#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016832.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016832_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Kubiak, Maria' _publ_section_title ; Products of the oxidation of 1-(diaminomethylene)thiourea with hydrogen peroxide ; _journal_coeditor_code GD3250 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o609 _journal_page_last o612 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.400 _cell_angle_gamma 90.000 _cell_length_a 3.9230 _cell_length_b 10.7010 _cell_length_c 10.7540 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7455 _[local]_cod_data_source_file gd3250Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MK67 in P2(1)/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 92.48 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1068.69 994.22 3.15 o 4 0 0 77.10 78.13 3.74 o 1 1 0 4467.92 4735.73 21.97 o 2 1 0 22.93 32.77 0.77 o 3 1 0 3.58 3.34 1.15 o 4 1 0 106.31 98.51 4.98 o 5 1 0 26.21 23.34 3.80 o 0 2 0 1.42 4.01 1.49 o 1 2 0 8552.81 8625.70 24.69 o 2 2 0 2457.14 2531.95 9.77 o 3 2 0 63.41 61.52 2.24 o 4 2 0 0.05 1.08 2.27 o 5 2 0 66.95 58.67 6.17 o 1 3 0 717.42 720.04 4.88 o 2 3 0 1757.20 1789.77 7.28 o 3 3 0 81.04 86.65 2.32 o 4 3 0 412.31 436.57 5.23 o 0 4 0 32.07 36.24 1.30 o 1 4 0 839.36 809.77 6.62 o 2 4 0 369.76 399.03 3.68 o 3 4 0 399.97 399.50 6.90 o 4 4 0 361.34 352.54 4.85 o 1 5 0 99.92 89.37 3.12 o 2 5 0 86.30 84.19 1.44 o 3 5 0 1893.21 1896.62 12.45 o 4 5 0 42.97 34.03 4.65 o 0 6 0 67.76 79.94 3.28 o 1 6 0 191.34 175.18 2.35 o 2 6 0 64.48 62.83 1.58 o 3 6 0 288.60 279.33 5.77 o 4 6 0 240.53 214.57 6.25 o 1 7 0 371.17 372.12 3.60 o 2 7 0 405.93 391.07 4.20 o 3 7 0 66.79 68.95 4.19 o 4 7 0 57.61 62.13 5.98 o 0 8 0 0.63 1.20 1.60 o 1 8 0 778.68 740.49 15.03 o 2 8 0 385.84 383.27 5.74 o 3 8 0 3.51 5.02 3.69 o 4 8 0 2.32 2.50 3.84 o 1 9 0 86.13 84.42 1.88 o 2 9 0 21.22 22.08 2.56 o 3 9 0 79.00 64.78 4.28 o 0 10 0 1338.45 1331.14 24.25 o 1 10 0 28.05 24.99 1.89 o 2 10 0 93.59 98.15 2.65 o 3 10 0 5.73 3.80 4.34 o 1 11 0 87.04 83.62 2.25 o 2 11 0 55.10 59.04 2.27 o 3 11 0 7.18 7.78 4.96 o 0 12 0 115.60 112.74 6.87 o 1 12 0 52.69 49.31 2.29 o 2 12 0 161.21 170.08 3.02 o 1 13 0 8.31 8.08 2.24 o 2 13 0 180.85 176.31 7.41 o 0 14 0 58.34 58.64 6.09 o -5 0 1 19.44 19.36 4.93 o -3 0 1 292.86 309.48 5.12 o -1 0 1 3058.18 3207.27 16.83 o 1 0 1 2891.36 3078.29 5.61 o 3 0 1 157.48 158.27 2.91 o 5 0 1 135.54 125.17 6.17 o -5 1 1 230.54 254.73 4.82 o -4 1 1 71.11 65.76 3.08 o -3 1 1 476.53 448.61 6.00 o -2 1 1 2.35 1.66 0.64 o -1 1 1 53.36 42.10 0.62 o 1 1 1 1.92 2.68 0.54 o 2 1 1 5.01 5.21 0.85 o 3 1 1 204.25 190.89 2.14 o 4 1 1 3.14 3.04 1.81 o -5 2 1 29.49 26.41 3.30 o -4 2 1 49.37 45.21 2.92 o -3 2 1 551.16 548.32 4.07 o -2 2 1 71.19 67.09 0.98 o -1 2 1 2507.89 2577.42 10.78 o 0 2 1 2621.69 2683.58 26.85 o 1 2 1 1548.20 1600.55 8.23 o 2 2 1 142.78 150.31 1.22 o 3 2 1 10.81 9.44 1.20 o 4 2 1 10.59 9.30 2.64 o -4 3 1 198.80 190.93 3.82 o -3 3 1 29.85 26.04 1.64 o -2 3 1 223.14 219.14 2.74 o -1 3 1 1014.17 1058.46 6.42 o 0 3 1 149.47 129.22 1.69 o 1 3 1 238.46 221.41 1.07 o 2 3 1 23.45 30.66 0.82 o 3 3 1 278.41 272.20 5.57 o 4 3 1 143.32 144.03 3.64 o -4 4 1 127.37 137.32 5.67 o -3 4 1 123.94 120.21 2.88 o -2 4 1 2556.17 2717.13 9.06 o -1 4 1 207.01 207.43 2.26 o 0 4 1 1148.29 1130.49 7.25 o 1 4 1 7.06 1.75 0.75 o 2 4 1 388.91 376.27 1.98 o 3 4 1 133.08 127.06 7.49 o 4 4 1 23.39 21.57 4.55 o -4 5 1 106.94 106.20 4.71 o -3 5 1 87.60 89.70 2.71 o -2 5 1 455.05 427.62 2.54 o -1 5 1 488.89 553.81 5.54 o 0 5 1 248.65 281.89 2.57 o 1 5 1 195.61 199.31 2.23 o 2 5 1 556.51 563.58 5.73 o 3 5 1 373.95 374.81 6.55 o 4 5 1 297.04 312.43 6.49 o -4 6 1 221.17 210.19 5.88 o -3 6 1 249.93 248.56 3.57 o -2 6 1 245.73 214.50 4.39 o -1 6 1 358.95 388.31 5.22 o 0 6 1 1400.30 1391.32 4.58 o 1 6 1 20.74 18.36 1.12 o 2 6 1 83.24 71.31 1.67 o 3 6 1 11.24 14.90 3.71 o 4 6 1 150.02 144.76 4.94 o -4 7 1 396.87 413.54 8.20 o -3 7 1 205.72 194.82 3.35 o -2 7 1 47.72 41.53 1.65 o -1 7 1 40.11 34.00 1.57 o 0 7 1 506.76 519.44 3.46 o 1 7 1 171.51 171.28 2.07 o 2 7 1 784.29 805.33 4.23 o 3 7 1 237.32 228.64 5.34 o 4 7 1 418.58 431.28 7.97 o -4 8 1 22.38 17.46 5.07 o -3 8 1 47.74 48.52 3.41 o -2 8 1 144.31 129.10 2.34 o -1 8 1 120.16 110.68 2.37 o 0 8 1 81.49 66.31 2.67 o 1 8 1 102.42 98.89 2.13 o 2 8 1 809.75 804.81 8.55 o 3 8 1 32.00 36.49 4.90 o 4 8 1 0.65 3.63 4.68 o -3 9 1 68.84 62.40 3.04 o -2 9 1 3.23 3.74 1.52 o -1 9 1 21.54 20.03 1.53 o 0 9 1 169.03 166.18 3.43 o 1 9 1 948.34 964.96 20.59 o 2 9 1 112.00 111.27 2.99 o 3 9 1 118.20 127.71 5.08 o -3 10 1 29.13 25.26 3.10 o -2 10 1 14.47 13.65 1.96 o -1 10 1 198.47 192.97 2.48 o 0 10 1 559.85 552.89 3.74 o 1 10 1 511.38 496.66 4.19 o 2 10 1 6.14 6.67 1.71 o 3 10 1 103.13 107.30 5.63 o -3 11 1 148.78 163.99 4.55 o -2 11 1 4.85 3.18 1.65 o -1 11 1 172.60 172.43 2.58 o 0 11 1 62.64 63.42 2.04 o 1 11 1 10.74 10.71 1.80 o 2 11 1 10.34 10.15 2.45 o 3 11 1 376.33 383.38 7.61 o -2 12 1 84.78 89.12 2.76 o -1 12 1 694.80 706.99 12.91 o 0 12 1 162.24 165.33 3.63 o 1 12 1 302.11 315.62 3.34 o 2 12 1 7.33 5.62 2.37 o -2 13 1 9.13 3.53 3.37 o -1 13 1 121.25 125.72 3.11 o 0 13 1 1.97 2.25 1.95 o 1 13 1 128.80 130.21 3.58 o 2 13 1 10.14 9.49 2.91 o -1 14 1 92.42 112.27 6.46 o 0 14 1 51.80 57.23 5.80 o -4 0 2 631.56 642.01 8.34 o -2 0 2 364.40 346.56 4.30 o 2 0 2 181.86 194.97 2.46 o 4 0 2 45.79 42.04 3.01 o -5 1 2 5.43 3.99 2.62 o -4 1 2 276.58 278.68 4.12 o -3 1 2 318.61 317.31 2.18 o -2 1 2 325.04 306.60 1.76 o -1 1 2 62.45 76.00 0.77 o 0 1 2 10.35 7.91 0.47 o 1 1 2 1128.27 1144.11 9.98 o 2 1 2 402.96 372.67 3.97 o 3 1 2 136.87 138.15 1.91 o 4 1 2 383.14 389.17 3.43 o -5 2 2 45.13 46.08 3.76 o -4 2 2 17.08 16.14 2.35 o -3 2 2 222.70 232.61 1.91 o -2 2 2 1368.80 1443.41 8.58 o -1 2 2 474.61 456.78 2.67 o 0 2 2 0.18 0.47 0.52 o 1 2 2 8.65 10.65 0.75 o 2 2 2 584.78 600.31 4.12 o 3 2 2 82.09 77.82 1.53 o 4 2 2 65.50 61.42 2.62 o -5 3 2 195.58 195.86 6.74 o -4 3 2 90.53 91.14 3.56 o -3 3 2 54.12 48.01 1.34 o -2 3 2 0.02 0.86 0.65 o -1 3 2 973.78 1086.60 7.33 o 0 3 2 861.34 822.40 6.67 o 1 3 2 843.74 868.64 4.04 o 2 3 2 719.43 700.40 8.78 o 3 3 2 68.55 61.90 2.29 o 4 3 2 275.06 291.93 6.78 o -4 4 2 55.76 44.02 3.20 o -3 4 2 275.06 282.74 3.46 o -2 4 2 0.26 1.19 0.75 o -1 4 2 343.00 356.99 2.56 o 0 4 2 1342.18 1409.95 8.74 o 1 4 2 224.14 213.84 1.72 o 2 4 2 8.95 5.99 0.70 o 3 4 2 0.03 0.29 1.33 o 4 4 2 256.25 260.08 6.09 o -4 5 2 1.50 1.28 3.29 o -3 5 2 340.74 336.48 3.29 o -2 5 2 86.28 90.49 1.65 o -1 5 2 351.26 338.41 3.48 o 0 5 2 43.41 49.72 0.69 o 1 5 2 305.14 282.43 3.36 o 2 5 2 65.32 58.99 2.27 o 3 5 2 1415.00 1477.47 11.07 o 4 5 2 1.63 2.70 3.27 o -4 6 2 2.07 2.51 4.10 o -3 6 2 213.96 209.09 3.37 o -2 6 2 116.96 112.91 1.77 o -1 6 2 1041.47 1051.68 8.42 o 0 6 2 2.91 6.10 0.64 o 1 6 2 353.60 348.14 2.48 o 2 6 2 265.91 255.19 7.39 o 3 6 2 172.27 178.84 4.78 o 4 6 2 28.97 22.10 4.31 o -4 7 2 88.94 84.41 5.33 o -3 7 2 11.73 11.39 2.08 o -2 7 2 3.65 4.84 1.33 o -1 7 2 0.05 0.74 0.75 o 0 7 2 1.10 4.25 1.09 o 1 7 2 796.14 810.61 7.23 o 2 7 2 351.26 358.53 4.47 o 3 7 2 113.63 114.77 5.47 o 4 7 2 50.27 52.47 5.23 o -4 8 2 2.03 3.32 3.90 o -3 8 2 350.46 347.31 6.11 o -2 8 2 240.72 246.85 5.06 o -1 8 2 568.75 547.37 5.85 o 0 8 2 20.02 20.89 1.46 o 1 8 2 889.61 864.92 17.33 o 2 8 2 161.82 168.22 5.59 o 3 8 2 19.24 18.21 3.65 o 4 8 2 10.17 8.77 4.14 o -3 9 2 23.80 27.74 2.97 o -2 9 2 34.28 33.61 2.09 o -1 9 2 91.17 91.47 1.90 o 0 9 2 208.76 203.21 4.62 o 1 9 2 4.86 4.35 1.35 o 2 9 2 132.42 130.01 3.08 o 3 9 2 110.92 112.05 5.71 o -3 10 2 52.88 53.26 2.94 o -2 10 2 287.55 290.21 3.45 o -1 10 2 241.39 236.24 4.41 o 0 10 2 878.48 876.36 9.11 o 1 10 2 45.46 42.75 1.85 o 2 10 2 117.56 118.29 3.33 o 3 10 2 26.25 26.39 4.86 o -3 11 2 23.07 24.44 4.06 o -2 11 2 0.23 2.44 1.67 o -1 11 2 11.07 9.29 1.58 o 0 11 2 58.74 58.71 2.43 o 1 11 2 7.00 7.83 1.79 o 2 11 2 274.55 279.24 6.09 o 3 11 2 0.01 5.36 3.51 o -2 12 2 511.48 550.22 5.05 o -1 12 2 28.02 24.82 2.37 o 0 12 2 387.79 389.49 3.96 o 1 12 2 12.24 12.05 1.81 o 2 12 2 160.56 174.83 4.86 o -2 13 2 2.64 0.88 3.78 o -1 13 2 0.66 1.57 2.04 o 0 13 2 31.92 30.45 2.35 o 1 13 2 53.83 52.04 2.54 o 2 13 2 91.99 87.89 6.05 o -5 0 3 96.66 87.32 6.22 o -3 0 3 269.88 265.33 3.80 o -1 0 3 298.55 289.11 1.70 o 1 0 3 245.05 214.26 1.60 o 3 0 3 171.45 166.14 2.93 o -5 1 3 117.77 120.56 4.58 o -4 1 3 39.40 34.40 1.87 o -3 1 3 104.93 104.00 1.41 o -2 1 3 15.60 12.01 0.71 o -1 1 3 869.18 841.07 5.23 o 0 1 3 1007.10 954.82 9.64 o 2 1 3 701.65 703.56 9.28 o 3 1 3 953.55 958.25 4.26 o 4 1 3 2.16 2.03 1.60 o -5 2 3 41.48 41.98 3.96 o -4 2 3 80.75 79.46 2.67 o -3 2 3 493.40 490.83 2.68 o -2 2 3 0.13 1.81 0.69 o -1 2 3 885.20 856.57 3.00 o 0 2 3 1.49 1.37 0.45 o 1 2 3 308.37 329.20 3.11 o 2 2 3 135.02 129.42 2.42 o 3 2 3 56.78 53.25 1.53 o 4 2 3 4.48 3.25 1.79 o -5 3 3 59.28 53.33 5.19 o -4 3 3 77.00 68.26 5.28 o -3 3 3 1.84 1.65 0.88 o -2 3 3 2.42 5.84 0.78 o -1 3 3 9.56 10.96 0.86 o 0 3 3 1475.25 1571.19 5.35 o 1 3 3 14.27 12.82 0.55 o 2 3 3 847.11 826.72 7.12 o 3 3 3 250.51 238.28 3.07 o 4 3 3 410.63 424.26 4.24 o -4 4 3 116.58 117.30 4.41 o -3 4 3 145.99 143.38 3.19 o -2 4 3 968.12 978.39 6.22 o -1 4 3 1165.93 1260.04 11.21 o 0 4 3 396.01 387.44 4.98 o 1 4 3 77.22 75.94 0.88 o 2 4 3 3.74 3.97 0.72 o 3 4 3 1.04 1.55 1.37 o 4 4 3 89.35 84.11 4.69 o -4 5 3 43.24 37.07 4.61 o -3 5 3 5.04 6.47 1.74 o -2 5 3 25.79 22.33 1.27 o -1 5 3 47.34 57.10 1.08 o 0 5 3 47.58 37.55 1.09 o 1 5 3 2.09 2.90 0.62 o 2 5 3 646.33 637.45 3.03 o 3 5 3 0.41 0.92 2.92 o 4 5 3 428.75 453.28 7.76 o -4 6 3 117.16 120.60 5.51 o -3 6 3 5.32 4.56 1.53 o -2 6 3 668.32 670.14 4.88 o -1 6 3 33.72 31.47 1.14 o 0 6 3 1345.03 1411.55 8.59 o 1 6 3 125.83 117.17 3.26 o 2 6 3 60.71 66.48 2.89 o 3 6 3 78.82 72.18 3.91 o 4 6 3 4.88 5.03 4.10 o -4 7 3 150.04 147.75 6.53 o -3 7 3 1.05 1.39 1.42 o -2 7 3 12.42 11.40 1.30 o -1 7 3 53.43 53.14 1.51 o 0 7 3 615.77 594.10 9.02 o 1 7 3 3.75 5.18 1.28 o 2 7 3 431.60 417.41 3.89 o 3 7 3 191.38 202.23 5.09 o 4 7 3 66.95 66.52 5.34 o -4 8 3 119.86 114.62 4.68 o -3 8 3 8.02 13.07 2.73 o -2 8 3 315.56 333.93 4.15 o -1 8 3 222.88 220.68 4.44 o 0 8 3 272.74 256.32 4.47 o 1 8 3 205.09 211.16 5.24 o 2 8 3 422.95 411.00 4.20 o 3 8 3 17.02 18.31 4.23 o 4 8 3 0.13 -0.83 4.51 o -3 9 3 17.84 15.55 2.92 o -2 9 3 57.13 51.87 1.74 o -1 9 3 134.79 117.70 1.94 o 0 9 3 60.98 57.63 2.89 o 1 9 3 788.96 794.94 4.60 o 2 9 3 85.53 81.40 2.72 o 3 9 3 83.46 91.43 5.50 o -3 10 3 249.75 237.86 9.46 o -2 10 3 179.65 162.70 2.47 o -1 10 3 194.17 200.91 2.51 o 0 10 3 88.94 85.15 2.46 o 1 10 3 373.67 379.63 4.52 o 2 10 3 51.61 49.54 4.71 o 3 10 3 54.90 48.78 4.37 o -3 11 3 115.25 120.02 6.06 o -2 11 3 0.12 2.64 2.00 o -1 11 3 5.33 6.55 1.90 o 0 11 3 187.11 191.68 2.57 o 1 11 3 93.57 90.97 2.22 o 2 11 3 7.80 7.84 2.10 o 3 11 3 229.36 243.15 6.62 o -2 12 3 8.05 11.02 2.59 o -1 12 3 693.94 703.62 11.54 o 0 12 3 15.77 13.01 2.44 o 1 12 3 18.08 16.11 2.10 o 2 12 3 12.03 9.82 2.71 o -1 13 3 35.70 36.69 2.78 o 0 13 3 16.50 15.02 2.67 o 1 13 3 11.60 8.93 2.35 o -4 0 4 864.35 889.17 10.17 o -2 0 4 1638.37 1687.99 8.88 o 0 0 4 0.58 4.57 0.84 o 2 0 4 3.21 6.26 1.05 o 4 0 4 1.25 4.64 2.44 o -5 1 4 0.01 1.05 2.62 o -4 1 4 41.24 39.15 1.78 o -3 1 4 59.06 58.92 1.35 o -2 1 4 10.81 12.97 0.76 o -1 1 4 395.42 450.97 2.61 o 0 1 4 896.16 887.94 9.99 o 1 1 4 477.96 497.93 2.58 o 2 1 4 2089.21 2177.38 8.09 o 3 1 4 420.68 437.84 5.04 o 4 1 4 475.07 482.29 5.47 o -5 2 4 199.93 203.74 6.43 o -4 2 4 171.08 176.08 3.07 o -3 2 4 621.37 616.55 7.47 o -2 2 4 669.12 650.54 2.54 o -1 2 4 48.31 49.92 1.17 o 0 2 4 2034.48 2302.39 17.47 o 1 2 4 220.63 248.05 2.51 o 2 2 4 141.56 151.87 1.95 o 3 2 4 6.27 7.50 1.16 o 4 2 4 63.71 62.27 2.71 o -5 3 4 1.36 3.50 4.37 o -4 3 4 3.02 2.37 1.75 o -3 3 4 10.83 10.71 1.10 o -2 3 4 695.67 708.48 4.01 o -1 3 4 217.25 192.54 1.57 o 0 3 4 1347.99 1469.90 10.73 o 1 3 4 1062.72 1106.90 8.12 o 2 3 4 7.92 5.52 1.05 o 3 3 4 544.79 536.81 3.94 o 4 3 4 17.20 19.05 1.96 o -4 4 4 22.30 19.47 2.26 o -3 4 4 300.10 290.07 2.58 o -2 4 4 140.92 135.34 1.81 o -1 4 4 1518.76 1522.87 5.79 o 1 4 4 1476.43 1584.72 13.05 o 2 4 4 65.15 57.29 1.30 o 3 4 4 0.46 1.30 1.50 o 4 4 4 69.53 66.80 3.67 o -4 5 4 26.27 24.61 3.37 o -3 5 4 171.51 159.54 3.07 o -2 5 4 0.70 1.23 1.16 o -1 5 4 1660.30 1706.16 14.51 o 0 5 4 12.72 13.42 0.58 o 1 5 4 621.32 584.06 4.84 o 2 5 4 17.61 19.91 1.73 o 3 5 4 112.35 116.78 2.22 o 4 5 4 0.08 2.63 3.83 o -4 6 4 63.99 57.09 3.64 o -3 6 4 163.94 178.08 2.92 o -2 6 4 23.65 21.67 1.75 o -1 6 4 1336.95 1336.33 6.31 o 0 6 4 597.29 627.48 6.27 o 1 6 4 490.92 479.91 4.83 o 2 6 4 136.60 135.33 2.06 o 3 6 4 3.02 1.98 3.13 o 4 6 4 0.01 -0.19 3.19 o -4 7 4 0.28 0.23 3.87 o -3 7 4 53.02 48.49 1.95 o -2 7 4 597.08 578.50 4.52 o -1 7 4 51.47 42.82 1.18 o 0 7 4 265.93 255.78 2.89 o 1 7 4 544.60 551.57 2.90 o 2 7 4 3.84 6.28 1.89 o 3 7 4 317.19 327.32 5.98 o 4 7 4 7.55 8.19 4.56 o -3 8 4 514.30 519.53 3.86 o -2 8 4 151.31 161.11 2.25 o -1 8 4 18.79 21.33 1.44 o 0 8 4 347.17 339.37 2.66 o 1 8 4 26.82 27.09 1.19 o 2 8 4 62.87 60.21 3.26 o 3 8 4 45.61 56.00 4.05 o 4 8 4 42.27 39.90 5.95 o -3 9 4 105.44 106.21 3.92 o -2 9 4 16.78 17.97 1.75 o -1 9 4 64.56 59.99 2.09 o 0 9 4 232.17 225.99 6.62 o 1 9 4 143.40 138.87 3.72 o 2 9 4 320.98 319.57 4.03 o 3 9 4 337.69 340.66 6.51 o -3 10 4 38.82 37.44 2.94 o -2 10 4 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256.17 247.96 7.56 o 2 4 12 1.74 1.49 3.59 o -2 5 12 4.61 4.84 3.35 o -1 5 12 637.59 704.81 6.69 o 0 5 12 3.06 3.29 2.49 o 1 5 12 146.55 153.44 4.70 o -1 6 12 124.00 128.07 3.92 o 0 6 12 7.62 7.21 3.59 o 1 6 12 127.09 129.39 5.74 o -1 7 12 126.42 124.62 5.96 o 0 7 12 155.03 147.91 5.82 o 1 7 12 18.22 13.36 4.12 o -1 0 13 88.45 71.61 6.43 o 1 0 13 526.67 557.98 7.04 o -2 1 13 54.65 54.56 3.91 o -1 1 13 193.84 191.05 4.54 o 0 1 13 0.01 1.34 2.35 o 1 1 13 38.34 36.02 2.42 o -2 2 13 6.57 8.64 4.86 o -1 2 13 170.17 176.78 4.00 o 0 2 13 99.42 102.15 3.41 o 1 2 13 106.16 96.14 2.62 o -2 3 13 76.72 74.20 5.77 o -1 3 13 96.27 104.62 3.41 o 0 3 13 118.24 119.39 3.81 o 1 3 13 1.80 2.25 2.23 o -2 4 13 15.84 11.06 4.13 o -1 4 13 4.19 3.45 2.57 o 0 4 13 163.90 164.09 4.25 o 1 4 13 52.19 54.81 5.30 o -1 5 13 19.32 16.51 2.34 o 0 5 13 61.47 57.66 5.80 o 0 6 13 85.96 79.20 5.56 o 0 1 14 6.03 9.25 4.88 o -1 2 14 10.48 9.07 3.96 o 0 2 14 180.87 185.43 7.07 o