#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2016842.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016842_Fobs loop_ _publ_author_name 'Karczmarzyk, Zbigniew' _publ_section_title ; Keto--enol tautomerism in crystals of 3-[hydroxy(phenyl)methyl]-2,5,7-trimethyl-2,3-dihydropyrido[3,2-e][1,2]thiazin-4-one 1,1-dioxide and 3-(1-hydroxyethylidene)-2,5,7-trimethyl-2,3-dihydropyrido[3,2-e][1,2]thiazin-4-one 1,1-dioxide ; _journal_coeditor_code SF3092 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o590 _journal_page_last o594 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.817 _cell_angle_gamma 90.000 _cell_length_a 8.9023 _cell_length_b 14.3095 _cell_length_c 10.6151 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7597 _[local]_cod_data_source_file sf3092IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' wm143 in P 21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 87.16 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.58 0.34 0.11 o 4 0 0 445.52 434.50 3.80 o 6 0 0 394.18 404.31 3.64 o 8 0 0 1104.49 1121.38 9.65 o 10 0 0 0.12 0.19 0.31 o 1 1 0 2764.40 2835.21 48.99 o 2 1 0 3835.88 3817.97 24.44 o 3 1 0 349.80 422.57 2.99 o 4 1 0 56.80 73.32 0.72 o 5 1 0 6.04 4.93 0.31 o 6 1 0 274.23 267.17 1.78 o 7 1 0 888.55 880.96 5.38 o 8 1 0 166.60 171.54 1.30 o 9 1 0 0.25 0.81 0.19 o 10 1 0 29.58 31.37 0.67 o 11 1 0 69.84 75.39 1.26 o 0 2 0 872.49 860.19 5.82 o 1 2 0 2528.70 2533.11 21.76 o 2 2 0 1535.85 1535.37 10.15 o 3 2 0 5193.08 5442.05 41.19 o 4 2 0 441.08 457.68 2.81 o 5 2 0 89.16 94.68 0.73 o 6 2 0 136.27 141.62 1.04 o 7 2 0 46.93 43.91 0.49 o 8 2 0 231.20 226.74 1.63 o 9 2 0 30.79 32.78 0.58 o 10 2 0 1.53 1.37 0.25 o 11 2 0 11.54 13.01 1.03 o 1 3 0 1222.08 1288.29 7.23 o 2 3 0 386.26 378.45 2.08 o 3 3 0 93.03 66.30 0.51 o 4 3 0 29.51 39.77 0.38 o 5 3 0 8.93 8.33 0.22 o 6 3 0 126.91 118.98 0.97 o 7 3 0 71.58 76.24 0.69 o 8 3 0 68.50 63.10 0.71 o 9 3 0 283.26 278.75 2.54 o 10 3 0 22.81 24.05 0.61 o 11 3 0 82.71 87.52 1.60 o 1 4 0 1320.69 1322.04 8.48 o 2 4 0 3476.64 3472.82 19.87 o 3 4 0 4820.61 5206.29 31.23 o 4 4 0 1886.41 1957.86 11.95 o 5 4 0 287.85 305.96 2.11 o 6 4 0 61.88 59.59 0.60 o 7 4 0 10.47 8.48 0.27 o 8 4 0 5.79 5.14 0.24 o 9 4 0 21.39 22.34 0.46 o 10 4 0 45.34 44.10 0.80 o 11 4 0 5.80 5.47 0.54 o 1 5 0 796.22 849.42 5.17 o 2 5 0 343.22 431.28 2.50 o 3 5 0 421.88 407.63 2.37 o 4 5 0 9.89 8.42 0.18 o 5 5 0 312.33 361.41 2.30 o 6 5 0 70.09 58.88 0.56 o 7 5 0 52.57 49.12 0.59 o 8 5 0 525.82 525.68 3.86 o 9 5 0 6.62 6.41 0.41 o 10 5 0 199.14 209.48 2.12 o 0 6 0 40.07 50.51 0.59 o 1 6 0 5443.59 5667.48 43.68 o 2 6 0 94.84 100.50 0.67 o 3 6 0 616.95 676.56 4.11 o 4 6 0 422.79 458.86 2.86 o 5 6 0 41.41 48.06 0.46 o 6 6 0 65.25 55.99 0.66 o 7 6 0 0.71 -0.06 0.14 o 8 6 0 15.41 11.86 0.40 o 9 6 0 8.23 8.49 0.37 o 10 6 0 59.05 62.17 1.11 o 1 7 0 497.53 563.18 3.44 o 2 7 0 6.49 6.12 0.13 o 3 7 0 127.48 156.19 1.01 o 4 7 0 41.16 45.60 0.47 o 5 7 0 392.17 402.91 2.78 o 6 7 0 10.12 11.85 0.30 o 7 7 0 268.95 286.71 2.96 o 8 7 0 89.03 85.87 0.99 o 9 7 0 78.07 76.47 1.07 o 10 7 0 11.20 10.55 0.55 o 0 8 0 1504.55 1580.16 13.56 o 1 8 0 3157.74 3155.46 19.15 o 2 8 0 88.86 82.85 0.60 o 3 8 0 104.98 103.74 0.86 o 4 8 0 137.95 132.81 0.97 o 5 8 0 187.74 184.14 1.57 o 6 8 0 21.19 23.68 0.45 o 7 8 0 3.13 4.04 0.24 o 8 8 0 33.88 30.91 0.57 o 9 8 0 38.06 34.35 0.72 o 10 8 0 2.12 1.63 0.37 o 1 9 0 63.26 49.46 0.47 o 2 9 0 354.42 373.93 2.67 o 3 9 0 12.57 13.44 0.37 o 4 9 0 40.80 41.43 0.58 o 5 9 0 248.16 226.56 2.13 o 6 9 0 37.52 35.98 0.63 o 7 9 0 134.64 130.83 1.33 o 8 9 0 135.87 137.91 1.49 o 9 9 0 2.79 2.55 0.34 o 0 10 0 2022.29 2016.18 17.27 o 1 10 0 380.56 370.58 2.43 o 2 10 0 1417.24 1391.95 8.33 o 3 10 0 2227.61 2163.45 13.83 o 4 10 0 4.95 8.49 0.33 o 5 10 0 337.81 308.23 2.46 o 6 10 0 0.02 0.20 0.18 o 7 10 0 0.14 0.18 0.20 o 8 10 0 10.92 11.72 0.41 o 9 10 0 6.92 6.35 0.46 o 1 11 0 321.11 326.92 2.15 o 2 11 0 1730.82 1618.22 10.31 o 3 11 0 729.24 675.52 4.90 o 4 11 0 113.22 114.71 1.24 o 5 11 0 166.21 165.79 1.52 o 6 11 0 215.18 211.64 2.10 o 7 11 0 34.54 37.94 0.65 o 8 11 0 15.59 17.27 0.63 o 9 11 0 184.22 193.71 2.37 o 0 12 0 104.78 109.67 1.26 o 1 12 0 343.46 343.86 2.45 o 2 12 0 35.35 37.69 0.52 o 3 12 0 75.67 77.76 1.25 o 4 12 0 57.23 51.95 0.71 o 5 12 0 306.58 303.82 2.49 o 6 12 0 8.52 10.95 0.41 o 7 12 0 0.94 0.99 0.26 o 8 12 0 0.13 0.36 0.33 o 1 13 0 5.71 7.91 0.28 o 2 13 0 0.28 0.14 0.18 o 3 13 0 13.12 16.07 0.42 o 4 13 0 108.16 100.14 1.09 o 5 13 0 2.19 2.32 0.25 o 6 13 0 136.00 141.33 1.62 o 7 13 0 19.78 18.64 0.54 o 8 13 0 25.13 21.56 0.75 o 0 14 0 1223.67 1219.06 12.08 o 1 14 0 15.76 17.41 0.45 o 2 14 0 36.28 36.87 0.60 o 3 14 0 3.03 3.79 0.26 o 4 14 0 64.83 65.93 0.86 o 5 14 0 0.91 0.61 0.24 o 6 14 0 76.15 75.11 1.00 o 7 14 0 4.99 5.79 0.40 o 1 15 0 25.82 25.80 0.62 o 2 15 0 64.88 56.33 0.88 o 3 15 0 89.50 79.79 0.97 o 4 15 0 36.74 37.28 0.66 o 5 15 0 22.82 23.57 0.57 o 6 15 0 230.47 241.05 2.36 o 0 16 0 2.15 3.09 0.98 o 1 16 0 104.37 102.31 1.28 o 2 16 0 29.96 27.32 0.73 o 3 16 0 61.14 62.21 0.97 o 4 16 0 0.12 -0.06 0.24 o 5 16 0 48.06 45.67 0.79 o 1 17 0 4.58 5.97 0.38 o 2 17 0 38.50 39.31 0.80 o 3 17 0 15.08 15.14 0.55 o 4 17 0 3.15 3.31 0.35 o 0 18 0 108.58 108.68 2.31 o 1 18 0 12.58 12.59 0.65 o 2 18 0 115.03 111.66 1.45 o 3 18 0 42.40 43.10 0.86 o -11 0 1 150.74 167.65 2.44 o -9 0 1 4.33 4.76 0.31 o -7 0 1 175.99 170.65 1.76 o -5 0 1 751.67 784.24 6.69 o -3 0 1 2665.16 2835.16 28.04 o -1 0 1 1028.74 1059.68 6.76 o 3 0 1 86.33 69.68 0.74 o 5 0 1 544.00 460.35 4.06 o 7 0 1 654.13 666.80 5.95 o 9 0 1 258.46 275.28 4.03 o 11 0 1 18.95 20.19 2.56 o -11 1 1 115.96 120.99 1.46 o -10 1 1 120.43 123.58 1.26 o -9 1 1 1.97 2.26 0.22 o -8 1 1 192.35 185.46 1.37 o -7 1 1 64.71 67.95 0.74 o -6 1 1 7.93 10.35 0.22 o -5 1 1 78.38 72.91 0.59 o -4 1 1 354.70 443.19 2.72 o -3 1 1 1290.45 1249.45 7.62 o -2 1 1 31.54 30.29 0.32 o -1 1 1 3254.48 3413.35 85.49 o 0 1 1 1304.47 1330.97 7.89 o 1 1 1 190.49 197.24 1.46 o 2 1 1 1919.01 1977.52 11.39 o 3 1 1 321.28 294.46 1.84 o 4 1 1 15.37 14.87 0.27 o 5 1 1 118.73 125.36 0.92 o 6 1 1 247.92 251.27 1.69 o 7 1 1 283.19 263.07 1.81 o 8 1 1 98.79 93.49 0.84 o 9 1 1 68.87 69.88 0.86 o 10 1 1 89.83 92.92 1.21 o 11 1 1 86.75 90.79 1.99 o -11 2 1 14.18 15.60 0.63 o -10 2 1 54.64 57.00 0.74 o -9 2 1 91.17 95.55 0.95 o -8 2 1 90.78 90.33 0.80 o -7 2 1 5.44 5.50 0.20 o -6 2 1 1.44 4.07 0.15 o -5 2 1 5.70 8.37 0.19 o -4 2 1 320.90 301.51 2.03 o -3 2 1 84.22 105.30 0.67 o -1 2 1 998.97 993.47 5.63 o 2 2 1 45.06 21.17 0.44 o 3 2 1 23.25 27.42 0.28 o 4 2 1 3733.76 3866.59 23.37 o 5 2 1 695.63 824.44 5.01 o 6 2 1 0.26 2.28 0.19 o 7 2 1 0.02 0.18 0.15 o 8 2 1 9.46 9.99 0.32 o 9 2 1 27.69 27.63 0.55 o 10 2 1 36.17 35.30 0.73 o -11 3 1 8.05 8.47 0.85 o -10 3 1 99.35 108.15 1.09 o -9 3 1 50.22 53.88 0.73 o -8 3 1 238.97 242.94 1.85 o -7 3 1 119.51 104.91 0.85 o -6 3 1 21.63 18.97 0.29 o -5 3 1 251.12 256.23 1.67 o -4 3 1 2435.03 2611.17 15.88 o -3 3 1 115.26 132.23 0.84 o -2 3 1 89.47 87.60 0.84 o -1 3 1 306.82 314.54 1.83 o 0 3 1 105.11 120.27 0.74 o 1 3 1 3768.63 3827.31 28.82 o 2 3 1 1293.35 1368.13 7.92 o 3 3 1 47.79 64.75 0.54 o 4 3 1 2227.52 2288.65 13.92 o 5 3 1 7.69 10.35 0.23 o 6 3 1 144.86 132.79 1.00 o 7 3 1 63.68 55.10 0.61 o 8 3 1 323.08 317.96 2.30 o 9 3 1 14.42 13.00 0.43 o 10 3 1 52.87 55.27 1.03 o -11 4 1 227.55 248.36 2.75 o -10 4 1 58.02 58.86 0.84 o -9 4 1 291.29 289.97 2.21 o -8 4 1 8.82 10.23 0.32 o -7 4 1 16.18 12.04 0.29 o -6 4 1 21.46 16.75 0.27 o -5 4 1 25.10 28.04 0.32 o -4 4 1 26.94 58.13 0.54 o -2 4 1 5025.42 5165.20 39.19 o -1 4 1 1511.91 1599.32 9.24 o 0 4 1 0.04 2.01 0.11 o 1 4 1 1720.12 1633.49 10.69 o 2 4 1 1.41 1.82 0.09 o 3 4 1 2643.89 2710.49 16.43 o 4 4 1 1195.48 1234.15 10.96 o 5 4 1 106.93 68.47 0.59 o 6 4 1 48.66 45.36 0.48 o 7 4 1 222.64 212.63 1.52 o 8 4 1 84.10 83.51 0.86 o 9 4 1 2.76 2.84 0.28 o 10 4 1 4.22 3.87 0.39 o -11 5 1 4.46 3.61 0.49 o -10 5 1 20.20 20.77 0.59 o -9 5 1 62.50 67.21 0.78 o -8 5 1 99.09 93.60 1.12 o -7 5 1 195.01 196.50 1.53 o -6 5 1 6.81 4.50 0.23 o -5 5 1 88.79 73.76 0.73 o -4 5 1 0.06 4.57 0.31 o -3 5 1 192.54 172.28 1.25 o -2 5 1 159.93 185.82 1.21 o -1 5 1 33.73 24.08 0.25 o 0 5 1 568.11 595.59 3.40 o 1 5 1 3101.11 3161.32 20.43 o 2 5 1 158.73 165.91 1.21 o 3 5 1 11.19 8.12 0.18 o 4 5 1 121.28 134.63 1.05 o 5 5 1 394.89 391.73 2.49 o 6 5 1 25.35 22.45 0.34 o 7 5 1 394.75 370.66 2.65 o 8 5 1 39.00 37.98 1.06 o 9 5 1 261.10 259.45 2.45 o 10 5 1 0.61 0.25 0.30 o -10 6 1 89.74 95.95 1.25 o -9 6 1 147.33 141.12 1.45 o -8 6 1 210.33 200.29 1.61 o -7 6 1 0.71 1.41 0.17 o -6 6 1 143.96 137.13 1.13 o -5 6 1 68.79 71.68 0.67 o -4 6 1 363.30 319.61 2.21 o -3 6 1 566.24 595.04 3.90 o -2 6 1 609.66 570.52 3.70 o -1 6 1 752.99 866.63 5.22 o 0 6 1 6183.45 6638.45 45.44 o 1 6 1 120.73 76.56 0.64 o 2 6 1 438.75 449.31 2.96 o 3 6 1 476.85 451.22 2.99 o 4 6 1 530.31 518.54 3.21 o 5 6 1 324.24 327.07 2.13 o 6 6 1 154.60 145.45 1.10 o 7 6 1 0.32 0.33 0.18 o 8 6 1 4.09 6.55 0.33 o 9 6 1 0.05 -0.09 0.25 o 10 6 1 25.39 25.77 0.75 o -10 7 1 34.36 37.36 0.88 o -9 7 1 28.56 25.65 0.55 o -8 7 1 67.26 71.74 0.87 o -7 7 1 21.09 26.71 0.43 o -6 7 1 371.17 340.24 2.42 o -5 7 1 97.22 106.97 0.92 o -4 7 1 149.97 125.90 1.01 o -3 7 1 33.59 27.52 0.36 o -2 7 1 3174.43 3348.78 20.27 o -1 7 1 1475.05 1573.00 9.58 o 0 7 1 871.83 994.13 5.95 o 1 7 1 247.73 276.38 1.91 o 2 7 1 574.23 591.53 3.87 o 3 7 1 19.94 19.56 0.30 o 4 7 1 111.48 109.93 0.83 o 5 7 1 142.84 128.49 0.97 o 6 7 1 745.21 677.78 4.92 o 7 7 1 46.94 41.22 0.62 o 8 7 1 168.80 169.18 1.88 o 9 7 1 46.29 43.84 0.90 o 10 7 1 58.22 62.81 1.15 o -10 8 1 119.60 124.58 1.72 o -9 8 1 31.83 33.36 0.70 o -8 8 1 9.41 11.56 0.39 o -7 8 1 19.51 14.92 0.39 o -6 8 1 6.50 1.30 0.18 o -5 8 1 41.74 43.40 0.51 o -4 8 1 261.02 280.18 2.00 o -3 8 1 408.16 435.36 3.24 o -2 8 1 646.97 744.20 4.51 o -1 8 1 1842.78 1908.45 11.63 o 0 8 1 264.06 225.19 1.49 o 1 8 1 2971.61 3082.06 17.73 o 2 8 1 989.42 1027.57 6.59 o 3 8 1 11.46 7.46 0.27 o 4 8 1 165.00 158.06 1.37 o 5 8 1 3.86 4.42 0.23 o 6 8 1 98.72 103.32 1.06 o 7 8 1 0.04 0.05 0.30 o 8 8 1 79.00 74.99 1.04 o 9 8 1 0.96 0.13 0.28 o -10 9 1 17.16 15.30 0.67 o -9 9 1 94.59 90.51 1.20 o -8 9 1 0.02 0.15 0.20 o -7 9 1 15.07 9.53 0.36 o -6 9 1 1.22 0.38 0.17 o -5 9 1 65.79 58.77 0.71 o -4 9 1 287.69 267.72 1.94 o -3 9 1 37.24 38.21 0.40 o -2 9 1 45.00 42.82 0.43 o -1 9 1 364.50 367.99 2.34 o 0 9 1 25.12 27.98 0.45 o 1 9 1 951.57 1043.00 5.93 o 2 9 1 163.85 186.63 1.40 o 3 9 1 907.26 856.38 5.57 o 4 9 1 72.94 73.65 0.77 o 5 9 1 10.11 8.33 0.33 o 6 9 1 121.53 118.04 1.18 o 7 9 1 88.65 92.60 1.04 o 8 9 1 12.19 12.58 0.50 o 9 9 1 114.28 111.07 2.22 o -9 10 1 1.13 1.68 0.31 o -8 10 1 0.36 0.97 0.26 o -7 10 1 0.21 0.36 0.20 o -6 10 1 11.81 14.13 0.39 o -5 10 1 10.71 7.58 0.45 o -4 10 1 0.08 0.01 0.17 o -3 10 1 106.07 105.96 0.97 o -2 10 1 1018.75 1003.97 6.06 o -1 10 1 454.64 422.82 2.68 o 0 10 1 47.83 44.94 0.48 o 1 10 1 186.15 192.53 1.34 o 2 10 1 0.36 2.77 0.32 o 3 10 1 685.87 670.82 4.45 o 4 10 1 192.78 193.82 1.67 o 5 10 1 64.77 68.55 0.96 o 6 10 1 15.71 15.89 0.42 o 7 10 1 78.97 81.21 1.05 o 8 10 1 85.20 81.70 1.14 o 9 10 1 75.17 77.99 1.46 o -9 11 1 44.87 47.38 0.90 o -8 11 1 50.90 53.40 0.90 o -7 11 1 29.87 31.23 0.59 o -6 11 1 25.51 20.94 0.48 o -5 11 1 575.49 553.13 4.13 o -4 11 1 51.21 54.73 0.70 o -3 11 1 3.97 1.82 0.27 o -2 11 1 225.81 203.55 1.43 o -1 11 1 327.47 311.97 2.06 o 0 11 1 41.03 33.61 0.41 o 1 11 1 95.47 82.39 0.78 o 2 11 1 1000.59 1020.12 6.62 o 3 11 1 533.68 506.87 3.46 o 4 11 1 44.98 42.86 0.62 o 5 11 1 12.84 12.04 0.38 o 6 11 1 27.45 27.22 0.55 o 7 11 1 2.90 1.59 0.25 o 8 11 1 52.31 54.32 0.93 o -8 12 1 1.27 0.77 0.29 o -7 12 1 68.97 61.17 0.96 o -6 12 1 116.70 114.94 1.21 o -5 12 1 2.29 3.92 0.29 o -4 12 1 120.44 132.37 1.28 o -3 12 1 149.11 151.76 1.40 o -2 12 1 1064.13 1058.51 6.87 o -1 12 1 174.11 165.65 1.23 o 0 12 1 234.97 230.73 1.61 o 1 12 1 19.73 19.30 0.39 o 2 12 1 383.66 369.25 2.62 o 3 12 1 9.63 10.24 0.34 o 4 12 1 266.32 261.88 2.18 o 5 12 1 5.46 6.17 0.31 o 6 12 1 11.19 13.53 0.45 o 7 12 1 50.90 48.12 0.87 o 8 12 1 0.46 -0.03 0.29 o -8 13 1 59.64 62.92 1.04 o -7 13 1 18.05 16.69 0.57 o -6 13 1 118.76 112.90 1.33 o -5 13 1 144.23 147.29 1.44 o -4 13 1 226.03 228.01 1.97 o -3 13 1 14.45 15.05 0.41 o -2 13 1 308.62 289.09 2.35 o -1 13 1 2.21 3.45 0.36 o 0 13 1 55.17 51.43 0.75 o 1 13 1 7.97 8.48 0.46 o 2 13 1 8.65 4.87 0.23 o 3 13 1 16.90 15.42 0.41 o 4 13 1 63.21 58.17 0.79 o 5 13 1 45.04 48.21 0.74 o 6 13 1 348.01 342.25 2.84 o 7 13 1 104.39 118.49 1.48 o -7 14 1 72.48 79.54 1.17 o -6 14 1 18.64 22.35 0.64 o -5 14 1 225.66 221.09 1.99 o -4 14 1 55.98 53.71 1.01 o -3 14 1 122.93 122.56 1.25 o -2 14 1 5.40 4.30 0.27 o -1 14 1 249.15 240.78 2.03 o 0 14 1 128.18 124.55 1.24 o 1 14 1 421.29 416.57 2.96 o 2 14 1 19.92 17.21 0.44 o 3 14 1 79.84 79.27 0.95 o 4 14 1 0.06 0.18 0.25 o 5 14 1 160.71 153.50 1.74 o 6 14 1 9.94 9.94 0.52 o 7 14 1 0.23 0.39 0.33 o -6 15 1 83.20 90.37 1.27 o -5 15 1 194.30 199.63 1.87 o -4 15 1 3.23 3.78 0.31 o -3 15 1 66.60 64.92 0.96 o -2 15 1 56.63 62.94 0.94 o -1 15 1 17.70 18.34 0.53 o 0 15 1 47.14 50.91 0.72 o 1 15 1 71.52 65.91 0.96 o 2 15 1 32.92 32.47 0.60 o 3 15 1 13.87 14.64 0.45 o 4 15 1 0.19 0.03 0.23 o 5 15 1 7.08 7.95 0.54 o 6 15 1 68.74 65.74 0.96 o -6 16 1 9.81 9.55 0.63 o -5 16 1 18.44 20.23 0.63 o -4 16 1 32.32 27.89 0.68 o -3 16 1 14.36 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