#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016819.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016819_Fobs loop_ _publ_author_name 'Qiao, Qian' 'Zhao, Ya-Juan' 'Tang, Tian-Di' _publ_section_title ; A six-connected \a-polonium net based on tetranuclear Cd^II^ nodes ; _journal_coeditor_code SQ3163 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m336 _journal_page_last m338 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.783 _cell_angle_gamma 90.000 _cell_length_a 10.1619 _cell_length_b 18.0401 _cell_length_c 24.1602 _exptl_crystal_F_000 2224.00 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file sq3163Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Tang in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 470.61 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 54436.05 55558.54 3031.10 o 3 0 0 31.38 10.14 18.69 o 4 0 0 798.49 710.59 57.61 o 5 0 0 49220.18 51087.39 692.89 o 6 0 0 14748.88 14155.12 204.26 o 7 0 0 13953.24 14403.68 244.36 o 8 0 0 6696.04 6272.92 128.48 o 9 0 0 499.03 537.51 61.38 o 10 0 0 242.08 268.45 68.21 o 11 0 0 0.88 -13.62 48.45 o 12 0 0 24.70 -20.43 58.44 o 13 0 0 70.25 153.31 75.84 o 2 1 0 54185.20 55954.00 488.92 o 3 1 0 31450.31 32000.46 309.83 o 4 1 0 18898.36 18427.25 181.01 o 5 1 0 19003.86 18701.98 179.14 o 6 1 0 3440.58 3431.51 60.74 o 7 1 0 1220.51 1220.71 39.43 o 8 1 0 106.36 285.08 57.25 o 9 1 0 1445.48 1480.56 50.39 o 10 1 0 247.79 319.34 49.41 o 11 1 0 251.30 355.41 61.09 o 12 1 0 198.51 266.83 102.01 o 13 1 0 184.31 184.04 53.78 o 1 2 0 3009.86 3659.03 50.91 o 2 2 0 39168.23 42332.92 362.60 o 3 2 0 5198.88 4963.89 47.78 o 4 2 0 22826.71 22657.44 214.66 o 5 2 0 4612.42 4446.66 59.56 o 6 2 0 56.97 76.87 20.13 o 7 2 0 1891.61 1867.42 53.48 o 8 2 0 6728.00 6441.21 98.54 o 9 2 0 4184.74 4322.22 99.54 o 10 2 0 6599.31 6431.34 101.75 o 11 2 0 3096.86 2981.53 96.42 o 12 2 0 906.45 949.00 58.81 o 13 2 0 4.34 -11.89 41.80 o 1 3 0 15111.44 14819.30 120.43 o 2 3 0 48359.92 51537.02 501.61 o 3 3 0 629.58 612.92 22.62 o 4 3 0 4399.91 4267.98 49.38 o 5 3 0 5730.24 5440.13 69.20 o 6 3 0 10161.71 9581.13 108.26 o 7 3 0 13984.89 13765.10 145.13 o 8 3 0 5297.03 5356.86 85.60 o 9 3 0 770.82 796.63 87.74 o 10 3 0 0.10 35.59 35.18 o 11 3 0 175.02 402.65 69.53 o 12 3 0 1511.25 1592.39 83.50 o 13 3 0 1637.45 1672.36 80.69 o 0 4 0 11789.47 10924.80 149.56 o 1 4 0 40697.65 42316.38 453.27 o 2 4 0 1865.62 2078.01 30.92 o 3 4 0 12966.09 13667.80 131.37 o 4 4 0 2923.56 2996.74 54.58 o 5 4 0 2299.78 2431.79 44.99 o 6 4 0 3825.83 3947.14 72.48 o 7 4 0 3487.27 3434.74 65.88 o 8 4 0 5414.99 5029.48 82.35 o 9 4 0 2839.27 2684.46 72.89 o 10 4 0 1377.22 1352.57 113.81 o 11 4 0 370.30 562.56 94.55 o 12 4 0 24.60 12.13 39.50 o 1 5 0 143.41 236.15 23.45 o 2 5 0 28112.03 27227.04 344.55 o 3 5 0 52792.75 54517.86 554.02 o 4 5 0 37413.17 38206.32 392.15 o 5 5 0 10119.57 9830.75 113.11 o 6 5 0 800.24 809.39 42.89 o 7 5 0 1386.64 1413.29 54.15 o 8 5 0 2137.22 2196.34 68.56 o 9 5 0 2920.47 3071.57 90.88 o 10 5 0 1704.99 1770.99 70.94 o 11 5 0 274.27 227.62 48.05 o 12 5 0 12.22 -15.25 47.95 o 0 6 0 30362.19 28893.07 466.02 o 1 6 0 16235.33 15689.50 167.55 o 2 6 0 16092.04 16993.63 190.25 o 3 6 0 4141.10 4256.06 49.64 o 4 6 0 2053.74 1995.74 41.88 o 5 6 0 3143.81 3082.51 63.87 o 6 6 0 1879.05 1992.61 65.32 o 7 6 0 2343.60 2396.01 150.24 o 8 6 0 2006.57 2111.82 85.54 o 9 6 0 472.78 514.75 53.34 o 10 6 0 5.64 34.98 37.37 o 11 6 0 3.99 6.52 39.80 o 12 6 0 17.41 -25.97 45.45 o 1 7 0 24.23 4.04 17.49 o 2 7 0 568.83 716.74 31.14 o 3 7 0 477.58 598.99 47.50 o 4 7 0 6563.42 6899.00 83.43 o 5 7 0 1070.88 1059.50 44.24 o 6 7 0 5300.44 5342.63 73.34 o 7 7 0 4976.96 4886.35 100.97 o 8 7 0 4434.50 4427.48 99.08 o 9 7 0 343.22 344.06 48.79 o 10 7 0 0.32 -19.13 44.24 o 11 7 0 299.18 321.33 54.04 o 12 7 0 525.97 652.48 62.80 o 0 8 0 2748.65 3087.58 101.33 o 1 8 0 323.63 338.62 24.37 o 2 8 0 479.33 495.94 25.44 o 3 8 0 606.17 697.15 46.65 o 4 8 0 796.12 791.17 48.37 o 5 8 0 6707.72 6827.23 81.96 o 6 8 0 1479.29 1551.91 77.44 o 7 8 0 31.94 54.68 54.07 o 8 8 0 764.29 830.26 64.70 o 9 8 0 4028.67 4154.67 115.86 o 10 8 0 3750.19 3946.74 160.87 o 11 8 0 1393.00 1445.60 78.57 o 12 8 0 370.29 382.82 64.80 o 1 9 0 873.19 959.29 45.11 o 2 9 0 1829.57 2007.39 65.44 o 3 9 0 3278.39 3344.12 98.20 o 4 9 0 5303.13 5409.39 97.47 o 5 9 0 1506.45 1428.37 64.67 o 6 9 0 3072.32 3107.97 60.50 o 7 9 0 1704.61 1815.22 44.87 o 8 9 0 1398.35 1355.38 61.46 o 9 9 0 2.57 31.25 32.91 o 10 9 0 22.27 -10.60 32.92 o 11 9 0 836.30 990.69 58.94 o 12 9 0 597.19 694.45 61.42 o 0 10 0 18610.80 17674.59 482.11 o 1 10 0 22891.74 22052.61 262.14 o 2 10 0 3033.18 2692.82 46.09 o 3 10 0 112.50 127.83 27.63 o 4 10 0 1136.88 1079.61 43.58 o 5 10 0 5217.71 5138.33 82.62 o 6 10 0 5184.35 4963.64 82.53 o 7 10 0 3241.87 3113.23 53.52 o 8 10 0 297.22 444.38 56.67 o 9 10 0 348.43 466.19 69.06 o 10 10 0 43.47 178.96 38.12 o 11 10 0 22.32 19.94 35.79 o 1 11 0 927.50 1003.12 55.20 o 2 11 0 2779.13 2604.78 58.57 o 3 11 0 5973.14 5828.70 85.02 o 4 11 0 2950.83 2994.39 68.96 o 5 11 0 384.39 435.95 69.40 o 6 11 0 874.18 791.51 44.43 o 7 11 0 852.00 787.35 40.31 o 8 11 0 907.04 753.24 55.90 o 9 11 0 30.37 21.54 30.37 o 10 11 0 17.68 -7.50 30.32 o 11 11 0 80.69 91.05 54.56 o 0 12 0 8333.14 8973.84 175.43 o 1 12 0 1.11 31.16 37.58 o 2 12 0 1072.60 1002.49 55.98 o 3 12 0 559.57 651.05 52.53 o 4 12 0 2139.49 2168.33 50.36 o 5 12 0 375.57 360.06 42.62 o 6 12 0 58.79 76.08 25.57 o 7 12 0 49.27 40.00 36.46 o 8 12 0 32.04 43.01 40.54 o 9 12 0 254.58 250.41 57.64 o 10 12 0 60.72 73.42 48.00 o 11 12 0 361.91 289.83 60.81 o 1 13 0 26.32 10.22 49.72 o 2 13 0 494.91 539.71 39.53 o 3 13 0 980.79 953.55 68.13 o 4 13 0 288.08 294.48 31.55 o 5 13 0 69.49 63.26 34.88 o 6 13 0 623.38 691.67 35.27 o 7 13 0 1225.05 1339.66 59.67 o 8 13 0 840.44 886.48 87.58 o 9 13 0 1078.68 1075.30 103.53 o 10 13 0 85.42 80.86 50.22 o 0 14 0 1.86 25.81 78.23 o 1 14 0 0.03 -24.95 36.08 o 2 14 0 42.15 23.91 35.68 o 3 14 0 7.28 26.72 27.16 o 4 14 0 2.39 46.01 35.50 o 5 14 0 956.68 950.90 62.34 o 6 14 0 33.83 23.33 28.00 o 7 14 0 377.98 421.81 41.96 o 8 14 0 232.57 160.72 66.64 o 9 14 0 304.87 243.05 50.57 o 10 14 0 873.48 954.17 84.61 o 1 15 0 620.07 680.48 66.28 o 2 15 0 2308.01 2580.12 107.56 o 3 15 0 1345.77 1401.91 64.64 o 4 15 0 320.88 333.38 42.72 o 5 15 0 1891.84 1816.46 57.15 o 6 15 0 60.68 100.90 40.18 o 7 15 0 4.72 27.39 28.18 o 8 15 0 195.41 206.07 47.94 o 9 15 0 177.33 318.21 144.48 o 10 15 0 159.93 157.78 56.64 o 0 16 0 1284.85 1256.95 85.68 o 1 16 0 836.18 929.90 55.86 o 2 16 0 910.94 954.45 62.25 o 3 16 0 36.61 9.82 24.66 o 4 16 0 289.12 230.23 43.46 o 5 16 0 461.76 568.88 69.59 o 6 16 0 513.69 578.42 73.73 o 7 16 0 235.10 305.19 57.58 o 8 16 0 3.31 -25.67 43.83 o 9 16 0 144.22 70.56 63.40 o 1 17 0 26.66 55.51 37.54 o 2 17 0 24.32 12.62 24.71 o 3 17 0 211.29 288.17 61.44 o 4 17 0 34.76 36.63 36.06 o 5 17 0 143.92 156.23 42.10 o 6 17 0 102.40 73.79 40.39 o 7 17 0 10.93 33.09 36.22 o 8 17 0 20.01 1.68 48.47 o 9 17 0 199.78 230.87 62.68 o 0 18 0 912.16 714.26 194.97 o 1 18 0 417.14 413.94 123.08 o 2 18 0 16.11 36.60 28.33 o 3 18 0 5.34 10.95 35.24 o 4 18 0 602.60 671.63 54.13 o 5 18 0 752.04 706.42 107.02 o 6 18 0 397.36 269.72 43.08 o 7 18 0 202.33 177.02 47.71 o 8 18 0 42.83 22.97 55.19 o 1 19 0 96.66 150.28 58.75 o 2 19 0 26.02 2.83 34.85 o 3 19 0 16.83 50.72 42.39 o 4 19 0 29.73 82.91 69.64 o 5 19 0 18.95 7.72 27.58 o 6 19 0 96.10 147.03 45.61 o 7 19 0 239.08 232.01 57.42 o 0 20 0 0.81 -57.31 100.44 o 1 20 0 2.65 68.20 50.34 o 2 20 0 19.02 99.43 48.64 o 3 20 0 155.71 125.04 39.07 o 4 20 0 1.21 -12.59 30.41 o 5 20 0 74.44 104.62 83.11 o 6 20 0 40.52 9.79 42.83 o 1 21 0 4.54 46.63 54.74 o 2 21 0 76.06 43.58 34.39 o 3 21 0 185.91 161.71 51.17 o 4 21 0 1.32 -15.29 65.16 o 5 21 0 3.16 39.12 63.50 o 0 22 0 0.97 32.96 117.68 o 1 22 0 2.18 -5.29 57.05 o 2 22 0 26.08 46.05 41.78 o 3 22 0 27.56 110.35 82.24 o 4 22 0 12.09 -33.18 79.96 o 1 23 0 22.42 32.14 38.96 o 2 23 0 125.39 35.66 70.38 o -13 1 1 211.31 188.97 58.83 o -12 1 1 519.18 643.71 54.19 o -11 1 1 626.89 716.83 55.46 o -10 1 1 445.14 514.27 47.21 o -9 1 1 9.15 16.67 31.31 o -8 1 1 691.78 744.64 38.88 o -7 1 1 3675.00 3582.39 64.48 o -6 1 1 4880.13 5214.42 66.39 o -5 1 1 7671.70 7720.28 81.61 o -4 1 1 10496.93 10211.91 95.83 o -3 1 1 4.10 40.09 13.09 o -2 1 1 14555.17 15200.48 114.50 o 2 1 1 13064.70 13248.87 122.21 o 3 1 1 5459.40 5652.32 59.91 o 4 1 1 5766.83 5155.47 70.10 o 5 1 1 19540.61 20239.89 211.37 o 6 1 1 2127.22 1960.66 46.19 o 7 1 1 40.48 55.54 27.26 o 8 1 1 1587.33 1651.84 55.22 o 9 1 1 2055.84 2000.24 58.21 o 10 1 1 305.41 506.34 70.15 o 11 1 1 638.26 751.52 57.73 o 12 1 1 31.05 21.81 36.60 o 13 1 1 39.30 -2.22 42.66 o -13 2 1 260.10 296.33 59.94 o -12 2 1 111.86 287.74 79.82 o -11 2 1 9.83 75.61 45.82 o -10 2 1 251.91 345.76 48.10 o -9 2 1 3064.99 2954.44 67.99 o -8 2 1 6189.40 5816.99 91.19 o -7 2 1 2788.98 2870.03 65.17 o -6 2 1 702.56 848.95 35.44 o -5 2 1 554.03 638.19 25.94 o -4 2 1 33.00 62.37 16.98 o -3 2 1 2887.89 2792.20 35.73 o -2 2 1 31653.72 33996.95 277.88 o -1 2 1 735.57 808.84 19.68 o 1 2 1 3240.80 2834.17 32.48 o 2 2 1 12743.40 13376.55 122.69 o 3 2 1 404.89 354.61 25.69 o 4 2 1 176.51 231.35 20.24 o 5 2 1 2808.56 2863.95 47.84 o 6 2 1 621.65 584.35 40.35 o 7 2 1 5747.48 5667.73 78.53 o 8 2 1 2435.16 2379.18 63.54 o 9 2 1 995.02 1068.74 119.04 o 10 2 1 60.38 170.18 78.59 o 11 2 1 435.01 485.60 71.96 o 12 2 1 588.31 744.22 57.11 o 13 2 1 432.36 523.61 60.87 o -13 3 1 36.94 28.07 41.10 o -12 3 1 58.45 82.35 53.69 o -11 3 1 168.31 203.41 44.42 o -10 3 1 285.60 327.51 53.56 o -9 3 1 174.53 293.55 58.26 o -8 3 1 64.67 110.99 46.41 o -7 3 1 139.79 254.56 37.46 o -6 3 1 4351.11 4329.55 65.06 o -5 3 1 241.59 236.38 21.99 o -4 3 1 297.13 396.82 23.88 o -3 3 1 4563.90 4802.19 72.43 o -2 3 1 8818.95 10163.27 96.38 o -1 3 1 48579.36 50108.74 472.13 o 0 3 1 1223.96 1108.11 19.59 o 1 3 1 4498.15 4552.20 47.14 o 2 3 1 11829.64 12520.02 111.35 o 3 3 1 265.58 281.78 15.51 o 4 3 1 19731.69 19994.66 200.80 o 5 3 1 8887.79 8671.05 106.34 o 6 3 1 2144.09 1984.13 44.75 o 7 3 1 1164.66 1208.26 84.02 o 8 3 1 0.51 62.92 32.58 o 9 3 1 304.20 347.13 58.70 o 10 3 1 1790.66 1910.25 85.60 o 11 3 1 598.92 780.57 55.90 o 12 3 1 204.89 121.51 59.72 o 13 3 1 16.30 16.00 62.24 o -12 4 1 162.60 157.71 46.80 o -11 4 1 168.14 253.15 51.83 o -10 4 1 1939.31 1948.81 66.63 o -9 4 1 3177.74 3112.16 92.01 o -8 4 1 1248.58 1280.53 51.58 o -7 4 1 46.08 76.92 28.50 o -6 4 1 1502.89 1536.23 44.30 o -5 4 1 13955.69 14258.64 132.76 o -4 4 1 49666.55 52690.05 547.81 o -3 4 1 37394.39 40246.92 508.47 o -2 4 1 303.68 260.53 36.93 o -1 4 1 603.41 766.87 32.83 o 0 4 1 27333.74 27597.22 289.30 o 1 4 1 68923.75 71362.30 831.48 o 2 4 1 221470.67 240438.66 3585.19 o 3 4 1 36908.83 36787.76 357.51 o 4 4 1 8713.11 8893.07 96.15 o 5 4 1 1954.24 2080.26 50.22 o 6 4 1 1284.07 1293.39 48.39 o 7 4 1 3421.56 3288.15 77.63 o 8 4 1 3872.19 3641.08 75.71 o 9 4 1 5273.70 5129.69 150.99 o 10 4 1 773.90 799.85 62.77 o 11 4 1 6.54 29.91 42.60 o 12 4 1 61.91 33.34 39.13 o -12 5 1 111.11 164.83 68.70 o -11 5 1 8.53 -3.31 44.11 o -10 5 1 16.25 -4.31 34.99 o -9 5 1 475.00 434.43 53.01 o -8 5 1 104.62 102.96 33.68 o -7 5 1 90.64 112.54 30.61 o -6 5 1 613.47 735.24 48.59 o -5 5 1 1073.91 1039.26 34.74 o -4 5 1 156.98 81.87 23.03 o -3 5 1 2059.64 2171.12 39.19 o -2 5 1 13.36 5.23 19.64 o -1 5 1 15988.98 15525.46 155.80 o 0 5 1 22152.75 21534.94 224.41 o 1 5 1 776.56 721.13 37.86 o 2 5 1 5013.33 5123.10 67.96 o 3 5 1 20814.80 21656.56 215.27 o 4 5 1 3960.63 3780.40 57.40 o 5 5 1 7159.88 7151.04 94.30 o 6 5 1 2656.62 2636.28 64.01 o 7 5 1 1160.92 1087.49 49.82 o 8 5 1 211.21 248.47 52.08 o 9 5 1 114.31 145.24 47.16 o 10 5 1 85.11 65.92 37.22 o 11 5 1 83.25 117.02 46.00 o 12 5 1 0.17 -14.46 60.13 o -12 6 1 116.93 163.81 51.05 o -11 6 1 0.39 -3.18 42.21 o -10 6 1 887.83 757.39 52.53 o -9 6 1 1736.48 1533.40 64.18 o -8 6 1 3993.87 3730.91 84.59 o -7 6 1 2153.33 2202.20 79.90 o -6 6 1 962.29 937.62 36.28 o -5 6 1 88.39 90.06 20.98 o -4 6 1 4006.18 4029.00 65.21 o -3 6 1 7823.73 7920.33 92.18 o -2 6 1 145.70 127.71 19.17 o -1 6 1 2887.03 2971.09 47.38 o 0 6 1 1316.49 1126.62 46.13 o 1 6 1 2867.60 3020.65 46.31 o 2 6 1 5.03 3.98 12.14 o 3 6 1 264.32 382.26 20.36 o 4 6 1 9972.88 11777.84 129.54 o 5 6 1 208.30 232.78 22.22 o 6 6 1 2644.20 2798.58 69.22 o 7 6 1 3575.98 3339.40 81.24 o 8 6 1 318.03 322.74 45.70 o 9 6 1 96.98 62.29 38.28 o 10 6 1 244.37 181.73 55.20 o 11 6 1 481.71 628.80 71.14 o 12 6 1 765.72 793.05 73.47 o -12 7 1 507.46 546.90 104.56 o -11 7 1 1281.76 1368.60 79.92 o -10 7 1 1446.99 1482.89 66.53 o -9 7 1 3858.13 3864.78 98.10 o -8 7 1 406.25 440.01 46.48 o -7 7 1 144.88 103.79 28.78 o -6 7 1 2686.40 2646.30 95.77 o -5 7 1 6863.69 6606.27 126.06 o -4 7 1 4396.62 4043.13 50.88 o -3 7 1 71.38 56.52 19.70 o -2 7 1 8863.06 9690.19 96.59 o -1 7 1 484.79 458.52 23.74 o 0 7 1 2143.56 2096.35 44.44 o 1 7 1 6716.78 6924.22 90.49 o 2 7 1 2840.97 2979.83 64.30 o 3 7 1 1697.88 1866.06 48.61 o 4 7 1 9256.02 9668.76 100.34 o 5 7 1 843.22 918.66 34.13 o 6 7 1 171.76 239.99 33.16 o 7 7 1 1254.55 1411.74 73.65 o 8 7 1 3381.02 3376.92 110.35 o 9 7 1 4927.04 4664.19 93.37 o 10 7 1 1771.17 1650.26 122.82 o 11 7 1 422.24 413.27 60.95 o 12 7 1 21.32 77.49 53.41 o -12 8 1 179.20 136.81 53.15 o -11 8 1 82.24 95.39 47.85 o -10 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