#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016835.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016835_Fobs loop_ _publ_author_name 'Aghabozorg, Hossein' 'Derikvand, Zohreh' 'Olmstead, Marilyn M.' 'Attar Gharamaleki, Jafar' _publ_section_title ; Hydroxonium hydrate tris(2,4,6-triamino-1,3,5-triazin-1-ium) bis[bis(pyridine-2,6-dicarboxylato)manganate(II/III)] hydroxide pyridine-2,6-dicarboxylic acid solvate pentahydrate ; _journal_coeditor_code GZ3154 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m372 _journal_page_last m374 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.819 _cell_angle_gamma 90.000 _cell_length_a 27.1406 _cell_length_b 23.1672 _cell_length_c 9.7838 _exptl_crystal_F_000 3012.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file gz3154Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 3(melaminium)(H5O2)(pydcH2)[Mn(II/III(pydc)2]2(OH)5(H2O) _shelx_refln_list_code 4 _shelx_F_calc_maximum 580.80 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 36940.66 34523.64 609.47 o 6 0 0 120796.68 114798.12 1179.67 o 8 0 0 6236.58 6647.67 94.06 o 10 0 0 1257.09 1214.18 39.89 o 12 0 0 31503.99 29923.85 287.80 o 14 0 0 6813.11 5968.80 81.19 o 16 0 0 48480.76 45639.33 432.88 o 18 0 0 13482.47 13141.47 154.85 o 20 0 0 11519.50 11037.66 176.82 o 22 0 0 13348.29 11970.67 195.06 o 24 0 0 1744.77 2121.91 97.02 o 26 0 0 21.00 -32.94 46.30 o 28 0 0 2228.15 2001.97 129.34 o 30 0 0 4392.21 3837.40 161.25 o 32 0 0 16035.55 16241.61 1449.26 o 5 1 0 38.08 186.48 9.57 o 7 1 0 256.91 203.83 12.00 o 9 1 0 11800.03 12815.55 122.28 o 11 1 0 6803.74 6420.85 95.26 o 13 1 0 18008.05 17196.59 127.21 o 15 1 0 4966.33 6071.73 60.18 o 17 1 0 12835.48 13245.53 120.26 o 19 1 0 14518.16 13517.73 142.00 o 21 1 0 21.51 14.12 21.78 o 23 1 0 817.80 1113.04 42.75 o 25 1 0 3949.41 3503.86 91.03 o 27 1 0 159.98 291.29 45.05 o 29 1 0 1715.16 2059.02 126.84 o 31 1 0 3634.16 3898.73 115.26 o 33 1 0 102.98 174.31 52.82 o 4 2 0 58.29 98.48 7.86 o 6 2 0 18047.26 16316.37 140.72 o 8 2 0 3271.66 3295.80 36.94 o 10 2 0 2721.69 2647.31 31.99 o 12 2 0 5003.50 5182.36 51.18 o 14 2 0 1738.23 1913.25 31.12 o 16 2 0 30.05 112.60 14.80 o 18 2 0 6887.08 6812.75 88.58 o 20 2 0 312.59 444.09 28.92 o 22 2 0 48.37 375.24 37.56 o 24 2 0 527.97 632.31 44.90 o 26 2 0 1651.98 1592.70 69.49 o 28 2 0 758.94 760.37 59.18 o 30 2 0 1297.84 1480.96 77.28 o 32 2 0 1306.45 1286.91 107.08 o 1 3 0 315.33 223.37 10.78 o 3 3 0 1435.95 1268.14 17.95 o 5 3 0 6468.72 6538.53 54.73 o 7 3 0 11935.38 13583.36 103.25 o 9 3 0 5511.44 5110.30 50.57 o 11 3 0 1248.66 1423.36 30.74 o 13 3 0 40902.81 39542.67 286.42 o 15 3 0 2506.87 2293.10 35.29 o 17 3 0 1752.16 2103.53 36.30 o 19 3 0 41542.84 40392.38 461.67 o 21 3 0 4789.39 4962.68 79.59 o 23 3 0 2839.76 2847.48 64.20 o 25 3 0 79.73 255.73 40.10 o 27 3 0 548.12 583.83 52.21 o 29 3 0 2848.15 3213.39 102.15 o 31 3 0 14.96 -29.35 68.53 o 33 3 0 15.78 89.94 50.38 o 0 4 0 35.75 -13.61 13.61 o 2 4 0 978.76 1318.96 22.70 o 4 4 0 2545.75 2523.89 27.11 o 6 4 0 32654.49 32674.44 244.30 o 8 4 0 5702.98 5498.58 50.47 o 10 4 0 28593.13 29005.82 196.99 o 12 4 0 7410.60 7515.05 68.28 o 14 4 0 1040.91 784.74 22.80 o 16 4 0 65802.22 62260.59 388.00 o 18 4 0 3946.28 4185.70 51.07 o 20 4 0 1761.83 1796.51 70.78 o 22 4 0 1455.13 1454.03 48.62 o 24 4 0 136.97 192.69 31.46 o 26 4 0 3401.48 3621.08 123.26 o 28 4 0 1175.22 1333.70 69.90 o 30 4 0 175.47 188.17 48.91 o 32 4 0 6217.61 6141.99 144.63 o 1 5 0 118.19 29.22 8.04 o 3 5 0 3236.44 3100.38 31.53 o 5 5 0 1018.29 1204.91 21.17 o 7 5 0 3177.13 3350.25 37.10 o 9 5 0 47946.81 45113.93 294.18 o 11 5 0 996.31 1562.92 32.98 o 13 5 0 6221.95 6446.30 63.84 o 15 5 0 18903.17 19730.71 149.70 o 17 5 0 203.16 353.36 20.17 o 19 5 0 5550.01 6107.45 87.87 o 21 5 0 1165.72 1022.45 41.65 o 23 5 0 237.23 186.04 29.68 o 25 5 0 1579.34 1735.51 62.35 o 27 5 0 92.46 134.18 41.06 o 29 5 0 1968.24 1983.43 84.14 o 31 5 0 18.20 21.92 45.72 o 0 6 0 12268.17 12065.72 181.02 o 2 6 0 11651.58 11090.87 87.83 o 4 6 0 1190.68 1303.00 22.35 o 6 6 0 29186.95 27948.33 187.75 o 8 6 0 26.70 139.96 12.28 o 10 6 0 3910.74 5066.54 52.61 o 12 6 0 1709.32 2009.63 43.41 o 14 6 0 487.49 1143.71 28.10 o 16 6 0 85.10 205.74 18.09 o 18 6 0 4554.01 4387.00 56.98 o 20 6 0 1343.71 1933.12 54.40 o 22 6 0 68.42 46.37 26.70 o 24 6 0 148.18 405.93 37.15 o 26 6 0 1243.06 1871.92 67.41 o 28 6 0 25.87 173.45 44.47 o 30 6 0 460.06 415.84 57.04 o 32 6 0 98.59 51.93 49.03 o 1 7 0 754.37 704.78 29.15 o 3 7 0 592.35 700.04 19.43 o 5 7 0 1655.89 1388.82 24.49 o 7 7 0 19649.86 18287.56 132.04 o 9 7 0 25649.11 26657.47 185.69 o 11 7 0 5011.09 5772.55 66.83 o 13 7 0 5916.40 6332.23 65.63 o 15 7 0 8211.03 7857.30 82.68 o 17 7 0 4924.60 4787.68 59.98 o 19 7 0 7921.92 7053.51 96.81 o 21 7 0 3401.81 3397.68 69.30 o 23 7 0 6968.98 6744.45 103.05 o 25 7 0 606.44 1643.67 64.09 o 27 7 0 340.45 1210.89 98.94 o 29 7 0 1406.04 1174.18 70.58 o 31 7 0 476.98 467.91 58.93 o 0 8 0 98421.48 97652.11 1235.17 o 2 8 0 23552.99 22774.66 182.01 o 4 8 0 26.70 23.13 13.72 o 6 8 0 2498.80 1952.95 30.09 o 8 8 0 1821.84 1817.82 31.01 o 10 8 0 30391.81 29048.22 203.29 o 12 8 0 73658.47 72432.14 469.22 o 14 8 0 55.59 44.65 22.10 o 16 8 0 1532.54 1410.76 48.05 o 18 8 0 6003.93 5793.09 68.92 o 20 8 0 4321.10 4331.51 81.61 o 22 8 0 4285.74 3994.21 77.88 o 24 8 0 913.05 1119.93 49.40 o 26 8 0 471.00 987.91 54.07 o 28 8 0 1558.64 1619.14 75.22 o 30 8 0 14.24 34.37 59.33 o 32 8 0 1606.51 1632.80 86.31 o 1 9 0 9.14 631.66 28.87 o 3 9 0 11580.44 12481.12 103.31 o 5 9 0 862.16 834.31 21.07 o 7 9 0 1702.95 1615.61 29.37 o 9 9 0 398.35 595.76 23.27 o 11 9 0 5601.02 6515.62 67.10 o 13 9 0 8075.36 7444.29 75.33 o 15 9 0 29.46 82.68 19.14 o 17 9 0 2153.06 3019.38 49.41 o 19 9 0 415.42 586.41 30.73 o 21 9 0 3516.24 3659.30 73.67 o 23 9 0 20.60 29.53 28.19 o 25 9 0 2544.49 2871.25 79.98 o 27 9 0 102.95 139.11 43.94 o 29 9 0 273.34 160.09 48.93 o 31 9 0 858.50 1053.04 73.68 o 0 10 0 58794.22 57601.83 760.36 o 2 10 0 10017.95 11121.57 135.44 o 4 10 0 32.49 324.03 15.33 o 6 10 0 3658.28 3162.22 41.67 o 8 10 0 2739.49 3067.77 42.66 o 10 10 0 3088.09 3391.66 46.47 o 12 10 0 294.17 271.64 18.60 o 14 10 0 3933.78 4073.43 54.79 o 16 10 0 3753.06 3977.13 56.10 o 18 10 0 376.33 468.60 25.98 o 20 10 0 5162.93 4987.01 83.98 o 22 10 0 1791.43 1616.08 53.45 o 24 10 0 4.20 20.04 30.85 o 26 10 0 1082.64 1062.68 56.07 o 28 10 0 53.01 53.51 44.10 o 30 10 0 0.97 213.02 51.54 o 1 11 0 34230.24 35339.44 350.31 o 3 11 0 46773.47 45557.05 323.37 o 5 11 0 3726.90 4335.37 63.11 o 7 11 0 16769.41 16876.10 130.89 o 9 11 0 21349.63 20209.64 153.44 o 11 11 0 433.95 411.04 20.84 o 13 11 0 22368.82 21195.73 164.31 o 15 11 0 7235.48 7414.41 80.09 o 17 11 0 4359.29 4660.80 63.95 o 19 11 0 18146.48 17939.89 152.88 o 21 11 0 175.80 310.32 33.98 o 23 11 0 1634.44 1709.25 56.84 o 25 11 0 812.78 1257.37 58.70 o 27 11 0 210.14 189.12 44.74 o 29 11 0 2852.26 3119.06 102.10 o 31 11 0 1843.72 2042.51 90.96 o 0 12 0 9944.73 10373.21 193.71 o 2 12 0 1592.05 1532.55 53.70 o 4 12 0 80933.69 81546.73 558.81 o 6 12 0 11965.48 10625.73 92.73 o 8 12 0 436.68 664.11 23.36 o 10 12 0 3767.65 3726.37 51.27 o 12 12 0 2986.40 2671.96 45.04 o 14 12 0 3348.18 3543.87 53.51 o 16 12 0 11076.86 11518.17 109.42 o 18 12 0 1773.45 1967.27 45.79 o 20 12 0 2807.19 3110.32 69.79 o 22 12 0 78.75 64.72 29.73 o 24 12 0 3217.19 3553.18 91.69 o 26 12 0 5762.77 6448.73 120.45 o 28 12 0 1992.26 2000.61 83.65 o 30 12 0 1034.07 1218.50 73.62 o 1 13 0 4331.52 4110.21 81.19 o 3 13 0 5378.11 7052.55 93.45 o 5 13 0 1415.93 1611.47 32.92 o 7 13 0 11142.28 10975.06 97.40 o 9 13 0 2858.20 2762.22 44.66 o 11 13 0 2993.05 2939.57 47.46 o 13 13 0 2254.68 2304.77 44.70 o 15 13 0 540.24 1052.69 40.49 o 17 13 0 1915.99 2023.92 76.28 o 19 13 0 807.48 1103.22 47.83 o 21 13 0 2499.49 3211.69 73.12 o 23 13 0 191.28 492.13 40.32 o 25 13 0 540.96 972.43 54.77 o 27 13 0 67.33 373.42 47.98 o 29 13 0 188.68 206.85 49.56 o 0 14 0 37637.83 34894.10 509.97 o 2 14 0 29.86 210.26 28.80 o 4 14 0 7007.77 6692.74 94.30 o 6 14 0 14964.74 14353.60 192.78 o 8 14 0 26.61 149.36 18.04 o 10 14 0 8450.19 9244.54 91.25 o 12 14 0 8403.80 7887.10 84.17 o 14 14 0 4942.21 4774.39 64.92 o 16 14 0 10809.97 10431.27 105.42 o 18 14 0 2200.48 2197.63 49.91 o 20 14 0 1060.21 1705.05 54.96 o 22 14 0 961.11 1032.77 56.50 o 24 14 0 144.76 406.17 43.79 o 26 14 0 3596.47 3836.54 94.59 o 28 14 0 1092.47 1115.40 81.46 o 1 15 0 30.30 87.58 26.85 o 3 15 0 364.42 277.05 28.08 o 5 15 0 1382.60 1491.41 36.46 o 7 15 0 28120.53 27011.45 200.57 o 9 15 0 16920.91 16824.03 139.78 o 11 15 0 2096.90 2174.98 44.23 o 13 15 0 13834.57 13771.23 131.45 o 15 15 0 6402.10 6778.96 81.23 o 17 15 0 1584.51 2030.05 48.17 o 19 15 0 2887.45 3475.08 62.18 o 21 15 0 146.11 88.74 33.01 o 23 15 0 9634.76 9637.73 134.10 o 25 15 0 10051.51 9681.88 171.08 o 27 15 0 4.20 34.25 46.96 o 0 16 0 7795.61 7914.36 185.48 o 2 16 0 393.42 530.90 40.14 o 4 16 0 1220.59 1324.60 47.33 o 6 16 0 1276.07 1276.68 33.60 o 8 16 0 369.53 402.04 24.10 o 10 16 0 13652.81 13274.15 120.16 o 12 16 0 4804.56 4787.66 65.86 o 14 16 0 2676.20 3404.84 57.72 o 16 16 0 8291.87 8294.98 94.21 o 18 16 0 1884.01 2040.60 54.09 o 20 16 0 1231.79 1402.55 59.76 o 22 16 0 563.68 604.49 50.63 o 24 16 0 556.53 996.46 64.40 o 26 16 0 487.78 460.50 56.04 o 28 16 0 2210.22 2293.22 106.22 o 1 17 0 966.07 1097.21 53.84 o 3 17 0 8663.41 8398.86 116.57 o 5 17 0 2.97 39.60 23.45 o 7 17 0 1332.17 1562.02 38.43 o 9 17 0 1824.98 1964.36 46.47 o 11 17 0 2.61 61.86 22.29 o 13 17 0 5.31 789.66 37.99 o 15 17 0 1144.57 1207.44 43.24 o 17 17 0 13950.44 14433.27 148.49 o 19 17 0 9154.09 8719.12 110.35 o 21 17 0 45.46 1123.32 58.20 o 23 17 0 3155.53 3537.64 153.44 o 25 17 0 1520.57 1571.53 99.74 o 27 17 0 99.75 83.07 72.63 o 0 18 0 4732.83 3991.42 135.29 o 2 18 0 102.63 108.01 35.80 o 4 18 0 4316.07 3972.59 80.74 o 6 18 0 1003.16 1431.30 52.22 o 8 18 0 11.48 233.93 24.61 o 10 18 0 273.41 276.54 26.44 o 12 18 0 178.15 422.10 30.88 o 14 18 0 503.53 683.57 44.83 o 16 18 0 3143.84 3584.22 69.19 o 18 18 0 3991.27 4306.93 91.87 o 20 18 0 2833.57 3094.89 85.42 o 22 18 0 495.10 383.27 48.14 o 24 18 0 648.44 629.13 60.20 o 26 18 0 1248.88 1199.36 75.24 o 1 19 0 4447.68 4429.11 104.32 o 3 19 0 1361.60 1255.90 61.56 o 5 19 0 642.41 740.19 54.25 o 7 19 0 102.28 14.75 27.48 o 9 19 0 8013.71 7636.65 94.31 o 11 19 0 2954.72 3086.85 61.11 o 13 19 0 11320.29 10597.73 120.78 o 15 19 0 660.51 1273.57 45.83 o 17 19 0 922.55 1290.75 47.27 o 19 19 0 10025.69 10277.98 131.97 o 21 19 0 3527.32 3597.79 107.30 o 23 19 0 876.36 999.07 76.84 o 25 19 0 3445.75 3643.25 130.38 o 0 20 0 1287.40 1477.49 145.28 o 2 20 0 7203.60 6880.05 135.13 o 4 20 0 99.09 98.35 31.24 o 6 20 0 876.65 983.02 56.14 o 8 20 0 52.00 646.32 43.68 o 10 20 0 4068.34 4038.81 77.22 o 12 20 0 379.39 393.34 35.53 o 14 20 0 160.89 671.67 46.75 o 16 20 0 19314.09 18811.42 283.56 o 18 20 0 100.48 138.21 39.35 o 20 20 0 356.19 649.21 58.53 o 22 20 0 1226.32 1286.42 72.77 o 24 20 0 507.91 681.08 72.28 o 1 21 0 1009.57 939.90 71.60 o 3 21 0 12.57 184.68 43.41 o 5 21 0 14.07 208.02 46.58 o 7 21 0 354.49 577.87 45.51 o 9 21 0 4474.32 4650.87 96.89 o 11 21 0 452.62 522.96 53.07 o 13 21 0 7730.71 7751.59 128.52 o 15 21 0 4912.94 5656.85 98.28 o 19 21 0 2215.19 2313.86 77.10 o 21 21 0 740.35 769.28 64.32 o 23 21 0 894.50 1085.57 84.57 o 0 22 0 4408.86 4205.85 258.67 o 2 22 0 2386.56 2396.92 145.70 o 4 22 0 361.62 540.14 54.15 o 6 22 0 18946.25 17788.89 248.39 o 8 22 0 1187.16 998.67 64.64 o 10 22 0 13968.94 13537.21 264.93 o 12 22 0 8467.52 8370.49 157.49 o 14 22 0 7520.92 7217.57 146.87 o 16 22 0 1745.12 1781.92 82.34 o 18 22 0 205.45 225.92 52.20 o 20 22 0 272.39 418.98 178.94 o 22 22 0 2525.27 2377.64 226.78 o 1 23 0 909.93 1082.78 70.86 o 3 23 0 38557.05 33442.52 396.31 o 5 23 0 125.33 213.58 48.55 o 7 23 0 1860.75 2008.08 84.95 o 9 23 0 337.87 497.60 56.44 o 11 23 0 38.74 44.01 45.60 o 13 23 0 6681.75 6502.24 143.24 o 15 23 0 3032.18 3035.82 104.85 o 17 23 0 1698.67 1712.58 82.00 o 19 23 0 3616.74 3771.48 140.43 o 21 23 0 38.29 71.18 98.95 o 0 24 0 3816.30 4135.21 361.43 o 2 24 0 33.00 253.20 71.09 o 4 24 0 2466.15 2239.97 92.15 o 6 24 0 1142.08 1071.10 105.64 o 8 24 0 517.69 792.78 65.20 o 10 24 0 354.31 531.39 59.00 o 12 24 0 250.64 361.42 55.85 o 14 24 0 112.08 56.66 52.14 o 16 24 0 574.16 745.86 78.76 o 18 24 0 31.03 243.36 62.91 o 20 24 0 837.44 1047.71 129.64 o 1 25 0 186.24 315.59 57.83 o 3 25 0 4958.11 4639.46 154.20 o 5 25 0 94.71 71.33 50.85 o 7 25 0 3963.57 3938.50 215.83 o 9 25 0 2214.01 2181.44 93.12 o 11 25 0 67.54 272.11 67.51 o 13 25 0 2031.61 2036.53 91.81 o 15 25 0 2078.59 2321.31 96.86 o 17 25 0 11.95 5.46 52.14 o 0 26 0 20.08 22.98 71.08 o 2 26 0 33.11 29.62 48.70 o 4 26 0 235.62 308.53 59.75 o 6 26 0 4970.70 5512.10 142.11 o 8 26 0 1205.23 1134.38 88.99 o 10 26 0 850.45 985.51 75.62 o 12 26 0 928.26 911.13 73.90 o 14 26 0 761.21 917.36 74.48 o 16 26 0 145.35 235.97 59.72 o 1 27 0 4660.40 4345.58 165.71 o 3 27 0 1205.50 1200.00 81.97 o 5 27 0 6.33 -50.55 50.55 o 7 27 0 804.11 1026.84 88.77 o 9 27 0 330.71 527.01 65.83 o 11 27 0 976.42 1047.29 92.57 o 13 27 0 2508.39 2684.69 106.50 o 0 28 0 3331.88 3265.02 253.36 o 2 28 0 772.24 796.68 104.68 o 4 28 0 203.43 478.80 67.55 o 6 28 0 93.98 241.07 63.55 o 8 28 0 308.29 685.61 140.65 o 10 28 0 1653.44 1526.33 92.09 o 12 28 0 224.34 308.28 65.16 o 1 29 0 769.68 756.31 76.45 o 3 29 0 248.01 198.22 61.50 o 5 29 0 21.52 339.82 68.25 o 7 29 0 1829.37 1715.32 111.41 o 0 30 0 4106.60 4257.47 262.21 o 2 30 0 21.69 -24.82 57.03 o -33 1 1 441.65 607.63 64.64 o -31 1 1 36.46 18.14 43.27 o -29 1 1 97.49 49.35 42.24 o -27 1 1 893.11 1102.93 62.80 o -25 1 1 0.57 17.38 32.40 o -23 1 1 2367.62 2333.91 56.93 o -21 1 1 7470.46 7251.65 95.10 o -19 1 1 74.67 1053.41 29.65 o -17 1 1 10583.80 9961.06 88.51 o -15 1 1 230.58 252.55 15.67 o -13 1 1 1078.73 964.38 24.80 o -11 1 1 177.82 331.88 15.62 o -9 1 1 7543.89 8112.94 64.68 o -7 1 1 12948.49 13891.15 112.60 o -5 1 1 1529.81 2029.94 25.74 o -3 1 1 838.97 849.04 33.92 o 1 1 1 882.46 892.24 21.76 o 3 1 1 795.47 1089.03 20.81 o 5 1 1 3568.83 3740.18 52.15 o 7 1 1 9995.90 10736.69 97.55 o 9 1 1 57.43 130.82 13.22 o 11 1 1 11918.82 10413.25 104.31 o 13 1 1 5285.33 5178.77 69.11 o 15 1 1 4323.30 4045.09 63.32 o 17 1 1 7488.91 7276.20 93.44 o 19 1 1 5846.93 5309.54 92.17 o 21 1 1 2952.89 2690.53 61.81 o 23 1 1 901.33 964.64 43.42 o 25 1 1 698.39 1024.69 46.92 o 27 1 1 1999.79 1898.18 61.57 o 29 1 1 14276.86 14982.89 230.88 o 31 1 1 7.38 136.26 50.81 o -34 2 1 3091.18 2902.51 109.61 o -32 2 1 686.54 664.75 63.67 o -30 2 1 742.90 888.47 73.89 o -28 2 1 1085.77 1314.83 68.06 o -26 2 1 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