.99 o 2 12 1 133.31 160.55 9.68 o 3 12 1 123.06 124.51 3.81 o 4 12 1 90.94 96.11 4.52 o -4 13 1 97.74 103.59 4.46 o -3 13 1 267.61 292.63 6.94 o -2 13 1 353.22 357.32 10.89 o -1 13 1 459.23 491.00 10.60 o 0 13 1 378.30 411.44 9.05 o 1 13 1 218.61 239.68 5.56 o 2 13 1 84.08 90.14 3.18 o 3 13 1 11.10 11.60 1.84 o 4 13 1 0.02 -1.96 1.96 o -3 14 1 6.08 7.40 2.16 o -2 14 1 0.06 -0.52 1.83 o -1 14 1 33.64 47.03 4.93 o 0 14 1 203.73 220.46 5.66 o 1 14 1 253.47 280.73 7.54 o 2 14 1 348.12 371.20 9.63 o 3 14 1 279.71 305.70 10.18 o -3 15 1 187.19 198.18 7.68 o -2 15 1 373.73 384.11 11.83 o -1 15 1 384.28 404.63 8.05 o 0 15 1 383.33 405.44 9.19 o 1 15 1 189.69 191.94 7.59 o 2 15 1 73.61 71.68 3.92 o 3 15 1 8.03 6.63 2.73 o -2 16 1 0.01 2.79 3.50 o -1 16 1 15.19 20.32 4.25 o 0 16 1 76.03 82.65 4.38 o 1 16 1 167.07 184.92 6.43 o 2 16 1 188.66 206.06 8.01 o 0 17 1 102.62 110.27 8.07 o -6 0 2 437.24 447.64 18.59 o -5 0 2 1809.48 1860.54 47.36 o -4 0 2 4336.90 4428.30 89.17 o -3 0 2 11214.72 12269.92 644.16 o -2 0 2 10409.29 10727.19 280.15 o -1 0 2 25116.13 29168.63 764.20 o 0 0 2 3018.06 3322.29 96.62 o 1 0 2 2753.32 2858.72 58.20 o 2 0 2 103.70 146.52 7.19 o 3 0 2 1603.28 1662.71 29.67 o 4 0 2 1737.57 1713.96 30.78 o 5 0 2 1654.07 1762.76 44.43 o 6 0 2 757.40 764.52 29.63 o -6 1 2 252.75 272.98 9.11 o -5 1 2 366.37 378.89 6.93 o -4 1 2 37.68 61.61 1.76 o -3 1 2 239.98 271.72 8.98 o -2 1 2 2925.97 2994.74 55.57 o -1 1 2 15096.12 15268.70 439.09 o 0 1 2 17491.62 20490.48 469.39 o 1 1 2 32074.11 35638.88 1128.30 o 2 1 2 13559.82 13696.78 325.97 o 3 1 2 9629.32 9909.04 131.72 o 4 1 2 2577.51 2639.98 38.20 o 5 1 2 791.96 812.72 15.08 o 6 1 2 68.82 81.55 4.71 o -6 2 2 274.26 285.43 9.24 o -5 2 2 1184.56 1189.77 19.43 o -4 2 2 2752.72 2828.75 38.12 o -3 2 2 6876.48 6960.18 149.19 o -2 2 2 8410.00 8283.30 152.88 o -1 2 2 10038.81 9448.39 281.21 o 0 2 2 4970.44 4998.78 87.73 o 1 2 2 1138.06 1181.38 17.35 o 2 2 2 69.42 99.72 5.13 o 3 2 2 971.91 973.87 15.71 o 4 2 2 1142.94 1173.41 17.35 o 5 2 2 1137.98 1155.15 24.32 o 6 2 2 444.49 437.55 12.94 o -6 3 2 124.24 124.11 7.73 o -5 3 2 186.41 194.90 3.90 o -4 3 2 19.30 25.78 1.53 o -3 3 2 13.92 24.27 1.39 o -2 3 2 1345.50 1389.92 21.11 o -1 3 2 3568.23 3441.91 78.18 o 0 3 2 8032.42 7842.59 240.86 o 1 3 2 8866.48 9339.96 166.25 o 2 3 2 6297.29 6181.91 108.41 o 3 3 2 3041.57 3083.16 45.08 o 4 3 2 1191.26 1228.12 19.85 o 5 3 2 215.04 217.50 4.56 o 6 3 2 34.99 30.08 4.19 o -6 4 2 40.55 41.08 3.62 o -5 4 2 126.73 120.60 3.61 o -4 4 2 649.14 656.78 10.23 o -3 4 2 858.37 882.71 12.35 o -2 4 2 1900.22 1969.41 32.14 o -1 4 2 1656.76 1612.22 26.16 o 0 4 2 929.64 959.28 15.77 o 1 4 2 163.56 188.88 3.08 o 2 4 2 0.77 6.56 2.29 o 3 4 2 165.86 173.51 3.15 o 4 4 2 262.54 270.85 5.07 o 5 4 2 146.01 154.34 5.05 o 6 4 2 121.95 121.08 5.75 o -6 5 2 20.94 24.64 7.69 o -5 5 2 2.96 1.25 1.63 o -4 5 2 92.80 98.14 2.25 o -3 5 2 1.74 0.32 0.70 o -2 5 2 22.68 22.56 1.19 o -1 5 2 28.61 33.82 1.04 o 0 5 2 184.56 212.28 3.93 o 1 5 2 15.56 24.68 1.89 o 2 5 2 283.04 315.42 5.56 o 3 5 2 11.56 16.39 0.98 o 4 5 2 22.97 25.68 1.71 o 5 5 2 3.77 1.74 1.44 o 6 5 2 1.06 -1.08 2.63 o -6 6 2 27.70 30.39 3.48 o -5 6 2 48.58 45.95 3.09 o -4 6 2 114.97 127.65 6.29 o -3 6 2 214.79 208.59 4.28 o -2 6 2 72.97 67.24 2.11 o -1 6 2 342.91 335.44 5.81 o 0 6 2 1.80 2.11 0.41 o 1 6 2 29.47 24.38 0.85 o 2 6 2 1.14 1.27 0.78 o 3 6 2 59.52 57.75 3.16 o 4 6 2 13.30 9.37 1.94 o 5 6 2 36.93 34.96 3.00 o 6 6 2 11.14 8.19 2.95 o -5 7 2 5.42 2.48 1.94 o -4 7 2 0.23 0.11 1.03 o -3 7 2 167.90 176.86 3.84 o -2 7 2 406.04 437.70 7.67 o -1 7 2 1527.66 1459.95 21.75 o 0 7 2 1593.38 1554.10 23.13 o 1 7 2 2525.57 2448.30 39.99 o 2 7 2 1351.48 1311.02 24.29 o 3 7 2 980.28 936.62 20.08 o 4 7 2 257.84 236.23 5.54 o 5 7 2 135.07 130.67 4.09 o -5 8 2 427.99 443.32 8.62 o -4 8 2 639.77 642.50 11.57 o -3 8 2 1884.57 1907.52 31.62 o -2 8 2 1318.36 1305.80 24.49 o -1 8 2 2512.76 2433.78 36.06 o 0 8 2 361.00 340.48 5.00 o 1 8 2 247.56 268.17 4.91 o 2 8 2 32.29 41.34 1.99 o 3 8 2 214.33 220.28 5.76 o 4 8 2 268.00 243.35 6.15 o 5 8 2 302.79 299.49 7.99 o -5 9 2 84.70 95.32 3.59 o -4 9 2 7.10 11.78 1.47 o -3 9 2 40.16 57.23 2.49 o -2 9 2 807.53 851.10 14.63 o -1 9 2 2474.25 2478.95 36.80 o 0 9 2 2587.55 2492.51 34.01 o 1 9 2 5441.54 5341.52 86.46 o 2 9 2 2097.75 2032.53 37.34 o 3 9 2 2170.48 2080.33 38.58 o 4 9 2 564.11 526.01 10.91 o 5 9 2 178.30 166.70 5.50 o -5 10 2 337.30 336.49 15.23 o -4 10 2 904.58 917.34 16.09 o -3 10 2 1546.16 1551.11 29.60 o -2 10 2 2079.19 2015.97 33.57 o -1 10 2 1706.58 1661.26 28.32 o 0 10 2 956.44 946.86 15.91 o 1 10 2 160.84 153.06 4.08 o 2 10 2 13.41 19.91 2.05 o 3 10 2 239.48 252.08 5.84 o 4 10 2 329.48 337.37 7.67 o 5 10 2 298.76 296.59 8.37 o -4 11 2 41.61 45.09 2.35 o -3 11 2 74.97 88.08 3.61 o -2 11 2 342.75 370.99 7.96 o -1 11 2 958.10 950.16 22.55 o 0 11 2 2807.73 2820.29 52.12 o 1 11 2 1598.92 1584.89 26.25 o 2 11 2 2756.85 2702.20 49.61 o 3 11 2 775.29 735.80 14.62 o 4 11 2 509.45 475.18 18.77 o -4 12 2 429.07 412.39 8.89 o -3 12 2 581.16 590.72 14.26 o -2 12 2 1120.96 1063.14 20.68 o -1 12 2 679.00 670.92 15.70 o 0 12 2 529.75 482.51 9.73 o 1 12 2 58.86 56.05 2.63 o 2 12 2 3.51 6.29 1.39 o 3 12 2 80.40 88.22 4.32 o 4 12 2 195.18 193.09 5.99 o -4 13 2 7.21 6.43 1.81 o -3 13 2 0.78 1.02 1.70 o -2 13 2 69.76 75.00 3.41 o -1 13 2 306.50 330.74 10.31 o 0 13 2 388.06 372.10 8.32 o 1 13 2 839.71 827.88 18.76 o 2 13 2 389.59 375.19 8.15 o 3 13 2 346.93 318.72 9.59 o 4 13 2 115.24 110.70 4.61 o -3 14 2 124.90 115.48 5.58 o -2 14 2 167.32 157.18 6.74 o -1 14 2 156.70 146.20 4.98 o 0 14 2 90.88 90.09 3.49 o 1 14 2 22.80 17.94 2.08 o 2 14 2 0.80 1.60 1.83 o 3 14 2 13.82 14.09 2.43 o -3 15 2 0.25 -2.35 2.55 o -2 15 2 0.55 1.49 3.33 o -1 15 2 0.54 -1.79 1.79 o 0 15 2 65.43 59.20 4.27 o 1 15 2 1.42 -0.06 3.38 o 2 15 2 90.84 79.01 3.99 o 3 15 2 2.52 -0.94 2.67 o -2 16 2 9.80 6.60 2.99 o -1 16 2 0.23 -2.34 2.34 o 0 16 2 11.23 10.10 3.67 o 1 16 2 0.14 -1.04 2.81 o 2 16 2 1.36 3.50 2.76 o 0 17 2 27.41 34.80 5.17 o -6 1 3 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19.55 6.43 o 0 1 12 2.90 5.78 3.28 o 1 1 12 130.95 127.28 6.92 o 2 1 12 141.90 137.18 7.14 o -2 2 12 262.24 268.15 10.17 o -1 2 12 358.93 363.18 12.40 o 0 2 12 467.09 502.74 15.77 o 1 2 12 521.53 573.37 25.46 o 2 2 12 210.55 235.88 9.41 o -2 3 12 46.60 50.69 4.67 o -1 3 12 52.96 71.74 5.45 o 0 3 12 0.04 0.30 3.12 o 1 3 12 4.83 -0.10 2.47 o 2 3 12 71.88 69.77 4.49 o -2 4 12 9.96 9.45 3.28 o -1 4 12 79.70 75.08 5.54 o 0 4 12 87.68 95.67 5.93 o 1 4 12 81.15 87.46 4.87 o 2 4 12 93.11 107.66 6.66 o -1 5 12 15.34 12.89 3.53 o 0 5 12 22.95 25.00 3.97 o 1 5 12 6.42 5.78 2.82 o -1 6 12 46.80 59.99 5.16 o 0 6 12 10.15 15.62 4.48 o 1 6 12 3.05 3.06 2.31 o 0 1 13 10.47 12.95 3.97 o