#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016833_Fobs loop_ _publ_author_name 'Ho\/ly\'nska, Ma\/lgorzata' 'Kubiak, Maria' _publ_section_title ; Products of the oxidation of 1-(diaminomethylene)thiourea with hydrogen peroxide ; _journal_coeditor_code GD3250 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o609 _journal_page_last o612 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.480 _cell_angle_beta 66.480 _cell_angle_gamma 78.430 _cell_length_a 6.8400 _cell_length_b 7.3740 _cell_length_c 8.0190 _exptl_crystal_F_000 208.00 _reflns_d_resolution_high 0.7460 _[local]_cod_data_source_file gd3250IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' hautdc in P-1 New: P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 100.63 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15.01 15.22 0.30 o 2 0 0 2931.94 2923.90 61.85 o 3 0 0 520.56 547.61 13.39 o 4 0 0 27.90 25.96 0.41 o 5 0 0 28.03 31.12 0.70 o 6 0 0 253.69 242.92 12.55 o 7 0 0 60.20 59.13 1.21 o 8 0 0 318.38 329.52 8.58 o -8 1 0 48.61 49.89 1.44 o -7 1 0 119.49 112.22 5.59 o -6 1 0 257.57 248.30 8.86 o -5 1 0 449.61 441.65 7.12 o -4 1 0 123.27 113.39 1.99 o -3 1 0 73.34 66.96 1.66 o -2 1 0 319.87 328.83 0.94 o -1 1 0 1418.26 1443.06 29.05 o 1 1 0 705.10 700.86 21.46 o 2 1 0 10125.64 9174.27 75.93 o 3 1 0 253.94 251.99 6.01 o 4 1 0 1398.63 1490.23 12.15 o 5 1 0 84.72 83.64 1.02 o 6 1 0 25.94 20.24 1.03 o 7 1 0 3.37 4.08 0.73 o 8 1 0 26.54 27.48 0.96 o -7 2 0 16.86 17.60 1.15 o -6 2 0 136.23 126.33 2.34 o -5 2 0 11.08 10.81 0.39 o -4 2 0 203.47 219.16 7.66 o -3 2 0 14.49 18.33 0.30 o -2 2 0 1112.62 1305.44 14.02 o -1 2 0 1.94 0.75 0.22 o 0 2 0 1164.08 1166.63 8.98 o 1 2 0 795.59 783.69 4.30 o 2 2 0 234.10 213.25 5.39 o 3 2 0 10.05 6.73 0.37 o 4 2 0 202.56 184.23 3.59 o 5 2 0 28.64 24.21 0.96 o 6 2 0 154.31 146.89 6.10 o 7 2 0 4.18 4.15 0.67 o 8 2 0 87.54 90.68 4.07 o -7 3 0 5.69 5.86 1.10 o -6 3 0 80.19 78.50 2.51 o -5 3 0 55.16 52.46 1.47 o -4 3 0 58.03 55.99 2.68 o -3 3 0 2.42 2.39 0.25 o -2 3 0 411.68 445.89 1.36 o -1 3 0 70.68 64.31 0.67 o 0 3 0 4603.32 4717.70 70.14 o 1 3 0 89.81 118.40 0.85 o 2 3 0 88.61 82.13 1.42 o 3 3 0 780.01 787.02 17.64 o 4 3 0 13.60 13.46 0.52 o 5 3 0 460.46 468.80 7.73 o 6 3 0 127.37 113.96 1.94 o 7 3 0 118.40 118.58 6.01 o 8 3 0 80.86 79.14 1.83 o -7 4 0 12.69 10.87 1.44 o -6 4 0 15.13 13.37 0.98 o -5 4 0 252.93 249.35 16.60 o -4 4 0 8.28 8.49 0.42 o -3 4 0 77.50 71.07 0.62 o -2 4 0 39.88 40.04 1.53 o -1 4 0 81.11 73.43 0.87 o 0 4 0 58.30 56.37 1.44 o 1 4 0 151.28 154.81 1.85 o 2 4 0 837.95 908.89 1.90 o 3 4 0 515.66 522.51 9.17 o 4 4 0 360.10 368.80 15.68 o 5 4 0 46.32 42.80 0.77 o 6 4 0 20.06 20.68 0.76 o 7 4 0 107.95 109.01 3.36 o -4 5 0 272.55 268.94 1.52 o -3 5 0 26.05 29.73 1.23 o -2 5 0 118.37 115.47 1.25 o -1 5 0 128.17 113.69 1.03 o 0 5 0 319.74 311.31 4.65 o 1 5 0 136.87 151.65 2.51 o 2 5 0 116.10 106.25 2.75 o 3 5 0 12.22 10.73 0.46 o 4 5 0 124.94 124.03 1.47 o 5 5 0 131.79 137.94 1.77 o 6 5 0 1.65 2.20 0.96 o 7 5 0 98.70 110.03 1.88 o -4 6 0 6.89 4.24 0.54 o -3 6 0 402.68 398.46 2.52 o -2 6 0 240.26 212.45 1.44 o -1 6 0 313.07 293.41 1.66 o 0 6 0 1.50 0.86 0.39 o 1 6 0 5.49 7.69 0.57 o 2 6 0 45.41 40.62 0.55 o 3 6 0 581.91 600.81 17.68 o 4 6 0 19.11 18.87 0.80 o 5 6 0 330.78 353.07 2.77 o 6 6 0 42.77 47.84 1.34 o -4 7 0 63.06 65.98 1.41 o -3 7 0 15.31 13.42 1.29 o -2 7 0 63.91 71.67 1.03 o -1 7 0 94.34 83.43 1.09 o 0 7 0 2.57 1.22 0.45 o 1 7 0 27.34 20.75 1.87 o 2 7 0 23.15 23.55 0.70 o 3 7 0 1.75 2.52 0.54 o 4 7 0 118.42 116.21 1.81 o 6 7 0 27.31 28.71 1.55 o -3 8 0 19.27 18.45 0.89 o -2 8 0 7.69 7.75 0.68 o -1 8 0 56.23 57.77 1.07 o 0 8 0 67.16 65.65 2.09 o 1 8 0 4.56 4.21 1.03 o 2 8 0 51.18 52.21 1.29 o 3 8 0 51.06 51.26 0.96 o 4 8 0 62.81 61.47 1.57 o 5 8 0 45.73 46.13 1.39 o 0 9 0 27.32 27.70 1.66 o 1 9 0 15.01 17.04 1.01 o 2 9 0 152.64 159.67 6.50 o 3 9 0 82.86 86.74 2.39 o -2 -9 1 58.91 63.43 1.70 o -1 -9 1 34.58 36.42 0.93 o -4 -8 1 3.09 2.13 0.98 o -3 -8 1 40.58 40.98 1.42 o -2 -8 1 35.55 32.21 0.85 o -1 -8 1 6.79 3.86 0.68 o 0 -8 1 9.02 5.56 0.75 o 1 -8 1 105.67 115.04 1.36 o 2 -8 1 43.16 35.25 1.05 o 3 -8 1 172.63 183.28 3.20 o -4 -7 1 74.80 72.35 1.45 o -3 -7 1 14.04 13.39 0.69 o -2 -7 1 90.00 91.78 1.14 o -1 -7 1 18.52 17.48 0.82 o 0 -7 1 47.84 49.12 0.92 o 1 -7 1 88.87 77.01 1.08 o 2 -7 1 81.10 72.73 2.11 o 3 -7 1 73.73 65.30 1.04 o 4 -7 1 83.76 79.11 1.11 o -6 -6 1 96.88 99.25 1.84 o -5 -6 1 41.39 40.34 1.10 o -4 -6 1 199.90 189.54 2.01 o -3 -6 1 12.76 12.32 0.52 o -2 -6 1 195.85 188.30 1.33 o -1 -6 1 0.97 0.35 0.41 o 0 -6 1 11.30 12.96 0.63 o 1 -6 1 7.50 8.05 0.80 o 2 -6 1 63.46 62.57 0.92 o 3 -6 1 6.18 5.45 0.47 o 4 -6 1 52.84 58.26 1.10 o 5 -6 1 123.88 121.92 1.80 o -6 -5 1 102.80 111.35 1.84 o -5 -5 1 165.37 170.06 2.03 o -4 -5 1 4.35 3.94 0.59 o -3 -5 1 1269.32 1364.41 48.92 o -2 -5 1 69.13 71.62 1.16 o -1 -5 1 308.88 309.74 1.53 o 0 -5 1 273.21 280.72 2.31 o 1 -5 1 222.21 215.74 1.38 o 2 -5 1 42.28 39.45 0.82 o 3 -5 1 355.79 351.66 5.94 o 4 -5 1 8.17 6.97 0.45 o 5 -5 1 193.55 191.14 2.04 o -7 -4 1 22.20 18.64 0.88 o -6 -4 1 73.52 70.38 3.24 o -5 -4 1 2.25 8.46 4.00 o -4 -4 1 662.65 666.21 15.77 o -3 -4 1 0.28 0.79 0.26 o -2 -4 1 812.18 819.60 6.86 o -1 -4 1 1071.26 1188.57 23.65 o 0 -4 1 41.10 37.66 0.52 o 1 -4 1 683.51 790.97 4.68 o 2 -4 1 28.42 26.13 0.57 o 3 -4 1 0.51 1.45 0.43 o 4 -4 1 227.97 224.93 1.30 o 5 -4 1 184.77 186.14 1.89 o 6 -4 1 469.93 495.34 3.09 o 7 -4 1 122.99 113.29 1.95 o -7 -3 1 13.73 12.52 1.31 o -6 -3 1 7.56 8.87 0.66 o -5 -3 1 111.64 111.27 1.13 o -4 -3 1 5.96 6.45 0.51 o -3 -3 1 407.08 382.68 10.88 o -2 -3 1 8.38 7.43 0.32 o -1 -3 1 342.51 326.52 8.96 o 0 -3 1 1026.06 1138.97 21.86 o 1 -3 1 7.30 14.42 0.30 o 2 -3 1 23.55 24.46 1.03 o 3 -3 1 124.37 142.98 1.48 o 4 -3 1 13.14 13.88 0.32 o 5 -3 1 177.24 177.38 1.75 o 6 -3 1 29.82 30.54 0.92 o 7 -3 1 34.89 33.10 1.25 o -7 -2 1 8.84 11.30 0.93 o -6 -2 1 5.35 5.31 1.62 o -5 -2 1 154.86 161.45 1.33 o -4 -2 1 154.24 145.78 1.76 o -3 -2 1 2609.97 2779.28 83.86 o -2 -2 1 99.32 76.99 2.09 o -1 -2 1 77.10 68.52 1.94 o 0 -2 1 390.80 413.50 14.65 o 1 -2 1 78.57 83.63 0.78 o 2 -2 1 1.91 0.67 0.14 o 3 -2 1 137.35 140.95 1.97 o 4 -2 1 80.01 79.78 3.79 o 5 -2 1 74.57 75.83 2.22 o 6 -2 1 317.44 326.62 8.62 o 7 -2 1 2.00 2.01 0.93 o -7 -1 1 7.22 7.59 0.86 o -6 -1 1 126.10 122.47 4.90 o -5 -1 1 1.80 0.83 0.50 o -4 -1 1 320.58 318.70 7.88 o -3 -1 1 170.60 167.88 0.87 o -2 -1 1 155.62 152.06 4.33 o -1 -1 1 4761.78 4563.34 80.79 o 0 -1 1 45.20 56.86 0.86 o 1 -1 1 3094.33 3003.67 9.02 o 2 -1 1 490.78 464.83 10.40 o 3 -1 1 5.96 8.50 0.42 o 4 -1 1 2.98 4.86 0.49 o 5 -1 1 258.22 248.50 8.20 o 6 -1 1 27.36 24.59 1.08 o 7 -1 1 85.87 85.67 1.14 o 8 -1 1 26.24 28.34 2.00 o -7 0 1 17.12 19.24 1.29 o -6 0 1 48.57 45.47 2.88 o -5 0 1 17.49 17.47 1.63 o -4 0 1 383.35 356.58 11.47 o -3 0 1 900.33 986.75 25.64 o -2 0 1 0.29 3.97 0.17 o -1 0 1 218.80 220.29 0.88 o 1 0 1 0.13 0.72 0.14 o 2 0 1 12.77 16.01 0.59 o 3 0 1 227.83 248.02 8.26 o 4 0 1 606.53 605.31 22.58 o 5 0 1 128.68 121.08 1.84 o 6 0 1 41.94 41.65 0.95 o 7 0 1 33.09 30.22 0.97 o 8 0 1 30.03 29.33 0.98 o -7 1 1 0.09 0.33 0.58 o -6 1 1 146.49 140.75 2.54 o -5 1 1 16.69 14.07 0.68 o -4 1 1 368.98 354.01 12.95 o -3 1 1 138.66 153.43 3.36 o -2 1 1 93.10 107.57 2.22 o -1 1 1 550.82 580.21 18.08 o 0 1 1 2099.59 2106.20 9.39 o 1 1 1 594.39 625.20 10.01 o 2 1 1 3719.96 3731.49 27.09 o 3 1 1 121.46 121.10 2.50 o 4 1 1 285.60 278.01 9.44 o 5 1 1 79.34 76.39 0.93 o 6 1 1 24.31 23.64 1.23 o 7 1 1 44.83 43.14 0.92 o 8 1 1 5.32 6.17 1.48 o -7 2 1 22.95 25.26 1.16 o -6 2 1 0.43 0.40 0.51 o -5 2 1 129.55 123.58 1.19 o -4 2 1 172.12 159.02 1.22 o -3 2 1 194.27 195.47 4.87 o -2 2 1 311.63 327.78 0.98 o -1 2 1 962.84 994.69 5.90 o 0 2 1 79.79 80.74 0.77 o 1 2 1 1399.97 1403.38 6.58 o 2 2 1 121.26 119.17 2.02 o 3 2 1 0.18 1.74 0.15 o 4 2 1 2440.13 2628.62 60.05 o 5 2 1 133.95 129.12 1.05 o 6 2 1 243.05 258.88 4.79 o 7 2 1 8.02 8.26 0.76 o 8 2 1 62.47 67.32 1.52 o -7 3 1 32.18 30.65 1.81 o -6 3 1 96.16 91.40 2.43 o -5 3 1 0.32 0.39 0.39 o -4 3 1 297.31 281.71 4.02 o -3 3 1 61.93 57.20 0.61 o -2 3 1 228.58 262.56 5.26 o -1 3 1 67.62 67.99 0.70 o 0 3 1 0.07 2.34 0.46 o 1 3 1 10.48 8.02 0.43 o 2 3 1 356.42 329.15 7.69 o 3 3 1 363.79 361.04 6.80 o 4 3 1 232.13 209.31 9.32 o 5 3 1 0.02 0.94 0.44 o 6 3 1 127.91 121.59 3.41 o 7 3 1 7.18 8.41 0.69 o 8 3 1 28.45 24.12 1.68 o -6 4 1 66.09 62.59 1.45 o -5 4 1 172.14 162.74 2.68 o -4 4 1 69.48 62.34 0.86 o -3 4 1 7.39 7.16 0.35 o -2 4 1 25.80 28.95 2.11 o -1 4 1 439.44 431.42 5.02 o 0 4 1 983.51 1106.29 2.22 o 1 4 1 245.99 228.10 3.44 o 2 4 1 710.70 748.04 3.20 o 3 4 1 56.24 44.29 0.78 o 4 4 1 14.25 16.67 0.46 o 5 4 1 80.88 76.95 0.95 o 6 4 1 0.02 0.77 0.50 o 7 4 1 68.83 66.43 1.00 o 8 4 1 20.47 16.55 1.27 o -3 5 1 46.08 50.98 0.72 o -2 5 1 139.53 133.57 1.08 o -1 5 1 240.37 250.47 4.64 o 0 5 1 172.01 162.01 4.00 o 1 5 1 116.12 123.92 1.38 o 2 5 1 606.82 637.09 19.04 o 3 5 1 18.86 16.03 0.51 o 4 5 1 1160.16 1267.87 4.27 o 5 5 1 91.31 90.90 1.46 o 6 5 1 90.06 94.81 1.71 o 7 5 1 0.02 0.52 0.88 o -3 6 1 1.74 2.31 1.23 o -2 6 1 4.94 3.84 0.43 o -1 6 1 223.58 232.27 4.60 o 0 6 1 174.15 176.64 4.75 o 1 6 1 411.72 416.63 17.36 o 2 6 1 17.72 19.01 1.03 o 3 6 1 368.15 374.26 9.51 o 4 6 1 2.52 3.73 0.79 o 5 6 1 51.64 53.15 1.27 o 6 6 1 79.04 80.71 1.53 o 7 6 1 146.26 149.08 2.11 o -3 7 1 0.46 0.73 0.56 o -2 7 1 100.26 92.25 1.17 o -1 7 1 302.40 294.59 1.80 o 0 7 1 49.00 40.73 0.82 o 1 7 1 70.22 67.35 1.74 o 2 7 1 157.64 146.15 3.81 o 3 7 1 23.72 22.37 0.67 o 4 7 1 165.19 165.48 1.86 o 5 7 1 1.91 1.31 0.64 o 6 7 1 5.39 5.32 1.01 o -3 8 1 0.23 0.75 0.63 o -2 8 1 64.13 62.41 2.55 o -1 8 1 10.46 10.74 0.63 o 0 8 1 64.42 72.46 1.10 o 1 8 1 50.42 44.38 0.90 o 2 8 1 8.54 11.10 0.69 o 3 8 1 139.60 131.03 1.32 o 4 8 1 29.38 30.77 1.29 o -1 9 1 98.79 103.53 1.62 o 0 9 1 3.97 5.32 0.78 o 1 9 1 162.36 174.50 1.84 o 2 9 1 4.00 3.02 0.65 o 3 9 1 79.87 81.32 2.41 o -3 -8 2 181.98 182.39 2.30 o -2 -8 2 88.78 89.24 1.25 o -1 -8 2 60.67 62.68 1.91 o 0 -8 2 100.35 103.45 1.31 o 1 -8 2 0.72 0.61 0.70 o 2 -8 2 124.62 137.67 1.55 o 3 -8 2 31.09 31.33 1.22 o -3 -7 2 237.04 239.58 1.66 o -2 -7 2 0.40 0.56 0.49 o -1 -7 2 5.49 4.91 0.85 o 0 -7 2 1.49 1.26 0.52 o 1 -7 2 15.95 13.04 0.56 o 2 -7 2 52.62 58.09 1.33 o 3 -7 2 202.60 213.60 3.23 o 4 -7 2 30.63 37.48 0.91 o -3 -6 2 14.63 16.35 0.61 o -2 -6 2 51.32 50.05 0.91 o -1 -6 2 10.34 14.27 0.57 o 0 -6 2 32.86 33.93 0.80 o 1 -6 2 59.38 50.36 0.91 o 2 -6 2 295.10 288.74 2.17 o 3 -6 2 312.86 298.58 6.73 o 4 -6 2 21.71 19.22 0.68 o 5 -6 2 23.53 25.52 1.29 o -6 -5 2 101.21 111.64 1.85 o -5 -5 2 28.67 29.18 1.10 o -4 -5 2 34.34 33.86 0.93 o -3 -5 2 377.30 372.02 2.30 o -2 -5 2 274.37 264.57 1.60 o -1 -5 2 22.10 20.00 1.28 o 0 -5 2 169.34 152.31 3.42 o 1 -5 2 29.70 27.27 0.46 o 2 -5 2 70.07 63.90 1.84 o 3 -5 2 291.73 282.36 3.65 o 4 -5 2 3.76 3.27 0.66 o 5 -5 2 516.15 510.12 3.27 o 6 -5 2 0.00 0.66 0.92 o -6 -4 2 8.40 7.86 1.42 o -5 -4 2 108.39 111.46 3.24 o -4 -4 2 185.11 177.47 5.29 o -3 -4 2 181.60 181.45 2.44 o -2 -4 2 154.93 146.55 1.30 o -1 -4 2 30.56 25.03 0.36 o 0 -4 2 531.77 532.25 2.44 o 1 -4 2 41.91 38.84 0.70 o 2 -4 2 1228.79 1274.54 9.33 o 3 -4 2 294.75 297.46 1.50 o 4 -4 2 165.50 160.72 3.42 o 5 -4 2 5.35 4.53 0.79 o 6 -4 2 86.91 91.70 1.53 o -7 -3 2 12.53 10.39 0.86 o -6 -3 2 83.73 85.70 1.93 o -5 -3 2 78.57 74.76 1.31 o -4 -3 2 20.52 23.64 0.99 o -3 -3 2 292.90 288.99 3.98 o -2 -3 2 100.06 99.83 1.15 o -1 -3 2 102.84 103.09 1.51 o 0 -3 2 26.00 24.05 0.38 o 1 -3 2 563.09 542.37 7.62 o 2 -3 2 37.90 37.24 0.57 o 3 -3 2 83.93 81.92 0.78 o 4 -3 2 265.70 268.28 2.66 o 5 -3 2 384.86 394.51 2.56 o 6 -3 2 0.07 0.00 0.87 o 7 -3 2 75.98 77.18 1.45 o -7 -2 2 123.26 129.82 3.02 o -6 -2 2 2.85 2.83 0.68 o -5 -2 2 4.33 4.75 0.57 o -4 -2 2 92.82 85.46 2.69 o -3 -2 2 80.80 70.95 1.27 o -2 -2 2 123.01 119.22 2.22 o -1 -2 2 3.60 9.28 0.25 o 0 -2 2 24.69 21.57 0.44 o 1 -2 2 203.25 172.76 5.84 o 2 -2 2 170.42 169.18 2.31 o 3 -2 2 26.50 25.76 0.65 o 4 -2 2 30.07 25.21 0.38 o 5 -2 2 16.17 15.40 0.83 o 6 -2 2 5.41 6.31 0.68 o 7 -2 2 4.88 3.81 0.88 o 8 -2 2 1.13 1.93 1.14 o -7 -1 2 8.72 10.04 1.25 o -6 -1 2 52.51 54.92 1.09 o -5 -1 2 17.45 15.98 0.65 o -4 -1 2 199.49 197.22 6.50 o -3 -1 2 96.79 104.69 1.80 o -2 -1 2 100.86 88.86 1.01 o -1 -1 2 243.22 290.21 3.07 o 0 -1 2 886.63 879.13 6.73 o 1 -1 2 0.85 3.80 0.43 o 2 -1 2 1409.09 1498.66 5.65 o 3 -1 2 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205.27 1.45 o -1 2 8 37.06 34.40 1.09 o 0 2 8 467.80 464.22 3.70 o 1 2 8 24.65 22.21 0.96 o 2 2 8 388.00 386.12 4.15 o 3 2 8 70.55 66.08 0.90 o 4 2 8 89.82 90.22 1.02 o 5 2 8 177.60 168.64 3.21 o 6 2 8 84.56 86.00 1.52 o 7 2 8 77.36 70.85 1.60 o -2 3 8 22.58 23.92 1.37 o -1 3 8 48.54 58.45 1.49 o 0 3 8 6.31 5.63 1.07 o 1 3 8 50.74 52.53 0.88 o 2 3 8 157.02 146.24 1.24 o 3 3 8 310.14 311.12 2.56 o 4 3 8 2.66 1.52 0.64 o 5 3 8 17.74 16.19 0.80 o 6 3 8 1.92 1.55 0.80 o 7 3 8 4.33 4.13 1.03 o -2 4 8 12.57 14.74 1.33 o -1 4 8 43.77 43.56 1.42 o 0 4 8 55.86 56.17 1.40 o 1 4 8 15.66 9.68 0.92 o 2 4 8 121.16 120.55 1.84 o 3 4 8 89.57 82.14 1.57 o 4 4 8 6.99 5.93 0.83 o 5 4 8 0.41 0.59 0.56 o 6 4 8 34.57 34.32 0.82 o 7 4 8 2.11 1.82 0.76 o -1 5 8 9.27 10.84 1.19 o 0 5 8 126.92 128.40 2.08 o 1 5 8 32.78 33.61 1.42 o 2 5 8 7.55 8.57 1.04 o 3 5 8 72.69 63.96 1.44 o 4 5 8 22.13 20.03 0.84 o 7 5 8 105.89 105.81 1.37 o 0 6 8 6.73 6.08 1.14 o 1 6 8 35.91 36.51 1.43 o 2 6 8 152.88 156.09 2.15 o 3 6 8 117.28 119.31 1.86 o 4 6 8 0.25 0.75 0.80 o 2 7 8 162.05 177.91 2.35 o 3 7 8 0.79 1.00 0.80 o 4 7 8 12.31 11.66 1.00 o 4 8 8 21.53 22.32 1.48 o 1 -2 9 0.13 0.39 0.85 o 2 -2 9 29.10 33.00 1.22 o 3 -2 9 23.49 22.83 1.28 o 4 -2 9 161.01 185.75 2.42 o 0 -1 9 2.55 3.96 1.36 o 1 -1 9 54.83 55.71 1.53 o 2 -1 9 0.25 1.24 0.73 o 3 -1 9 89.57 100.80 1.86 o 4 -1 9 0.02 0.18 0.93 o 5 -1 9 119.74 119.71 1.96 o 6 -1 9 23.79 26.94 1.43 o 0 0 9 64.91 64.68 1.62 o 1 0 9 0.81 0.47 0.72 o 2 0 9 6.94 7.38 1.18 o 3 0 9 0.86 0.53 0.81 o 4 0 9 106.61 107.29 1.81 o 5 0 9 10.03 10.90 1.10 o 6 0 9 63.18 65.57 2.22 o -1 1 9 128.27 126.77 1.44 o 0 1 9 56.21 58.25 1.04 o 1 1 9 2.17 1.60 0.56 o 2 1 9 8.06 8.85 0.66 o 3 1 9 6.88 9.56 3.20 o 4 1 9 141.03 143.28 1.94 o 5 1 9 44.18 45.43 1.26 o 6 1 9 15.38 15.45 0.69 o 7 1 9 71.91 71.00 1.74 o -1 2 9 41.99 40.57 1.00 o 0 2 9 64.74 72.21 1.15 o 1 2 9 0.61 0.61 0.53 o 2 2 9 33.47 34.33 0.80 o 3 2 9 144.17 143.56 2.14 o 4 2 9 42.11 39.15 0.89 o 5 2 9 279.17 295.24 2.62 o 6 2 9 108.80 110.04 3.63 o 7 2 9 21.02 20.68 1.40 o 0 3 9 73.98 82.51 1.84 o 1 3 9 6.68 6.29 1.05 o 2 3 9 10.31 8.09 1.23 o 3 3 9 5.87 6.36 0.82 o 4 3 9 117.81 115.92 1.74 o 6 3 9 37.75 35.22 1.09 o 7 3 9 275.17 278.90 2.82 o 0 4 9 1.16 2.99 0.96 o 1 4 9 23.72 27.93 1.46 o 2 4 9 79.59 83.70 1.76 o 3 4 9 95.99 105.03 1.77 o 4 4 9 9.09 8.13 1.05 o 6 4 9 26.15 23.99 1.30 o 7 4 9 41.82 43.88 1.55 o 1 5 9 26.88 25.85 1.38 o 2 5 9 94.80 101.04 1.96 o 3 5 9 20.70 24.79 1.20 o 4 5 9 12.85 12.75 1.14 o 2 6 9 2.15 2.74 1.06 o 3 6 9 62.30 68.52 1.65 o 4 6 9 0.35 1.23 0.96 o 4 7 9 84.22 80.50 1.70 o 2 0 10 3.71 4.91 1.19 o 3 0 10 132.57 144.73 2.18 o 4 0 10 36.74 34.31 1.36 o 1 1 10 1.96 1.49 1.05 o 2 1 10 54.00 54.49 1.03 o 3 1 10 0.00 0.22 0.65 o 4 1 10 123.04 135.69 2.05 o 5 1 10 17.49 21.62 1.40 o 1 2 10 11.16 9.57 1.27 o 2 2 10 3.29 4.03 0.72 o 3 2 10 3.53 3.22 0.82 o 4 2 10 0.21 0.43 0.64 o 5 2 10 118.06 124.48 1.90 o 6 2 10 3.92 3.45 1.05 o 2 3 10 211.02 224.19 2.67 o 3 3 10 1.36 1.23 0.96 o 4 3 10 148.01 159.84 2.19 o 3 4 10 13.08 8.48 1.03 o 4 4 10 36.02 34.94 1.53 o 4 5 10 0.09 0.29 0.99 o